Beruflich Dokumente
Kultur Dokumente
Emery White
SCH3UE- 03
Mr. Porter
26th January 2009
Purpose:
To prepare a sample of magnesium oxide and determine the simplest formula and percentage
composition for the compound
Apparatus/ Materials:
– Crucible and lid
– Crucible tong
– Electronic balance
– Retort stand
– Ring clamp
– Wire gauze
– Clay triangle
– Bunsen burner
– Magnesium ribbon
Procedure:
1. Obtained and got out equipment ready before obtaining the magnesium ribbon
2. Measured the mass of the crucible and the lid- after cleaning and drying it.
3. Placed the magnesium spiral into the crucible and measured the mass of the crucible,
magnesium spiral and the crucible lid
4. Began to heat the crucible – containing the magnesium spiral, with the lid kept on –
carefully, while moving the bunsen burner around under it
5. Removed the lid – to check on the magnesium – with the tong
6. After all the oxygen seemed to be gone, we removed the lid, and heated it strongly for
four minutes
7. Cleaned our work area, before measuring the mass of the room tempered crucible, lid and
remaining magnesium
Quantitative observations:
Quantitative Observations
Material/ substance
(±0.01 g)
Crucible + lid 15.33 g
Crucible+ lid+ magnesium 15.40 g
Room tempered magnesium oxide+ crucible
15.45 g
and lid
Qualitative observations:
Substance
– silver
– solid
– lustrous
Magnesium
– metallic
– malleable
– opaque
– solid
– white clumps ( in a coiled shape)
Magnesium Oxide – opaque
– dull
– powder
Analysis:
1. Mass of Magnesium used in the reaction:
(15.40 g 0.01g ) (15.33g 0.01g )
0.07 g 0.02 g
0.07 g 28.6%
Discussion:
In this experiment we prepared a sample of magnesium oxide, and used the results – after
oxidising the magnesium – to determine the simplest formula for Magnesium Oxide: MgO. We
also calculated the percentage composition of both magnesium and oxygen. The percentage
composition of magnesium was theoretically calculated to be 60.304 %, but the actual value (the
results from our lab) was 58.3 % ± 62 %, indicates a 2.004 % error in our results. Even with
these inaccurate results, we were able to determine the simplest formula of magnesium oxide,
through calculating the ratio between the elements. MgO is the correct formula for magnesium,
is we calculated.
Conclusion:
In this experiment we managed to calculate the empirical formula of magnesium oxide, using our
ratio and percentage composition. Even with an imprecise percentage composition of magnesium
– there was an error of 2.004 % - we were able to succeed in completing the purpose of this lab:
To prepare a sample of magnesium oxide and determine the simplest formula and percentage
composition for the compound.