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(1) Preparation Weight(g) 94.023 92.775 1.

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Crystals + petri dish Empty petridish Crystals (2)Quantitative analysis (a) Determination of the oxalate ion Mass of potassium permanganate used=0.8226g Standardising solution
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Final reading/cm Initial reading/cm3 Volume of KMnO4 used/cm3 Mass of complex used=0.176g, 0.177g

1st 9.80 0.00 9.80

2nd 19.50 9.80 9.70

Final reading/cm3 Initial reading/cm3 Volume of KMnO4 used/cm3 (b) Determination of copper content Final reading/cm3 Initial reading/cm3 Volume of sodium thiosulphate used/cm3

1st 22.00 0.00 22.00

2nd 43.90 22.00 21.90

1st 12.70 0.00 12.70

2nd 25.40 12.70 12.70

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