SPE 18977
SPE
Society of Putraoum Engrs
Summary Results of COz EOR Field Tests, 1972-1987
by W.R, Brock and L.A. Bryan, Exxon Co. U.S.A.
SPE Members
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‘ABSTRACT
Since the early 1970s, nunerous presentations have
non’ made ‘and’ articies "written about pilot. tests
Sn” Fleld-acate, enhanced ost» recovery projects
Wing’ carbons dioxide (COg) as, "s. solvent. This
popes Suma ises publicly avatvable data) on” 30
Projecta.theuse™ gh Cy pat ghown sfaniieatiy
Binge the early-1980s,. cepecially inthe Permian
Savin, ‘bs Velfable supplies of Og. becane. nore
Svailibte, "Today, even with depressed. crude “ofl
aurketsy the oe of COp continues to grow. The use
BF Cbg tn the Rocky Mauseasn region 1s tacreasing,
Srimeiny stony’ those with prior C02" flocding
Biperience inte Permian Basin. As the-denara for
Gop Snereases in the Rocky Mountains, so wil’ the
Stppivs and the sane. groeth experienced” in_ the
Perbian Gasin’shogig. be seen, “As with. any ‘calor
Project inthe ott industry, the enhanced recovery
BeoiT “tequires thorough’ advance. planning. to
determine tne. optimum £08 method. This sumary of
GB projects: te intended to provide @ brief on each
prajecty describe. the reservoir paraneters, and
Fovlew the ‘conclusfons of the. individual authors,
in’ aadition to providing a. qiick reference. oF
Maitable papers {0 which those interested ray turn
For" greater: details “Since she use of (0p hasbeen
Successfully tried in a wide range of Feservoirs
dnd under varisty "of operating. conditions, the
Bpelication. of Cop’ tn. Rocky. Holntain. reservoirs
Sfoulé' be every bft as successful” a5 it has been
eisevhere
NIRODUCTION
The use of COp, both miscibly and inmiscibly, has
grown dramatically since the start of this decade,
Spurred by the installation of COz pipelines in the
Bermian Basin in the early-19805.". While many
challenges still face ‘the user of CO, the
increased use of CO to recover residual oi)
evidences the optinish the industry has towards
enhanced oi recovery using C02. The use of C02 to
References and TIUSEFatTons at end of paper.
‘recover additional crude oil includes iemiscible
Flooding and an individual well stimulation
techniqie known as "huff 'n’ puff." This paper
sumarizes 21 miscible floods, 4 inmiscible
ulti-well floods and § immiscible "huff ’n’ puff
projects.
The origina) intent of this paper was to present
both successful and unsuccessful projects so. that
conparisons could be made. However, the search of
available’ data banks for papers’ published on
Unsuccessful projects was fruitiess. ‘Tt is likely
that sore of the projects discussed could be
considered marginally economic with depressed crude
oil prices even “though they were technical
Successes. This paper does not, attempt to draw
Conclusions of the projects reviewed but instead
presents, without interpretation, conclusions as
pubiished in the individual references. The reader
Should bear in mind while reviewing this paper that
many of | the extrapolations of incremental
Fecoveries and other factors “are based on
performance “data from relatively early. in 2
project’s Tife.
DEFINITIONS
Terminology used in this paper is consistent with
That used Yn the EOR\arends The term *inerenental
il" refers’ tothe of! production. in excess af
Saae decline curve for continued operations, Grose
WtiTiation of Op 18" defined as the total injected
olume. of Cog, nclucing. any” recycied volumes,
divided by the'totat incremental recovery. “The net
utilization ts, the: purchased volume of Gp, divided
ty he “toca “ngrenental “recovery. cHiscvole
Flooding refers tothe use of chy se a reservoir
pressure greater than that necessary for” the Cbg to
fix with the reservoir ov, commonly referred £8 35
the minisum miscibility pressure (WP), lemiscible
Flooding or stinutation Uses Cop at pressures Tess
fhan the HHP and relies ore. oh the reduction of
Viscosity and interfacial ‘tension, and the. swelling
of the git contacted by the COp.° In iscussing
various (Og Floods, the volune of Cop injected is,
comonly Feferred’ to in terms of percent. of
hydrocarbon pore volumes (HPV)SUMMARY RESULTS OF CO, EOR FIELD TESTS 1972-1987
SPE 19977
NISCIBLE--FIELD-SCALE
The first group reviewed are field-scale miscible
floods ‘whose paraneters are summarized in Table 1
These. projects employ eithor continuous” slugs or
water-alternating-gas) (WAG) injection ‘scheses” The
IV projects" discussed are in variety of different
reservoirs vanging fron the ‘shallow to. the deep,
from the tight. to the very permeable, and in both
Carbonate and sandstone
Some of [the projects utitize. purchased op. very
efficiently: ad noted by Tow net Cog util tzctionse
while others” appear Tess efficient. In all of
these, “it has ‘been’ qualitatively proven ‘that. COp
Ean enhance oiT recovery; however it should bs
noted that the quantity of Incremental ‘ofl in. most
ases 1s based on extrapolations of data very carly
in'the'1sfe of the project. Projected. incremental
recoveries. “ranged” fron” around. 7 percent.
Original 017 In-Place (Q01P) to"2e\ percent “OOlP on
net utitizatjons. of 2.4 net (thousind cubic. rect)
0p per stock tank barrel" (ST8) of incremental ot)
to" nef c0g/StB-
DOLLARHIDE DEVONIAN! UNOCAL initiated a phased
miscible CO» project in. the Dollarnide ‘Devonign
Field Tocated in Andrews County, Texas. in May 1988.
The praject was designed around’ low perseability,
tripolitic chert. Devonian reservoir ata depth ef
7200" feet, “with high conformance and “sininal
heterogeneities. "uring waterfloading an
exceptionally high sweep efficiency was, real ized
with” greater "than “va secondary-to-prinary
Tecovery ratio. This. high sweep. efficiency
expected to be exhibited in” tertiary. recovery
operations. To date greater ‘than 99.5 percent of
the Cop has been retained tn the reservoir after
nore than’ 8.8 percent. HcPV of Gop Injection. The
First breakthrough of COz did not occur until I?
months after the start of injection. According to
UNOCAL,” “the “total” Tack of prenature. "Coy
breakthrough. is “indicative of “unusually hich C09
syeep efficiency.” Originally designed for
2 percent HcPV siug chased by water, the project
as modiTied to benefit. fron the mobility conceal
Of WAG injection while. stil! capturing the benefits
of acceleration from the slug process." Following
the Ninitial slug ‘of 9 percent’ HCPY, the project
wiNl ‘be placed ‘on a 21 percent HOPY' 1:1) WAG. The
Bhasing of the project’ will decrease peak C09
Purchase requirenents by spreading C02 requirenents
over 'a longer period of tine and wll. allow for
axinin use of "less expensive recycled CO.” the
vide difference between’ the 1600 psi MMP and. the
fracture ‘pressure of "S500 pst allows. for. the
injection "oF Cop ‘at_‘the waterflood, reservele
pressure of 3200 gsi. Although COp utilization mitt
be ‘ess efficient at” 3200 psi “than. at a. lover
ressure, it will be possible to reinject the
Contaminated gas stream whose HNP 38 less then 3200
Psi but greater” than “1600 "psi without costly
Up-front investments necessary ‘to clean-up the COs
and without the risk of losing product ton due’ to\a4
inability to, maintain MMP. “The Field was infill
arivied ‘to “40-acre, “five-spot. patterns ‘which. 1s
anticipated to increase recovery about percent
O01P. "The, 30'percent HCPV of Cop injected "¢
anticipated ‘to increase’ the ultinate recovery by
416 percent. o01P,"vresult ing’ in. an. estisated” COs
utilization of 2.4 mcf/STB. No" Op injectivity
problems have bees encountered.
EAST VACUUM GRAYBURG/SAN ANDRES? This miscible Cop
flood of ‘the San Andres oolitic dolomite in Leg
County, New Mexico initiated by Phillips. Petroleum
in September 1985, gives a1? indications of being
Successful, Increnental recovery 1s. projected. to
fe'6 percent 001P following a WAG infect on oft
50 percent CPV. at a 2:1 ratio. Since ingection
eononced, ‘the. eli “production decline has been
Srrested ang 011” prodiction appears. to. be on the
‘nerease. "The project. has experienced an increased
occurrence ‘of "ealelus sulfate. scaler and the
precipitation of asphaltenes and paraffins in wells
Experiencing Cp. breakthrough. Although "the
frcreae’ im exlcfim State ts oncrrant wi, 0p
breakthrough, tt. Is postulated by” PhIVlips. the!
these occur concurrent iy. due to the dissolution of
the anhydrite stringers oy the water. The calcium
SuIfate” problew hes reqivred periodic! dnhibstion
Squeezes "using "a Vow ‘pH ‘phosphonate scale
inhibitor. “The asphattene/parartin depositions are
{reated using heavy aronatte solvents to dissolve
the butld-up. "the Yorat injection. of 230" Ber
(bintion ‘cubic feet) “er Cog'witl yield & gross
Uti zation. @F Tiel wct/sTB°. “Since ‘an estimated
100. BeF wilt” be recycled, the "net “utilization
Should approach 6.9 mct/S18
FORD-GERALDINES | Conaco initiated a miscible C0p
flood of the Ford Geraldine Unit located in Reeves
and Culberson Counties, Texas In February 1981 when
iE became apparent that unless tertiary recovery
was ‘Inittated, the Unit would have to be abandoned
The poor waterFlood’ perforaance, as evidenced. by
the ‘0.25:1" Secondary-to-primary recovery “ratio,
left an estinated 77 percent OOIP in the reservoir
Buoyed by. the success at the nearby, and. similar,
Tworreds Cg. project. and by their own feasibility
study, injection comenced using an’ erratic. COy
Supply fraa-a gas plant. for the first. five. years
during whieh. oi) production ‘resained relatively
Flats” Wen a ‘stable CO, supply was obtained in
Jate’ 1985," the productign increased. dranat ically
fron 381 Bopd: to" 1160. bopd. "The project 1s being
staged with the second stage ta be implecented a3
excess (0p becomes avetlable and as the first stage
{s-placed-on a brine flush following injection of 2
30 percent HGPV slug. This relatively shallow 2680
Foot Ransey Sand. recervoir is anticipated £0 yield
an increnental 17 percent OOIP due to. the tertiary
Broject. Cop utilization is expected. to. ber 9
BeE/STB. on a gross basis and’ around 9 nef/St on
net’ basis
KELLY-SNYDER (SACROC)$ The Scurry Area Canyon Reef
Operators Committee (SACROC) has bean ‘conducting a
niscible CO. flood in the Kelly-Snyder” field in
Scurry County, Toxas’ since 1972. Much of | the
SACROC COp project was implenented’ coincident with
a pattern ‘waterflood. “However, the two” areas
discussed below are believed to’ reflect tertiary
ecovery since. these areas were near watered-out
From water flooding
These two multi-pattern areas were studied in-depth
to better “understand the flood efficiency and
anticipated recoveries. The two areas are referred
to as the 4 pattern area (4PA) and the 17 pattern
area (17PA). "The 4P& contains 24 wells and covers
603 acres. “This area was at'a 95 percent watercut
When placed on COp injection in mid-1981. ‘Using 3
cumulative 3:1 WAG “injection ratio, the 4A was
Flooded with a 30 percent HCPV of Cp ‘through Nay
1986. Estimated "incremental "recoveries are
9.8 percent OOIP with a gross Cop utilization of
9.5 mef/STB and a net of 3.2 mcfATB. The larger
17a covered ‘roughly 2700 acres. and contained over
100 wells. "this pattern was also started on C09 in
‘mid-1981 and through Decenber. 1987, a 17.5 pergent
NcPV of COg had been injected ‘resulting in aSPE 10977 We R. BROCK,
Le A. BRYAN 3
cumulative WAG of 5:1 ultimate
jincrenental recovery is" anticipated ta reach
7-5 percent OOIP. The current gross CO utilization
in this pattern is'9.7 nct/SiB with an estinated
net utilization of 6.5 mct/STB.
MEANS, SAN ANORESS | This, miscible, COp project in
Andrews County, “Texas, operated by Exxon Company
U.S.A‘, commenced injection of COg in Novenber 1983
and 1s'expected to recover 7.1 pefcent of the OO(P.
This project is utilizing @ 2:1 NAG Injection in
the San “Andres dolomite, with an estimated
58 percent HCPY to be injected. This higher MAG
ratio was used to. improve sweep efficiency. Not
included in the estimated tertiary recovery is an
additional 9.2 percent O01? to "be recovered by
improved secondary performance through infil
drilling, and” improved reservoir managenent,,
associated with the tertiary recovery project. The
gross CO" utilization is estimated to be
18 ncf/ST®. No apparent WAG injectivity problems
were encountered in the laboratory or pilot. studies
and none have been encountered in the full-scale
project,
N.E.PURDY UNITS Cities Service (now OLY USA)
initiated a full-scale miscible C0, Flood in the
Springer "A* sandstone of the N. E. Purdy Unit. in
Garvin County, Oklahona. in Septenber 1882. The
majority of the Field is being processed with a
30 percent. HCPY siug while three patterns are on
Was injection. These ‘patterns. were placed on MAG
injection to 1) raise the pattern pressure or 2)
due to unfavorable production characteristics of
offset producing wells. Most of the wells in the
project had shown response to C02. injection
Following the injection of 15 percent. of the HCPV
of C02." Peak oi) production rates of two to four
times ‘the pre-response rates were conmonly observed
while the water-oil ratio was reduced from 30 to 8.
Observation well logging indicated good. vertica
sweep at a distance of 255 feet fron the injector
and also indicated a reduction of all saturations
fron 44 percent to. 25 percent... COp injectivity
appears to have improved with the cumulative CO
{nection whereas post-COz water injection appears
to be conparable to the pre-CO ingectivity. gross
Utilization of Cog is estimated to be 6.5 mef/SIB
white "the “net” utiTization should approach
4.6 mcf/STB. The anticipated incremental recovery
i8°7.5 percent OO1P.
NORTH CROSS?»®.9 The Flooding of this tripolitie
ratio The
chert ‘reservoir Tocated in Crane” and. Uston
Counties, Texas was initiated by shell in 1972
following primary depletion. by” augmenting the:
solution’ gas drive with gas” injections” The.
decision to forgo secondary waterflooding of this
reservoir was based on uniformly low permeability
The miscible use of COz 1s expected to result in en
incremental recovery f roughly 22 percent DIP.
with a gross COp utitization of over 18 mcf/ST3”
The estimated nef utilization will be between 7 and
Bnct/STB.
RANGELYIO This miscible Cop Flood operated by
Chevron U.S.A.” in. northwestérn Colorado in. Rig
Blanco County has "shown a slant ficant rapid
Fesponse since start-up in the fall of 1486. The
tertiary ‘project is designed for the 1:1 WAG
injection of a 30 percent HCPV ‘of Cop “in
approxinately 20 equal cycles. The Increnental
vrocovery attributable to CO, is forecast to be 106
Nipo of the 1413 Mbo OOIP ‘in the project ares, oF
7.5 percent. As of the fall of 1987, the production
build-up was in excess’ of 5000 bopd. “Estimated
timate recovery through secondary. operations 1s
Youghly 80 percent of OOIP. The major” operational
Ghaltenges facing this proJect are the development
of-effective diversion techniques. such a3. polimers
and foan diverters to control Gg injection and the
Snprovenent of scate snhibition treatuent. Tite and
costs. the occurrence "of barium sulfate, present
prior to the Coa Flood, has increased as the Tower
Bh has “resulted ina’ reduced effective life of
Seale treatnents. This miscible project tn the 6500,
foot’ deep eber sandstone 13 anticipated to have
gross. Cby “utilization of 9.2 Rcf/ST8 and 3 net
Utitization'on the order of 4-6 mef/STB.
SOUTH WELCH! The sisulation of the initial phase
Of this miscible COp flood by Cities Service. (now
OXY USA)" in the San Andres. dolomite in. Dawson
County, Texas indicates that’ an increnental
Fecovery on the order of 7 percent OOIP can. be
expected. ‘The similation of this project, which had
been infilled ‘to 10-acre. spacing, concludes that
the single variable — which fost. influences
incresental recovery is the value of (02 injected.
It was also determined that if a strong water
blocking” phonomena exists, a. continuous “slug
process would be more efficient ‘than a WAG process,
Simulation of South Melch indicates. an estinated
Ultinate recovery through secondary of 40.1 percent
OOTP whereas a C02 flood utilizing a 25 percent
HCY 2:1, WAG would ultimately recover 27.7 percent
OOIP."” Wo data indicating the anticipated CO
utilizations were presented,
TWOFREDS!2 This full-scale miscible C02 Flood
located in Loving, Reeves and Ward Counties, Texas
was the First such flood in a sandstone formation
in Texas. C0 injection commenced in early 1974 in
this reservoir with an average depth of 4620 feet
and. is projected to yield. an. additional
15.6 percent GOIP. The COp was followed by a
water‘alternating-exhaust gifs "(64.4 percent Noy
8:6 percent Cop 7 percent Chg) since 1980 asa
Flush. “The need to use exhaust gas Instead of the
originally planned ‘water was “due to. the low
inJectivity capacity of the injectors as compared
to the product ve capacity of the producers and the
higher viscosity of the ‘water as. conpared to the
Cog. While ‘the initial COp was "slugged, the
‘operator, HNG (now Enron), used WAG ‘injection in
the post “cog flood in order to contro} the viscous
Fingering of the exhaust. Nov apparent. inject vity
problens” occurred. and the injectivity of the
exhaust gas was 29 percent greater than. water
following Og.” et utiszation of COp 15 estimated
to approach & ncf/ST8. Corrosion of tubutars and
weliheads has been controlled. with 2 chemical
treatnent program using an oi1-soluble blend of
dinertrimer acid and imidazoline. This progran hes
resulted) In no. spectalized. metallurgy being
required for the wellhead, downhole ar” surface
equiprent..
WERTZI3 The perforsance of this project since its
start-up in the fall of 1986, clearly indicates
that miscible COg is displacing’ significant acount
of tertiary oil. This Anoco-operated project. in
central Wyoming has experienced better than
anticipated CO, inject ivity ‘with only "Vimited
deterioration of water injectivity foltowing the
og.” Log analysis indicate that both the vertical
and areal sweep efficiencies are favorable. The
anticipated increnental recovery from the Tensleep
Formation is 10 percent ‘of OOIP in the processed
area. The gross CO utilization factor is expected
to be between If and “18 mcf/STB. The net
utilization factor will be considerably less due toSUMMARY RESULTS OF CO, EOR FIELD TESTS 1972-1987
SPE_10977
the recycling of 0g and should be less than
10 mcf/STB.
MISCIBLE--PRODUCING PILOTS
This, second group consists of 8 miscible producing
pilots, whose various parameters are summarized in
Fapte i.”"These projects employed either cont inuous
slugs or water-alternating-gas (WAG) injection
Schemes, and were ina” variety of different,
feservoirs ranging fron the shallow to the ‘deep,
Fron low to high permeability, "and In, bath
Earoonate and. sandstone. "in alt ‘of these It has
bean qualitatively proven that CO can enhance off
Fecovery, however, "it should be noted. that the
Quantity’ of tncrecental oot in Some’ eases is. based
Gn ata. from s mich smaller" area_ than” ight. be
Taprecentetive of ‘commercial application.” Sone
Othe’ projects “utilized purchased —COp very
efficiently a6 noted by Ion net Cop util izattonsy
hile others. appeared Tess efficiant. Projected
‘nerenental recovertes ranged fros around 8 percent
QOIP to 21 “percent OO1P on net utilizations of
2.4 nef CO2/STB to near 13 mof CO2/STB.
GARBER FIELDS This central Oklahoma field,
operated by ARCO Oil & Gas Company, had a
Successful miscible COz pilot. in the waterflooded
Crews ‘Sand at an average depth of 1950 feet,
(W™P-1075 psig). The pilot area has. recovered an
estimated ‘T4 ‘percent "OOIP ‘Since “initiating COz
injection in’ October, 1981. This pilot was
originally designed to ‘inject a 25 percent HCPY of
Cop, yet a total of 35 percent HCPY was injected
The’ initial plan called for the injection of a
T percent HCPV slug followed by a 1:1 WAG to
control an anticipated. severe gravity override.
When’ the gravity override did not materialize,
continuous slug was injected. Following injection
Of the 25 percent HCPV slug, numerous producers had
yet to show response so the slug was increased to
435 percent HCPV. Once this larger slug had been
injected Cop injection was terminated in June, 1982
and the infectors put on water, since the optimun
Slug size had been attained even though production
had yet to show a decline trend. No injectivity
problems were encountered after the conversion to
water, Reservoir heterogeneities appear, to have
Contributed to the. control of the anticipated
gravity override. The pilot demonstrated that it
Was feasible to COp flood fields at. depths of less
than, 2000 feet and that good of1 recovery was
possible even when waterflood residual oft
Saturations were as low as 25 percent PV. Net COz
Utilization is estimated to approach 6 mcf/STB.
LITTLE CREEKI5,18,17 The het! operated cop pilot
in the Little ' Crock field “in southwestern
Mississipp in the mid-1970s denonstrated that C02
can effectively recover tertiary oi fron a
thoroughly waterflood depleted sandstone reservoir
such as the 10,400 foot deep Tuscaloosa Denknan
The average waterflood residual ‘ol! saturation in
this pilot was estimated to be 21 percent. A large
(160 percent CPV) slug of COz was injected during
the. pilot "without ‘alternating "water. slugs. The
ultimate tertiary recovery was estimated tobe 2s
high as. 45 percent of the waterflood residual oi
in the area, including the area between the pilot
injectors and producers and the “nearby. Field
pinchout, This equates to nearly 21 percent OOIP
Tecovered due-to tertiary. ‘Due to the large slug
injected the gross Coz” utilization. approached
27 mcf/STB and the net’ was around "13. mcf/STB.
Subsequent simulation of this pilot showed that. if
water were injected cyclically or simultaneously
with the COp, the effective mobility ratio of the
Gisplacenent would be decreased thereby increasing
the volumetric sweep efficiency
SepaElon ane By, Oe SEN Er aan
ihe gated” fe Coat caiens 3 ee
NorTH COLES LEWEE2® ARCO. of and, Gas, Cospany
initiated the first application of Cp injection in
the Kern. River Valley of california, ‘in dune 1981
The plist 1s in an area where many deep, Tight off
reservoirs are approaching their economic Vinit.
While a technical success, this pilot, consisting
of tio S-acre inverted five-spot patterns and one
Io-acre Tine drive pattern, was plagued with many
supply and pechanical.problens that masked
incremental oil recoveries. Pilot patterns were
also badly ‘out of balance due to either a
directional permeability trend or mechanical
problens, which resulted in reduced oi] recovery.
Using simulation, this 9200. foot deep sandstone
reservoir, with @ net pay thickness of 135 feet,
was. predicted " to ‘produce an incremental
15-20 percant.Oo1P with’ gross: Cog utsTizatton of
8-31 mc#/STB and a ‘slug size of 63 percent HCPY.
The simulation showed gravity override into the
upper zone of the Stevens. Main Western | sand
dominated the displacenent efficiency. Simulator
rasults indicated that the simultaneous, injection
OF Op tow Sn the reservoir ‘and water high ‘in the
Feservoir would greatly enhance sweep efficiency.
The C02 supply was from an area refinery that had
occasional upsets during the pilot, thereby
Tiniting the “supply, ard causing the pftot to be
terminated in mid-1986.
QUARANTINE BAY21 The pilot flood of the Quarantine
Bay 4RC field in Plaquemines Parish, Louisiana
gemonstrated that the COp-MlG "process ts
technically viable for. mobifizing considerable
anounts of residual of)" from the watered-out
Miocene semi-consolidated sand reservoirs of the
GuTF Coast of Louisiana. ARCO O{1 and Gas Company,
the operator, started inJecting COp in October 1981,
in a bJ-acre’area of the Field located southeast of
New Orleans.” Injection continued on a 1:1 WAG
until a total of 18.9 percent HcPY of CO had been
injected. In February 1983 injection was converted
to water and anticipated recovery is expected to
reach 15.8 percent GOI. ‘The net utilization of8977 WR BROCK, L. AL BRYAN
Op is. slightly less than 3 mcf/STB. The small
Stig size was Selected because larger slug_stzes
could not "be economically justified. Reservoir
Simulations indicated. the increnantai recoveries
for slug sizes between 15 and 38 percent CPV did
not vary ‘significantly and. therefore the -snaler
Slug "size and. resulting Tower utilization would
prove economics. Because. of the dissolution of
carbonate cementation by the carbonic acid, the
injectivity appears to have increased. “Ths has
also led. to the inereased ‘occurrence of sand
reduction ‘not previously noticed in the field.
his flood "experienced tone nechanical problems
related to corrosion which resulted ‘in the
Premature shut-in of producers. The operator
estimated the incremental recovery could have
approached 20 percent OOIP had these problens been
avoided.
SLAUGHTER ESTATEI8,22 This miscible WAG pilot in
the carbonate San ‘Andres reservoir underlying the
Slaughter Estate Unit operated by Amoco in Hockley
County, Texas has shown that significant quantities
of tertiary of7 can be recovered using a solvent of
72 percent COp and 28 percent HyS. The water
alternating solvent injection resulted in reduced
injectivity during the solvent phase but subsequent,
ofl production has shown. that. the alternatin
sequence of injection provided excellent area
sweep. A26 percent HCPY. of the solvent. gas. was
injected between August 1976 and October 1979. This
solvent injection was then chased by a 30 percent
HcPV" "slug of nitrogen. The projected Solvent
utilization, not including the nitrogen, 15,
anticipated’ tobe in the range of "3-5 mct/STB.
Incremental recovery is estinated by simulation to
be at Teast 20 percent O01
WEEKS ISLAND23 The Weeks Island S Sand Reservoir B
in New Iberia Parish, Louisiana, typical of many
plercenent salt-done fields in the Gulf Coast area,
vas the target of a gravity stable COz pilot test
by Shell in October 1978. This plot demonstrated
that a gravity stable COp flood is very effective
jn. these reservoirs which have highly. efficient
strong. water-drives. "Rt the start of ‘the COz
injection in 1978, the residual oil saturation was
estimated to be 22 percent, The very permeable
(1200" “nd),” steeply” dipping "(26") Sandstone
Feservoir received an initial CO slug equal to
24 percent 'HCPV mixed with about Six sole percent
of matural gas, primarily ethane. The COz was
dituted to Tessén ‘the risk of gravity instability.
When gas production rates began to increase tn
1983, “the "Cd contaminated gas was re-injected.
This’ pilot 18 expected to recover an estimated
8.9 percent OOIP. Gross Cop” utilization 1s
Projected to be 7.9 mcf/STB at. the end of the
pilot, with net utilization around 3.3 me¥/STS.
WEST SUSSEX?# This of]-in-the-tank pilot by Conoco
Supports the feasibitity of miseibly (Op. Flooding
Ene" Shamnan "sandstone and" other’ siailar. Tow
Fesidual, Tight ofl. reservoirs Sn the Powder River
Basin of Wyoming. Between id-1982 and Tate-1985 4
30 pereent HCPV" slug. of (Oz, preceded and fol lowed
by ‘water, was. injected into this 9.6-acre pilot
without’ any" apparent ‘injectivity impairment. "The
Option of using WAG was Teft open during the’ pilot
Should prenature CO breakthrough justify a switch
from the slug. The’ estimated incremental. recovery
from this 3000, foot deep watered out. shaly maring
sandstone is. 8.9 percent of O01P.. The resultant
gross utilization OF COp was 12.9 mcf/STB. It was
@stinated that. 20 percent of the “cumulative COp
‘injected was produced. Lack of of1 response in ong
of three pilot producers Ted to the conclusion by
Conoco. that @ waterflood injector should not be
converted toa tertiary producer without careful
consideration.
‘MISCLBLE--NON-PRODUCING PILOTS
These two non-producing pilots were conducted with
observation wells offsetting the injection well to
monitor the movenent of the COg inthe reservoir,
By logging these wells the operator is able to
detect the changes” in residual. oil saturations as
the COg front passes. Conbined with pre-and
post-piot core” analyses, the data from the
Sbservation wells is used to simulate the recovery
process. Based on these similations, predictions
Ere made of expected incremental recoveries and
anticipated injected volumes. AS with the
Predictions of other projects, these pilots proved
that C02 can mobilize waterflood residual of!
However,” due to the nature of the data these
predictions should be used with caution.
‘CEDAR CREEK ANTICLINE?5 The non-producing miscible
2 pilot conducted by Shell in. the South Pine
Field of the Cedar Creek Anticline in eastern
Montana between 1983 and 1985, showed that tertiary
oil can be effectively sobilized and displaced by
C02. The residual off saturation after waterflood
was’ estinated to. be between 38 percent and
40 percent, and after miscible CO injection
averaged 20 percent. The. test also showed that
Vertical conformance of ‘Op was the same as for
brine in the pre-flush leading to the conclusion by
Shell thatthe volunetrie: sweep eFFicfency.of 2 cdg
Flood in this Red River crystalline dolomite woul:
bersinilar to that of the waterflood, provided the
effective nobility of COp ts controtied. It, was
also concluded that the waterflood behavior of the
Red River formation could be profitably studied to
predict CO flood behavior. the injectivity of COg
was found fo be roughly 1€ tines that of the brine
in the pre- Flush.
LITTLE KNIFE26 This five-acre inverted four-spot,
fon-producing pilot conducted by Gulf (now Chevron}
{n' 1980-1981 was in. the dolomitic Mission Canyon
Formation. Located in the Williston Basin of North
Dakota, "this 9800 foot deep reservoir. was CO
flooded using a 1:1 WAG injection. With. data
obtained from logging of observation wells and from
pre: and post-flood core analyses, simulation using
Both a black ofl and compositional simulators was
conducted. The results” of these simulations
revealed that the WAG injection of a 22 percent
HCPV of COp into this” highly stratified and
relatively. Flat’ reservoir would improve the
Uitimate recovery by 8 percent ‘of O01P, 4f flooded
on 160-acre spacing. The simulation also predicted
et COp utilization of a comercial scale flood
Would Be around'5 nef/STB.
BLE--FIELD-SCALE
The, immiscible use of (Op can be classified as
ENiher a multiewelt, Sngeetfon of 8 continuous Ta
or WAG, “or as individual wel? stioulations referred
fo Nae’ Shute ni putree The prieary” recovery
Hichanisns of Inatscible. COp. projects are the
Viscosity reduction and. svelT¥ng”of the. contacted
rage off,""Recuctvon of the off viscosity creates
snore favorable. sobility" ratio. witch in turn
Tesults in improved: seep efficiency and 2" lower
residual ‘i "saturation to watertioding at the
Economie init. "OFT averting ‘nereases retovery bySUMMARY RESULTS OF CO, FOR FIELD TESTS 1972-1987
SPE 18977
reducing the stock tank residual of1 saturation
From water flooding
The paraneters of the Field-scate miscible Floods
are "shown. on “Table 2. These two” Floods. had
predicted incremental recoveries. between 9 and 10
percent OOIP, and net COp Utilizat’ons were between
Brand 12 mcf/STB. "As with the fleld-scale miscible
Floods, the incremental. recoveries are In. sone
cases based on extrapolations of early performance
Gata and shoutd be used with caution
HANSFORD MARMATON!S.27 This project in Hansford
County, Texas, has proven that 'COg can be used to
epressure a depleted reservoir. Although the tine
to repressure was considerably Tonger. than with
water, the existing free gas phase in the reservoir
Gistributed the CO throughout, contacting nore of
the OO1P than would have been contacted by miseibie
Gisplacenent. given the unfavorable CO mobility
ratio. At start-up in mid-1980, the® reservoir
pressure was an exceptionally "low 250 psig.
Inmiscible injection of purchased (Op has raised
the pressure to near the miscibility pressure after
which the recycle gas will be injected in a yet to
be determined WAG ‘sequence. "Projected incremental
Fecovery due to the immiscible effects of CO is
about 3 percent OO1P with a net utilization of
12 ncf/STB. As this project starts the tertiary
miscible recovery phase, the field is producing
ver $50 bopd as compared to 30 bopd at the start
of op injection, “The Final net ubittzation of Cop
Js anticipated do bees, than 7. mct/STb, whic
based on a purchase of 13.7 Bef of (Og translates
to an incremental recovery from COp Injection of
about 15.6 percent OO1P, inmiscible and miscible.
LICK CREEKIS.28 This full scale COp flood in
Bradley and Union Counties, Arkansas ty Phillips
Petroleum has successfully proven the viability oF
an ‘impiscible WAS process’ for” the recovery of
tertiary ofl ‘from thin, heavy oil. sands. Started
in’ 1978 Using’ Cog" from” an” anmonia "planty. this
project. is" anticipated to. recover’ an "increnental
1O percent, oe the aby 18) ep ell
originally-in-place in this. "high permeabi) sty
Heakin. sandstone reservoir. "Injection of |
40 percent HCPV slug’ of (Op on a 1:1 WAG Patio. was
done'in "three phases. ‘The first phase involved
eyelic "C0" injection into all the’ producers. snd
hany of ‘the Injectors." This helped increase the
reservoir pressure and allowed wells, to be. flowed
haturally." The. second phase involved ‘Injection ef
‘large yolimes ‘of COp'into. the permanent. injectors
the third phase. alternated (Op and water injection
into tho Injectors, After. this phase, the Unie
willbe ‘waterflooded. The” expected gross
utilization of COp is 8.8 mcf/STB, which will net
to approximately $.3 mcf/STB.
ImScIBLE-- ING PILOTS
These two producing pilots, whose parameters are
also shown in Table 2, have projected incremental
recoveries of § and 10 percent OOIP. In both of
these pilots, it has been qualitatively proven. that
op can enhance oi! recovery, however, it should be
noted that the quantity of incremental of] in some
cases is based on data from a much smaller area
than might’ be representative ‘of a conmercial
application.
HILLY UPLAND29 This minitest in West Virginia
conducted by the Alleghany Land & Mineral Conpany
in conjunction with the Departnent of Energy
Morgantown Energy Technology Center’ showed that. low
permieabil ity (3 md) dovs not prevent the injection
Of low-viscosity. fluids “suchas COp, It also
Showed that when water cannot be “injected” at
economical rates to repressure a reservoir or to
displace the solvent slug in a tight dolomitized
Limestone reservoir that C02 “could possibly. be
used. This pilot showed that although’ miscibility
was only attained ‘in the near wellbore region of
the “injectors, the swelling of the olf, the
viscosity reduction and. the increase in reservoir
eneray, dug to Og” injection ‘resulted "in an
estimated 5 percent S01? increnental recovery.” The
estimated “gross utilization. was "6.4 nef/STB.
Although the resultant. incremental recovery was
Tower than for most Cz floods, the fact” that
95 percent of the Cz was still in the reservoir at
‘the tine of the paper could continue to benetit
recovery.
WILMINGTON The use of immiscible CO in a WAG
Flood of highly viscous ‘rude ofls 40 enhance
recovery has. ‘been. demonstrated by Champlin,
Petroleum (now UPR) in the Wilmington Tar Zone in
the Los Angeles Basin of California. The test
shows that’ the "displacement effictency of
imniscible Cop on viscous crudes is not as good 35
the miscible displacesent of lighter crudes by CO
However, since waterflood residual oil saturatioss
are typically much higher for the viscous crude
Oils, opportunities ‘still exist for significant
incréased oi] recovery. The Tar Zone crude, with 3
viscosity of 283 "cp, is "swollen to "about
105 percent of original ‘voluse when contacted with
Cop." the viscosity is” reduced dramatically” to
is"cp when contacted at a pressure of 1080 psig.
By chasing the swollen and less viscous crude of
with water, the anticipated incremental recovery
will “approach II percent O0IP. The gross
Utilization of Cop 1S calculated to be 6 mcf/STB,
with much of thfs supplied through the "recycle
process.
IMMISCIBLE "HUFF *N? PuFE*
Inmiscible Huff 'n? Puff well stinulations appear
to'be gaining. in popularity possibly due to their
relatively quick payout nature, These single well
Tecovery projects utilize C0,” froma variety oF
Sources” which is typically’ rucked “to. the well
site. This. tertiary’ recovery “method is. ideally
Suited for’ small leases which ‘cannot stand’ the
large’ up-front | Snvestnents associated with. many
fFieldewide floods.” While the procedure ts sim lar
to the" steam stimulations in the heavy off basing,
these cyclic 02 projects are not limited to heavy
oil since the technique has been successfully. used
to “recover. lighter oils. While. increyental
Fecoveries as a porcent ‘of OIP are not available,
the consensus of the papers reviewed ts that. these
projects do recover increnental o') with relatively
Yow utilizations. of C02. The incresental ott
Fecovered was production’ in ‘excess of the. bese
Production “dectine curve and “in most’ caves “the
Wells. were at or near ‘the economic Tisit, prior to
the test
The general procedure 1s to inject large volunes of
Cog, own’ a producing wel bore and. then shut=tn the
wel) or ‘afew weeks to. allow ‘the Opto. soaks
Following “this. Soak, ‘the’ well “is returned. to
production, Some "increases in oi] “rate were
fustained for up to 48 months. The efficiencies of
the “process. are measured. ‘by’ the mcf/Si8. oF
increnental ofl recovered and also by the volune
injected. per” foot of UtiMzations ranged
Between 1 Bcf/STB and sVightly over 3 net/sTB while10977
MLR. BROCK, L.A, BRYAN
1
stimulations ranged between 0.1 Micf/ft_ to
0.4 HUcf/FL. Shown on Table 3 are’ some parancters
of the projects discussed below.
APPALACHIAN BAIN® Huff 'n" PUFF Op field tests
on 65 wells in a pressure depleted Appalachian
Basin reservoir. in eastern Kentucky indicate. the
economic viability for light ofl recovery. These
tests" were. conducted in conjunction” with a
Vaboratory evaluation at Louisiana state University
which addressed the potential of recovering Tight
O51 with the application of immiscible cyclical C0;
injection. The field tests ‘targeted the unnane
Appalachian Field because of the low permeability
formation and disappointing pilot" waterflood
results. The procedure used was to first pull the
ods from the well and inject large volumes of C02
down the tubing at the rate of several barrels per
minute. The well was then shut-In without
corrosion inhibitors for approxinately ‘one. week
After the initial soak period, the well was then
placed back on production. Response was a sharp
ise in ofl production which continued for 15 to 48
hnonths after. which production returned to. the
original hyperbolic decline curve. The resulting
Tow COg ut izations of about 1 mcf/STB attest to
the economic viability of Huff ‘n? Puff in Tight
ON “reservoirs. Field’ tests | suggest that the
Fesponse improves with thicker pay, that C0
reduced. the water cut and that. a Second cycticat
application could recover additional reserves.
PARADIS32 This COz Huff 'n” Puff project was one
of eleven wells in five fields which Texaco tested
in South ‘Louisiana during 1984 and “1965. The
results fron this test west of New Orleans in the
Paradis Main Pay Sand, Reservoir T, ‘indicate. that
cyclical use of COp is effective in the tertiary
Tecovery of light O11. “The process involved the
injection of COp in the well, followed by a soak
period after which the well was returned. to
production. In this particular case, two cycles of
Cop were utilized. The first cycle involved the
indgction of 18 Mcf of COp aver a three-day period
in Merch 1884 followed by three week soak. "After
being returned to production, the initial rate was
180" bopa a compared fo £2 Sep prior to. the test
‘he well produced 8000 barrels of ot! in excess. of
the “base” decline curve prior to. receiving. an
additional 21 Mlct oF 'COp in February 1985 over a
Five day. period... After ‘being opened. up. in. March
1985, the. well “flowed” 228 bopd The “cumulative
inerésental” recovery. fron these two. cycles. was
20:7 Hoo. This resulted In a nat COp utilization
of only 1.8 ‘mef/S1B. The. tests shoved. that the
faster the’ rate of injection the further the cop
Mii Fieger Out Into the reservoir thus contacting
TEXAS GULF COASTS Texaco tested the feasibility
of an immiscible Cop Huff ’n* Puff on 28 wells in
Texas Gulf Coast Mfocene Reservoirs. Fro these
tests in twelve unnamed off fields, viscosity
reduction and oi] swelling appear to. be the
principal ‘mechanisms of recovery since ‘no
Compositional changes were noticed nthe produced
oil.” These tests. were conducted on’ gravities
ranging, from 23" "to 30°API, and viscosities. of
1,633.4 ‘cp. "Increased recoveries were only
slightiy improved for the more viscous crudes and
for lower API gravities.. Wo correlation was seen
between the pre-test oil cuts or permeabilities,
and’ ‘the resulting of1 recoveries. Based on
‘increnental recovery, these tests did show that for
these reservoirs 2 ‘soak period of 2 to 3 weeks
seened better than shorter or Tonger tines.
TIMBALIER BAY24 This immiscible Huff *n” PUFF test
conducted by Chevron, proves the feasibility of
Using COp in’ this’ bottomeater-drive sandstone
reservoir in ‘Louisiana. The tast in two. wells
showed that when properly administered the CO Huff.
*n’ PUFF process’ can provide for a guick payout
with a Tow” capital "investment." The results
indicate that increnental ofl was recovered through
the o1T swelling and viscosity reduction effects on |
fractional-flow. AS in similar imaiscible
applications of Cop, “the rocess was to inject §
large volune of bq inthe producer and then
shutein “for a” soak’ period after which it was
returned to production. Thase two tests. measured
Cop stimulation efficiencies of 0.3-0.36 Me#/foot
of pay and COg utilizations of 1.1-3.2 mef/STB. The
fests’ iso. “showed that “for” this “particular
Teservojr 2 soak period ef about 7 weeks Gia better
than’ s &!week soak on’ one wel»
WEST COTE BLANCHE BAY22 This COp Huff °n’ Puff.
project was one of eleven such tests conducted by
Yexaeo.in South Cousstana’ betwoon 1984cand. 1985.19
evaluate tertiary recovery. The results from this
fest'n the 14 'sand Reservoir. 3iz indicate that
tertiary ‘olt_can''be effectively recovered. using
yetical °''c0p. the. process was the
‘nject-soak-praduce method of previously eiscussed
huPt ta" pu? tests, “This particular test involved
the injection of 8 Mic of 0g in te hours in Haren
eee "Fottoming 'a!isosk” of out four. weeks. the
well was. placed” on continuous productions Withis
the! weeks, production” had increased from @ bopg
prior to the vest to" 170; bopt. the well” produces
{rcrepental of? until February 1805.""% total of
BEET barrels of increzental off were’ protucee at
net Og utilization of only 2-8 met/Stb. this, test
td others showed that “the higher ‘the rate’ of C0
‘ndeetion inte, the reservoir the further” out 1
would Finger thereby "contacting more ott. “Texaco
oneluded that the C02 Hutt Sn’ Putt process oF
Eyelical injection cane recover “incremental ot) In
Péservotrs gf various rock and fluid properties n
South Louistana
Summary
A variety of methods qualitatively prove the use of
op" does”ethance the Pecovery of restaual 011 fron
Tebervoirs of ifferent depositional. environments:
These range from the. smmiscible, Hurt nt Path
single wel stimilation to the full-scale misciole
projects. It has also been used. in Tjeu of the
Eraditional secondary” waterfiood.." Tncromentat
Fecoveries predicted” by" the. vartous operators
reviewed ranged from 5 "to “22 “percent oF
original ofi-in-place. Sone of these projects wore
fore eftietent: than ethers as evidenced by the Coy
UUIT fzation values, which ranged. from a 2-4 met/SI
0 13-nc1/51B on a'net basis.” Phasing of a profect
ney! ainisize the. ‘purchased cog" requirocents: by
Spreading sane over’ 4 greater riod of time, and
aay 'also “naxinize the use Of less’ expensive
retyeted cop.
These projects do show a need for adequate data
management in the primary ‘and secondary recovery
Stages as wel], a5 in the tertiary process. This
will permit the operators to properly evaluate
appropriate enhanced recovery Bathods” prior to
depletion. knowledge gained from projects or tests
in other ‘parts of the country can be used as a
guide in formulating an enhanced recovery. plan.
However, the predicted recoveries and efficiencies
reported by “other projects should be viewed
qualitatively rather than quantitatively since mostSUMMARY RESULTS OF CO, EOR FIELD TESTS 1972-1987
SPE 18977,
of the performance extrapolations are from data
relatively carly In a project’s Jife. As the
projects currently in operation age the performance
predictions will be further refined and will becone
more quantitative.
ACKNOWLEDGEMENT.
The authors wish to thank Exon Conpany U.S.A, for
the “permission” to” publish this paper, "and the
Ingividual authors ofthe reference ater) for
bl ishing the results of their EOR projects... They
B20. thank ‘those Involved “in. the ‘review of ‘the
paper ‘and. Shiriey ‘Keesey. for her ‘assistance “In
preparing the manuscr‘pt
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32. Palmer, F.S.. Landry, RoW. and Bou-Michael,
Si:NDesign’ ahd Inplementation Of Imiscible
Carbon Dioxide | Displacerent’ Prosects "(C0
Huff-Puff) in South Louisiana,” Paper SPE 1549
resented at the 61st. Annual Technical
jonference “and Exhibition, New Orleans,
Louisiana, October 5-8, 1985.
33, Haskin, H,K, and Alston, 8.B.:"An Evaluation of
HUEF Sn? PUFF Field Tests in Texas.” Paper
SpE 15502 presented at the Gist’ Annual
Technical Conference and _ Exhibition, New
Orleans, Louisiana, October 5-8, 1986.
34. Simpson, M.R.:"Tho COp Huff 'n’ Puff Process in
4a Bottomater-Drive Reservoir," Paper SPE 16720,
presented at the 62nd Annual Technical
Eonference ‘and Exhibition, Dallas, Texes,
September 27-30, 1987,SPE 18977
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