number of tray 61 sieve trays plus reboiler and condenser
efficient trays 54% condenser total feed on tray 31 reflux ratio 1.24 tray spacing 12 inch 0.304801 m weirs 1 inch 0.0254 m column height 18.6 m diameter 3 m Aliran 16 17 18 Temperatur (C) 65 69.9 125 Pressure (Kpa) 65 45 65 Ethylbenzene Mol Flow (kmol/h) 226.21 3.34 222.88 Styrene Mass Flow (kg/h) 23709.6 289.5 23420 Benzene Vapor density (kg/m3) Toluene Liquid density (kg/m3) Surface tension (dyne/cm) Component flow (kmol/h) Ethylbenzene 102.88 0.1 102.78 Styrene 120.09 0 0.06 Benzene 1.37 1.37 0 Toluene 1.86 1.86 0 T-401 Component feed distilat bottom C8H10 106.2 0.448706 0.024352 1680.740113 C8H8 104.2 0.53382 0 1 C6H6 78.11 0.008124 0.453593 0 C7H8 92.14 0.00935 0.522056 0 total 1 1 1681.740113 T-401 BM (kg/kmol) fraksi formula Mass Balance Overall F = D + B F = 226.21 D = 3.34 B = 222.88 Mass Balance 'Vapor Product' V = D + L R = L/D = 1.5 Liquid flow above feed (L) = R x D dimana : L = 5.01 L = Refluks rate V = 8.35 V = Vapor Rate Liquid flow below feed (Lm) = LD + F R = Reflux Ratio Lm = 242.9434 Vm= 8.35 number of stages 61 stages reboiler 1 Number of real stages = = 61 stages Pressure Drop = 9.81 x 10 -3 *ht*densitas liq = 18581.84234 Pa 18.581 Distillate Product , T = 195 C Bottom Product , T = 330 C vapor density (kg/m3) = 1.314 vapor density (kg/m3) = liquid density (kg/m3) = 824.1 liquid density (kg/m3) = surface Tension (N/m) = 22.54 x 10 -3 surface Tension (N/m) = Flv Bottom = 1.438913578 Flv distillate = 1.161786579 tray spacing 0.3048 K1 distillate = 0.023 K1 bottom = 0.019 correction for surface tension bottom K1 = 0.018845508 Vf = 0.380592305 distillate K1 = 0.023556601 Vf = 0.589465488 assume : design for 85% flooding at maximum flow rate : Un = %flooding x Uf bottom Un = 0.323503459 distillate Un = 0.501045665 3. Column Diameter 1. Flow Rate Number of stages / efficient stage 2. Physical Properties maximum volumetrik flow rate : (mol x BM) / rho bottom (m3/s) = 0.236554101 top (m3/s) = 0.487983574 Net area required : volume rate / Un bottom (m2) = 0.731225879 distillate (m2) = 0.973930339 first trial = downcomer area as 12% of total column cross-sectioned area : bottom (m2) = 0.830938498 distillate (m2) = 1.106739021 column diameter : bottom (m) = 1.028844196 tanyain bapak ini diameter apa ? Terus diameter tower itu yg mana distillate (m) = 1.187374678 tinggi kolom = jumlah plate x tray spacing tinggi kolom Lm/Vm= 29.09502 Kpa 2.063 843.465 19.2 x 10 -3 3. Column Diameter maximum volumetric liquid rate (m3/s) = the column diameter is still unknown, but I assume that a double pass plate can be used 4. Liquid Flow Pattern 1. Flow Rate 2. Physical Properties column diameter, Dc = Column area, Ac= Downcomer Area, Ad = net area, An = Active area, Aa = Ac-2Ad Hole area, Ah (asumsi 10% dari Aa) weir Length (fig.17.39) (mm) Take weir height(mm) hole diameter(mm) 6.Check Weeping 5. Provisional Plate Design 7. Plate Pressure Drop 8. Downcomer Liquid Backup 10.Trial Layout tanyain bapak ini diameter apa ? Terus diameter tower itu yg mana tinggi kolom = jumlah plate x tray spacing tinggi kolom 11.Perforated area 12.Number Of Holes 13. Colum Height 9. check entrainment 0.016834 1.187374678 1.106739021 0.132808683 0.12 0.973930339 0.841121656 0.420560828 0.76 12 5 plate thickenes(mm) 5 Maximum liquid rate = 14.19869204 minimum liquid rate = 70%turndown 9.939084431 Maximum weir liquid crest, h ow (mm) 0.122652208 Minimum weir liquid crest, h ow (mm) 0.060099582 at minimum rate hw+h ow = 50.06009958 at.figure 11.32 , K2 = 30.3 Uh min 8.31294128 Dry Plate Drop Maximum Vapor Velocity through holes : Uh max (m/s) 0.562472978 from figure 17.42 for plate thickness/hole diameter=1 and Ah/Ap sebanding dengan Ah/Aa=0.1, Co=0,84 hd (mm liquid) = 0.055930293 Residual Head, hr (mm liquid) = 14.81982062 Total Plate Pressure Drop, ht (mm liquid) = 36.81483534 Downcomer Pressure Lose Take hap = hw-10 = (mm) 40 area under apron, Aap (m2) 0.0304 As this is last than Ad, use Aap in equation 17.60 Hdc (mm) 50.90066643 Backup in downcomer, Hb (mm) 99.77560136 0.0997756 0,5 (Lt+Hw) 0.2124 0,16 m < 0,5 (Lt+Hw) maximum volumetric liquid rate (m3/s) = the column diameter is still unknown, but I assume that a double pass plate can be used 4. Liquid Flow Pattern column diameter, Dc = Column area, Ac= Downcomer Area, Ad = net area, An = Active area, Aa = Ac-2Ad Hole area, Ah (asumsi 10% dari Aa) weir Length (fig.17.39) (mm) Take weir height(mm) hole diameter(mm) 6.Check Weeping 5. Provisional Plate Design 7. Plate Pressure Drop 8. Downcomer Liquid Backup tray spacing is acceptable Check Residence Time (second) 0.787171839 residence time kurang dari 3 uv (m/s) = 0.242886059 % flooding = uv/uf 75% with Flv = 0,627 ; from fig 17.36, fractional entrainment () = 0.75 at figure 11.34 lw/Dc = 0.6400675 c 82 angel subtended by the edge of the plate = 98 mean length,unperforated edge strips (m) 1.9444052 area of unperforated edge strips (m2) 0.0972203 mean length of calming zone , approx (m) 0.81 area of calming zone 0.081 total area for perforation Ap (m2) = (Aa-area of unperforated-area on calming) 0.6629014 Ah/Ap 0.6344244 From figure 11.35 lp/Dh 2.85 Area of One Hole (m2) 1.96E-05 Number of holes 2.14E+04 tinggi kolom = jumlah plate x tray spacing 18.59283719 11.Perforated area 12.Number Of Holes 13. Colum Height 9. check entrainment 7. Plate Pressure Drop