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NURULAINAPUTERI
113194033
PENDIDIKANKIMIAINTERNASIONAL2011
UNIVERSITASNEGERISURABAYA
G.ANALYSISDATA
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1.TitrationWeakAcid(C2H2O4)andStongBase(NaOH)
No
1
Nof
C2H2O4
Vof
C2H2O4
moleqof
C2H2O4
Vof
NaOH
(normal)
(mL)
(mol)
(mL)
moleqof
NaOH
(mol)
0,05
5,0
2,5x104
0,10
5,0
5,0x104
0,10
4,8
4,8x104
0,10
4,7
4,7x104
0,05
5,0
2,5x104
0,05
5,0
2,5x104
NofNaOH
(normal)
Titrationweakacid(C2H2O4)andstongbase(NaOH)aimtodeterminetheconcentrationofNaOH
solutionattheequivalencepointoftitration,
byusing:M1xV1xe=M2xV2xe
ThereactionofC2H2O4andNaOH:
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C2H2O4(aq)+2NaOH(aq)Na2C2O4(aq)+2H2O(l)
Atthatreaction,thereare2molesofionH+whichresultingfromeverymolesofC2H2O4
(because1
moleofionH+usedby1moleofNaOH).Sothat,webeablecalculatetheconcentrationofNaOHwitha
knownvolumeofNaOH.
Fromthetitrationofweakacid(C2H2O4)andstrongbase(NaOH)inthisexperiment,wegetthat
theaverageconcentrationofstrongbase(NaOH)is0,1M.
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April (2)
2.TitrationStongAcid(HC)andStrongBase(NaOH)
March (7)
No
NofHC
(normal)
Vof
HC
(mL)
1
2
3
0,090
0,112
0,088
5,0
5,0
5,0
Nof
NaOH
(normal)
0,100
0,100
0,100
Vof
NaOH
(mL)
4,5
5,6
4,4
Total
Volume
(ml)
9,5
10,6
9,4
Analysis and
discussion
"TITRATION
EXPERIMENT"
ThereactionbetweenHClandNaOH:
HCl(aq)+NaOH(aq)NaCl(aq)+H2O(l)
Basedonthatreaction,HClwillhavecompleteionizationinwater.Andthereactionwillbelikethis:
http://ainaputeri-world.blogspot.com/2012/03/analysis-and-discussion-titration.html
Hak Asasi
Manusia ~~
Hak Asasi
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HCl(aq)H+(aq)+Cl(aq)
Schedules of
Reinforcemen
t
ThesamethinghappenedtoNaOH:
Operant
conditioning
NaOH(aq)Na+(aq)+OH(aq)
Antecedents ~~
Theneutralizationreaction
2011 (5)
H+
(aq)+OH (aq)
H2O()
AftercompleteneutralizationofHC,theamountofNaOHleftis0.Thisisasimplecalculation
becauseitinvolvesacompleteneutralizationreactionandthesalt(NaC)doesnotundergohydrolysis.
Attheequivalencepoint,(H+)=(OH)andthepHsolutionis7,00.
TocalculatetheconcentrationofHClsolution,weuse:
M1xV1=M2xV2
Fromthetitrationofstrongacid(HCl)andstrongbase(NaOH)inthisexperiment,wegetthatthe
averageconcentrationofstrongacid(HCl)is0,096M.
3.TitrationStrongAcid(HC)andStrongBase(NaOH)withNaturallyIndicator
No
NofHC
(normal)
VofHC
(mL)
NofNaOH
(normal)
Vof
NaOH
Total
Volume
(mL)
(mL)
1
0,086
5,0
0,100
4,3
9,3
2
0,084
5,0
0,100
4,2
9,2
3
0,104
5,0
0,100
5,2
10,2
Inthislastexperiment,weusecurcumintobeindicator.Curcuminisyellowinacidic
and dark yellow in basic solution, but if strong base, it become dark brown. And, because the pH
rangeofcurcumicis>7(morethan7),itllbaseindicator,anditcanusedasindicatoroftitration,
andwithit,wecandeterminetheequivalentpointwhentheendpointfinallyreached.Andso,we
can concluded that when the colour of the solution change into dark yellow, that signing if the
solutionhasreachedtheendpoint,andthepHofthesolutionafterthatismorethan7butitdidnt
reach14(becomestrongbase).
Fromthetitrationofstrongacid(HCl)andstrongbase(NaOH)inthisexperimentandusingnatural
indicator,thatiscurcumin,thenwegetthattheaverageconcentrationofstrongacid(HCl)is0,091M.
H.DISCUSSION
THECHANGECOLOUR
Inourexperiment,weusedsomesolution,suchasNaOH,HCl,C2H2O4,phenolphthaleinindicator
andplantextract.Allsolution,exceptplantextractatfirsttimeiscolourless.Sodowhenacid(C2H2O4and
HCl)addedwithphenolphthalein.But,whenacidaddedwithindicatorthendroppedbybase(NaOH),the
colourofsolutionbecamepink.Thisoccursbecausephenolphthaleinisindicatorofbase,ifphenolphthalein
droppedintoacid,itllbecolourless,butifdroppedintobase,thecolourbecomered.Andinthiscase,in
ourexperiment,thechangingofcolourissigningthatthesolutionintheequivalentpoint.
In plant extract (curcumic plant) the colour is yellow, but after dropped with NaOH, the colour
becamedarkyellow.Thisoccursbecausecurcumicextractwhendroppedwithacidsolutionbecamebright
yellow,andifdroppedwithbasesolutionbecamedarkyellow.So,thesigningcolourtoknowingthatthe
solutionatequivalentpointisifthesolutionchangeintodarkyellow.
Inourexperiment,theentirechangecolourofallsolutionissuitablewiththehypothesis.
THECONCENTRATIONOFACIDBASESOLUTION
Theaimofthisexperimentistodeterminetheconcentrationofacidbasesolutionbyneutralization
reactionthatistitration.
WecancalculateordeterminetheconcentrationofNaOHsolutionandHClsolution,whichfirstby
knowing the volume of NaOH then we can determine the concentration of NaOH with oxalic acid
(C2H2O4),whenthetitrationprocessbetweentheequivalencepointandattheendpoint,whichistheres
changingcolourofthesolutionbecamepink(becauseoftherearephenolphthaleinthatbeanindicatorif
the solution at the end point) like in the basic theory. But when we repeated in the third experiment
(determiningtheconcentrationofHClbyusingplantindicator),experimentforthesecond,wegotdifferent
volume, that didnt same with the first and the third. This occurs because maybe caused by our mistake
when we adding HCl into the conical flask more than 5 mL, so it reached end point must with the large
volumeofNaOHtooormaybewegetdifficultieswhendeterminedtheendpointofthetitration.
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I.CONCLUSION
Fromtheexperimentwehaddone,first,wegottheconcentrationofNaOHwithC2H2O4 solution
usingphenolphthaleinindicatorthatis0,1M.Second,wegottheconcentrationofHClwithNaOHsolution
usingphenolphthaleinindicatorthatis0,096M.Andthethird,wegottheconcentrationofHClwithNaOH
solutionusingplantextractthatis0,091M.Andaswehadcalculated,theconcentrationofHCldifference
betweenusingphenolphthaleinandusingplantextractisnotfar.
REFFERENCES
Brady,E.James.GeneralChemistry:PrincipleandStructure.5thEd.2006.USA:JohnWiley&SonsInc.
Chang,Raymond.2005.GeneralChemistry:TheEssentialConcepts.3rdEd.USA:McGrawHill
ATTACHMENT
C2H2O4addedwithphenolphthalein
Postedbyainaputeriat12:34p.m.
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