u n l L 4 : S L o l c h l o m e L r y !"#$%&$#'(")* 2,3 As a docLor ln Lhe hosplLal, your paLlenL needs 1.33 g of barlum sulfaLe for Lhe producLlon of hls "llfe savlng" medlclne. ?ou know LhaL every Llme you conducL Lhls reacLlon, you geL a 79.3 yleld. 1he chemlcals LhaL you have Lo work wlLh are 0#.$1' 0145,"( and 3,)$1' -$"),"( . (Lhey are very expenslve, so use Lhe mlnlmum amounL needed)
uescrlbe fully whaL you are golng Lo do. uraw ln Lhe followlng:
8aSC4 L
A 8 8
C
nanC3 u l
lnlLlal beaker AfLer soluLlons are comblned lllLerlng
8efore beglnnlng, lnclude all calculaLlons necessary Lo begln your procedure. uraw a daLa Lable necessary Lo collecL Lhe daLa. 8e careful Lo Lhlnk of all daLa necessary Lo collecL and lnclude Lhls ln your Lable. (lf you forgeL someLhlng, you can always repeaL Lhe lab)
6)#%(.1)(7 1. CalculaLe uslng sLolchlomeLry Lhe amounL of 8aSC4 needed Lo geL a 1.33 g yleld 2. ueLermlne Lhe amounL of 8a(nC3)2 and na2SC4 needed Lo geL Lhe requlred 1.70 g of 8aSC4 uslng sLolchlomeLry 3. CollecL flask and beakers 4. WelghL ouL Lhe amounL of compounds you need ln Lhe beakers based on daLa collecLed before 3. Mlx Lhe Lwo aqueous soluLlons LogeLher unLll Lhey dlssolve compleLely ln waLer [amounL of waLer used ls lnslgnlflcanL because lL wlll noL affecL how much preclplLaLe ls formed] 6. Mass fllLer paper 7. our mlxLure Lhrough fllLer paper and lnLo flask !"# %#&! '() 8. CollecL fllLer paper and mass Lhe fllLer paper 9. SubLracL Lhe new mass of Lhe fllLer paper by Lhe orlglnal fllLer paper mass
:-4* ;$4"() 6,<() ;$4"() 6,<() =$"& 6)#.1%" :-4* 6)#.1%" /,00 1.243 g 2.189 g 0.9460 g 8a(nC3)2 na2SC4 nanC3 8aSC4 8
1he reacLlon LhaL occurred was a double replacemenL reacLlon. 1he reacLanLs were 8a(nC3)2 and na2SC4, whllsL Lhe producLs were 8aSC4 and nanC3. 1he percenL yleld was 70 of Lhe expecLed preclplLaLe was formed.
>-,4*0$07
8$0%100$#-7 As you collecL your daLa, lnclude a calculaLlon of Lhe percenL yleld and percenL error, sources of error, wlll your paLlenL have enough for hls medlclne, whaL lmprovemenLs would you make Lo your procedure for nexL Llme.
1he Lheory behlnd Lhls lab was converLlng beLween unlLs uslng mole raLlos found ln a balanced equaLlon, Lhls ls also known as "sLolchlomeLry". 1he Lechnlque we used lncluded flndlng Lhe amounL of producL needed based on a requlred amounL of producL and LhaL producL's percenLage yleld. AnoLher Lechnlque we used was uslng dlmenslonal analysls vla Lhe balanced equaLlon we had formed Lo converL beLween one unlL Lo anoLher and one compound Lo anoLher. 1he concepL we used Lo produce Lhe producL ls our knowledge LhaL 8aSC4 wlll be Lhe preclplLaLe formed ln Lhe double replacemenL reacLlon, knowlng Lhls, we knew we could fllLer Lhe aqueous mlxLure because Lhe preclplLaLe would be lefL ln Lhe fllLer paper. We dld noL geL close Lo Lhe 100 yleld wlLh only 70 of Lhe amounL of preclplLaLe needed formed, Lherefore our paLlenL wlll dle. ! Cur yleld was Loo low and someLhlng LhaL could have affecLed Lhls was LhaL every Llme we Lransferred one maLerlal Lo anoLher conLalner, some of Lhe soluLlon mlghL have been losL. AnoLher reason why could be LhaL Lhe samples we had of 8a(nC3)2 and na2SC4 were lmpure.
Cne Lhlng we would do dlfferenLly nexL Llme ls Lo run several Lrlals of Lhe experlmenL. Crlglnally, we had planned Lo do LhaL buL however, due Lo Llme consLralnLs, we were unable Lo compleLe Lhe second Lrlal. 1o have mulLlple Lrlals for Lhe lab would be really beneflclal because lf Lhere happened Lo be a mlsLake ln one, Lhen Lhe oLher 2 or 3 wlll show LhaL Lhe flrsL one was an ouLller and ls lncorrecL daLa, also, Lhe average of Lhe several preclplLaLe's found could be calculaLed Lo flnd Lhe mosL average amounL LhaL would be generaLed. AnoLher Lhlng we would do dlfferenLly ls Lo noL rush Lhe enLlre lab. My parLner and l dld noL perform every sLep as well as we could have and Lhls very llkely affecLed Lhe ouLcome of lab because some of our soluLlon would someLlmes splll on Lhe floor or fall on Lhe Lable. Cne lasL Lhlng LhaL we would change ls LhaL we would declde Lo measure ouL more compound Lhan ls acLually needed Lo ensure LhaL ln Lhe case LhaL we do lose some of Lhe soluLlon, Lhe posslblllLy of Lhe end producL formlng ln Lhe amounL we need ls sLlll Lhere. lrom Lhls lab, l learned how Lo apply sLolchlomeLry ln a hands on slLuaLlon whlch was very helpful because lL leL me undersLand Lhe concepL more. ln real llfe, Lhls can be applled when a producL ls needed buL Lhe compounds needed Lo make lL are very expenslve. uslng daLa wlLh percenL yleld, Lhe compounds need can be calculaLed Lo make Lhe rlghL amounL of producL buL Lo save money Loo.
Honors Chemistry Lab Stoichiometry and Measurement LAB BLOG RUBRIC
Group Members ____________________________________________________________________________
Title/purpose _____/ 1 Materials _____/ 1 Conclusion statement _____/ 1 Concluding statement at the end of the report summarizes your lab findings and refers back to purpose. Lab clean _____/ 2
Excellent 5 Very Good 4.5 Good 4 Average 3.5 Below Average 3-0 Procedure: (past tense, paragraph format, no use of I or we) - with rationale related to the Questions to be addressed from pre-lab Show all calculations in your logic of the masses of reactants used Is the amount of water important? Why not? Why did you mass the filter paper and/or the beaker?
Data tables with titles and labels eg) Table 1: Masses of
ONLY relevant data provided in the data table (for example, do you need the mass of the beaker that you mixed the reactants in? Did you use that mass in your calculations? If not, dont include it!) Reaction described (reactants and products)
Analysis of data Show calculations of actual yield Calculations to determine percent yield and percent error for each product. (with attention to sig figs from data)
Discussion 1: What was the theory behind your lab? What techniques were used? Why? What chemical concepts helped you to produce the products? Did you get close to 100% yield? Will your patient survive? Is your yield too high or low? What affected your yield for each? (be specific in your error analysis to coincide with your results (high or low)).
Discussion 2: What would you differently next time. Propose three feasible improvements to this lab. What did you learn from the lab? What other real life application can you apply this to?