Organic Synthesis - Experiment Observations

Practical No.4

Density of Butyl Acetate = 0.8818 gm/ml

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No. of obs. Temperature C Measured volume of ester (ml)
1 65 10.5
2 70 11.2
3 80 9.5
4 90 12
5 95 13.2

Calculate yield %

Practical no. 5

Density of Butyl Acetate = 0.8818 gm/ml

No. of obs. Time (min) Measured volume of ester (ml)
1 20 12
2 30 11.5
3 35 11.5
4 50 9.5

Calculate yield %

Practical no. 6

Density of ethanol = 0.816 gm/ml

Density of diethyl ether =0.7147 gm/ml
volume of diethyl ether =7 ml

Calculate yield %

Note: Complete and Submit the practical journal 10 days before OS viva voice