YOUR PARTNER IN X-RAY DIFFRACTION

STOE

HIGH TEMPERATURE ATTACHMENTS

HIGHEST TEMPERATURE STABILITY

The STOE STADI P Powder Diffractometer System with its PSDs for rapid measurements is the ideal equipment for the observation and evaluation of phase transitions in nonambient environments. Therefore STOE has developed the capillary furnace series for powder investigations at high temperatures for three different temperature ranges:
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All STOE furnaces are delivered with a referring temperature controller in a 19 rack containing power supply, flow meter for the cooling water control and interface to the PC. STOE's WinXPOW software provides full operation control and data visualization. All three versions provide sample spinning to avoid effects from preferred orientation. The temperature programs are easy to being set-up and executed. The temperature stability in the whole range is below +/-1C. The STOE furnaces can be mounted on every STADI P diffractometer (moving circles or fixed stage); heating elements are available for capillaries with diameters from 0.2 to 1.0 mm.

The basic version 0.65.1 from room temperature to 1000C The extended temperature version 0.65.3 from room temperature to 1500C The furnace with the low temperature option 0.65.LT for a range from -50 to 1000C

TECHNICAL SPECIFICATIONS

Heating element

Model 0.65.1 mounted on a fix stage with STOEs large IP-PSD, video CCD and tube housing.

Basic Version 0.65.1 Temperature range: Thermo couple: Heating power: Max. heating rate: 2Theta range: Sample holder:

Extended Version 0.65.3

Low Temp. Version

RT - 1000C Ni/CrNi 1000 W 50/min 0 - 90 Capillary

RT - 1500C Pt/PtRh 1300 W 50/min 0 - 90 Capillary + Pt-/Ir-Wire

-50 - 1000C Ni/CrNi 1300 W 50/min 0 - 90 Capillary

STOE & Cie GmbH | P.O.Box 101302 | D-64213 Darmstadt Phone: (+49) 6151/98870 | Fax: (+49) 6151/988788 E-mail: stoe@stoe.com | www.stoe.com