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c:\rossana\data\050508.012
c:\rossana\methods\Lig60m7.met
c:\rossana\pretreat\Bbb1.aoc
1 1 1
0 0 0
Minutes Minutes Minutes
Volts Volts Volts
0.02 0.02 0.02
1.00E-06 1.00E-06 1.00E-06
MAB1006 St2_0
Date 6-May-08 Lig60m7.met 7-Feb-08 Lig60m7.met 6 vessels microwaved 7-Feb-08 Lig60m7.met 6 vessels microwaved fr2 vol 500 ul
Filename 050508.011phenol 20ng 050508.002 MAB1006 St2-0A total FR2 smp 4.2 050508.003 MAB1206 St 14-0 R1 Btotal
(400FR2
ul) smp 4.2
Parameter RT (min) AREA RRF RT (min) AREA corr AREA wgt (ng)/1ul smpconc ug/ L RT (min) AREA corr AREA wgt (ng)/1ul smpconc ug/ L AVG STD CV (%)
Vanillyl Phenols (V)
VAL 19.7 32957 19.74 1544 1204.83 0.38 0.03 19.72 2592 1925.08 0.59 0.05 0.04 0.01 31.11
VON 22.14 37960 22.21 620 483.8 0.2 0.02 22.19 931 691.46 0.26 0.02 0.02 0 19.25
VAD 26.5 50655 26.5 2262 1765.1 0.55 0.05 26.49 2851 2117.44 0.64 0.05 0.05 0.01 10.83
total V 0.09 0.12 0.11 0.02 61.2
Date 6-May-08 Lig60m7.met 7-Feb-08 Lig60m7.met 6 vessels microwaved 7-Feb-08 Lig60m7.met 6 vessels microwaved fr2 vol 500 ul
Filename 050508.011phenol 20ng 050508.005 MAB1006 St2-200A total FR2 smp 5.1 050508.006 MAB1006 St2-200B total FR2 smp 5.1
Parameter RT (min) AREA RRF RT (min) AREA corr AREA wgt (ng)/1ul smpconc ug/ L RT (min) AREA corr AREA wgt (ng)/1ul smpconc ug/ L AVG STD CV (%)
Vanillyl Phenols (V)
VAL 19.7 32957 19.73 3383 2474.26 0.75 0.08 19.79 494 366.98 0.13 0.01 0.04 0.04 99.83
VON 22.14 37960 22.19 1169 854.98 0.31 0.03 22.19 501 372.18 0.16 0.02 0.02 0.01 43.29
VAD 26.5 50655 26.49 4885 3572.79 1.01 0.1 26.5 1618 1201.96 0.4 0.04 0.07 0.04 61.04
total V 0.21 0.07 0.14 0.1 204.16
Date 6-May-08 Lig60m7.met 5-May-08 Lig60m7.met 6 vessels microwaved 5-May-08 Lig60m7.met 6 vessels microwaved fr2 vol 400 ul
Filename 050508.011phenol 20ng 050508.004 microblk050508A total FR2 smp 6.4 050508.007 microblk050508B total FR2 smp 6.4
Parameter RT (min) AREA RRF RT (min) AREA corr AREA wgt (ng)/1ul smpconc ug/ L RT (min) AREA corr AREA wgt (ng)/1ul smpconc ug/ L AVG STD CV (%)
Vanillyl Phenols (V)
VAL 19.7 32957 nd 0 0 0.02 0 nd 0 0 0.02 0 0 0 0
VON 22.14 37960 22.15 2246 2124.17 0.69 0.11 nd 0 0 0.05 0.01 0.06 0.07 121.42
VAD 26.5 50655 26.57 513 485.17 0.22 0.03 26.57 1119 1026.42 0.36 0.06 0.05 0.02 34.33
total V 0.15 0.07 0.11 0.09 155.75