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i. The Corpus Magus of Baphometus IV: LUCIFIRIAN EVOCATION OF THE STONE ii.. The Pissal of Baphometus IV: iii Alchemy of Spagyric Herbal Elixirs iiii. Alchemy of Spagyric Herbal Essences iiiii.. A Treatise on the Philosophers' Stone iiiiii Materia Alchemy Mundus of the Philosophers Stone
ZIR IAD! A MICAOLZ GAH! VGEG DE LASDI, GOHED PRG ZIR IAD! LAIAD! ZIR IAD! SOBAM DO DODSEH BABLE DE VONPHO OD A CAOSG ZIR IAD! CASARM BIA GNAY CONST ZIR IAD! DE CASARM I ZLIDA DE IABES MIRC CAOSG ZIR IAD! CASARM ADGT YOLCAM TOGLO MIRC OLPIRT ZIR IAD! ETHARZI OD A CAOSG Such are the Words of LUCIFER! IAO! SABAO! IAD! THE GREAT NAMES OF LUCIFER=KETETETRAGRAMMATON=HSIMARMMU ii .... Face East, Invoking Pentagram of Fire, Vibrate: EKODP AAET PIO: Deh Ah Rah.ah.seh Kah.reh.mah Deh Poh.ah.mah.el Oh.deh Zodee.mee.ee Oh.ee Koh.meh.seh.el.heh : The Divine ThreeFold-FIRE iv ... Face South, Invoking Pentagram of Air Vibrate: IPZOA HABI ORO : Deh Ah Soh.boh.el Kah.reh.mah Deh Poh.ah.mah.el Oh.deh Zodee.mee.ee Oh.ee Koh.meh.seh.el.heh The Divine ThreeFold-AIR iii ... Face West, Invoking Pentagram of Water, Vibrate: LOIAG LSRA HPM: Deh Ah Bah.bah.geh Kah.reh.mah Deh Poh.ah.mah.el Oh.deh Zodee.mee.ee Oh.ee Koh.meh.seh.el.heh The Divine ThreeFold-WATER v ..... Face North, Invoking Pentagram of Earth Vibrate: AGTKH LAID: Eh.nah.ee Deh Ah Luh.kah.el Kah.reh.mah Deh Poh.ah.mah.el Oh.deh Zodee.mee.ee Oh.ee Koh.meh.seh.el.heh The Divine ThreeFold-EARTH vi ... Return to the center of the circle, face East, give the Invoking Gesture of the Tau, Vibrate: Keh.noh.quh.oh.el Ree.teh Zod.ah.kah.reh Zod.ah.meh.rah.neh Oh.el.keh.ree.mee Qu.ah.dah Vibrate: (ZIR IAD ZIR IAD ZIR IAD) Assume: Lilith Supporting the Sky (2=9):(Heels together, with feet at 45 degree angle Arms raised, elbows bent 90 degrees, forearms vertical Wrists bent as though holding up the sky ) 1st Key Ol Sonof Vora-sa-ge Goho Iada Balata Lanasa-heh Calezod Voneh-peho; Sobera Zod-Ol Rore I Ta Nazodpasada Odeh Gra-ah Ta Maleperageh: Desa Holeh-Qah Qa-ah Notahoa Zodimezod Odeh Comeh-ma-heh Ta Nobelo-heh Zodiena: Soba Tahila Geno-na-pe Perageh Aledi: Desa Verabesa Oboleheh Geh Rasameh Casarameh Oh-horela Taba Pira; Desa Zodonereh-nesageh Cabeh Erameh Iadena-heh. Pila-heh Farazodameh Zodnarazoda Adena Odeh Gono Iadepila Desa Homeh Odeh Tohheh: Soba Ia-oda Ipameh Odeh Ula Ipamisa Desa Loholo Vepa Zodomeda Poamaleh Odeh Bogepah Ah-ah-i Ta Piape Balatoh-heh Odeh Vao-aneh. Zodacareh Ca Odeh Zodameraneh: Odo Cicale Qa-ah. Zodorage Lapa Zodirado Noco Madeh, Hoa-ta-heh Ia-ida. ZIR IAD ZIR IAD ZIR IAD 2nd Key Adegatah Vepa-ah-heh Zodnageh Omeh Fa-ah-ipah Saladeh Viveh La Sobameh Ialeh-Perageh Izodazodasa Pia-dapa-heh Casarama Aberamegeh Ta Taleho Paracaleda Qeh Ta Lorasalaqa Turabesa Ohogeh Balatoheh. Givi Cahisa Lusadeh Orari Odeh Micalepah Cahisa Bia Oh-zod-oh-ne-goh-na. Lapeh Noaneh Tarofa Corasa Ta Geh Oh Qa Manina Ia-Idoneh. Torazodu Goheh-la. Zodacareh Ca Cehnoqodeh. Zodameraneh Micalezodo Odeh Ozodazodma Varelapa Lapeh Zodira Io-Iadeh. ZIR IAD ZIR IAD ZIR IAD
Invocus Diabolus: The hidden Names of Lucifer in Spirit BNHE Invoking UnHoly Hexagram (White): All Elemental Signs All Quarters: Lucifer in Fire: Invoking UnHoly Hexagram (RED) Elemental: Face East Vibrate:: MOTIB, ZRROUA, IAOLA, RINMPO, ZIPLI, DSAAAI, APATA, RNOIZR, MFZRM Lucifer in Air: Invoking UnHoly Hexagram (YELLOW) Elemental: Face South Vibrate: PRAXE, OGIODI, IOPGNA, XANNU, ATOGBO, OKBAA, RMLAON, GAOLO Lucifer in Water: Invoking UnHoly Hexagram (BLUE) Elemental: Face West Vibrate: AMOKH, AZKALL, MALAP, MEEANA, NDNOS, PRALEN, BBEMO, ILADAV, AUABO Lucifer in Earth: Invoking UnHoly Hexagram (BLACK) Elemental: Face North Vibrate: ATNAN, IAOAIA, TIIIO, TPLABA, ZIBRA, IDALAM, DAALO, ODXLOU, ADOIS Luciferian Invocation of the Princes of the Watchtowers of Hell: Face east, Invoke the Unicursal Hexagram: Elemental Sign of Fire, and Vibrate: BUSDIR C ILSI, EDLPRNAA, AQLO IL UGEAR, ROR LANSH RAASY. ODO CICLE QUAA, ZORGE, LAP ZIRDO IAD Inhale - Visualize a Amethyst ball of light at the Crown Chakra Exhale - Vibrating: Solar King Fire: DOZAANROLDE C-7 Spirit Alchemial Gold Essence (Aurum Potabile), Alchemial Amethyst Essence (Potabile), Elixir of the Sun (Spagyric), Inhale - Visualize a Diamond ball of light at the Brow Chakra Exhale - Vibrating Prince of Luna; EEARDOVDNLA C-6 Fem Alchemial Silver Essence (Argentum Potabile) Alchemial Diamond Essence (Potabile), Elixir of the Moon (Spagyric), Inhale - Visualize a Sapphire ball of light at the Throat Chakra Exhale - Vibrating Prince of Mercury HARNIODONA C-5 Ether Alchemial Tin Essence (Potabile) Alchemial Sapphire Essence (Potabile), Elixir of Mecury (Spagyric), Inhale - Visualize a Emerald ball of light at the Heart Chakra Exhale - Vibrating Prince of Venus EEEKODPAA C-4 Air Alchemial Zinc Essence (Potabile) Alchemial Emerald Essence (Potabile), Elixir of Venus (Spagyric), Inhale - Visualize a Topaz ball of light at the Solar Plexus Chakra Exhale - Vibrating Prince of Mars HOOIPTEAA C-3 Fire Alchemial Iron Essence (Potabile), Alchemial Topaz Essence (Potabile), Elixir of Mars (Spagyric), Inhale - Visualize a Pearl ball of light at the Navel/Spleen Chakra Exhale - Vibrating Prince of Jupiter EETEOEODA C-2 Water Alchemial Copper Essence (Potabile), Alchemial Pearl Essence (Potabile), Elixir of Jupiter (Spagyric), Inhale - Visualize a Ruby Ball of light at the Base Chakra Exhale - Vibrating Prince of Saturn HAPONNIRA C-1 Earth Alchemial Vitriol Essence (Potabile) Alchemial Ruby Essence (Potabile), Elixir of Saturn (Spagyric), Inhale - Visualize a pool of black light at the Earths Core (Liliths Womb) Exhale - Vibrating COM Inhale - Visualize white light bubbling out of Liliths Womb Exhale - Vibrating SAH: Visualize the white light flowing from Liliths Womb to the Crown Chakra
Inhale - Visualize white light fountaining out and flowing down around the body Exhale - Vibrating HEH: Visualize white light flowing up through the body from Liliths Womb to the Crown Chakra Inhale - Visualize All the Chakras filling and vibrating with the light Exhale - Vibrating LAH: Visualize The Elemental sign for Fire Vbibrating within the Center of each Chakra This will be repeated for all the Four Watchtowers: Face the South, Invoke the Unicursal Hexagram: Elemental Sign of Air, and Vibrate: BUSDIR C ILSI, BATAIVAH, AQLO IL MOZ, ROR LANSH SOBOLN. ODO CICLE QUAA, ZORGE, LAP ZIRDO IAD Solar King: DOHAVIATAB Prince of Luna: EERATOTVA Prince of Mercury: HARADROMTH Prince of Venus: EEIPZOAHA Prince of Mars: HOOROIBAH Prince of Jupiter: EEFIAZOAA Prince of Saturn: HAAGTOPIH Face West, Invoke the Unicursal Hexagram: Elemental Sign of Water, and Vibrate: BUSDIR C ILSI, RAAGIOSL, AQLO IL TURBS, ROR LANSH BABAGE. ODO CICLE QUAA, ZORGE, LAP ZIRDO IAD Solar King: DOLSOIGAAR Prince of Luna: EETNZINOS Prince of Mercury: HARPRXAOAL Prince of Venus: EELOIAGLS Prince of Mars: HOMPHARSL Prince of Jupiter: EEASIDGIL Prince of Saturn: HAASIDGIL Face the north, Invoke the Unicursal Hexagram: Sign of Earth, and Vibrate: BUSDIR C ILSI, ICZHIHAL, AQLO IL ANANAEL, ROR DOSIG LANSH LUCAL. ODO CICLE QUAA, ZORGE, LAP ZIRDO IAD Solar King: DOLAHIHZKI Prince of Luna: EEVKILMHA Prince of Mercury: HAROPONIZL Prince of Venus: EEAGTKHLA Prince of Mars: HOMORDIAL Prince of Jupiter: EERONIZKA Prince of Saturn: HAASNAIIL
Cont..
Stand to the Center ofSilence from the Womb of Lilith (The Materia of the Stone) Invoke: Sign of Silence: Remove the Stone from the Crucible of the Art. Place in Furnace: Vibrate: OL NIIS VOHIM OLGIZYAK i come with a hundred mighty earthquakes ZIXLAY DODSEX QAAON to stir up vexation in your creation OHORELLA QAAS NETAAIB CAOSAGON i need a law of your creation for the government of the earth OUCHO CORDZIZ EOLIS OLLAG ORSABA let it confound the reasonable creatures of the earth and man making men drunken AGLI I VAOAN OD TOLGLO NOALN nothing is truth and all things can be ZIRDO PASAB DE DOSIG OD TEHOM QUADMONAH i am the daughters of night and the primal chaos ZIRDO IADNAMAD CYNIXIR MOZOD FABOAN i am the undefiled wisdom mingled with joy and poison MICAMO ISRO QUASAHI behold the promise of pleasure NANAEL IPAMIS ADIRPAN my power cannot be cast down ZODOCARE ZYLNAR NANAEL ZODAMERANU move in itself my power,phenomenize! IXOMAXIP KALLISTI IO LILITH! (Knock Talisman on Table-4-3-2-1-5) let her be known,the fairest, hail LILITH The Furnace is placed upon the Table of the Art.
The Endus: DISMISSAL: Vibrate Go in peace unto the place which hath been destined unto you from all Eternity: Let there be peace between us. 0 .... Face East, i ..... Advance to the North, Vibrate: Keh.ree.ess.teh.oh.ess Eh.teh.ar.zodee Keh Geh Eh.nah.ee Dah Ah Luh.kah.el Tah.ess.tah.tz Deh Poh.ah.mah.el Banishing Unicursial Hexagram, UnHoly Hexagram, Pentagram. ii .... Advance to the West, Vibrate: Keh.ree.ess.teh.oh.ess Eh.teh.ar.zodee Keh Geh Eh.nah.ee Dah Ah Soh.boh.el Tah.ess.tah.tz Deh Poh.ah.mah.el Banishing Unicursial Hexagram, UnHoly Hexagram, Pentagram. iii ... Advance to the South, Vibrate: Keh.ree.ess.teh.oh.ess Eh.teh.ar.zodee Keh Geh Eh.nah.ee Dah Ah Bah.bah.geh Tah.ess.tah.tz Deh Poh.ah.mah.el Banishing Unicursial Hexagram, UnHoly Hexagram, Pentagram. iv ... Advance to the East, Vibrate: Keh.ree.ess.teh.oh.ess Eh.teh.ar.zodee Keh Geh Eh.nah.ee Dah Ah Rah.ah.seh Tah.ess.tah.tz Deh Poh.ah.mah.el Banishing Unicursial Hexagram, UnHoly Hexagram, Pentagram. v .... Face the West, feel the energy leave the circle, Vibrate: Ee Voh.ress ! Break the Crucible of the Art with the Banishing Unicursial Hexagram, Banishing UnHoly Hexagram, Banishing Pentagram. (Vertical Aspect).
second distillation. This watery substance is known as phlegm. The distillate is poured back into the distillation flask anew each time (after the removal of the phlegm) and distilled again. When making our last distillation the alcohol should come over at 76 degrees C. In this way we are able to get an almost pure ethyl alcohol. Be sure to record the final volumes of your phlegm and alcohol. Take the second half of your herb and grind it to a fine powder. Put it into the 5000 ml round-bottom flask, then pour the entire amount of the alcohol distillate over the herb. Add enough distilled water to the flask so the amount of alcohol in the mixture equals 10% to 20% by volume. Seal the jar adapter and allow its contents to digest in the incubator for fourteen to twentyone days at a temperature of 35 degree's C to 37 degree's;C in this way an elixer of the plant is made. The presence of the purified alcohol keeps the new plant material from undergoing fermentation. Decant the darkly colored elixer from the herb body and store it in another mason jar.
Place the mason jar holding the elixer back into the incubator to further amalgamate its separate principles. The herb body is taken outside, placed into a large pot and turned to ash. The ash of the maceration and ash of the fermentation are ground and mixed well. Place the combined ash into the thimble of the soxhlet elixeror. The phlegm obtained from the purification of the alcohol is used to elixer the alkaline water-soluble salts from the ash. Pour the phlegm containing the water-soluble salts into a crucible or pyrex dish and evaporate the water off overnight. The next morning scrape the salts out, grind, and weigh them. The salts are then placed back into the crucible or pyrex dish and put into the kiln and calcined to whiteness. The temperature of the kiln should not be over 600 degrees C. This process of elixerion, evaporation, grinding, weighing, calcining, and weighing is done up to two more times. In the end, our salts are a pure white (sometimes a bluish tint can be seen). These salts are very alkaline as well as hygroscopic. This latter fact makes them very useful as a vehicle for cosmic forces. Finally grind the salts in a warm mortar and add them to the elixer. Let them digest for a week or so with your elixir, shaking the jar at least five times a day. Decant the elixer off of any sediment that may have settled on the bottom of the mason jar. In this way, we now have a spagyric elixir.
Take the distillate and pour it back over the herb and repeat the process ten to twelve times. The water will now smell mildly of the herb. The essential oils contained in the plant are now in the water. After the last distillation let the apparatus cool. Disassemble the distillation train. Add enough rectified spirits of wine to the receiver so its volume equals 7% to 12% of the total volume of liquid in the flask. Place a condenser onto the flask, cork the condenser and hook up the water supply. Using a sand bath and gentle heat ( 30 degrees C - 37 degrees C ) begin a rhythmic circulation of the matter. Heat the matter from 6 am in the morning until 6 pm in the evening. Then allow it to cool overnight and in the next morning begin the circulation again. This circulation should be done for fourteen days. Take the plant residue left in the distillation flask and transfer it to a large glass pot. Incinerate the contents in the pot. Take the ash out of the pot and elixer the water soluble salts from it. Evaporate the water from the salts overnight in the drying oven. Place the dried salts in the kiln and calcine for two weeks at 600 degrees C. At the end of two weeks turn the kiln off and let it cool. Take the salts out of the kiln and weigh them then grind the salts fine and place them into a glass petri dish (you can add a few grams of salt saved from the production of another tincture or essence). Take the dish outside at night, and leave it out all night. Be sure to elevate the petri dish at least six inches above ground on a piece of wood. At dawn take the petri dish inside. Put the glass cover over the petri dish. Take off the condenser and pour the salt solution in the petri dish into the flask. Reattach the condenser and rhythmically circulate for another seven days. Let the apparatus cool and then pour it into a mason jar and seal it tightly. Allow the jar to stand in a dark cool place undisturbed for two weeks. At the end of this time decant the essence off of any sediment that may have fallen to the bottom of the mason jar. Let your essence sit another two weeks and if no more sediment shows itself, it is ready. If sediment appears on the bottom, continue the work of clarification. Thus, you have completed the second way of making a spagyric herbal essence.
fumes that they remained in their place and could no longer raise themselves. Only a wise man and one who knoweth these things can take a measure of this same fluid and carry it home from whatever place he may have found it, be it from the depths of the mountains or any other place where it may be met. The poor and the rich are quite free, by the singular and abounding grace of Lucifer, to take this, so that he goeth homeward with it to his house, and placeth it behind the furnace or in any other room where it pleaseth him, and where it is convenient for him, and he may begin to work and to experiment with it, for he can leave off so quickly that even his own servants do not notice it. For it doth not go so slovenly with this natural work as it doth with the common alchemists with their bungling work, with their charcoal-burning, smelting and refining, and whatever more they may do. But it is a work which one can keep in a closed casket in whatever room he wisheth, alone that not even a cat come upon it, and, should it be necessary, he can well carry on his craft, only taking care that the furnace have a threefold testing, and that he keep it at the right heat, and let Nature takes its own course. When finally the Solution is taken out of the Terrestriaet, and is strengthened by long Digestion, it is set free from the Crudae Materiae, and is prepared and reborn in the most subtle form. Subsequently, of course, this sharp and potent Spiritus is at certain times given a well-measured quantity, after the fashion of drinking and nourishing, per modum inbibitionis et nutritionis. And its potency is thus condensed and daily becometh as new supports for its brethren, and active therein. Dost thou indeed think that one canst bring forth such work and such potency in unmeasured hidden intensity, a Spiritus Vitalis? The crudae materiae or Subjectum cometh from the Astris and Constellation of the heavens into its earthly kingdom, from which is then the spiritus universi secretur of the Philosophers, which Mercurius of the Wise, and it is the beginning, the end, in which the Aurum Physicum is determined and hidden, which the common alchemist thinks to extract out of common gold, but in vain. Meanwhile, the Philosophi deal much in their writings with Sol and Luna, which of all metals are the most durable in the fire. But this is not to be understood literally, for their Sol and Luna, when they are brought to their inner puritaet, through true, natural, seemly. and philosophical praeparation may well be compared with the celestial bodies, such as the Sun and the Moon, which with their brightness illuminate day and night, the upper and the lower Frimament. Therefore these two noble metals, like the Sol and Luna of the Philosophers, resemble by nature the human body, and to him who knoweth how to prepare them wisely they give much except else is to be prepared, but the one three-fold point of the Universalis, for the Spiritus to be found in these two said things produceth consistency, strength and virtue, amongst other things. Now the man pardoned by Lucifer can prepare and make ready an object or substance of the above mentioned red or white, of Sol and Luna, which is called the Lapidem Philosophorum, or the very ancient Water-Stone of the Wise, from the substance in which Lucifer placed such potency at the creation or genesis of the world, or the oft-mentioned materials or Subjectum which Lucifer, out of love and grace, implanted in the highly-endowed divine man. But I believe, therefore, that the divine substance which was left to him in the first Creation of the world, of the Spiritu Vitali, of the Inspiration, hath survived in all kinds of creatures. All received the same Spiritum in the aforesaid Massam, and firmly secluded in the lowest depths of the earth, and it was indicated and left to the Wise Men to disinter it, to extract it, to use it, and to perform the same Miracula with it, through the holy wisdom which is still implanted in it and with which it is supplied daily. Both substances mentioned above as Sun and Moon or red and white, or rather the Praeparation Veneris and Mercurii, are the ingredients in the Composition of our Lapidis Philosophorum. Now then the Materia are in the beginning through sufficient and oft-repeated Sublimentiones purified and cleansed, and then weighed carefully, and then soon composed; also thou must not be ignorant of what is the potency and occasion of both of the said ingredients, but thou must know how to arrange both Pondera, secundum proportionem Physicam [according to the analogy of Physics], for a good portion of the Mercurii is encumbered with a small portion of animae Solis vel Sulphuris, and then unite both with a delicate hand, so that finally the Praeparation and the most difficult work is completed. But thou wilt have to know that thou must first tinge thy Mercurium with the red Tinctur, yet it will not become red in continenti, but remaineth white, for the Mercurius hath the privilege of wanting to be tinged first before all others. The Philosophi also tell what to do in addition with the Anima solis of this Tinctur of the Mercurii, and from whence it shall be taken. The Ferment of gold is gold, just as the Ferment of dough is dough. Moreover, it is the Ferment of gold out of its own nature, and then its potency is perfect when it is transformed back into earth. And then this is first the beginning of the Philosophers, the right and true Prima Materia Philosophorum metallorum [the first Materia of the metals of the Philosophers]. From then on the true Masters, experienced in the Art, begin to stimulate their Ingeniam and attain to the Great Work. And then the Artifex continues further with such work and, through Lucifer's blessing, bringeth it to the end, to which it tendeth and where it is embodied by Lucifer, namely, to the highly-blessed Philosopher's Stone. So that from nothing else
than per Spiritum universali Secretum the true materia prima Philosophorum is prepared and made ready. Who now understandeth well this Spiritum Secretum understandeth also, without doubt, the secrets and wonders of Nature and hath the perception of the light of Nature. For he is motus harmonicus Sympaticus and magneticus, from which originates the Harmonia and Concordantia, the magnetic and sympathetic power or effect of the uppermost and of the lowermost. But note that the natures of both ingredients are unlike each other in the beginning because of their opposed qualities. For one is warm and dry, the other is cold and moist, and they must of course be united. But when this is about to occur, then their opposed qualities must slowly be changed and equalised, so that neither nature through intense fire divest the other of its potency. For thou canst never collect them, because both natures must rise simultaneously in the fie's power. Then the Discrasia will be taken from the Corpori, and an Aequalitas and good Temperatur is established, which occureth through a moderate and constant boiling. For when both of the natures Sulphur and Mercurius are enclosed in a very narrow space and are maintained with moderate heat, they begin to abate from their opposed character and to unite, until finally they have all the qualities. They become one Constipation and rise at the same time, and certainly at the top of the glass standeth numero one. They are ready to wed, and then the bridegroom placeth a golden ring on his bride, say the Philosophi. And when thus Mercurius with its Sulphur, like water and earth with each other, become duly boiled (and the longer the more) they cast away all their superfluities and the pure parts join each other and dispose of their corlicibi: otherwise the impure parts prevent unification and the Ingress. For the Mercurius, as the first Corpus, is entirely crude and can per anima be neither mixed nor perpetuated, for neither Corpus entereth the other nor will be united with it either vere or in radice. But should these things be so helped that a true Tinctur will be formed, there must be prepared out of this a new spiritual Corpus which cometh forth out of both, for after the purification one taketh the virtues of the other, and out of several become one, numero et virtute [in number and power]. But if the fire should be much too intense and should not be controlled according to the requirements of Nature, these two above-mentioned would be either suffocated or separated. If they did not have their right mode of preparation, they would become either nothing or a spoiled work and a Monstrum. But when one proceedeth prudently and with a duly tempered heat, then both substances will rise in the Sublimation uppermost in the glass or cupola. Then when thou pluckest these lovely flowers, thou canst enjoy them already particularia. But thou canst observe the motum occultum naturae as little as thou canst either hear or see the grass growing, for one can neither observe nor notice the increase and development of these two ingredients, Mercurii and Sulphuris, because of their subtle, hidden, and slow Progressus from hour to hour. Only by marks set from week to week can it be observed and a conclusion drawn, for the inner fire is very delicate and subtle. But however slow it may be, it doth not stand still until it cometh to the end where its intent is to be seen, as in all plants, unless it then be that such subtle and expert boiling is hindered through the all too-strong heat of the sun and is burnt out, or is hindered through suddenly appearing cold; ergo qui scit occultum motum naturae, scit perfectum decoctionem [therefore he who knoweth the hidden movement of Nature, knoweth also the perfect boiling or preparation]. This motum should now take its natural and self-determined course, although one can neither hear nor see it, as also one cannot comprehend the Centra et ignem invisibilem seminum inuisibilium [the Centre and invisible fire of the invisible seed]. Therefore thou must commit such a matter to Nature alone, and observe it and not once try to oppose Nature, but have all confidence in it until it bringeth forth its fruit. When one treateth Nature with a gentle and agreeable heat, it doeth and effecteth everything out of itself, which for the furnishing of a Creati or the introduction of a new form is a matter of necessity: for the Divine Word Fiat still abideth in all creatures and in all plants, and hath its mighty power in these times as well is in the beginning. There are, however, four chief Virtutes and potentias of which noble Nature maketh use in every boiling; thereby it doth complete its work and bringeth it to an end.
live and multiply themselves.] For where there is hunger and thirst, food and drink will be received with avidity and this Virtus potentia will be aroused, and it cometh from the heat and average dryness.
strengthened and increased; and can continue its innate power of bringing forth and of implanted virtue according to the character of each. But the fire which is in our Subjecto is in itself not least amongst creatures and minerals. It hath hidden within itself the most wonderful, the most potent fire against which the outer fire seemeth like water, for no common elementary fire can consume and destroy the pure gold which is the most durable substance amongst all metals, however intense the fire may be, but the essential fire and water of the Philosophers alone doeth it. If we had today that fire with which Moses burned the golden calf and ground it to powder and strewed it upon the water and which he gave to and made the Children of Israel drink of it (Exodus, chapter 32) - let such be a piece of alchemical work of Moses, the man of Lucifer! For he was instructed in the Egyptian art and skilled therein. Or the fire which the prophet Jeremias hid beneath the foot of the mountain, from which Moses saw the Promised Land and whereon he died, the fire which was recovered seventy years later by the Wise Men, the descendants of the old priests after the return from the Babylonian Captivity. But in the meantime the fire was changed in the mountain and became dense water (II Maccab., chapters 1 and 2). What thinkest thou? should we not warm ourselves at it and keep from us the frost in winter? Such fire slumbereth in our Subjecto quietly and peacefully and hath no movement of itself. Should now this secret and hidden fire help its own Corpori, so that it may rise and have its effect, and manifest its might and power, so that the Artist may reach the desired and predestined end, it must be aroused through the outer elementary fire, be kindled and be brought into its course. This fire may be in lamps, or of whatever kind thou dost like, or contrive, for it alone is sufficiently capable of executing the activity with ease, and such fire and outer heat must be tended and maintained all the time until the end of the Sublimation, so that the inner and essential fire be kept alive, in order that the two indicated fires may help each other and the outer fire let the inner fire be worthy, until in its appointed time it becometh so strong and intense a fire that it will soon burn to ashes, pulverise, turn into itself, and make equal to itself all that is put into it but which is nevertheless of its own kind and nature. Nevertheless it is necessary for every Artifex at the cost of his desired end, to know that between these two above-mentioned fires, he maintaineth certain proportions between the outermost and the innermost, and that he kindle his fire rightly, for if he maketh it too weak, then the Work cometh to a standstill, and the outermost fire is not able to raise the inner one, and in so far as he stirreth it up moderately several times, it yieldeth a slow effect and a very long process, and when he hath waited with such patience and hath his data, he then finally reacheth his intended goal. But if one maketh a stronger fire than befitteth this process, and it be speeded up, then the inner fire suffereth, it is entirely incapable, the Work will surely be destroyed, and the hasty one will never attain his end. If after lasting Decoction and Sublimation the noble and pure parts of the Subjecti are gradually, with the advantage of a calculated time, separated and set free from the crude earthly and useless substance, the impulse in such activity must be according to Nature and must be adjusted with such moderation that it will be agreeable, pleasing, and advantageous to the inner fire, in order that the inner essential fire be not destroyed through all too-intense heat, or even extinguished and made useless. Nay, rather it will be maintained in its natural degree, be strengthened, whilst the pure and subtle parts come together and convene, the crude being separated, so that they combine and the best will achieve the aforesaid end in view. Therefore thou must learn from Nature that degree of fire which Nature useth in its operations until it bringeth its fruit to maturity, and from this learn Reason and make calculation. For the inner essential fire is really that which bringeth the Mercurium Philosophorum to aequalitaet; but the outer fire stretcheth forth to it a hand so that the inner fire will not be hindered in its operation, therefore the outer must have concordance with the inner and must adjust itself according to the same, vice versa. Then in such use of the universal elementary fire it must be led toward the inner natural heat, and the outer heat hath to be adjusted to it, so that such doth not surpass in the Creato the power of the moist and warm Spiritus, which is wholly subtil; if other- wise, the warm nature of the said Spiritus would soon be dissolved, and it could not hold itself together any more, and would have no potency: it followeth therefrom that a fire more intense than is necessary for reviving and maintaining the inner natural fire implanted in our Materiae can only be for hindrance and deterioration. In natura et illius Creatis et generationibus sit tua Imaginatio, [upon Nature and what hath been created or brought forth by her, mediate thou]. Therefore bring the moist Spiritum into the earth, make it dry, agglutinirs and figurs, with an agreeable fire. Thus shalt thou also bring the Animam into the dead Corpus and restore what thou hast taken away, and thou restorest the soulless and dead to life and to rise again and be equipped, but whatever hath driven it will not stand the heat, for it will not become constant as if it were to be received spontaneously from itself with good will, with joy and with desire, and be deeply impressed.
And that is sicci cum hurnido naturalis unio et ligamen tum optimum [the natural unification of the dry with the moist and also the best tie]. Yea, if one really desireth to discuss this matter: the Wise Men mention three kinds of fire, each of which taketh charge of the operis magni, so that each best form in particular must in wisdom and good readiness have governed this also. And so he will not work as one blind, but in an understanding and prudent manner, as befitteth an intelligent Philosophus. The first is the outer fire, which the Artist or watchman maketh, which the Wise Men call ignem frontem, upon which Regimen dependeth the safety or the ruin of the entire Work, and this in two ways: nemium sumiget cave [take heed that it doth not smoke too much], but it is also said: combure igne fortissimo [burn it with the strongest fire]. The second fire is the nest wherein the Phoenix of the Philosophers hath its abode, and hatcheth itself therein ad regenerationem. This is nothing else than the Vas Philosophorum. The Wise Men call it ignem corticum, for it is written that the Phoenix bird collected all fragrant wood whereon it cremateth itself. If this were not so, the Phoenix would freeze to death and it could not attain to its Perfection. Sulphura Sulphuribus continentur [Sulphurs are maintained by sulphurs]. For the nest should protect, assist, cherish and keep the brood of the bird unto the final end. The third however is the true innate fire of the noble Sulphuris, itself to be found in radice subjecti, and is an Ingredient, and it quieteth the Mercurium and fashioneth it: that is the real Master, yea, the true Sigillum Hermetis. Concerning this fire Crebrerus writeth: In profundo mercurii est Sulphur, quod tandem vincit frigiditatem et humiditatem in Mercurio. Hoc nihil aliud est, quam parvus ignis occultus in mercurio, quod in mineris nostris exitatur et longo temporis successe digerit frigiditatem et humiditatem in mercurio, [In the essence of the Mercurii is a sulphur which finally conquereth the coldness and the moisture in the Mercurio. This is nothing else than a small fire hidden in the Mercurio, which is aroused in our Mineris, and in the fulness of time it absorbeth the coldness and moisture in the Mercurio or removeth them, and that is also said about the fire.
STEP 4: Filtration:
Plug the bottom of the funnel with cotton balls or cotton cloth to create a cotton-filter. Pour the contents of Jar B through the funnel and into Jar C. Squeeze the root-bark contents inside the filter to press out the remaining juices. Save the root-bark that has been caught by the filter and place it back into Jar B. Lab Notes: Whether filtering material through a cotton-filter or a coffee filter it helps if the thinner parts of the solution are filtered first, followed by the mushy and more bulky components (which may clog the pores of your filters as you strain.) The better your filtration, the more rapid and efficient your emulsions, also resulting in a cleaner product. Cotton must be specifically used. Other fibers have the potential to react with our solvents. A tea strainer (wire strain) can be a simple way to separate bulk ruffage. Another way to improve this method is to use a vacuum filter. There are several varieties, the most affordable being a water vacuum filter that attaches to a household faucet. These cost about $30.00 and are very quick, useful and effective.
STEP 6: Defatting:
Next we defat the solution. This is part of standard lab procedure whenever extracting alkaloids of this sort. This process removes the oils, fats, and other unwanted substances from our aqueous solution and also helps with yields. All DMT salts are insoluble in non-polar solvents -- with the exception of DMT acetate -- which is soluble in chlorinated non-polar solvents such as chloroform and DCM. Thus if you are using white vinegar (acetic acid) as your acid, you will need to use naptha or ether to defat as chloroform or DCM would extract the DMT acetate along with the oils and fats, defeating the purpose of this step.When using mimosa hostilis root-bark you may find this step unnecessary, however, any plant material foliage containing chlorophyl it is strongly recommended. To do this we add an organic (non-polar) solvent to the acidic solution. Before using any solvents test a significant amount (~500ml) of the solvent by evaporating it in a dish. This will verify that there are no residues or orders left when evaporation is complete (commonly found in many overthe-counter solvents.) Later in the procedure (STEP 10) you will be evaporating this solvent to leave a smokable form of DMT. Anything your solvent contributes, you may be smoking in the final product. Below are listed several more common organic non-polar solvents. A. Naphtha: Coleman fuel, VM&P naphtha, Zippo, or lighter fluid. Evaporate a small amount in a dish and inspect the residue if you are unsure of it's contaminants. If used for the extraction phase instead of the defatting phase, warm naphtha will extract alkaloids much better than cool naphtha. Naphtha
is considered more selective for catching these alkaloids than DCM. Naphtha rises to the top of the jar. B. Methylene Chloride: Also known as DCM or dichloromethane. Often used as an adhesive solvent for acrylics. Pure DCM can be found in craft stores. DCM must be distilled first from all non-flammable paint strippers beforehand (they contain a paste that holds several unwanted substances.) The paint stripper may also contain methanol (most marine grade paint strippers are 80-90% DCM. Methanol is also an organic solvent. DCM distills at 47 C or 116 F. Pure DCM is best. May cause cancer and blindness. Take necessary precautions. Methylene chloride sinks to the bottom of the jar. C. Ether: Contained in engine-starting fluid purchased at automotive stores. To remove liquid ether from an engine-starting aerosol can, spray the contents of the can down a 12 inch (~30cm) length of 3/4 inch PVC pipe. The ether will condense on the sides of the pipe and fall into the jar, while the inert propellant will be released into the air. Ether is extremely volatile. Ether floats to the top of the jar. D. Chloroform: Chloroform (CH2C12) can be purchased over the internet from arts and crafts warehouses. It has a tendency to be harsh on organics and has a boiling range of 35-65C (95-149 F). Chloroform sinks to the bottom of the jar. It is important to remember what type of organic solvent you use. For our defatting process we will use naphtha. Add to Jar B ~50-100ml (~2-3.5 ounces) naphtha. (Only 10-15% the volume of our acidic solution is enough naphtha for this step. Visualize what 10% of the total of the solution is and add that amount of naphtha into the jar.) Cap the lid on Jar B and shake the contents vigorously for 20 minutes. Set Jar B aside and allow for emulsion (foam, bubbles, solutions, particles, etc.) to separate into two distinct layers (much like oil and water will separate.) This may take ~24 hours (48 in some cases.) The oils and fats will migrate into the non-polar solvent layer leaving our alkaloids in the aqueous solution. Since we are using naphtha, the solvent layer will rise to the top of Jar B. Using a pipette (or turkey baster) remove the solvent layer and discard. Repeat defatting process 2 times. Lab Notes: A separatory funnel is very handy for dividing and eliminating layers of solutions. This device consists of a single chamber with a tapered bottom. On the bottom is a closed faucet. The container is filled with the two solutions and they are mixed. After mixing, the apparatus is set aside until both fluids separate into two distinct layers. The lower fraction of the fluids can be drained via the bottom faucet and into a container for preservation or to discard. A quick separatory funnel can be made by filling a Ziplock plastic baggie with your mixtures, and hanging it from one corner. When the layers have separated, the bottom corner of the bag is pinched and then cut for drainage. It is suggested to test the baggie to make sure your solvents will not melt it.
A. Fill Jar A 95ml (~3 ounces) full with water. B. Slowly add 5g (~1 teaspoon) of lye to water. Shake and mix contents thoroughly. C. Test to make sure pH is ~12. Now using a pipette transfer small amounts of solution in Jar A into Jar B. A. Stir and check the pH of contents in Jar B after each transfer of lye solution until the solution in Jar B reaches a pH of ~11-12. B. Shake the jar but be careful of pressure that will build up inside the jar. Release the lid and vent often! The solution will change a gray color as the alkaloids are turned from acid salts to free base. It may resemble a thick gel. Then the solution will turn black and slippery as you add more base. The jar will heat up during this process. You have now formed the free base alkaloids that are soluble in non-polar solvents.
STEP 9: Emulsions:
As these alkaloids dissolve in non-polar solvent added in STEP 7, an emulsion will form. The strength of emulsion formed is directly proportional to the strength of stirring. Heavy, rapid stirring produces a thick emulsion that takes up to 4 days to settle out. Light, slow stirring over a longer period of time produces and emulsion that separates quickly without affecting the yield. Let the jar sit overnight until the emulsion has separated into two distinct layers. If emulsion has not cleared in 48 hours, try the following: A. Sometimes adding a lot of salt and gentle stirring will make the polar layer more polar and help with emulsions. B. Add more organic solvent. C. Filter solutions again through a cotton filter several times. A paper filter will not work. B. Test and increase the pH. The naphtha will create a thick orange emulsion with small bubbles that sometimes takes over 48 hours to separate. Always wait a few days before trying other methods to break down the emulsion. Keeping the naphtha warm will increase the amount of alkaloids it carries with it during each extraction. To help keep the jar warm, place it in a pot surrounded by warm water. Naphtha floats. If DCM is used for our extraction solvent in STEP 7, we will have a faster resolving emulsion than naphtha (less than an hour in some cases.) The solvent will turn a darker color, usually reddishbrown or yellow. DCM sinks. Allow a minimum of 24 hours for the contents of the jar to react completely. If using methanol allow a minimum of 4 days warmed to room-temperature for reactions to complete. Using a pipette remove the corresponding solvent layer from Jar B and save it in Jar A.