Beruflich Dokumente
Kultur Dokumente
11
Vol.51
2015 11 1391-1399
Nov. 2015
No.11
pp.1391-1399
TC4 *
1)
1)
1)
2)
1)
1) , 110136
2) , 100024
(friction stir welding, FSW) 2 mm TC4 ,
. , 50 mm/min 300 r/min ,
b . ,
b . b , a a b ,
a . , a b , b a
. 350 r/min , b , a ,
a . a , , .
, TC4 , , ,
TG453
0412-1961(2015)11-1391-09
ABSTRACT As a solid state technology, friction stir welding (FSW) has been used to join titanium alloys for
avoiding the fusion welding defects. So far, many previous studies have attempted to elucidate the microstructure
characteristics and evolution during the FSW process of titanium alloy, but few are about the mechanism of microstructure transformation along the thickness direction of joint. For solving this problem, in this work, 2 mm thick
TC4 titanium alloy is successfully welded by FSW. On the basis of numerical simulation, the effects of temperature
distribution on the microstructure along the weld thickness direction and the tensile strength of welding joint were
investigated. The results show that the peak temperatures of material close to weld surface exceed b phase transus
temperature under the rotational speed of 300 r/min and the welding speed of 50 mm/min. With the increase of distance away from the weld surface, the peak temperature decreases. The peak temperature of weld bottom near the
backing board is difficult to be higher than b phase transus temperature owing to quick heat radiation. The region,
where the peak temperature is higher than b phase transus temperature, consists of primary a, lath-shape a and residual b phases. The size of lath-shape a inside the weld is larger than that near the weld surface. Primary a and b
* 51204111 2013024004 2014024008
: 2015-02-05, : 2015-07-03
: , , 1977 , ,
DOI: 10.11900/0412.1961.2015.00099
1392
51
phases with smaller size are attained in the weld bottom owing to the dynamic recrystallization, and the distribution
of b phase on primary a matrix is more homogeneous. When the rotational speed reaches 350 r/min, the area where
the peak temperature is higher than b phase transus temperature becomes wider along the thickness direction,
which makes the size and quantity of lath-shape a phase increase and then the lath-shape a clump appears. Lathshape a phase with different orientations hinder the propagation of crack and be beneficial for the tensile strength
of FSW joint.
KEY WORDS friction stir welding, TC4 titanium alloy, peak temperature, microstructure, tensile strength
,
,
,
[1~4]. ,
,
[5,6].
(friction stir welding, FSW)
, Cu, Mg Ag
[7,8]. , FSW
, [9,10].
, FSW
, , FSW
[11~13].
[11] TC4 FSW
, , b
a + b , a
a + b . Zhou [12] TC4 FSW
, ,
a+b .
[13] TC4 FSW
, ,
a/b .
, FSW
.
,
, FSW
,
. , ABAQUS/Standard TC4 FSW
,
.
. : 300
350 r/min, 50 mm/min.
W-La , 12 mm,
6 mm, 4 mm, 1.8 mm.
H2, O2 N2
, Ar .
.
Kroll (13 mL HF + 26 mL HNO3 + 100 mL
H2O). Instron
, 5 mm/min.
GB/T 2651-2008 ,
1 . GX71
(OM) SU3500 (SEM)
.
2 FSW
2.1
ABAQUS/Standard FSW
.
. 2 .
FSW ,
1
Fig.1 Schematic of dimension of tensile specimen (unit:
mm; RSretreating side, ASadvancing side)
1
200 mm100 mm2 mm
TC4 ,
(, %): Al 6.17, V 4.08, Fe 0.30, C 0.1,
11
: TC4
1393
, .
20 . 2 mm
. 0.25 mm .
, ( 2). , 250880
DC3D8 .
. ,
2.2
FSW
100 W/(m2). ,
. [14]
50 W/(m2),
0.7; ,
, .
90 W/(m2). 5
3
0
(1)
, QS , R 0 , r 0
3.1
, T .
NiCr-NiSi .
, R eL (T) , n
,
300 350 r/min
:
Q P = 0.25QS
(2)
6 . , l
, Q P .
. ,
12 mm , 6 mm,
. ,
1.8 mm . (1)(2)
Ar
, ABAQUS DFLUX
.
2.3
FSW
,
.
, , 4450 kg/m3. 3 4
TC4
1394
51
2.467% 1.815%.
. ,
( 5).
, .
, TC4 FSW
476.139 368.589 ,
7 . 0.5 mm
487.887 375.279 ,
4 . ,
1080~983 1100~1000 .
FSW , ,
,
, 300 r/min
350 r/min . ,
, ,
,
,
NiCr-NiSi
3.2
TC4 FSW
8 . ,
, .
Ar ,
Color online
7 TC4
Fig.7 Cross section temperature distributions of TC4 titanium alloy weld joints under rotational speeds of 300 r/min (a)
and 350 r/min (b)
8 TC4
Fig.8 Macrostructures (a, c) and cross section morphologies (b, d) of TC4 titanium alloy weld joints at rotational speeds of
300 r/min (a, b) and 350 r/min (c, d) (HAZheat affected zone, SZstir zone, BMbase metal, SAZshoulder
affected zone)
11
: TC4
1395
. ,
. 10
( 7)
. 4 :
. , d .
(SZ)(SAZ)(HAZ)
, .
(BM).
a a
3.3
b ( 10a). ,
TC4
a , FSW
, .
. ( 7b),
()
1080 , b ,
FSW , (b ).
, .
[15]
[19~21]
[16~18]
, . TC4 V
b , (a+b)/b (b ) 1003 ,
Qazi [23] b 1005
.
TC4
a b ,
b a , 9
. , a
b .
FSW , TC4
9 TC4 SEM
Fig.9 SEM image of base material of TC4 titanium alloy
1396
51
, b ,
Ar
, ,
. ,
b a b ,
, a
bcc-bhcp-b . a b
, 10b a
, a . a
. 10c b
b ,
, 10c
a b a + b
a .
. , TC4 b
10d .
, a b ,
a , a b
b a . 10a b
, b a .
a , . ,
, b
, a + b .
, a b . FSW
,
ab ba , 2
, a .
, b
, a ,
b a . [12],
a . TC4 FSW
11 .
7b ,
, 1.5 mm
b ,
( 10a~c).
b a
TC4 700 .
,
, . ,
a b .
300 r/min , TC4
12 .,
0.75 mm
11 TC4
Fig.11 Schematic illustrations of microstructural evolution mechanism of TC4 titanium alloy weld joint
(a) initial stage
11
: TC4
1397
b ,
b a + b ,
a a b (
( 12c).
12a~b).
3.4
, b a ;
, a
, 12b a ,
, . , FSW
a a .
[24~27].
, , b
b ( 7a),
, b a .
a ( 12c d),
a ,
a b
. ,
12 10 ,
a b . b a
a , a
, ,
a ( 10b c),
, .
, (
13 . FSW
7). FSW ab
, (RS)(AS)
. , b
, HAZ
a . ,
[28,29], 2
, a
AS .
. ,
( 10b 12b),
b ,
45, .
10c a
1398
51
TC4 . ,
,
. , a
13 TC4
( 10 12),
11
: TC4
1399
, . ,
[10] Zhou L, Liu H J, Liu P, Liu Q W. Scr Mater, 2009; 61: 596
( 14b 15b). ,
a ,
( 14c). , ,
b ,
a , 14 , 15
4
(1) , TC4
,
b ,
b .
(2)
, .
a , a
.
, a b , b a
.
(3) ,
a , a .
a
.
(4)
. ,
,
, .
(:)