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SAFETY GLASSES AND LAB APRONS OR LAB COATS MUST BE WORN IN THE LABORATORY. FAILURE TO DO SO WILL RESULT IN DISMISSAL FROM THE LABORATORY 1 Experiment Videotape2 Reading3 1: Check-in, Pipet Calibration (1) 8: pH titration of an amino acid (2) ) (Handout) Determination of iron in Vitamin (1) (Handout) Spectrophotometric M p. F95-F102 Extraction (#3132) IR (#3139) Safety (#5805) Use of a Pipet M p. 2-27; p 42-44 AJ p. 579-609; B p. 1034-1048 B p. 533 ; M 429
7a: Extraction of Caffeine (2) 7b: Spartan Infrared spectroscopy (1) 7a: Analysis of Caffeine (1) Titrimetric Analysis of Vitamin C (2) (Handouts) 6: Aldol condensation (1) Molecular Modeling (1) Isolation of Chlorophyll and Carotenoid Pigments from Spinach (Handouts) (1) Characterization of Pigments isolated from Spinach (1) 15: 13C NMR and DEPT Spectra (1) 10: Oxidation of Borneol to Camphor (1) (handouts) 9: Distillation & Gas chromatography (1) 10: Analysis of Camphor (1) Lab Clean-up (Attendance is required)
M p.113 - 124 B Ch. 12 & 14; M 277-300 M p. 221-235; p. 277-300; 434-437 AJ p. 633-642; p. F 95-F 102
One postlab for 7a refer to due date shown below 2/6 & 7 2/6 &7 2/13 & 14 2/25 & 26 2/25 & 26 One postlab for Spinach 2/27 & 28
Melting Point Determination (#3138) Column Chromatography (#3133) Thin layer Chrromatography
M p.371-396; B p. 498-500 M p. 56-71; AJ p. 633-638; Distillation (#3134) GC (#3134) M p. 145-177 M p. 256-272 M p. 277-300; AJ p. 633-638;
2/25 & 26 refer to due date shown below 3/11 & 12 3/13 & 14
3/13-14
(Attendance is required)
1) Chemistry Experiments for Life Science Majors, Second Edition, A.A. Russell, Burgess Publishing Company. 2) Instructional Media Library, Powell 270 or on the WWW (http://www.oid.ucla.edu/Webcast/Chemistry/index.html) 3) Mohrig (Organic Techniques) = M, Brown (Organic chemistry) = B, Atkins and Jones, The Quest for Insight, 2nd Edition = AJ. 4) Pre-lab reports (if any) are due at the beginning of the lab period; observations and data are due at the end of the lab period in which the data are taken; post-lab reports are due at the beginning of your regularly scheduled lab period one week after the experiment is finished. NO WORK WILL BE ACCEPTED AFTER 4:00 P.M. Friday, 3/14/2014