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Analytical Report

Bill To: Pure Spirit Water Services Project: Lot ID: 685365
Report To: Pure Spirit Water Services ID: Control Number:
Spirit River, AB, Canada Name: Date Received: Jun 2, 2009
T0H 3G0 Location: Date Reported: Jun 5, 2009
Attn: Vern Howrish LSD: Report Number: 1224418
Sampled By: P.O.:
Company: Acct code:

Reference Number 685365-1


Sample Date June 02, 2009
Sample Time NA
Sample Location
Sample Description DI Water
Sample Matrix Water
Nominal Detection Guideline Guideline
Analyte Units Result Limit Limit Comments
Physical and Aggregate Properties
Colour Apparent, Potable Colour units <5 5 15 Acceptable
Turbidity NTU <0.1 0.1 5 Acceptable
Routine Water
pH 6.29 6.5 - 8.5 Low
Temperature of observed °C 22.7 n/a
pH
Electrical Conductivity µS/cm at 25 C 1 1 n/a
Calcium Extractable mg/L <0.2 0.2 n/a
Magnesium Extractable mg/L <0.2 0.2 n/a
Sodium Extractable mg/L <0.4 0.4 200 Acceptable
Potassium Extractable mg/L <0.4 0.4 n/a
Iron Extractable mg/L <0.01 0.01 0.3 Acceptable
Manganese Extractable mg/L <0.005 0.005 0.05 Acceptable
Chloride Dissolved mg/L 0.4 0.4 250 Acceptable
Fluoride mg/L <0.05 0.05 1.5 Pass
Nitrate - N mg/L <0.01 0.01 10 Pass
Nitrite - N mg/L <0.005 0.005 1 Pass
Nitrate and Nitrite - N mg/L <0.01 0.01 10 Pass
Sulfate (SO4) mg/L <0.9 0.9 500 Acceptable
Hydroxide mg/L <5 5 n/a
Carbonate mg/L <6 6 n/a
Bicarbonate mg/L <5 5 n/a
P-Alkalinity as CaCO3 mg/L <5 5 n/a
T-Alkalinity as CaCO3 mg/L <5 5 n/a
Total Dissolved Solids mg/L <1 1 500 Acceptable
Hardness as CaCO3 mg/L <1 Soft
Ionic Balance % <1 n/a

Approved by:
Darren Crichton, BSc, PChem
Operations Chemist
Bodycote Testing Group www.bodycote.com www.bodycotetesting.com
7217 Roper Road NW · Edmonton · AB · T6B 3J4 · Canada · Tel: +1 (780) 438-5522 · Fax: +1 (780) 438-0396
Terms and Conditions: www.bodycotetesting.com/terms&conditions
Page 2 of 5

Methodology and Notes

Bill To: Pure Spirit Water Services Project: Lot ID: 685365
Report To: Pure Spirit Water Services ID: Control Number:
Spirit River, AB, Canada Name: Date Received: Jun 2, 2009
T0H 3G0 Location: Date Reported: Jun 5, 2009
Attn: Vern Howrish LSD: Report Number: 1224418
Sampled By: P.O.:
Company: Acct code:

Method of Analysis
Method Name Reference Method Date Analysis Location
Started
Alkalinity, pH, and EC in water APHA * Conductivity, 2510 04-Jun-09 BTG Edmonton
Alkalinity, pH, and EC in water APHA * Electrometric Method, 4500-H+ B 04-Jun-09 BTG Edmonton
Alkalinity, pH, and EC in water APHA * Titration Method, 2320 B 04-Jun-09 BTG Edmonton
Anions (Routine) by Ion APHA * Ion Chromatography with Chemical 03-Jun-09 BTG Edmonton
Chromatography Suppression of Eluent Cond., 4110 B
Approval-Edmonton APHA Checking Correctness of Analyses, 03-Jun-09 BTG Edmonton
1030 E
Chloride in Water APHA * Automated Ferricyanide Method, 4500- 04-Jun-09 BTG Edmonton
Cl- E
Colour (Apparent) in water APHA * Visual Comparison Method, 2120 B 05-Jun-09 BTG Edmonton
Metals Trace (Extractable) in water APHA Hardness by Calculation, 2340 B 03-Jun-09 BTG Edmonton
Metals Trace (Extractable) in water APHA * Inductively Coupled Plasma (ICP) 03-Jun-09 BTG Edmonton
Method, 3120 B
Turbidity in Water APHA * Nephelometric Method, 2130 B 05-Jun-09 BTG Edmonton
* Bodycote method(s) based on reference method

References
APHA Standard Methods for the Examination of Water and Wastewater
Guideline Guidelines for Canadian Drinking Water Quality, 6th Edition, May 16, 2006

Comments:
• Sample 685365-1; 3054880 The ion balance was outside the range 90 - 110% for sample 685365-1. The ion balance can be variable in samples with
TDS less than 100 mg/L.

Please direct any inquiries regarding this report to our Client Services group.
Results relate only to samples as submitted.
The test report shall not be reproduced except in full, without the written approval of the laboratory.
Bodycote Testing Group www.bodycote.com www.bodycotetesting.com
7217 Roper Road NW · Edmonton · AB · T6B 3J4 · Canada · Tel: +1 (780) 438-5522 · Fax: +1 (780) 438-0396
Terms and Conditions: www.bodycotetesting.com/terms&conditions
Page 3 of 5

Quality Control

Bill To: Pure Spirit Water Services Project: Lot ID: 685365
Report To: Pure Spirit Water Services ID: Control Number:
Spirit River, AB, Canada Name: Date Received: Jun 2, 2009
T0H 3G0 Location: Date Reported: Jun 5, 2009
Attn: Vern Howrish LSD: Report Number: 1224418
Sampled By: P.O.:
Company: Acct code:

Metals Extractable
Blanks Units Measured Lower Limit Upper Limit Passed QC
Sulfur mg/L <0.3 -0.3 0.3 yes
Date Acquired: June 05, 2009

Replicates Units Replicate 1 Replicate 2 % RSD Criteria Absolute Criteria Passed QC


Sulfur mg/L 218 219 10 0.1 yes
Date Acquired: June 05, 2009

Control Sample Units Measured Lower Limit Upper Limit Passed QC


Sulfur mg/L 48.9 44.1 54.1 yes
Date Acquired: June 05, 2009
Sulfur mg/L 1 0.9 1.1 yes
Date Acquired: June 05, 2009

Physical and Aggregate Properties


Blanks Units Measured Lower Limit Upper Limit Passed QC
Turbidity NTU <0.1 0.1 0.1 yes
Date Acquired: June 05, 2009

Replicates Units Replicate 1 Replicate 2 % RSD Criteria Absolute Criteria Passed QC


Turbidity NTU 7.2 7.1 10 0.2 yes
Date Acquired: June 05, 2009

Control Sample Units Measured Lower Limit Upper Limit Passed QC


Turbidity NTU 2370 2291.2 2420.2 yes
Date Acquired: June 05, 2009
Turbidity NTU 9130 8998.4 9839.0 yes
Date Acquired: June 05, 2009
Turbidity NTU 178 173.1 187.5 yes
Date Acquired: June 05, 2009
Turbidity NTU 15.8 15.6 16.4 yes
Date Acquired: June 05, 2009
Turbidity NTU 1.6 1.5 1.6 yes
Date Acquired: June 05, 2009

Routine Water
Blanks Units Measured Lower Limit Upper Limit Passed QC
Calcium mg/L <0.2 -0.1 0.1 yes
Magnesium mg/L <0.2 -0.1 0.1 yes

Bodycote Testing Group www.bodycote.com www.bodycotetesting.com


7217 Roper Road NW · Edmonton · AB · T6B 3J4 · Canada · Tel: +1 (780) 438-5522 · Fax: +1 (780) 438-0396
Terms and Conditions: www.bodycotetesting.com/terms&conditions
Page 4 of 5

Quality Control

Bill To: Pure Spirit Water Services Project: Lot ID: 685365
Report To: Pure Spirit Water Services ID: Control Number:
Spirit River, AB, Canada Name: Date Received: Jun 2, 2009
T0H 3G0 Location: Date Reported: Jun 5, 2009
Attn: Vern Howrish LSD: Report Number: 1224418
Sampled By: P.O.:
Company: Acct code:

Routine Water - Continued


Blanks Units Measured Lower Limit Upper Limit Passed QC
Sodium mg/L <0.4 -0.3 0.4 yes
Potassium mg/L <0.4 -0.4 0.4 yes
Iron mg/L <0.01 -0.02 0.02 yes
Manganese mg/L <0.005 -0.003 0.003 yes
Chloride mg/L <0.4 -0.4 0.4 yes
Fluoride mg/L <0.05 -0.05 0.05 yes
Nitrate - N mg/L <0.01 -0.01 0.01 yes
Nitrite - N mg/L <0.005 -0.005 0.005 yes
Date Acquired: June 03, 2009

Replicates Units Replicate 1 Replicate 2 % RSD Criteria Absolute Criteria Passed QC


pH 9.29 9.25 10 0.10 yes
Calcium mg/L 7.9 7.6 10 0.6 yes
Magnesium mg/L 1.2 1.2 10 0.4 yes
Sodium mg/L 787 791 10 1.2 yes
Potassium mg/L 2.8 2.9 10 1.2 yes
Iron mg/L 0.32 0.33 10 0.05 yes
Manganese mg/L <0.005 <0.005 10 0.010 yes
Chloride mg/L 89.0 89.6 10 0.5 yes
Fluoride mg/L <0.5 <0.5 10 0.05 yes
Date Acquired: June 03, 2009

Control Sample Units Measured Lower Limit Upper Limit Passed QC


Chloride mg/L 2080 1900.0 2230.0 yes
Date Acquired: June 04, 2009
pH 9.19 9.07 9.27 yes
Electrical Conductivity dS/m at 25 C 2.69 2.620 2.860 yes
Calcium mg/L 249 224.6 274.4 yes
Magnesium mg/L 96.1 90.0 110.0 yes
Sodium mg/L 248 224.5 274.5 yes
Potassium mg/L 238 225.1 274.9 yes
Iron mg/L 9.69 9.01 10.99 yes
Manganese mg/L 2.37 2.251 2.749 yes
Chloride mg/L 81.3 76.1 85.1 yes
Fluoride mg/L 10.2 9.31 10.81 yes
Nitrate - N mg/L 9.95 9.60 10.58 yes
Nitrite - N mg/L 10.1 9.510 10.530 yes
Nitrate and Nitrite - N mg/L 20.0 18.09 22.11 yes
P-Alkalinity mg/L 497 419 551 yes
T-Alkalinity mg/L 1010 900 1100 yes
Date Acquired: June 04, 2009
pH 6.83 6.77 6.97 yes

Bodycote Testing Group www.bodycote.com www.bodycotetesting.com


7217 Roper Road NW · Edmonton · AB · T6B 3J4 · Canada · Tel: +1 (780) 438-5522 · Fax: +1 (780) 438-0396
Terms and Conditions: www.bodycotetesting.com/terms&conditions
Page 5 of 5

Quality Control

Bill To: Pure Spirit Water Services Project: Lot ID: 685365
Report To: Pure Spirit Water Services ID: Control Number:
Spirit River, AB, Canada Name: Date Received: Jun 2, 2009
T0H 3G0 Location: Date Reported: Jun 5, 2009
Attn: Vern Howrish LSD: Report Number: 1224418
Sampled By: P.O.:
Company: Acct code:

Routine Water - Continued


Control Sample Units Measured Lower Limit Upper Limit Passed QC
Electrical Conductivity dS/m at 25 C 0.075 0.070 0.082 yes
Calcium mg/L 5.0 4.6 5.6 yes
Magnesium mg/L 2.0 1.8 2.2 yes
Sodium mg/L 5.4 4.5 5.5 yes
Potassium mg/L 5.2 4.5 5.5 yes
Iron mg/L 0.22 0.19 0.23 yes
Manganese mg/L 0.052 0.045 0.055 yes
Chloride mg/L 15.0 13.6 16.6 yes
Fluoride mg/L 0.48 0.45 0.57 yes
Nitrate - N mg/L 0.51 0.46 0.55 yes
Nitrite - N mg/L 0.494 0.452 0.548 yes
Nitrate and Nitrite - N mg/L 1.01 0.79 1.19 yes
P-Alkalinity mg/L 52 22 82 yes
T-Alkalinity mg/L 128 112 138 yes
Date Acquired: June 04, 2009

Bodycote Testing Group www.bodycote.com www.bodycotetesting.com


7217 Roper Road NW · Edmonton · AB · T6B 3J4 · Canada · Tel: +1 (780) 438-5522 · Fax: +1 (780) 438-0396
Terms and Conditions: www.bodycotetesting.com/terms&conditions