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Austenitic Stainless steels is heated to above 1050C and held for the desired
time followed by cooling to room temperature within few minutes by quenching /
blowing the air.
Solution annealing is done on stainless steel and non ferrous alloys to achieve
following:
To soften the material To remove carbide precipitation formed at grain
boundaries during manufacturing process To improve Corrosion Resistance
AGEING
The Material is heated to a certain temperature, and held for the desired time;
followed by quenching or cooling in air
Ageing is done on materials susceptible for ageing characteristics : Maraging
Steels Normally increases strength Improve Toughness
STRESS
RELIEVING
The steel is heated to a temperature below or close to the lower critical
temperature with a specific rate of heating. It is held at the temperature for a
desired length of time, followed by cooling with a specific rate up to certain
temperature.
There is no change in grain structure.
Stress relieving is done Fabricated Components of CS & LAS:
To reduce Internal Stresses To soften the steel partially To soften HAZ
Ni -Steels Nickel Steels : 1,2,3% Ni SA 203 GrA ,D Temperature : 593 C
Min Normally 600 - 640 C, Time : 60 mts min Time : 1 hr / inch thick
Heating Rate : 200 C per hr per inch thick Cooling Rate : 260 C per hr per
inch thick
Steels enhanced by Heat Treatments Q&T Steels : 9.5% Ni
Steels , SA 517 Gr E Temperature : 538 C Typ Normally < 600 C Time :
Minimum 15 minutes to 2 Hr Time : 1 hr / inch thick Heating Rate : 200 C per
hr per inch thick Cooling Rate : 260 C per hr per inch thick
C-Mn , C-Mo ,
Cr-Mo (< 2% Cr) C - Mn Steels , C - Mo Steels, Cr-Mo Steels SA 515Gr 70 ,
SA204GrA, SA387GR11CL1 Temperature : 593 C Min Normally 600 - 640 C,
650-690 C Time : 15 minutes min Time : 1 hr / inch thick Heating Rate :
200 C per hr per inch thick Cooling Rate : 260 C per hr per inch thick Cr-Mo
Steels Cr - Mo Steels (Cr >2%) SA 335P22 ,SA335P5
THERMOCOUPLE MATERIAL
TYPES OF THERMOCOUPLE BEING USED IN HZW
PRINCIPLE OF THERMOCOUPLE
The basic principle of thermoelectric thermometry is that a thermocouple
develops an emf which is a function of the difference in temperature of its
measuring junction & reference junction. If the temperature of reference junction
is known, the temperature of the measuring junction can be determined by
measuring the emf generated in the circuit.
THERMOCOUPLE MATERIAL REQUIREMENT
1. High coefficient of thermal emf. 2. Continuously increasing relation of emf to
temperature over
a long range. 3. Freedom from phase changes or other
phenomenon giving rise to discontinuity in temperature emf relationships. 4.
Resistance to oxidation, corrosion and contamination.
5. Homogeneity and reproducibility to fit an establish temperature & emf
relationship. SPEED OF RESPONSE MAY BE IMPROVED AND RADIATION &
CONDUCTION ERRORS MAY BE REDUCED BY THE USE OF SMALL DIAMETER
THERMOCOUPLES. TYPES OF THERMOCOUPLE BEING USED IN HZW
K type :
Material
: Chromel
+
Alumel
Nickel based
( 10
%Cr ) + ( 2 % Al ) Properties :
Non-Magnetic + Magnetic In this type
of thermocouple, the wires are joined at one end only to form a point-type
temperature sensor. Instrumentation converts the millivolt signal to related
temperature. S TYPE THERMOCOUPLE
S TYPE THERMOCOUPLE ARE THE STANDARD
THERMOCOUPLES.
MATERIAL OF CONSTRUCTION
PLATINUM
COMPENSATING CABLE
on unused wire .
52
BLOWER
3700 1/D OF BAFFLE
4150 ( REFRACTORY I/S )
4961
1000
250125
1380
4020
TROLLEY STRUCTURE
CERAMIC BLANKET
ROOF
BAFFLE
HEATING ELEMENT
CERMIC FIBER SLABER BLOCK
INSULATING CASTABLE
FIRE BRICK
OUTER SHELL
CERMIC BLANKET
GROUND LEVEL
PIT FURNACE SKETCH
STANDARD OPERATING PROCEDURE FOR PIT FURNACE
1. Receive heat treatment request duly authorized by metallurgy engineer. 2.
Receive the job for heat treatment with inspection clearance. 3. Put the job
either on support or on heat treatment fixture inside the furnace. 4. Ensure that
equal clearance is available on all sides between job and baffle. 5. Ensure that
the furnace is calibrated. 6. Connect thermocouples with compensating cable to
PID. 7. Set the program in the programmer as per heat treatment request. 8.
Take a trial run of program to ensure the accuracy. 9. Calibrate all 5 PIDs prior
to starting the furnace.
10. Insert the graph inside the recorder and take the signature of inspector on
the graph paper. 11. Close the furnace door. 12. Start the furnace by giving
power supply ON 13. Start recording the time and temperature in the logbook
every 30 minutes. 14. Ensure that the cycle is functioning as per program. 15.
After the heat treatment is over, open the furnace cover. 16. If the job calls
for water quenching, lift the job and dip it in quench tank. 17. It the job calls
for air cooling in still air, lift the job and put it outside on supports in open
air. 18. It the job doesnt call for anything above, allow the job to cool down in
furnace. 19. Keep the job outside after removing from furnace. 20. Submit the
heat treatment graph to inspection for approval of heat treatment cycle. 21.
Close the furnace cover after the furnace is cooled down to room temperature.
PROCEDURE FOR EMPTY FURNACE CALIBRATION
ACCURACY
1.
20 Nos. big K-type thermocouples +/- 0.25% 2.
10 Nos. small K-type
thermocouples +/- 0.25% 3.
Millivolt source (wahl unit )
( 1 micro volt
at 1000 micro volts ) 4.
Heat treatment fixture. 5.
Temperature indicators
(PID) +/- 10C 6.
Recorder
+/- on temperature scale.
+/minutes on time scale.
PIT FURNACE CALIBRATION PROCEDURE
1. Ensure that the PIDs are calibrated as mentioned above. 2. Ensure that the
recorder is calibrated as mentioned above. 3. Ensure that all the thermocouples
used are calibrated. 4. Ensure that the thermocouples are attached to the heat
treatment fixture as shown in sketch-I. 5. Place the heat treatment fixture inside
the furnace with thermocouples in position. 6. Close the furnace lid. Start the
furnace and the recorder. 7. Set the temperature of controller to 4000C. 8. After
reaching the set temperature, it is allowed to stabilize for half an hour. 9.
Measure and record the temperature indicated by each of the 20
thermocouples. The temperature is to be
read through WAHL UNIT. 10.
Three sets of readings are to be taken for each thermocouples at an
interval of 10 minutes. 11. Also record the readings indicated by each of the
thermocouples at an interval of 10 minutes. 7. Set the temperature of controller
to 4000C. 8. After reaching the set temperature, it is allowed to stabilize for half
an hour. 9. Measure and record the temperature indicated by each of the 20
thermocouples. The temperature is to be read through WAHL UNIT. 10. Three
sets of readings are to be taken for each thermocouples at an interval of
When only
HOW?
furnace is fired as per Ann-1 14. Spot check report shall be filled by supervisor
as per Annexure-2 during job is being heat treated. 15. Moonplate support and
welding inside surface prior to release for Heat treatment as per
Annexure-4
16. General idea about thermocouple locations and its
attachments is as per Annexure-6
GENERAL
1. Blocking the flame of the burner is not desirable 2. Burner shall have blue
flame and not yellow 3. Flame shall not directly impinge on job 4. All burners
shall be fired at a time 5. Keep all job nozzles open during heat treatment 6.
Above 24 nozzles / manways shall be located towards bottom 7. Deoxidization
agent shall be applied on all machined and gasket faces 8. Gasket / machined
face of loose assemblies shall not be touching any object.
THERMOCOUPLES
1. All the thermocouples shall be
identification hard punched
on it.
and
attach thermocouple
Eng.
after another. 7.
max. 3.0mm 8.
and DP shall be
If groove welds is not over in size or fillet weld with a throat thickness
of or less used for attaching non pressure parts to pressure parts provided
preheat to a minimum temperature of 200F is applied when the thickness of
pressure Part exceeds 1.25.
If studs are welded to pressure parts
provided preheat to a
minimum temperature of 200F is applied when the thickness of the pressure
parts exceeds 1.25.
for corrosion resistant weld metal overlay clad ding
or for welds attaching corrosion resistant applied lining provided preheat to
a minimum temperature of 200f is maintained during application of the first
layer when the thickness of the pressure part exceeds 1.25. The
temperature of furnace shall not exceed 800F ( 4270C) at the time when the
vessel or part is placed in it.
Above 8000F( 4270C), the rate of heating shall
not be more than 4000F Per hour (2000C/Hour) divided by the maximum metal
thickness of the shell or head plate in inches, but in no case more than 4000F Per
hour( 2220C Per hour ). During the heating period, There shall not be a
greater variation in temperature throughout the portion of the vessel being heat
treated than 2500F( 1390C) within any 15 feet ( 4.6m) interval of length.
During the holding period, there shall not be a greater difference than 1500f
( 830c) between the highest and the lowest temperature the portion of the
vessel being heated
During the heating & holding periods, the
furnace atmosphere shall be so controlled as to avoid excessive oxidation of the
surface of the vessel. The furnace shall be of such design as to prevent direct
heat impingement of the flame on the vessel.
Above 8000F ( 4270C), The rate of cooling shall not be more than 5000F
Per hour (2780C/Hour) divided by the maximum metal thickness of the shell or
head plate in inches, but in no case more than 5000F Per hour ( 2780C Per hour).
when it is impractical to postweld heat treat at the temperature specified in table
mentioned in Sr.. No. 9, It is permissible to carry out the post weld heat