Engineering Management Inc.: Support

ENGINEERING MANAGEMENT SUPPORT, INC.
West Lake OU-1
STANDARD LEVEL IV
REPORT OF ANALYSIS
WORK ORDER #13-07147-0R
August 29, 2013
EBERLINE ANALYTICAL/OAK RIDGE LABORATORY
OAK RIDGE, TN
TABLE OF CONTENTS
DESCRIPTION
SECTION
PAGE
Chain of Custody & pH Check Sheet
0004
II
Sample Acknowledgement
0013
III
Case Narrative
0016
IV
Analytical Results Summary
0020
Analytical Standards
0026
VI
Quality Control Sample Results Summary
0050
VII
Laboratory Technician's Notes
0061
VIII
Analytical Data (Isotopic Uranium)
0094
IX
Analytical Data (Isotopic Thorium)
0243
Analytical Data (Radium-226)
0357
XI
Analytical Data (Radium-228)
0466
XII
Barium-133 Analytical Tracer Data
0484
Last Page Number
0560
STANDARD OPERATING PROCEDURE
EBERLINE
---------------- sER-Vi"C-E:s
MP-001, Rev. 12
Effective: 10131112
Sample Receiving
Page 14 of14
Eberline Services -Oak Ridge Laboratory
LABORATORY DATA SUPPORT CHECKLIST
MP-001-3
~~-07~47
Eberline Services Work O r d e r # - - - - - - - - - - - - - - - -
The checklist items listed below are to be initialed by appropriate staff upon completion/verification.
Date for Partial
Initials
Date
Initials
Checklist Items
Sample Log-In
Data Compilation
First Technical Data Review
Second Technical Data Review
Data Entry/Electronic Deliverable
Case Narrative
16,
7/J3i 'i/) )
, 1
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Electronic Deliverable Proof

Samples.Aii.llyzed within Holding Time
1Nn?
VA<?
QNQC
~iew
Client in Possession of Data

' nr H~rrl r.nnv
Invoiced by Laboratory
-
Technical/Clerical Corrections, Signatures Needed, Problems, Etc
c=
Date package approved by:
~c;
Laboratory Manager
Copy No. _ _ __
Date/Initials
~(yq/0
Date
Radiochemistry Services
SECTION I
CHAIN OF CUSTODY
&
pH CHECK SHEET
Chain of Custody Record

Project
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Laboratory Receiving:
Phone:
Ebertlne
601 SCalbolo Road
oak Rldgo, TN 3'1830
(865)481-tl683 Phone (665)483-4621 FIUI
1604
Project Number:
Airbill Number:
13-07147
REC'
D JUL 2 2 2013
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Sample Custodian R8lnlllb (Completed By Laboratory):
QAJC/iC Level
Sample Receipt
Turnaround
Total # Containers Received?
11me:
Level I
RouUne 0
COC Seals Present?
Level II
24Hour 0
COC Seals Intact?
Love! Ill
0
0
Other
1 Week 0
Other _ _
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Temperatura?
----
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(13
EBERLINE
SERVICES
Oak Ridge Laboratory
Internal
Work Order#
Chain of
Custody
Lab Deadline
'
Analysis
Sample Matrix
Sample
Fraction
Comments
13-07147
8/13/2013
UUISO - Level 4
Water
HP 210 I 270
Detector Activity
Storage
Location
Fxns 04, 06, 08, 10, 12, 14, 16 & 18 are TOTAL
Fxns 05, 07, 09, 11, 13, 15, 17 & 19 are DISSOLVED
MUST USE FXN 04 FOR DUP
Location
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Internal
EBERLINE
.
Chain of
Custody
SERVICES
UUISO - Level 4
Re-Analysis: 2Fxns 94, 9&, 98, 1&,
HP 2101270
Detector Activity
Sample
Fraction
Comments
12, 1-4, I 8 & 1B-are TOTAL
Original Lab Deadline: 08/20/13

Rerun Lab Deadline: 08/20/13MUST USE-BEN 94 j;QR QlfP
Relinqulshe~~
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EBERLINE
SERVICES
Internal
Work Order#
13-07147
Chain of
Custody
Lab Deadline
8/13/2013
Analysis
Sample Matrix
Sample
Fraction
Comments
ThiSO - Level 4
Water
HP 210/270
Detector Activity '
Storage
Location
Vl.S
Fxns 04, 06, 08, 10, 12, 14, 16 & 18 are TOTAL
MUSTUSEFXN04FORDUP
Date
Location
Separations
Count Room
Count Room
Count Room
Sample Storage
Rough Prep
Prep
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Prep
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Relinquished by
Prep
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Printed: 7/23/2013 3:48PM
88&8
Internal
~EBER~~~c~
Chain of
Custod
Work Order#
Lab Deadline
Ra226 - Level 4
Sample
Fraction
Comments
HP 210 I 270
Detector Activity
Storage
Location
Fxns 04, 06, 08, 10, 12, 14, 16 & 18 are TOTAL
MUST USE FXN 04 FOR DUP
Location
Separations
Received by
Count Room
Count Room
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Sample Storage
Rough Prep
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Separations
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Sample Storage
Rough Prep
Prep
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Prep
Separations
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Rough Prep
Prep
Separations
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Printed: 7/23/2013 3:48PM
-w
Internal
EBERLINE
Chain of
Custody
SERVICES
8/13/2013
Lab Deadline
Ra228 - Level 4
Analysis
Water
Sample Matrix
Sample
Fraction
Comments
13-07147
Work Orde
I Detector
HP 210 I 270
Activity
1
I
I
Storage
Location
Fxns 04, 06, 08, 10, 12, 14, 16 & 18 are TOTAL
MUSTUSEFXN04FORDUP
Location
Received by
Separations
Count Room
Count Room
Count Room
Received by
Count Room
Prep
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Relinquished by
Sample Storage
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Printed: 7/23/2013 3:48PM
fii 111
Printed: 7/23/2013 3:18 PM
~E
Page 1 of 2
InternaiVVorkOrder
e . . E:: R.'-1.. . ~ . .1::
Sample Receiving Report
13-07147
(Volumes, pH,&. CPM)
Received By
SERVICES
KCOULSTON
FR
ClientiD
LCS
BLANK
DUP
04
D-12 TOT"'
OS
D-12
Rec Vol Ttl CPM Max
Comments
# Btls
01
02
03
0
0
DIS~
12.00
46
0.00
46
8.00
45
.container Number,
1
2
r~
06
DUP05
TOT~
WA
2
.
<2
<2
1
2
07
DUP05 DIS
Container Number
PZ-208-SS
TOT~
cVolume{t,j. .. CPM.
,,,,
pH. Final
....... ~..5.?........
<2
WA
V1.5
pHOrig
pH Final
0.00
Volume
45
t..F;
.CPM . .
45
42
r~-
08
2
..
V1.5
J:iffOrig .
Container Number
V1.5
WA
Container Number
PH Otig .
Container.Number
pHOria
8.00
. pH Final :
votumeiLrh
43
:Cf'M
1-~
09
PZ-208-SS DIS '
TOT~
PZ-304-AI
11
PZ-304-AI DIS
12
PZ-304-AS
TOT~
0.00
43
WA
V1.5
0.00
46
WA
V1.5
8.00
41
1
2
1--
10
V1.5
WA
2
~
Container. Number
....
2
13
PZ-304-AS DIS/
14
MW-104 TOT
...
Container Number
pH Orig
containe.r NUmber.
.pH Oriti
pH Final
Volume IU .I
CPM :
15
MW-104 DIS "'
WA
V1.5
0.00
41
16
PZ-204A-SS TOT/
WA
Container Number 1
pH Orig
Container Number
PH Orig
V1.5
.:' pH Final
8.00
. .,, Volume lU
40
. ,c: CPM
17
PZ-204A-SS DIS /
: pH Final
Volume (L);
'CPM ~
.....
18
PZ-302-AI TOT /
WA
.
Container Number :. PHOri!l

~
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19
PZ-302-AI DIS (
Container Number:
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8.00
44
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V1.5
0.00
pH Orig
pH Final
VoluirieJL.t
44
CPM ;;
MP-001, Rev 5
Effective: 11/22/02
11
Printed: 7/23/2013 3:18PM
Page 2 of 2
(Volumes, pH, & CPM)
ClientiD
Received by:
ell~ {
Comments
....,_
Date:
7/2.3 /C~
MP-001, Rev 5
Effective: 11/22/02
SECTION II
SAMPLE ACKNOWLEDGEMENT
---~-------
Client . Name
-----------
-----~
.. Contr_aE.tiPO~~_F>_J"()ll!_cl_TYJ)! __ f- -. -
--------
Engineering Management Support, Inc. West Lake

i
Prolect _Name
...
West Lake OU-1

lnternaiiD
'
Client ID
ou-1 i
ClientWO
Environmental
Sample Disp
!
Westlake OU-1 I
Matrix
Storage
. ..
_f!~quire_cJ_!<J_r_~ro_llll<l_[)iJrs_ __
-~---
13-07147
07/22/2013
28
Lab Deadline
Internal Deadline
08/13/2013
08/19/2013
1----
Sample Date
Date Received
--------~--
....
08/20/2013
J. i ~~ >I
!tj -
[::i
01
LCS
07/23/13
WA
Vl.S
02
BLANK
07/23/13
WA
Vl.S
03
DUP
04
07/23/13
WA
Vl.S
41
D-12 TOT
07/15/13 15:27
WA
Vl.S
OS
D-12 DIS
07/15/13 15:27
WA
Vl.S
06
DUPOS TOT
07/15/13 00:00
WA
Vl.S
07
DUPOS DIS
07/15/13 00:00
WA
Vl.S
08
PZ-208-SS TOT
07/16/13 09:25
WA
Vl.S
09
PZ-208-SS DIS
07/16/13 09:25
WA
Vl.S
10
PZ-304-AI TOT
07/16/13 12:05
WA
Vl.S
11
PZ-304-AI DIS
07/16/13 12:05
WA
Vl.S
12
PZ-304-AS TOT
07/16/13 12:34
WA
Vl.S
13
PZ-304-AS DIS
07/16/13 12:34
WA
Vl.S
14
MW-104 TOT
07/16/13 13:25
WA
Vl.S
15
MW-104 DIS
07/16/13 13:25
WA
Vl.S
16
PZ-204A-SS TOT
07/16/13 13:56
WA
Vl.S
17
PZ-204A-SS DIS
07/16/13 13:56
WA
Vl.S
18
PZ-302-AI TOT
07/16/13 15:18
WA
Vl.S
19
PZ-302-AI DIS
07/16/13 15:18
WA
Vl.S
Totals Per Analysis (non QA samples)
16116
Invoice
~EI:JE:RI_INE

601 Scarboro Rd.
Oak Ridge, TN 37830
SERVICES
Voice
Sample Log In Report
"'~AI,""'
I
I
Voice: (865) 481-0683

Fax:
(865) 483-4621
16 ! 16
Paul V. Rosasco, P.E.
Report Data
Engineering Management Support, lnc
7220 West Jefferson Avenue, Suite 406
7220 West Jefferson Ave, Suite 408
Lakewood, CO 80235
Lakewood, CO 80235
303-640-3426
Engineenng Management Support, lnc
Fax
Voice
303-940-3426
Fax
Contact
Lyn Fitzgerald
Voice
303-601-4255
Fax
Printed: 7/24/2013 10:13 AM
STANDARD OPERATING PROCEDURE
MP-001, Rev. 12
Effective: 10131112
Page 13 of 14
Sample Receiving
Eberline Services- Oak Ridge Laboratory

SAMPLE RECEIPT CHECKLIST
MP-001-2
1_3_-_0_7_1_4....:..7_
WORK ORDER # _ _
SAMPLE MATRIX/MATRICES:
(CIRCLE ONE OR BOTH)

(AQuEou:Y
NON-AQUEOUS
(CIRCLE EITHER YES, NO, OR N/A)

WERE SAMPLES
Received in good condition?
(j)
If aqueous, properly preserved
' YJ
tYJ
N/A
WERE CHAIN OF CUSTODY SEALS

Present on outside of package?
Unbroken on outside of package?
Present on samples?
Unbroken on samples?
Was chain of custody present upon sample receipt?
(])
G)
w
t0
N
N
N
N
IF THE RESPONSE TO ANY OF THE ABOVE IS NO, A DISCREPANT SAMPLE RECEIPT REPORT
(DSR) HAS BEEN ISSUED.
REMARKS:----------------------------------------------------
SIGNATURE:
Copy No. _______
c(Nit:IN CJ..dL.v
DATE:
'7 /Z-~/13
Radiochemistry Services
SECTION III
CASE NARRATIVE
EBERLINE ANALYTICAL CORPORATION

601 SCARBORO ROAD
OAK RIDGE, TENNESSEE 37830
PHONE (865) 481-0683
FAX (865) 483-4621
~.EBERLINE
Je}
SERVICES
EBS-OR-36004
August 29,2013
Engineering Management Support, Inc.
Lakewood, CO 80235
CASE NARRATIVE
Work Order# 13-07147-0R
SAMPLE RECEIPT
This work order contains eight water samples received 07/22/2013. All samples were analyzed as total
and dissolved for Isotopic Uranium, Isotopic Thorium and Radium-226/228.
CLIENTID
LABID
CLIENTID
LABID
D-12 TOT
D-12 DIS
DUP05TOT
DUP05 DIS
PZ-208-SS TOT
PZ-208-SS DIS
PZ-304-AI TOT
PZ-304-AI DIS
13-07147-04
13-0714 7-05
13-07147-06
13-07147-07
13-07147-08
13-07147-09
13-07147-10
13-07147-1 I
PZ-304-AS TOT
PZ-304-AS DIS
MW-104TOT
MW-104DIS
PZ-204A-SS TOT
PZ-204A-SS DIS
PZ-302-AI TOT
PZ-302-AI DIS
13-07147-12
13-07147-13
13-07147-14
13-07147-15
13-07147-16
13-07147-17
13-07147-18
13-07147-19
ANALYTICAL METHODS
Isotopic Uranium and Isotopic Thorium were analyzed using Method HASL 300, 4.5.2. Radium-226 was
analyzed using Method EPA 903.0. Radium-228 was analyzed using Method EPA 904.0.
Laboratory qualifiers are as follows:
J-
Indicates a situation where the result minus the error is less than the detection limit but greater
than zero.
U-
Indicates a situation where the result minus the error is less than or equal to zero.
ANALYTICAL RESULTS
Combined Standard Uncertainty is reported at 2-sigma value.
Page I of3
ANALYTICAL RESULTS CONTINUED

ISOTOPIC URANIUM
Samples were prepared by removing representative aliquots followed by mixed acid digestions as
appropriate. Uranium was selectively extracted by ion exchange. Uranium was eluted, micro
precipitated and mounted on micro-porous filter media. Sample activities were then determined by alpha
spectroscopy using energy specific regions of interest for Uranium-234, Uranium-235 and Uranium-238.
Chemical recovery was determined by the use of a Uranium-232 tracer. Activity of the Uranium-232
tracer was determined by alpha spectroscopy using an energy specific region of interest.
1"1 Analytical Attempt

Samples demonstrated acceptable results for all Uranium analyses. Chemical recovery was slightly low
for sample numbers PZ-304-AS TOT and PZ-304-AS DIS. Results for these samples also demonstrated
significant disparity between the dissolved and suspended fractions. Due to this condition and the low
analytical recovery, these samples were reanalyzed. Chemical recovery was acceptable for all other
samples. The Uranium-234, Uranium-235 and Uranium-238 method blank demonstrated acceptable
results. Results for the Uranium-234 duplicate demonstrated an acceptable relative percent difference and
normalized difference. Results for the Uranium-235 and Uranium-238 duplicate demonstrated a high
relative percent difference; however, normalized difference is within acceptable limits for the analytical
technique. Results for the Uranium-234 and Uranium-238 laboratory control sample demonstrated an
acceptable percent recovery.
2"d Analytical Attempt
Sample numbers PZ-304-AS TOT and PZ-304-AS DIS were reanalyzed due to a low chemical recovery
and disparity between the dissolved and suspend fractions. Samples demonstrated acceptable results for
all Uranium analyses. Total versus dissolved results are within reason. Due to limited sample volume for
the reanalysis, method detection limits are slightly high. Chemical recovery was acceptable for all
samples. The Uranium-234, Uranium-235 and Uranium-238 method blank demonstrated acceptable
results. Results for the Uranium-234, Uranium-235 and Uranium-238 duplicate demonstrated a high
relative percent difference; however, normalized difference is within acceptable limits for the analytical
technique. Results for the Uranium-234 and Uranium-238 laboratory control sample demonstrated an
acceptable percent recovery.
ISOTOPIC THORIUM
Samples were prepared by removing representative aliquots followed by mixed acid digestions as
appropriate. Thorium was selectively extracted by ion exchange. Thorium was eluted, micro-precipitated
and mounted on micro-porous filter media. Sample activities were then determined by alpha
spectroscopy using energy specific regions of interest for Thorium-228, Thorium-230 and Thorium-232.
Chemical recovery was determined by the use of a Thorium-229 tracer. Activity of the Thorium-229
tracer was determined by alpha spectroscopy using an energy specific region of interest.
Samples demonstrated acceptable results for all Thorium analyses. Chemical recovery was acceptable for
all samples. The Thorium-228 and Thorium-232 method blank demonstrated acceptable results. The
Thorium-230 method blank demonstrated results slightly greater than the detection limit. Results for the
Thorium-228 duplicate demonstrated an acceptable relative percent difference and normalized difference.
Results for the Thorium-230 and Thorium-232 duplicate demonstrated a high relative percent difference;
however, normalized difference is within acceptable limits for the analytical technique. Results for the
Thorium-228, Thorium-230 and Thorium-232 laboratory control sample demonstrated an acceptable
percent recovery.
Page 2 of3
ANALYTICAL RESULTS CONTINUED

RADIDM-226
Samples were prepared by removing representative aliquots as appropriate. This was followed by
selective sulfate precipitations of the Radium. Samples were then mounted by semi-micro-precipitations
onto micro-porous filters. Samples were counted by alpha spectroscopy using an energy specific region
of interest for Radium-226. Chemical recovery was calculated by the use of a Barium-133 tracer, which
was determined by HPGe gamma spectroscopy.
Samples demonstrated acceptable results for all Radium-226 analyses. Chemical recovery was acceptable
for all samples. The Radium-226 method blank demonstrated acceptable results. Results for the Radium
226 duplicate demonstrated a high relative percent difference; however, normalized difference is within
acceptable limits for the analytical technique. Results for the Radium-226 laboratory control sample
demonstrated an acceptable percent recovery.
RADIDM-228
Following alpha spectroscopy analysis of Radium-226, Barium/Radium Sulfate precipitates were
redissolved and allowed for sufficient ingrowth of the Actinium-228 daughter. After ingrowth, Actinium
228 was selectively precipitated. Precipitates were filtered and beta emissions for Actinium-228 were
then counted on a gas proportional counter. Chemical recovery was determined by the use of a Barium
133 tracer, the activity of which was determined by HPGe gamma spectroscopy and an elemental Yttrium
carrier by gravimetric measurements. The product of these two recoveries was used to calculate chemical
yield.
Samples demonstrated acceptable results for all Radium-228 analyses. Chemical recovery was acceptable
for all samples. The Radium-228 method blank demonstrated acceptable results. Results for the Radium
228 duplicate demonstrated a high relative percent difference; however, normalized difference is within
acceptable limits for the analytical technique. Results for the Radium-228 laboratory control sample
demonstrated an acceptable percent recovery.
CERTIFICATION OF ACCURACY
I certify that this data report is in compliance with the terms and conditions of the Purchase Order, both
technically and for completeness, for other than the conditions detailed above. Release of the data
contained in this hard copy data package has been authorized by the cognizant project manager or his/her
designee to be accurate as verified by the following signature.
"
M.R. McDougall
Laboratory Manager
Date: 8/29/2013
Eberline Analytical wants and encourages your feedback regarding our performance providing radioanalytical services. Please
visit http://www.eberlineservices.com/client.htrn to provide us with feedback on our services.
Page 3 of3
SECTION IV
ANALYTICAL RESULTS SUMMARY

Lakewood, CO 80235
Client Sample ID
~i!U
~
"l'
~"'"
Project: West Lake OU-1

SDG: 1307147
Received: 07/22/2013
Matrix: Water
Lab Sample ID
Analvsis Date/Time
LCS13-07147-01
LCS13-07147-01
LCS13-07147-01
LCS13-07147-01
LCS13-07147-01
LCS13-07147-01
LCS13-07147-01
LCS13-07147-01
LCS13-07147-01
LCS13-07147-01
LCS13-07147-01
13-07147-01
13-07147-01
13-07147-01
13-07147-01
13-07147-01
13-07147-01
13-07147-01
13-07147-01
13-07147-01
13-07147-01
13-07147-01
08/06/2013 16:35:16
08/14/201311:08:36
08/10/201314:55:07
08/10/201314:55:07
08/10/2013 14:55:07
08/08/2013 09:06:44
08/08/2013 09:06:44
08/08/2013 09:06:44
08/13/2013 09:05:58
08/13/2013 09:05:58
08/13/2013 09:05:58
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
BLANK13-07147-02
BLANK13-07147-02
BLANK13-07147-02
BLANK13-07147-02
BLANK13-07147-02
BLANK13-07147-02
BLANK13-07147-02
BLANK13-07147-02
BLANK13-07147-02
BLANK13-07147-02
BLANK13-07147-02
13-07147-02
13-07147-02
13-07147-02
13-07147-02
13-07147-02
13-07147-02
13-07147-02
13-07147-02
13-07147-02
13-07147-02
13-07147-02
08/06/2013 16:35:17
08/14/201311:08:36
08/10/2013 14:55:08
08/10/201314:55:08
08/10/2013 14:55:08
08/08/2013 09:06:45
08/08/2013 09:06:45
08/08/2013 09:06:45
08/13/2013 09:05:59
08/13/2013 09:05:59
08/13/2013 09:05:59
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
D-12 TOT_07_15_2013 DUP

D-12 TOT_07_15_2013 DUP
D-12 TOT_07_15_2013 DUP
D-12TOT_07_15_2013 DUP
D-12TOT_07_15_2013 DUP
D-12TOT_07_15_2013 DUP
D-12 TOT_07_15_2013 DUP
D-12 TOT_07_15_2013 DUP
PZ-304-AS TOT_07_16_2013 DUP
PZ-304-AS TOT_07_16_2013 DUP
PZ-304-AS TOT_07_16_2013 DUP
13-07147-03
13-07147-03
13-07147-03
13-07147-03
13-07147-03
13-07147-03
13-07147-03
13-07147-03
13-07147-03
13-07147-03
13-07147-03
08/06/201316:35:18
08/14/2013 11:08:36
08/10/2013 14:55:01
08/10/201314:55:01
08/10/201314:55:01
08/08/2013 09:06:37
08/08/2013 09:06:37
08/08/2013 09:06:37
08/13/2013 09:06:00
08/13/2013 09:06:00
08/13/2013 09:06:00
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
EBERLINE
SERVICES
Analvte
Final Report of Analysis

Date: 8/29/2013
Page 1 of 5
Result
Error
csu
MDA
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
11.04
8.18
4.58
5.00
4.93
9.09
1.75
9.50
7.03
0.95
8.61
1.39
0.91
0.72
0.77
0.76
1.32
0.46
1.37
0.99
0.27
1.16
2.71
2.06
0.84
0.99
0.88
1.48
0.48
1.53
1.11
0.28
1.32
0.26
1.17
0.12
0.08
0.07
0.11
0.11
0.09
0.08
0.10
0.07
0.12
0.57
0.06
0.17
0.07
0.11
0.12
0.11
0.11
0.08
0.07
0.12
0.61
0.06
0.18
0.07
0.11
0.12
0.11
0.11
0.08
0.07
0.24
1.08
0.13
0.10
0.08
0.09
0.10
0.10
0.10
0.13
0.06
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.04
1.01
0.00
0.45
0.08
0.20
0.19
0.19
0.19
0.06
0.09
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.12
0.38
0.08
0.83
0.06
0.67
0.22
0.23
0.59
0.49
-0.17
0.17
0.58
0.19
0.43
0.14
0.22
0.13
0.12
0.68
0.73
0.36
0.17
0.59
0.19
0.44
0.14
0.22
0.13
0.12
0.68
0.73
0.36
0.28
1.21
0.35
0.29
0.27
0.12
0.10
0.09
0.89
1.18
1.07
u
u
u
Method

601 SCARBORO ROAD OAK RIDGE, TN 37830
865/481-0683
FAX 865/483-4621
Qualifier
Units
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
u
J
J
J
J
u
J
u
J
u
u
u
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1

Lakewood, CO 80235
Client Samole ID
!l'J
1~:1
r~JI
i\JI

SDG: 1307147
Received: 0712212013
Matrix: Water
Lab Sample ID
Analvsis Date/Time
0-12 TOT_07_15_2013
D-12 TOT_07_15_2013
D-12 TOT_07_15_2013
D-12 TOT_07_15_2013
D-12 TOT_07_15_2013
D-12 TOT_07 _15_2013
0-12 TOT_07_15_2013
D-12 TOT_07_15_2013
13-07147-04
13-07147-04
13-07147-04
13-07147-04
13-07147-04
13-07147-04
13-07147-04
13-07147-04
08/0612013 16:35:19
081141201311:08:37
081101201314:55:02
081101201314:55:02
0811012013 14:55:02
08108/2013 09:06:38
0810812013 09:06:38
0810812013 09:06:38
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
D-12 OIS_07_15_2013
D-12 DIS_07_15_2013
D-12 DIS_07_15_2013
D-12 DIS_07_15_2013
D-1201S_07_15_2013
D-12 OIS_07_15_2013
0-12 DIS_07_15_2013
D-12 DIS_07_15_2013
13-07147-05
13-07147-05
13-07147-05
13-07147-05
13-07147-05
13-07147-05
13-07147-05
13-07147-05
0810612013 16:35:20
081141201311:08:41
081101201314:55:03
081101201314:55:03
08/1012013 14:55:03
08/0812013 09:06:39
08/0812013 09:06:39
08/0812013 09:06:39
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
DUP05 TOT_07_15_2013
DUP05 TOT_07_15_2013
DUP05 TOT_07_15_2013
DUP05 TOT_07_15_2013
DUP05 TOT_07_15_2013
DUP05 TOT_07_15_2013
OUP05 TOT_07_15_2013
DUP05 TOT_07_15_2013
13-07147-06
13-07147-06
13-07147-06
13-07147-06
13-07147-06
13-07147-06
13-07147-06
13-07147-06
08/0612013 16:35:21
08/141201311:08:42
08/1012013 14:55:04
08/101201314:55:04
08/101201314:55:04
08/0812013 09:06:40
08/0812013 09:06:40
08/08/2013 09:06:40
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
DUP05 OIS_07_15_2013
DUP05 DIS_07_15_2013
DUP05 OIS_07_15_2013
DUP05 DIS_07_15_2013
DUP05 DIS_07_15_2013
DUP05 OIS_07_15_2013
DUPOS OIS_07_15_2013
DUP05 DIS_07_15_2013
13-07147-07
13-07147-07
13-07147-07
13-07147-07
13-07147-07
13-07147-07
13-07147-07
13-07147-07
08/06/2013 16:35:22
08/14/2013 11 :08:42
08/10/2013 14:55:05
08/101201314:55:05
08110/201314:55:05
08/08/2013 09:06:41
08/08/2013 09:06:41
08/08/2013 09:06:41
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
r-J,EBERLINE
Jl!J
SERVICES
Analyte

Date: 812912013
Page 2 of 5
Result
Error
csu
MDA
Qualifier
Units
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.29
1.13
0.11
0.54
0.12
0.58
0.38
0.40
0.22
0.67
0.10
0.23
0.10
0.20
0.18
0.17
0.23
0.72
0.10
0.24
0.10
0.21
0.18
0.17
0.23
1.30
0.12
0.08
0.08
0.07
0.08
0.08
J
J
J
pCi/1
pCi/1
pCill
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
0.29
0.68
0.07
0.28
0.12
0.19
0.17
0.11
0.30
0.79
0.07
0.29
0.12
0.19
0.17
0.11
0.29
1.26
0.19
0.13
0.18
0.10
0.17
0.10
J
J
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.47
1.74
-0.03
0.54
0.10
0.34
0.22
0.12
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.36
0.97
0.03
0.54
0.17
0.66
0.22
0.26
0.22
0.70
O.Q7
0.22
0.12
0.25
0.16
0.15
0.23
0.73
O.G7
0.23
0.12
0.25
0.16
0.15
0.16
1.39
0.14
0.09
0.08
0.10
0.15
0.12
4.5.2
4.5.2
4.5.2
4. 5. 2
4.5.2
4.5.2
0.44
1.44
-0.02
0.54
-0.01
0.46
0.28
0.26
0.33
0.72
0.06
0.21
0.03
0.18
0.15
0.13
0.34
0.79
0.06
0.22
0.03
0.18
0.15
0.13
0.39
1.37
0.16
0.09
0.09
0.11
0.12
0.08
Method

865/481-0683
FAX 865/483-4621
u
u
J
J
J
J
u
J
J
J
J
J
u
u
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1

Lakewood, CO 80235
Client Sample ID
tl~~
11)~
~~~:tr
(,~-.)1

SDG: 1307147
Received: 0712212013
Matrix: Water
Lab Sample ID
Analvsis Date/Time
Analyte
13-07147-08
13-07147-08
13-07147-08
13-07147-08
13-07147-08
13-07147-08
13-07147-08
13-07147-08
08106/2013 16:35:48
08/141201311:08:43
081101201314:55:06
081101201314:55:06
081101201314:55:06
0810812013 09:06:43
0810812013 09:06:43
0810812013 09:06:43
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
PZ-208-SS
PZ-208-SS
PZ-208-SS
PZ-208-SS
PZ-208-SS
PZ-208-SS
PZ-208-SS
PZ-208-SS
DIS_07_16_2013
DIS_07 _16_2013
DIS_07_16_2013
DIS_07_16_2013
DIS_07_16_2013
DIS_07_16_2013
DIS_07_16_2013
DIS_07_16_2013
13-07147-09
13-07147-09
13-07147-09
13-07147-09
13-07147-09
13-07147-09
13-07147-09
13-07147-09
081061201316:35:49
08/1412013 11:09:23
081101201315:01:59
0811012013 15:01:59
0811012013 15:01:59
0810812013 09:08:28
0810812013 09:08:28
0810812013 09:08:28
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
PZ-304-AI TOT_07_16_2013
PZ-304-AI TOT_07_16_2013
PZ-304-AI TOT_07_16_2013
PZ-304-AI TOT_07_16_2013
PZ-304-AI TOT_07_16_2013
PZ-304-AI TOT_07_16_2013
PZ-304-AI TOT_07_16_2013
PZ-304-AI TOT_07_16_2013
13-07147-10
13-07147-10
13-07147-10
13-07147-10
13-07147-10
13-07147-10
13-07147-10
13-07147-10
0810612013 16:35:51
0811412013 11 :09:24
0811012013 15:02:01
0811012013 15:02:01
081101201315:02:01
08/0812013 09:08:29
08/0812013 09:08:29
0810812013 09:08:29
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
PZ-304-AI
PZ-304-AI
PZ-304-AI
PZ-304-AI
PZ-304-AI
PZ-304-AI
PZ-304-AI
PZ-304-AI
13-07147-11
13-07147-11
13-07147-11
13-07147-11
13-07147-11
13-07147-11
13-07147-11
13-07147-11
081061201316:35:53 Radium-226
081141201311:09:24 Radium-228
081101201315:02:02 Thorium-228
081101201315:02:02 Thorium-230
0811012013 15:02:02 Thorium-232
08/0812013 09:08:31 Uranium-234
0810812013 09:08:31 Uranium-235
0810812013 09:08:31 Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
EEIERLINE
SERVICES
Result
Error
csu
MDA
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.71
2.37
0.21
0.70
0.25
1.81
0.32
1.43
0.32
0.80
0.14
0.27
0.15
0.41
0.17
0.35
0.35
0.97
0.14
0.28
0.15
0.43
0.17
0.37
0.20
1.46
0.11
0.11
0.08
0.11
0.13
0.09
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.45
1.10
0.09
0.43
0.09
1.58
0.48
0.98
0.25
0.70
0.08
0.18
0.07
0.38
0.21
0.28
0.26
0.74
0.08
0.18
0.08
0.39
0.21
0.29
0.19
1.37
0.08
0.09
0.06
0.10
0.13
0.08
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
1.64
2.52
0.10
0.62
0.05
0.72
0.49
0.80
0.64
0.76
0.09
0.23
0.06
0.36
0.32
0.38
0.73
0.95
0.09
0.25
0.06
0.37
0.33
0.39
0.26
1.33
0.07
0.10
0.07
0.17
0.21
0.17
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
1.15
2.43
0.07
0.25
0.06
0.63
0.16
0.33
0.45
0.80
0.08
0.14
0.07
0.35
0.21
0.24
0.51
0.97
0.08
0.14
0.30
1.44
0.11
0.08
0.07
0.18
0.32
0.18
Method
PZ-208-SS TOT_07_16_2013
PZ-208-SS TOT_07_16_2013
PZ-208-SS TOT_07_16_2013
PZ-208-SS TOT_07_16_2013
PZ-208-SS TOT_07_16_2013
PZ-208-SS TOT_07_16_2013
PZ-208-SS TOT_07_16_2013
PZ-208-SS TOT_07_16_2013
DIS_07_16_2013
DIS_07_16_2013
018_07_16_2013
018_07_16_2013
DIS_07 _16_2013
DIS_07 _16_2013
DIS_07 _16_2013
DIS_07_16_2013

Date: 812912013
Page 3 of5
O.D7
0.35
0.21
0.25

865/481-0683
FAX 8651483-4621
Qualifier
J
J
J
u
J
u
u
u
J
Units
pCi/1
pCi/1
pCi/1
pCill
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCill
pCi/1
pCi/1
pCill
pCi/1
pCill
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1

Lakewood, CO 80235
Lab Samcle 10
Analvsis Date/Time
PZ-304-AS TOT_07_16_2013
PZ-304-AS TOT_07_16_2013
PZ-304-AS TOT_07_16_2013
PZ-304-AS TOT_07_16_2013
PZ-304-AS TOT_07_16_2013
PZ-304-AS TOT_07_16_2013
PZ-304-AS TOT_07_16_2013
PZ-304-A5 TOT_07_16_2013
13-07147-12
13-07147-12
13-07147-12
13-07147-12
13-07147-12
13-07147-12
13-07147-12
13-07147-12
08/06/2013 16:35:55
08/14/201311:09:24
08/10/2013 15:02:04
08/10/2013 15:02:04
08/10/2013 15:02:04
08/13/2013 09:06:01
08/13/2013 09:06:01
08/13/2013 09:06:01
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HA5L 300,
HASL 300,
HASL 300,
HASL 300,
PZ-304-AS
PZ-304-AS
PZ-304-AS
PZ-304-AS
PZ-304-AS
PZ-304-AS
PZ-304-AS
PZ-304-AS
13-07147-13
13-07147-13
13-07147-13
13-07147-13
13-07147-13
13-07147-13
13-07147-13
13-07147-13
08/06/2013 16:35:57
08/14/201311:09:25
08/10/2013 15:02:06
08/10/201315:02:06
08/10/2013 15:02:06
08/13/2013 09:06:02
08/13/2013 09:06:02
08/13/2013 09:06:02
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
MW-104 TOT_07_16_2013
MW-104 TOT_07_16_2013
MW-104 TOT_07_16_2013
MW-104 TOT_07 _16_2013
MW-104 TOT_07_16_2013
MW-104 TOT_07_16_2013
MW-104 TOT_07_16_2013
MW-104 TOT_07_16_2013
13-07147-14
13-07147-14
13-07147-14
13-07147-14
13-07147-14
13-07147-14
13-07147-14
13-07147-14
08/06/2013 16:35:59
08/14/201311:09:25
08/10/201315:02:07
08/10/2013 15:02:07
08/10/2013 15:02:07
08/08/2013 09:08:37
08/08/2013 09:08:37
08/08/2013 09:08:37
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HA5L 300,
HASL 300,
MW-104
MW-104
MW-104
MW-104
MW-104
MW-104
MW-104
MW-104
13-07147-15
13-07147-15
13-07147-15
13-07147-15
13-07147-15
13-07147-15
13-07147-15
13-07147-15
08/06/2013 16:36:02
08/14/201311:09:25
08/10/201315:02:09
08/10/2013 15:02:09
08/10/2013 15:02:09
08/08/2013 09:08:38
08/08/2013 09:08:38
08/08/2013 09:08:38
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
Client Sample ID
i:illl
ll;ll
~~,JI
Jl:.~~

SDG: 1307147
Matrix: Water
DIS_07_16_2013
DIS_07_16_2013
DIS_07 _16_2013
DIS_07_16_2013
DIS_07_16_2013
DIS_07_16_2013
DIS_07_16_2013
DIS_07_16_2013
015_07_16_2013
DIS_07_16_2013
DIS_07_16_2013
DIS_07_16_2013
015_07_16_2013
015_07_16_2013
DIS_07_16_2013
DIS_07_16_2013
EBERLINE
SERVICES
Analyte
Uranium-234

Date: 8/29/2013
Page 4 of 5
Result
Error
csu
MDA
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
2.00
1.79
0.03
0.64
0.15
0.46
0.72
0.45
0.73
0.70
0.06
0.26
0.12
0.69
0.98
0.68
0.84
0.81
0.06
0.27
0.12
0.69
0.98
0.68
0.45
1.28
0.12
0.11
0.13
1.11
1.53
1.10
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
1.68
1.93
0.09
0.64
0.10
1.27
0.35
0.54
0.65
0.79
0.10
0.26
0.09
0.91
0.60
0.56
0.74
0.91
0.10
0.27
0.09
0.91
0.60
0.56
0.45
1.49
0.12
0.10
0.09
0.89
1.05
0.59
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.98
1.72
0.71
1.15
0.60
2.89
0.74
2.39
0.44
0.79
0.25
0.34
0.22
0.59
0.28
0.52
0.49
0.88
0.26
0.37
0.23
0.63
0.28
0.54
0.26
1.49
0.09
0.10
0.07
0.12
0.12
0.08
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.24
0.85
0.00
0.46
0.05
2.21
0.36
1.65
0.21
0.72
0.04
0.20
0.06
0.50
0.19
0.41
0.22
0.75
0.04
0.21
0.06
0.52
0.20
0.43
0.28
1.46
0.11
0.10
0.09
0.10
0.14
0.12
Method

865/481-0683
FAX 865/483-4621
Qualifier
u
J
u
u
u
J
u
J
J
u
u
J
J
J
u
u
Units
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1

Lakewood, CO 80235
Client Sample ID
f~l
tf.ll
1-Jr
U11

SDG: 1307147
Matrix: Water
Lab Sample ID
Analvsis Date/Time
Analyte
13-07147-16
13-07147-16
13-07147-16
13-07147-16
13-07147-16
13-07147-16
13-07147-16
13-07147-16
08/06/2013 16:36:04
08/14/201311:09:26
08/10/201315:02:10
08/10/201315:02:10
08/10/2013 15:02:10
08/08/2013 09:08:40
08/08/2013 09:08:40
08/08/2013 09:08:40
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
PZ-204A-SS
PZ-204A-SS
PZ-204A-SS
PZ-204A-SS
PZ-204A-SS
PZ-204A-SS
PZ-204A-SS
PZ-204A-SS
13-07147-17
13-07147-17
13-07147-17
13-07147-17
13-07147-17
13-07147-17
13-07147-17
13-07147-17
08/06/201316:36:07
08/14/2013 12:03:03
08/10/2013 15:02:13
08/10/201315:02:13
08/10/201315:02:13
08/08/2013 09:08:43
08/08/2013 09:08:43
08/08/2013 09:08:43
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
PZ-302-AI TOT_07_16_2013
PZ-302-Al TOT_07_16_2013
PZ-302-Al TOT_07 _16_2013
PZ-302-Al TOT_07_16_2013
PZ-302-Al TOT_07_16_2013
PZ-302-Al TOT_07_16_2013
PZ-302-Al TOT_07_16_2013
PZ-302-Al TOT_07_16_2013
13-07147-18
13-07147-18
13-07147-18
13-07147-18
13-07147-18
13-07147-18
13-07147-18
13-07147-18
08/06/201316:36:09
08/14/201312:03:04
08/10/2013 15:02:14
08/10/2013 15:02:14
08/10/201315:02:14
08/08/2013 09:08:45
08/08/2013 09:08:45
08/08/2013 09:08:45
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
PZ-302-AI
PZ-302-Al
PZ-302-Al
PZ-302-Al
PZ-302-Al
PZ-302-Al
PZ-302-Al
PZ-302-Al
13-07147-19
13-07147-19
13-07147-19
13-07147-19
13-07147-19
13-07147-19
13-07147-19
13-07147-19
08/06/201316:36:11
08/14/201312:03:04
08/10/2013 15:02:16
08/10/201315:02:16
08/10/2013 15:02:16
08/08/2013 09:08:47
08/08/2013 09:08:47
08/08/2013 09:08:47
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
DIS_07_16_2013
DIS_07_16_2013
DIS_07_16_2013
DIS_07_16_2013
DIS_07_16_2013
DIS_07_16_2013
DIS_07_16_2013
DIS_07_16_2013
EBERLINE
SERVICES
Result
Error
csu
MDA
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
1.82
0.57
0.37
0.49
0.18
1.98
0.38
1.27
0.52
0.73
0.21
0.24
0.14
0.65
0.28
0.49
0.65
0.74
0.21
0.25
0.14
0.67
0.28
0.50
0.23
1.50
0.15
0.14
0.11
0.21
0.20
0.19
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
1.07
1.59
0.04
0.42
0.12
2.41
0.40
1.86
0.39
0.72
0.06
0.18
0.09
0.62
0.24
0.52
0.45
0.81
0.06
0.19
0.09
0.64
0.25
0.54
0.18
1.37
0.10
0.08
0.07
0.11
0.20
0.11
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.80
0.85
0.12
0.59
0.15
3.60
0.73
3.10
0.34
0.76
0.09
0.22
0.11
0.60
0.24
0.53
0.38
0.78
0.09
0.24
0.11
0.65
0.24
0.58
0.18
1.53
0.07
0.10
0.10
0.07
0.08
0.07
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.69
1.34
0.00
0.57
0.07
5.18
0.84
4.06
0.34
0.88
0.03
0.21
0.07
1.25
0.42
1.04
0.37
0.93
0.03
0.22
0.07
1.31
0.43
1.08
0.24
1.74
0.07
0.06
0.07
0.23
0.28
0.16
Method
PZ-204A-SS TOT_07_16_2013
PZ-204A-SS TOT_07 _16_2013
PZ-204A-SS TOT_07 _16_2013
PZ-204A-SS TOT_07_16_2013
PZ-204A-SS TOT_07_16_2013
PZ-204A-SS TOT_07_16_2013
PZ-204A-SS TOT_07_16_2013
PZ-204A-SS TOT_07 _16_2013
DIS_07_16_2013
DIS_07_16_2013
DIS_07_16_2013
DIS_07_16_2013
DIS_07_16_2013
DIS_07_16_2013
015_07_16_2013
DIS_07_16_2013

Date: 8/29/2013
Page 5 of 5

865/481-0683
FAX 865/483-4621
Qualifier
u
J
J
u
J
J
J
J
J
u
u
Units
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
SECTIONV
ANALYTICAL STANDARDS
LL-B
QA/OC REVIEWED CERTIFICATE OF CAUBRATION

~q(lnitialsJ ALPHA STANDARD SOLUTION
Radionuclide:
U-238NAT
Half Life:
(4.468 0.005) x 10"9 years
Catalog No.:
7338
Source No.:
479-50
Description of Solution
a. Mass of solution:
b. Chemical form:
c. Carrier content:
d. Density:
<.'"
;.:
TMAEBERLINE
Customer:
OR2778
P.O.No.:
Reference Date:
January 11995
12:00 PST.
Contained Radioactivity: (Total U) 8.016 p.Ci
Contained Radioactivity: (Total U) 297 kBq
65.2896 gin a 50 ml flame sealed ampoule

Uranyl Nitrate in H20
None
Approximately 1.3202
Radioimpurities
.:'.:
g/ml @20C.
Refer to attached technical data sheet
Radioactive Daughters
Refer to attached technical data sheet
.. '
Radionuclide Concentration
,.:.
(Total U) 0.1228
pCi/g.
Method of Calibration
,,
Activity calculations are based upon known specific activity and mass.
::. :.;
Uncertainty of Measurement
a. Systematic uncertainty in instrument calibration:
b. Random uncertainty in assay:
c. Random uncertainty in weighing(s):
d. Total uncertainty at the 99% confidence level:
.:..
3.0%
:.')'
.. .'. ...
0.0%
2.0%
3.6%
;.
'. , ,
:r.:,
;.:,.;:
1;.
-1
NIST Traceability
This calibration is implicitly traceable to the National Institute of Standards and Technology.
Leak Test(s)
See reverse side for Leak Test(s) applied to this source.
Notes
1. Nuclear data were taken from "Table of Radioactive Isotopes, edited by Virginia S. Shirley, 1986.
2. IPL participates in an NIST measurement assurance program to .:!otablish and maintain implicit traceability for a number of nuclides,
based on the blind assay (and later NIST certification) of Standard Reference Materials (As in NRC Regulatory Guide 4.15).
.;,:.:'
E!$1vAuA$
....,.:
YCONTROL
IF
S 0
Date Signed
ISOTOPE PRODUCTS LABORATORIES

J>
I'
PRODUCTS
3017 N. SAN fERNANDO BLVD.

BURBANK, CALIFORNIA 91504
.,
LABORATORJES
8188437000
FAX
,.
. ~
8188436168
.:>.,;,::
.:1
.'
i.'
QUALITY CONTROL PROGRAM

MP-009
Rev.S; 11/01/03
Title: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES OAK RIDGE LABORATORY
RADIOACTIVE REFERENCE SOLUTIONS
PRIMARY DILUTION RECERTIFICATION

MP009
Half Life, Days
Half Life, Years

4.4aae+a9l
1 ',
I . ...1.632E+12I
Reference Date I
<
1/1/1'99.5 O:OOj
Ampoule /Solution Gross ;:. ...97.6400 Weight, Grams

Empty Ampoule . >'32:5020 Weight, Grams
Solution Net
65.1380 Weight, Grams
Total Activity in Ampoule
8.0160 J,.lCi
Dilution Instructions:
Dilute to a volume ofl . 1000.00 ,.
Certified Total Activity of)
. . >I
Dilution Solvent Used
Imilliliters
Which Eauals
1.780E+07)dpm at the date listed above

This activity concentration is based on the original
And after dilution the activity of this solution is 1.77955E+D41 dpm/ml-eterence date listed above. All activities are corrected
to the date and time of analysis by the laboratory data
processing software.
Expiration Date: September 6, 2013
Date: _ _...;;;.;;.,;;.,.;;=..;.;;....;..--...
9/26/2012 0:00
Date:
----.:'-r-1u~/~...tL..
__
~!;; R~~!':'ofi
Ia E
MP-009
Rev.8; 11101/03
EBERLINE SERVICES -OAK RIDGE LABORATORY

RADIOACTIVE REFERENCE STANDARD SOLUTIONS
SECONDARY DILUTION RECERTIFICATION
MP-009
Solution Reference# IPL47g.;so .
PrinciPal Radionuclide
Half Llfe1 Years
234; 2~,. 23&-u
I 4.46aE+o9l
Date I
. I
Solution~
9/6/2012 0:001
. .. U-:Ba......... 1
Half Life1 Dals

. 1.632E+12l
: . : 23~.~r
~ U .
Radionuclide of lnteresttl "234
Parent Solution Conc.t 1:7796E+04 ldpm/ml
Reference Date
.
<
> 1/1i19ss o:oo
Chemical Composition of Standard Solution
IUraniY Nitrate 1111 ~ HN03
. >
.....
.....
..
j1MHN03
>
SECONDARY VOLUMETRIC DILUTION

Vol. Parent Solution: :.. \:< :: . 4:0000 ml
Total Activity: 7.1182E+04 dpm
Final Volume: . .... 1000~00 ml
Final Activity Concentration:!

reference date listed above. All activities are
corrected to the date and time of analysis by the
l11hnl'$ tory data processing software.
NOTES:
,
Isotopic Distribution as:
U-238 Atom % = 48.239
U-235 Atom % = 2.25
U-234 Atom o/o = 49.501
All values +/- 3.6%
7.1182E+01jdpmlml
U-238 =71. 182 dpmlml X 0.48249 34.345 dpm/ml

U-235 = 71.182 dpmlml X 0.0225" 1.602 dpm/ml
U-238 =71.182 dpmlml X 0.49501 = 35.236 dpm/ml
Expiration Date: September 6, 2013

Isotopic ratios from manufacturer's data sheet
Verified &
Approved~.
QCApproval
f\
~l'
~~lll
[\
I
Date:
9/26/2012 0:00
Date:
q_tz.(p/rz-
"
29
.... :. .~':".?:;.
:.~
RECORD COt-JY
Tracer Solution for Environmental Analysis & Disequilibrium Studies
{.!
Product Description & Measurement Certificate

Description
Principal radionuclide:
Daughter Nuclide:
Measurement
Reference date:
Radioactive concentration U-232
which is equivalent to
uranium 232 (U-232)

Th-228
Volume of solution
Total activity ofU-232
which is equivalent to
Product code: UDPlOOSO

Batch Number: 921232/67
01 March 2000
6.739E+03 becquerels per gram ofsolution
1.821E-Ol microcuries per gram ofsolution
5.35 gi"Cii:iS
5.035 millilitres
3.61E+04 becquerels
9.76E-Ol microcuries
Method of measurement (see reverse of this certificate)

Random uncertainty is: 0.7%
Systematic uncertainty: :1:0.5%
Overall uncertainty in the radioactive concentration quoted above: 1.7%
Overall uncertainty is defmed on the reverse of this certificate.
Accuracy
Radionuclidic
Purity
Any radioactive impurities measured are listed below, expressed as percentages

of the activity ofthe principle radionuclide at the reference date .
Th-228 and daughter activity removed 2 Feb 2000
U-232 daughters activity will increase with time. By alpha 88% U-232, 12% daughters on 1/3/00
Isotopic
Purity
"'"he isotopic composition, exprP.ssed as atom per cent at the reference date .
l'iot measured
Chemical
Composition
Calculated weight ofU-232, 4.42E-08 grams, as 2M HN03 solution in a flame sealed glass vial.
This Tracer solution has been produced 'carrier free'.
Physical
Data
Recommended half life of uranium 232: 6.980E+O 1 ye!U's

Principle energies of alpha emissions (MeV): 5.263 31.7%, 5.320 68.0%
Branching ratio for alpha emission: 100%
Calculated specific activity ofuranium 232: 8.167E+05 Bq per microgram U-232.
Remarks
For safety information and notes to ensure correct usage by all persons handling this radio'ictive Tracer
solution please read the instructions accompanying the package.
AEA Technology operates a quality management system which has been independently audited and
approved to ISO 900 I.
Approved
Signatory
Project Ref. AE2315
Roger Wiltshi.re
Prepared and characterised in the UK, for world wide distnbution by lsotrak, AEA Technology, QSA.
Trkcert.wps 10/03/00
AEA Technr>logy is the trading name ofAEA Technology pic i
G3 m

MP.()09
Rev.8; 11101103

PRIMARY DILUTION RECERTIFICAT/ON
MP009
Half Life, Years
I. . .
I . 7.200E+011
c..:=oz:::];.~;11l~cl
Certified Concentration
<
>>
2.630E+04I
Reference Datel. .. 3/1/2000 O:Ool
p.Ci per gram
Ampoule /Solution Gross~.

.. . ...Weight, Grams
Empty Ampoule > . . ... Weight, Grams
Solution Net . . . Weight, Grams
0.9760 !J.CI
Total Activity In Ampoule
:.:..
.................
I232Q(N03)6 in 2MHN03.>
. ..... I
_
Dilute to a volume ofl
Certified Total Activity of
1000.00
I . 0.9760itJ.CI
!milliliters
Which Eauals
1 . 2.167E+06Idpm at the date listed above

This activity concentration Is based on the original
And after dilution the activity of this solution Is 1 2.167E+03Idpm/ml reference date listed above. All activities are corrected
Expiration Date:
Date:
Date:
I December 7, 2013 I
12113/2012 0:00
13/"::J
1
~E~LNEI

MP009
EAVICII!tS
Rev.8; 11/01/03
Title: Radloaetfve Reference Standards Solutions & Records
EBERLINE SERVICES- OAK RIDGE LABORATORY

1217/2012 0:001
Date I
<
u~1oa >.I
Solution#!
Half Life, Da:l!
.
. .. 2.630E+041
MP-009
Solution Reference # AEA!Amersham 92/232/67 1
Principal Radionucllde
Half Life, Years
~zu
I
7 .200E+01l
I....
... 21~u ...,..

Radlonuclide of lnteresj
Parent Solution Cone. . 2.167E+03 : ldpm/ml
Reference Datel' < .. 31112oboo:ool
Chemical Com~ition of Standard Solution
I 2~U(N03)e in 2M HN03
.. . .. ...: . ..
. . ....... . . .. .
..
...
<
I
I2MHNOa.::
.. ..
...
,, ..
: ..

....
Vol. Parent Solution:

10.0000 ml
Total Activity:
2.1670E+04 dpm
., 1000.00 ml
Final Volume: .
Final Activity Concenb'ation:l
. 2.1670E+01Idpmlml

laboratory data processing software.
NOTES:
Expiration Date:l December 7. 2013
c~
~
~~
r~~ tJJll~ 0
Verified & Approved By
ac Approval
'--'
Date:
Date:
1211312012 0:00
t~lt2:::
I
RTIFICATE OF
ALffiRA
LPHA STANDARD SOLUTIO
(7.54
114944
P.O.No.:
Reference Date:
November 1 1991
Contained Radioactivity:
1.036
7230
Source No.:
388-116
b. Chemical form:
c. Carrier content:
d. Density:
q\
oc' \~:t\\~e
TMA EBaull..~\\\~t \.'0
Customer:
Th-230
0.03) x 104 years
IG
5.0042
Th(N03)4 in O.lN HN03
,,\l
12:00 PST.
"Ci.
grams.
None added
1.0016
Radioimpurities
See attached technical data sheet
See attached technical data sheet
0.207
Weighed aliquots of the solution were assayed using a liquid scintillation counter.
2.0%
O.S%
0.2%
2.7%
NIST Traceability
Notes
1. Nuclear data were taken from "Table of Isotopes", Seventh Edition, edited by Virginia S. Shirley.
2. IPL participates in an NIST measurement assurance program to establish and maintain implicit
traceability for a number of nuclides, based on the blind assay(and later NIST certification) of
Standard Reference Materials. (As in NRC Regulatory Guide 4.15)

1800 No. Keystone Street.,
~--------~~-s_ts_bum_~__,_~_,_:W_ornm
___9_t_s~--~--------------------------------------------m~833
Rev.8; 11/01/03

MP-009
Solution Reference# IPL 388-i116 : <
Half Life, Years
1.. T54ot:+041
Reference Datal<
"11/1/1991'0;001

Vol. Parent Solution: '. ..<. AO;OOOO ml
Total Activity: 2.2999E+04 dpm
Final Volume: >1000~00 ml
Final Activity Concentration:! .
2.2999E+01ldpmlml

NOTES:
Expiration Date:l
Recertified
Date:
By
Date:
QCApproval
Date:
Verified & Approved
March 4, 2014
312112013 0:00
je?.l \~
~t;l.-\(1/
34

MP~09
Rev.8; 11/01/03

MP009
CURRENT DATE I
3/4/2013 O:OOJ
SOLUTION REFERENCE #rniP::"I'L~-3:-:.8":1:"&;~J1::"::6:--..~. ,:. ,., .-.-. ,.,.,_. .,:.,. ,., . ,., _.:._-:..,.,._
. . ,
SOLUTION #[.. :_. : ~/ Th.::1. > <I
Principal Radlonuclide
_:
~h
Half Life, Years
Half Life, Days

2.7'54E+071
I 7:54dE+041
>
Radionuclide l 41~horiurn.
Certified Activity \ '1~036E:f;()O

J!Ci
Certified Concentration I<
.<.: ' J!Ci per gram
Ampoule /Solution Gross
,
Empty Ampoule .
Solution Net
9:2660 Weight, Grams

4:6218 Weight, Grams
4.6442 Weight, Grams
1.0360 ~J.Ci
Chemical_ Composition of Standard Solution
Certified Total Activity ofl
tooo~oo:
.. 1.0360l!J.Ci
Imilliliters
Which Eauals
2~300E+06jdpm at the date listed above
And after dilution the activity of this solution is 2.300E+03Idpm/ml

reference date listed above. All activities are corrected
Expiration Date:
Date:
Date:
'March 4, 2014
3/21/2013 0:00
{'J-1/r
8835
1h-8
CERTIFICATE OF CALIBRATION
ALPHA STANDARD SOLUTION
Radionuclide:
Th-232
Half Life:
(1.405 0.006) x 10... 10 years
Catalog No.:
7232
Source No.:
435-104-2
b. Chemical form:
c. Carrier content:
d. Density:
Customer:
P.O.No.:
Reference Date:
TMA EBERLINE
VH1632
November 1 1993
11.9712 g (in a 10 ml flame sealed ampoule)

Th(N03)4 in water
None added
Approx. 1.21
Radioimpurities
12:00 PST.
~i.
(Th-232) 0.0933
(Th-232) 3.45
kBq.
gtml @ZOc.
None detected (other than daughters).
.
Ra-228, Ac-228, Th-228, Ra-224, Rn-220, Po-216, Pb-212, Bi-212,Po-212, TI-208.
(Th-232) 0.00779
flCi/g.
Activity calculations are based upon known specific activity and mass.
3.0%
0.0%
2.0%
3.6%
NIST Traceability
Leak Test(s)
Notes
l. Nuclear data.'\Vere taken from "'rable of Radioactive Isotopes", edited by Virginia S. Shirley, . l986.
2. IPL partici~tes in an NIST measurement assurance program to establish and maintain implicit traceability for a number of nucli~,
based on the blind assay (and later NIST certification) of Standard Reference Materials (As in NRC Regulatory Guide 4.15).
QUALITY CONTROL
Date Signed
1800 North Keystone Street
Burbank, California 91504
818 843 - 7000

MP.009
Rev.B; 1110/03
P~MARYD~UnONRECERnRCATION
MP009
Radionuclide!"''~ea:':'l
Certified Activity 3::~: .9133()~;()2 J.LCi

Certified Concentration ;;:; \:;:::::;: J.LCi per gram
Ampoule /Solution Gross 'X',::;18i$4.1S Weight, Grams
Empty Ampoule 'i: JS:9296 Weight, Grams
Solution Net : 11:9119 Weight, Grams
Total Activity in Ampoule I
0:0933 J.LCi
Dilute to a volume orj:\ :._:1000.00: : !milliliters
Certified Total ACtivity
otl .._._.-. . 0,0933IJ.1Ci
Which eauals
I> ' 2.071E+osjdpm at the date listed above
And after dilution the ar;tivity of thh; $Oiution isi2;071E;,.,02Idpm/ml
:::r:!~:::mmr::e~s!~~':w':!::::cted
Expiration Date:l-.octobef9,2013.
Verified & Approved :Y

QCApproval
~ ~
~AltluA I
'-'"'
-\01'
"
!\0 .
Date: _ _10/9/2012 0:00
.;.;;;.;.;=~....;;..;.-
Date:
/,J
11
1 z.
_..........,.,_=1~--
(EBERL-'-"'~" I QUALITY CONTROL PROGRAM

MP-oo9
S&RVICI;.S.
Rev.8; 1/10/03
SECONDARY DILUTION RECERTfFICATION
a:oo
11/9/2012
I
Datal
Th.,;Sb ...... J
Solution #I ,
Half Life1 Dals
5.132E12!
MP-009
Solution Reference #IIPL43s-;1 04-2 . .
Principal Radionuclide
Half Life, Years
. Z2B & 232Th I
1.4o5E;..1ol
Radionuclide of lnteresd 2_28 & 232-Th

Parent Solution Cone. . . 2;071:+02
Reference Date
.f1H/1993.:o:ool
ldpm/ml
Chemical Come5!sltlon of Standard Solution
1Th(N03)4 in 1% HN03
I<
...
I
I1%NitrieAeid
. I

Total Activity:
Final Volume:
.. . 500;0000 ml
1.03651:+05 dpm
1000;00 ml
1.0356E+02ldpm/ml

NOTES:
Expiration Date:
Verffied & Approved
a~ ~
QCApproval
~JJJ ~\J"l11v ~""- - .,.
I . October 9, 2013 I
11/9/2012 0:00
Date:
Date:
1\
1..,
lvz..
1
Isotope Products
7/,-/8
24937 Avenue Tibbitts

Valencia, California 91355
Laboratories
An Eckert & Ziegler Company
Tel 6613091010
Fax 6612578303
ALPHA STANDARD SOLUTION
Radionuclide:
Half-life:
Catalog No.:
Source No.:
Th-229
7340 160 years
7229
867-54
Customer:
P.O. No.:
Reference Date:
(Th-229 only)
EBERLINE SERVICES
00009633
15-Jan-02 12:00 PST
1.013
J.tCi
37.48
kBq
Physical Description:
A. Mass of solution:
B. Chemical form:
C. Carrier content:
D. Density:
5.0147 g in 5 ml flame-sealed ampoule

Th(N03)4 in 0.1 M HN03
10!-!g Th/mL
1.0016 g/mL@ 20C.
Radioimpurities:
None detected (daughters in equilibrium)
Radionuclide Concentration:
0.2020
!-!Ci/g,
kBq/g
7.474
Method of Calibration:
This source was prepared from a weighed aliquot of solution whose activity in !JCi/g was determined
using gamma ray spectrometry.
Peak energy used for integration:

193.5 keV
Branching ratio used:
0.0441 gammas per decay
Uncertainty of Measurement:
A.
B.
C.
D.
Type A (random) uncertainty:

Type B (systematic} uncertainty:
Uncertainty in aliquot weighing:
Total uncertainty at the 99% confidence level:
0.7%
3.0%
0.0%
3.1%
Notes:
- See reverse side for leak test(s) performed on this source.
- IPL participates in a NIST measurement assurance program to establish and maintain implicit traceability
for a number of nuclides, based on the blind assay (and later NIST certification} of Standard Reference
Materials (As in NRC Regulatory Guide 4.15).
- Nuclear data was taken from IAEA Technical Report Series No. 261.
- This solution has a working life of 5 years.
CJ- Jtvh-02.
Quality'C<;ntrol
Date Signed
IPL Ref. No.:
867-54
----------------~ 1509001 CERTIFIED - - - - - - - - - - - - - - - -
Medical Imaging Laboratory

24937 Avenue Tibbitts
Valencia, California 91355
Industrial Gauging Laboratory


MP-009
Rev.8; 1/10/03
Title; Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES - OAK RIDGE LABORATORY


MP009
CURRENT DATE!
SOLUTION REFERENCE #lr.:IP:":"L-:::8-:-:67~.;s.t::-:--
~-..,....,......,...,......,....,.......,.._~.I
SOLUTION #J
22~
Radlonuclide~.'
. . . . .
Certified Activity J.013E+OO J.1CI
Certified Concentration. _...... . '. . . . JJ.Ci per gram
> Jri 0.1 MHN"O

. .......3 4 .......... ... ~: 3
1. 29fh(NO
2
. .. . . .
2.sa1 E+osl
Reference Datel :
Ampoule /SoluUon Gross

Empty Ampoule
Solution Net
Th-48 <
Half Life, Days
Half Life, Years
L 7.340E+o3l
11/9/2012 O:OOJ
8.7752
3.7591
5.0161
1.0130
1h5/2002'0:0ol
Weight, Grams
Weight, Grams
Weight, Grams
J.1CI
. . . 'I
Dilution lnstrucUons:
.. .. I
1000.00
Certified Total Activity ofl 1.0130IJ.tCi
!milliliters
Which Eauals
2.249E+06jdpm at the date listed above

And after dilution the activity of this solution is 1 2.249E+03j dpm/ml reference date listed above. All activities are corrected
Expiration Date:
~----=-~;;;.:::~~~---
Verified & Approved By __

QC
Approvai_~~~A~I.~~Aut.U.JL.JI.M~N_ __
""--"'
Date:
Date:
October 9, 2013 ]
11/9/2012
-------
0:00
--.:r,.u/rzf,z_
. . ,. ,- --
;:E.,_ER!..J_NE
SEAVICE:S
PROGRAM
I QUALITY CONTROL
MP.009
Rev.7; 9129199

MP..009
Solution Reference #IIPL86.7-54 . .
Half Life1 Years
. 22aTh ..
I . .. 7 .340E+03l
Radionucllde of lnteres1 .~.

Parent Solution Cone. . 2:25E+03 ldpmlml
Chemical Coml!osltion of Standard Solution

. ... ... ... .< .. . <
ITH{N~)41n0.1MHN03
11/9/2012 0:00)
Date!
Solution #I> . .. Jh.,,18a\ . ... I
Half Life1 Daxs
2~as1E+oel
Reference Date 1
1/15/20020:001
. .
!0.1MHN03' :
.. . .. '
.. I

Total ActiVIty:
Final Volume:
10.0000 ml
2.2490E+04 dpm
1000.00 ml
2.2490E+01jdpmlml

NOTES:
Expiration Date:l
I'
Verified &Approved By
QC Approval ~tA~.M_L.,L
K'
'-'
October9,2013
Date:
11/9/2012 0:00
Date:
UfiZ,t'"Z
I
j}attonal1fnstttutt of
~tanbarbs
& mecbnologp
C!Certificate'
Standard Reference Material 4251C ., "

l3arium-133 Radioactivity,_Standard . ,
I
Ir.
This Standard Reference Mat~rial.(SRM) consists o~ radioactive barium-133. c~loride,. non-radioactive barium
chloride, and hydrochloric acid diSsolved in 5 mL of distilled water. The solution is contain~d in a flame
sealed NIST borosilicate-glass ampoule. The SRM is intended for the calibration of ionization' chambers and
solid-state gamma-ray,:spectrometry .srstems.
r.
Radiological Hazard
The
SRM ~mpoule contains bariuni-133 with 'a total activity of approximately 2.5 MBq.
Barium-133 decays
by electron capture and during ~JJ.e decay process X-rays, and g~a;rays with energies from 4 ~o 400 keV are
emitted. Most of these photons escape from the SRM ampoule and can represent a radiatic:m hazard.
Approximate unshielded dose rates at several distances (as of the reference time) are given in note [a]*.
Appropriate shielding and/or distance should be used to ntinimiz~ personnel exposure. ,-,The SRM ~hould be
usec;l. . only by persons qualified
to handle
radioactive. .material. . .. ,
. .,
'
.
,. .
... ,
~
I.
'
Chemical Hazard
The SRM ampoule contain~ .hydrochloric acid (HCI) with l'!- concentration ()f l mole per liter of .water. The
solution is corrosive and represents a health hazard if 1t comes in contact with. eyes or.skin~. If the ampoule
is to be opened to transfer the solution, the recommended procedure is given on page 2. The ampoule should
be openedpnly by persons qualified to handle, both radioactive material and strong acid solution.
Storage and Handling
The SRM should be stored and used at a temperature between 5 and 65 C. The solution in an unopened
ampoule should remain stable and homogeneous until at least June 2004.
The ampoule (or any subsequent container) should always be clearly marked as containing radioactive
material. If the ampoule is transported it should be packed, marked, labeled, and shipped in accordance with
the applicable national, international, and carrier regulations. The solution in the ampoule is a dangerous
good (hazardous material) both because of the radioactivity and because of the strong acid.
Preparation
This Standard Reference Material was prepared in the Physics Laboratory, Ionizing Radiation Division,
Radioactivity Group, J.M.R. Hutchinson, Group Leader. The overall technical direction and physical
measurements leading to certification were provided by L.L. Lucas of the Radioactivity Group and D.B. Golas,
Nuclear Energy Institute Research Associate.
The support aspects involved in the preparation, certification, and issuance of this SRM were coordinated
through the Standar4 Reference Materials Program by N.M. Trahey.
Gaithersburg, Maryland 20899
October 1994
!
!
I.
!
I
I
II..
Thomas E. Gills, Chief

Standard Reference Materials Program
I
SRJvl 4251C, pl!ge 1 of 6
*Notes and references are. on pages? and 6.

QCP-009
Rev.B; 11/1 0/03
TiUe: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES~ OAK RIDGE LABORATORY

PRIMARY DILUTION RECERTIFICAT/ON
QCP 009-1
CURRENT DATEI . 611612013 0:001
SOLUTION REFERENCE #I"':'IN".':":IS::::.T~:S~R=.M:-::.4-=:25~1~0~:~:~<....,.... .,.,:.,.; .
SOLUTION #f/.::. \'/':.Ba;;a.\/' o(1
Half Life, Days
Half Life, Years
..'
J
,.1;,;31''
Barium~
i :3.828Ei{)3j
l";<:-;1:ee~c:l11
li
Reference Datei?~;:J:'_;'-~l:1/,1$$~<o:ool
Radlonuclide >::}~13~tiym:.
Certified Activity lc:;y;::'f:!e'iq;;,:.>:>> J.LCI
Certified Concentration )1.1 :atsE+01 J,1Ci per gram
Ampoule /Solution Gross . :\;::~;30$1 Weight, Grams

Empty Ampoule :f'/:4:2582 Weight, Grams
Solution Net .5;0499 Weight, Grams
Total Activity in Ampoulet , . . 66.5577 J.LCI
Dilute to a volume ofl:\ \1.Q00:00fi\~'lmilllllters
Certified Total Activity ofl
66:55771 JA.Ci
Which Eauals
'1A78E+08Idpm at the date listed above
And after dilution the activity of this solution lsi: 14.?S. E+OSidpm/ml


refen!f'lce date listed above. All activities are corrected
Expiration Date: 1 <June 16; 2014
'\
Verified & Approved By

QC Approval
~;J
~
..__...... lnr1 AJAM
/
"'
\\
"'
Date:
7/1/13
Date:
11~1:3
i'
"l
~EBER~ I QUALITYC~:OLPROGRAM
Rev.8; 11/10/03
Radioactive Reference Standards Solutions & Records
Trtle:

SECONDARYD~UT/ONRECERTIRCATION
Date(<
()11.8/13 --- j
Solution #l~:c..\(:,/':.ea::aa::c."'>: . c:::.l
Solution Reference #I NIS1YSRM4251 c>.)? ::: ,,:j

Half Life, Years
:.:}:t~sa\<:
l.:'cd:o48E+01'1
ChemicalComposition of Standard Solution

SECONDARYVOLUMETmCD~UnDN
Vol. Parent Solution: ./('>\'2510001) ml

Total Activity:
3~6950E+o6 dpm
Final Volume: ::,<':1000;00 ml
>. 3c6950E+03Idpm/ml

NOTES:
Expiration Date:
Date:
QCApproval
June 18, 2014
_____.........___
,..,.,_/:z.-l/~-.t;;;.:)
,
Date: _ _
......
7/1/13
__
CERTIFICATE OF CALIBRATI
ALPHA STANDARD SOLUTIO
Radionuclide:
Half Life:
Catalog No.:
Source No.:
Ra-226
1600 7 years
7226
453-26
b. Chemical form:
c. Carrier content:
d. Density:
TMA EBERLINE
Customer:
P.O.No.:
VH1888
Reference Date:
February 1 1994
12:00 PST.
Contained Radioactivity: (Ra-226) 1.001 p.Ci.
Contained Radioactivity: (Ra-226) 37.0 kBq.

5.1864 g (in a 5 m1 Flame Sealed Ampoule)
Ra(N03)2 in 1 N HN03
None added
1.. 0318
Radioimpurities
None detected(other tbail daughters)
Rn-222, Po-218, At-218, Pb-214, Bi-214, Po-214, Tl-210, Pb-210, Bi-210, Po-210 and Tl-206.
(Ra-226)
0.1929
.. : . ~tCilg.
Weighed aliquots of the solution were assayed using gamma spectrometry:
Energy peak(s) integrated under: 186 keV.
Branching ratio(s) used:

0.0351
gamma rays per decay.
3.4%
3.1%
0.2%
4.6%
NIST Traceability
Leak Test(s)
Notes
1. Nuclear data were tabnfrom "Table of Radioactive Isotopes", edited by Virginia S. Shirley, 1986.
2. IPL panicipates in an NIST measurement assurance program to establish and maintain implicit traceability for a numb\:r of nuclides,
- based on the.blind
assay"(ali<llater NIST cerlfficatioiifofstaiidiiid Reference Materiiils\AB"iii NRC.ReguiBroryGiiidif4; rs)~- -
QUALITY CONTROL
/iA,. ;
199 If
Date Signed
818 843- 7000

MP009
Rev.8; 11101103

MP009
CURRENT DATE!
SOLUTION REFERENCE #lr:":IIP~L-4~5~a.::"='26~._,.
_,..
.._,...-~--,1
SOLUTION #L
2
2\lRadium
Half Life, Days

5.844E+osl
r.
Half Life, Years

1.600E+03I
11/9/2012 0:00]
Ra-5
. . I
Radionuclide ~.6 Radiurr1.

Certified Activity 1'.00.1 E.f.OO JA.Ci
Certified Concentration 1.
IJ.Ci per gram
Reference Date
<. 2/111994 O:Ool
Ampoule /Solution Gross~

.. .. . .. . We~ght, Grams
Empty Ampoule..... ... We1ght, Grams
Solution Net
Weight, Grams
1.0010 1J.CI
Dilute
to a volume ofl 1000.00 ... !milliliters
Certified Total Activity otj. 1;0010htCI
Which Eauals
. 2.222E+06jdpm at the date listed above
And after dilution the activity of this solution is 2.222E+03jdpm/ml
This activity concentration i$ based on the original

Expiration Date:! November 9, 2013
Verified & Approved
QC
By_!??=:_~~-.
--t--~..,..-~--i~--
Approval_-;~~~~~w-=-l~
____
\j..;._ _
Date;
Date:
___
11/9/2012
___;..;.;..;;.;.,;;.;__;.;;..
rr
[,z,_hz.
-----11---+,---
46
Rev.B; 11/01/03
Trlle: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES - OAK RIDGE LABORATORY

Dater .1.119/2012 o:OOI
Solution #I?J;;;.{',:,<;?RI!f:5b'}'~):>''i{.l
Hatf Life, Days
MP009
Solution Reference# IPG45~26)i.:;::.,;:; : ,; . . :>;iJ
Hatf Life, Years
:2l1~Raaium~
;':31ceooE":f:Oal
'
5:844e+osl
Radionuclide of Interest ? ~R~di(irrF":

Parent Solution Conc.['\'i2t~E03;i dpm/ml
Dilution Solve.nt Used

Vol. Parent Solution: />!: <:2o:oooo ml
Total Activity: : 4.4440E+04 dpm
Final Volume: :: <i1000~00 ml
NOTES:
Final Activity Concentration:! . . ..: 4.4440E+01!dpm/ml

Expiration Date: November 9, 20131
Verified & Approved
B~-~
QC Approval
~~JJ.A 1 I ~
-
Date:
11/9/2012 0:00
Date:
''
/rz.JI 1Z..
RA-\\
ANALYTICS
1380 Seaboard Industrial Blvd.

Atlanta, Georgia 30318 U.S.A.
Phone (404) 352-8677
Fax (404) 352-2837
Standard Radionuclide Source
62680-416
Ra-228 5 mL Liquid in Flame Sealed Vial
This
standard
radionuclide
source
was
prepared
gravimetrically from a calibrated master solution.
The
master solution was calibrated using a germanium gamma
spectrometer system.
Radionuclide purity and calibration were checked using a
germanium gamma spectrometer system. The nuclear decay rate
and assay date for this source are given below.
ANALYTICS maintains traceability to the National Institute
of Standards and Technology through Measurements Assurance
Programs as described in USNRC Reg. Guide 4.,15, Revision 1.
ISOTOPE:
Ra-228
ACTIVITY (dps) :
2.585 E3
HALF-LIFE:
5.75 years
CALIBRATION DATE:
November 7, 2001 12:00 EST
TOTAL UNCERTAINTY*:
4.0%
SYSTEMATIC:
3.0%
RANDOM:
1. 0%
*99% Confidence Level
Impurities: y-impurities (other than decay products) <0.1%
5.07198 grams 0.1M HCl solution with 50 ~g/g Ba carrier.
P 0 NUMBER
9508, Item 1 (Part #4339A)
SOURCE PREPARED BY:
Q A APPROVED:

MP.009
Rev.8; 1/10/03
TiUe: Radioactive Reference Standards Solutions & Records

RECERTIFICATION
MP009
Half Life, Days
Hatf Life, Years
1~ .i'tt:5:t:so~t+oal
j:................ 2?100E+o31
Reference Datei;;;,;:Jd'i/7ti1'i.olool
Ampoule /Solution Gross '\:h:2~:49e2

Empty Ampoule '5,>;:4:489$
Solution Netr' :'5.0087
Total Activity in Ampoule[ :\ .0.0699
Weight, Grams
Weight, Grams
Weight, Grams
J.l.Ci
Certified Total Activity oft< .. 0.0699lJ.l.Ci
Which Equals
,.. . :t;s5tEt05ldpm at the date listed above
And after dilution the activity of this solution isi1~551E+.02 Idpmlml

Expiration Date: I .'. March 26, 2014
Date:
5/30/13
SECTION VI
QUALITY CONTROL SAMPLE RESULTS SUMMARY
Eberline Services
Analysis Control Chart
Printed: S/S/20131:15 PM
Page 1 of 2
Analysis
WO
Run
Activity Units
Aliquot Units
Client Name
pCi
-----~~--------~-
UUISO
13-07147
Laboratory Control Sample

Normalized
Difference
Analyte
U-234
LCS
Measured
1.32
112.34%
16.23%
---~---
U-23S
2.05
CSU
Measured
II
I
1
LCS
Expected
I
I
Uncert.
Expected
100.00%
3.60%
Known
Error
Result
csu
Standard
1
S.09E+OO
2.91E-01
I 9.09E+OO
Standard
ACT(dpm)
ID
i
I 3.60E+OO
1.4SE+OO I
U-Sa
I 3.52E+01
U-Sa
Standard
Added (g)
Standard
Error
5.10E-01
--
16.10%
Known
------~
120.39%
I 100.00%
3.60%
I 7.S9E+OO I 2.S4E-01
9.50E+OO i 1.53E+OO
3.44E+01
I 3.60E+OO i 5.10E-01
Matrix Spike
Normalized
Analyte
MSActual
%Rec
Difference
Expected
MSResult
Expected
MS Uncert
Actual
MSResult
Sample
Result
Sample
Sample
Aliquot
csu
Replicate Sample
Normalized
Analyte
Original
Result
RPD
Difference
U-234
0.56
13.S5
5.S4E-01
"----~--------
U-23S
1.60
54.29
---
U-235
li<ll:!ll
~t~
U1
.....
Version
1.44
54.91
I
1
4.00E-01
Original
Ii
csu
I 2.0SE-01
~-~-~;;~0-1
!
3.7SE-01
Standard
ACT(dpm)
Standard
Standard
Added{g)
Error%
QCSummary
I
Standard
ID
Replicate
Replicate
Result
csu
LCS Relative
Bias
6.71E-01
2.22E-01
1.12
LCS%R
OK
------
2.29E-01
1.23E-01
~~~~-01 -r~.~5E-01
I 1.31E-01
OK
1.20
I
I
OK
I
I
LCSND
MS%R
MSND
1-::-+--+----
i
OK
RepRPD
RepND
OK
OK
INV
OK
NA
OK
Printed: 8/8/20131:15 PM
Page 2 of 2
Eberline Services
WO
____ --~n_alysis __
Run
UUISO
13-07147
Acti'!i_!Ll!_nit_s____ ~---
pCi
Replicate Sample RPD
LCS % Recovery
130.00
---------~
120.00
110.00
40.00
35 00
30 00
100.00
25.00
20.00
90.00
15.00
80 00
10 00
7o.oo
U-234
U-238
100.70
5 00
0.00
+-------------,-----------------,---------------,
140.09
120.39
U-234
U-238
U-235
16.23
66.87
69.28
80
11.47
13.85
41.70
54.29
35
54.91
35
100
Client Name
Aliquot Units
35
-UCL
Normalized Difference
3.50 . - - - - -
--------
3.00 ~-------
-~-~-~~~~--~~~
2.50 + - - - - - - - - - - - - - - - - - - - - -
!L.l1'11
f'I,J
Version
No Matrix Spike
40.55
Printed: 8/13/20131.2:56 PM
Page 1 of 2
Eberline Services
wo
_____ Analysis___ _______
. --.
Activity Units
UUISO
13-07147
~quot_U_flit~ - - - - - - - - -
_ _ _ _ _ ____cC--_1--,ie:::nt Name_________________
pCi

Analyte
U-234
csu
Nonnalized
Difference
Measured
------+---~~__j_--~=-66%
-----r~" i
U-238
10770%
1-15.76%
LCS
Expected
Uncert.
Expected
1oo.oo%
3.60%
i ~I
3.60%
Known
Error
Known
i
1
csu
Result
s.20E+oo
2.95E-o~J
7.99E+OO
2.88E-01
7.03E+oo
Standard
10
Standard
Error
Standard
ACT(dpm)
I 3.52E+01
U-Sa
~-~~11_E_+_oo--+-----tI
~61E+OO 132E~O
'
U-Sa
I 3.44E+01
3.60E+OO
Standard
Added (g)
5.17E-01
3.60E+O~ 7E-01
---
----
Matrix Spike
Analyte
Normalized
Difference
MS Actual
%Rec
Expected
MS Uncert
Expected
MSResult
Actual
MSResult
Sample
Result
Actual
MSCSU
Sample
Sample
Aliquot
csu
Standard
ID
Standard
ACT(dpm)
Standard
Error%
Standard
Added(g)
RepRPD
Rep NO
----T
I
QCSummary
Replicate Sample
Analyte
Normalized
Difference
RPD
Original
Result
i
i
Original
csu
Replicate
Result
Replicate
LCS Relative
Bias
csu
LCS%R
LCSND
MS%R
MSND
U-234
0.28
U-238
1.59
0.38
U-235
~i~JI
~~~
Ul
t.~ll
Version
6.87E-01
5.94E-01 II 6.85E-01
6.84E-01
-1.73E-01 I 3.62E-01
7.23E-01-t 9.84E-01
~-~~-;~~T 7.33E-01
26.23
4.56E-01
'
445.66
4.54E-01
38.98
----::-l-
+
I
0.86
OK
OK
NA
OK
1.08
OK
OK
NA
OK
OK
OK
NA
OK
Eberline Services
Printed: 8/13/2013 12:56 PM
Page 2 of 2
wo
Analysis
13-07147
UUISO
+--- _Run___----4-- _
Activi!}'_ Units
pCi
-1---------'A"'Iiquot Units
---
Client
Name
-------------
LCS % Recovery
130.00
120.00
110.00
100 00
90 00
80.00
7000}---------~---------,-------------------,
U-234
U-238
88.80
126.60
U-238
1273.48
-382.15
445.66
-10~-
--------
3.50,-
3.00
2.50
t'~~
ll<ll:~
u~
.11':...
Version
+-
+-------
--
-----
--------- -------
No Matrix Spike
U-235
66.62
11.34
38.98
--~
Eberline Services
Printed: 8/12/2013 8:47AM
Page 1 of 2
wo
__________fllnalysis
ThiSO
13-07147
Run
Activity Unit~--
pCi
--------~C~IientName
Aliquot Units

I
Nonnalized
Difference
Ana lyle
TH-228
TH-230
-
_ _____
TH-232
LCS
csu
LCS
Measured
Measured
Expected
93.51%
18.37%
.,.71%
1100.65%
--~-73 I
-1
~89
0.::
'
-~~8~E+OO
4.58E+OO
8.41E..1
I 1.76E-0_1--+-------t----
100.00%
3.60%
19.79%
100.00%
2.70% +'.46E+oo_J1.47E_,1
17.82%
100.00%
3.60%
Standard
csu
I 4.89E+OO
Th-8b
11.04E+02
9-:~~~1-r-~~~1-b-- - 2.35E+01
S.OOE+OO
4.93E+OO i 8.78E-01
1.76E-01
Th-8b
1.04E+02
Standard
Added (g)
Standard
Error
Standard
ACT(dpm)
ID
3.60E+OO
2.70E+OO
1.05E-01
I 3.60E+OO
1.05E-01
Matrix Spike
Normalized
Difference
Analyte
MSActual
Expected
MSResutt
%Rec
Expected
MS Uncert
Actual
MSCSU
Actual
MSResult
Replicate Sample
Normalized
Difference
Analyte
RPD
Original
Result
TH-228
TH-230
TH-232
Q;'
U11
t.II'JI
II
Original
Replicate
csu
0.19
22.00
1.05E-01
Version
Replicate
Result
Standard
Added(g)
Standard
ID
QCSummary
csu
LCS Relative
Bias
1.85E-01
0.94
I
I
LCS%R
LCSND
MS%R
MSND
RepRPD
RepND
I 1.02E-01
8.45E-02
OK
OK
NA
OK
o~K
INV
OK
OK
NA
OK
-+------
1.16
43.36
5.35E-01
2.37E-01
8.32E-01
-----
!tilt~
II
I
I
I
I
Sample
Aliquot
0.60
57.98
1.16E-01
9.88E-02
6.39E~~2
I
I
4.41E-01
0.92
~-~--
I 1.38E-01
1.01
__
OK
Eberline Services
Printed: 8/12/2013 8:47AM
Page 2 of 2
wo
!'-_rl~ly~is_ _ _ ~
ThiSO
13-07147
---+--1
Run_~--
Activity Units
pCi
Aliquot Units
-~--~--~----------------
Client Name
_____
_____
"
LCS % Recovery
130.00
--------------i
40.00
120 00
-------------
... ucL
35.00
110 00
30 DO
100 00
25.00
20 00
90.00
15.00
80.00
-----
LCL
10.00
70.00 +---------------.-------4------~-----------~
TH-228
TH-230
TH-232
71.54
69~22
79.22
~~5~9
1--
-~:14 ;~
5.00
ooot-------------,--------------.------------~
122~07
TH-228
100.65
100
120
RPD
-CL
TH-230
96~ 19
32~61
43.36
19.76
-----sr9s-
-----
35
35
3.50 -.--------- ~
3.00
~a'
!l:lliJI
-------~
- - - -
2.50
2.00
+--
1.50
-r------
Version
-----
TH-232
54.11
No Matrix Spike
Eberline Services
Printed: 8/7/2013 9:57AM
Page 1 of 2
wo
Analysis
13-07147
Ra226
Aliquot lJili~-- _
_ _----~C!i~I)'LJ_nits
Client Name
--~---------
pCi

Analyte
RA-226
Normalized
Difference
LCS
csu
LCS
Measured
Measured
Expected
Uncert.
Expected
Known
Known
Error
Result
0.54
107.32%
24.59%
100.00%
4.60%
1.03E+01
4.73E-01
1.10E+01
Sample
Result
Sample
csu
Standard
Standard
ID
ACT(dpm)
Standard
Error
Standard
Added (g)
Ra-5b
4.41E+01
4.60E+OO
5.18E-01
Standard
Standard
ACT(dpm)
Matrix Spike
Analyte
Normalized
Difference
MS Actual
Expected
MSResult
%Rec
Expected
MSUncert
Actual
MSResult
Actual
MSCSU
Sample
Aliquot
csu
Replicate Sample
Analyte
RA-226
Normalized
Difference
1.22
Original
RPD
87.54
ID
Standard
Error%
Standard
Added(g)
RepRPD
RepND
NA
OK
QCSummary
Original
csu
Replicate
Result
Replicate
Result
2.95E-01
2.33E-01
1.15E-01
i 1.68E-01 I
csu
I
I
LCS%R
Bias
1.07
OK
LCS Relative
LCSND
MS%R
MSND
l
OK
-~r-
;j'JP
f~~
tJ111
-..J
Version
Printed: 8/7/2013 9:57AM
Page 2 of 2
Eberline Services
LCS % Recovery
130.00
-.v.uv
120 00
35.00
110 00
30.00
100 00
25.00
20.00
90 00
15.00
80.00
10.00
70.00
+-----------------------------------------,
Lower Error
_LJpeer Error
%R
RA-226
5.00
78.13
0.00
-----136-:51_____
---
----
RA-226
-------------------1
-UCL
Lower Error
130.44
Uooer Error
44.64
87.54
RPD
-CL
35
3.50 ,.
3.00
2.50
200
+---
1.50
+-
1.00
~~I
~~~'
Version
------------
No Matrix Spike
Printed: 8/14/2013 2:47PM
Page 1 of 2
Eberline Services
wo
Analysis
13-07147
Ra228
~ctillity_lJ_ni!S_____
Client Name
Aliquot Units
pCi

Normalized
Difference
Analyte
RA-228
0.59
t-
I
LCS
Expected
Measured
--~
Uncert.
Expected
8.81E+OO
~r-
----t
Standard
Added(g)
Known
100.00% ~
~+:25%
I
csu
LCS
Measured
iI
~
4.49E-01
8.18E+OO I 2.06E+OO I
Ra-11
3.77E+01
I 5.10E+OO I 5.18E-01
Matrix Spike
Analyte
Normalized
Difference
MSActual
%Rec
Expected
MSResult
Expected
MS Uncett
Actual
MSResutt
Actual
MSCSU
Sample
Result
Standard
ID
RA-228
U!
t;Cll
Version
Normalized
Difference
RPD
1.59
100.14
Original
Result
Standard
Error%
Standard
Added(g)
RepRPD
RepND
NA
OK
QCSummary
Replicate Sample
Analyte
Standard
ACT(dpm)
Original
csu
1.13E+OO I 7.18E-01
LCS Relative
Replicate
Result
Replicate
csu
Bias
3.76E-01
5.89E-01
0.93
LCS%R
LCSND
OK
OK
MSND
Eberline Services
Printed: 8/14/2013 2:47PM
Page 2 of 2
---~n<llysi~---
WO
Ra228
13-07147
Run
Activity Units
pCi
Aliquot_l,J!!i!~----------f--~-----
Client Name
I Engineering Management Support, Inc.
LCS % Recovery
130.00
40.00
120.00
35.00
110.00
30.00
100.00
25.00
20.00
90.00
15.00
80.00
10.00
RA-228
7o.oo
~~Errorj
-
Uooer Error
%R
5.00
-----i-6~2~.5~2~--------------------------------- ~~
t--=--l2'A'.er Error
UpperError
RPD
-CL
-LCL
-----Mean
-------
0.00
-UCL
-------
--------
RA-228
143.53
56.75
100.14
35
No Matrix Spike
3.50 .----------------------------
3.00+------
--
2.50 +-----------------------------
2.00 t------------------------ --------
1.50
1.00
w
Q~l
m
Gl!:!li
Version
+----~~~~-
-----
--------
SECTION VII
LABORATORY TECHNICIAN'S NOTES
ISOUNOTES
Run 1
SSS2
Printed: 8/2/2013 8:39AM
Page 1 of 1
~
1;;.13 J;;J~ L ~~ E
~
SERVICES
Work Order Analysis Notes
Date
Dept
08/02/13 08:39
PREP
User
JWOLFE

601 Scarboro Rd.
Oak Ridge, TN 37830
Voice: 865.481.0683
www.eberlineservices.com
Internal Work Order
Analysis Code
Run Number
13-07147
UUISO
1
Notes
ALIQUOTED AND ADDED SPIKES AND TRACERS- PRESERVED FRACTIONS 4-7, 10-15 AND 18 AND 19
WITH HN03 AND DRIED SAMPLES DOWN
Printed: 8/7/2013 6:08PM
Page 1 of 1
~E'"'ERbiNE

601 Scarboro Rd.
Oak Ridge, TN 37830
Voice: 865.481.0683
SERVICES
Internal Work Order
Analysis Code
Dept
User
08/02/13 08:39
PREP
JWOLFE
08/07/13 18:08
CHEM
JDEMELAS
Date
13-07147
UUISO
Notes
Added concentrated HCI to sample beakers and heated to dryness; Added 20 ml 8N HCL to samples and
transferred to new, labeled C-Tubes, rinsing with 8N HCI to bring volume to -35 ml; Preconditioned resin
columns with 35 ml 8N HCI; Centrifuged samples and loaded onto columns; Rinsed C-Tubes with 20 mi8N
HCI, centrifuged as needed and loaded onto columns; Rinsed columns with 35 ml 8N HCI- 0.1 N NH41, 35 ml
of 6.5N HCI- 0.04N HF, and 10 ml of 6.5N HCI; Eluted Uranium with 50 ml of O.SN HCI into clean, labeled 100
ml beakers; Dried-down samples on hotplate; Dissolved samples in -10 ml of concentrated HCI; Transferred to
new, labeled C-Tubes with Dl H20. Set samples aside for later precipitation and filtering.
Printed: 8/8/2013 6:04AM
Page 1 of 1
~~
I::II:::RL,..I Nl:::
~

601 Scarboro Rd.
Oak Ridge, TN 37830
Voice: 865.481.0683
SERVICES
Date
08/02/13 08:39
08/07113 18:08
Dept
PREP
CHEM
, ... ._.
.-~--~
08/08/13 06:04+-CHEM
Analysis Code
UUISO
1
~~~~~-~--~--.-r-~-~~----
Run Number
~~~~~~-~-~~
Notes
User
JWOLFE
andheatedio-dryness:Added26mi.8i'JHcCI"osamPies"a"r1(r
"""""""~
JDEMELAS
I
I
II
13-07147
Added concentrated HCI to sample beakers

columns with 35 ml 8N HCI; Centrifuged samples and loaded onto columns; Rinsed C-Tubes with 20 m18N
HCI, centrifuged as needed and loaded onto columns; Rinsed columns with 35 ml 8N HCI - 0.1 N NH41, 35 ml
of 6.5N HCI- 0.04N HF, and 10 ml of 6.5N HCI; Eluted Uranium with 50 ml of 0.5N HCI into clean, labeled 100
-;-;-:-;::::;:::::---~---i'll~n e::-w;::-,;::la:::--beled C-Tubes with Dl H20. Set samples aside for later precipitation and filtering.
RMARTZ
ADDED 0.1 ML NEODYMIUM CARRIER, 0.3 ML TITANOUS CHLORIDE, & 1 ML HF TO c:Tl.JBES; LET SET
SIT IN ICE BATH FOR ONE HOUR. SET UP FILTERS BY ADDING ALCOHOL & CARBON SUBSTRATE
THEN ADDED SAMPLES; WHEN SAMPLES WERE THROUGH FILTERS, ADDED 10 ML Dl H20 RINSES
FROM C-TUBES, REMOVED FILTERS, LET DRY IN DESSICATOR, THEN SENT SET TO COUNT ROOM.
Printed: 8/8/2013 6:07AM
Page 1 of 1
Eberline Analytical
Internal Work Order
13-07147
e::.a~.R .SERVICES
L-1~~
Analysis Code
Reagents Used in an Analysis
UUISO
Reagent
ID
Reagent
Name
~~~.~~~~~-~~~
014142D01
..
1
Analyst
ID
Reagent
Concentration
Nitric Acid
f~-~~-
Run
OLFE
Reagent Grade
Anion Exchange Resin
Reagent Grade
Hydrochloric Acid
O.SN
JDEMELAS
6.5N
JDEMELAS
~--~~--+-
0141995
Hydrochloric Acid
0142255
Hydrochloric Acid
JDEMELAS
,,,,,,,............... .....
~
JDEMELAS
~~--
--~~
__
............
6.5N- 0.04N
,,,.~{
Solution .........................
,.,_,~~
Reagent Grade
0131915
1 mg/ml
013574P
Reagent Grade
f..., -~~~-----+~---~---~---""""'"'"'''""'"' ...........~.-..,.,.__,,,,+~~--..-~----
I 014220P
Grade
L:.::..............-~~~~~~~~~~-~-~-~-~~-~---~--------"'
.......................
~~~~+~
JDEMELAS
Date
Recorded
TZ
10
-~~ ~--- ------~___?aY~:~t_t'f, ) ____ \_,t_~--~-
_.i_l~n_-~__l'?S>}-_\~Jf_(~\ - - . . -~~~ _ q \_').!.?___ J '2 C)31~~ f!_(t -:x) __ ~\:> N ~.-
--~l~.t''?-~ _\_'}_~~\'-\\.(_~_~\~})
-;
-~_!Vl.?.
.... 1:~
~"
\'1~~-
-'
_.
--~-------------1----~-~+--------~----
-----------------------
---------------~-
----------------.L.-----~--11----- .. -------~---
--------------------
-----------~-f----------- --~-----1---
-----~------------~---------r-------------------
------------------~
- - - - - - - - - - - - - - 1 . - - - - f----.. --~-~------------1--- _______________,_.______ -----
_, __._ __________._,___,__.
--------------- -----------------:- - -
----------1--~-----1-----
---------------------!-------~------ ---~--
----------~---1------1------------~---------~- ----------------11--~--r---._ ___._ __,._ _ _ _ _
--------
----~-------1-------1---------------------
-----------------..----
----------------------l----~-1--------- -.-----------.-~--
------~ -----~--
---
- - -
------
----..------------ - - - - - - - - - - - - - - - -
.--- ----~-----------l-------+------~--------- - - - - - - - - - - - - -1---------~ - - - - - - - - 1 - - - - - - - - - - - - 1 - - - - -

--------------~-----1-----~-
------.--------- ------- ---- -----------r------------1--------- f------
1--------
--------------'----1--------'l-----------------
- - - - - - - - - - - - - ------~--1----
----------- ------------t------.. ----,11------------------- -------------------------- ---- _______..____
-----------1---------
1--~
~----------_____:_"-----lt---------'1---------------- - - - - - - - - - - - - ! - - - - - - - - - - - ---------------1~--~----J-~~---
-----t--------!1---------------------- ------------------ (---------- - - - - - - - - - - 1 - - - - -
-------------------~--~-__
----r---- ____:___________,--------- ..._..__________,____ --- ----------- -------------- -----~ -----
- - - - - - -----1------'~--------~-----
-------~--~-- ------~
-.------------ - - - - - - - - - - -
- - - - - - - - - - - - - - - - - - - t - - - - - . J - - - - - - - - - - - - - - - - - --------------------..- -..- - - - - - - - - - - - ----~----1--------
---------.-----t----------, ---------------..-.------ ---------------- - - - - - - ----..---------- - - - - - - - --

- - - - ----~--t----------- 1--------------------- .____._._________________ ------------- - - - - - - - - 1 - - - -
- - - - - - - - - - ' - ' - - - - - - - - - - - - - 1 - - - - - - - - - ---------- ------------------ .. - - ---------------- - - - - -..- - - - 1 - - - - - - - - - 1 - - -
- - - _____ ,___,. - - - - ' - - - - - - t - - - - - - - - - 1 - - - - - - - - - - - - ------1-------------------- -------------- _.___ ~---- - - - - - - - - - - - -
ISOUNOTES
Run2
Printed: 8/12/2013 5:28PM
Page 1 of 1
~
1:;: 13 E::.. .R L . J.. N~E;
~
SERVICES

601 Scarboro Rd.
Oak Ridge, TN 37830
Voice: 865.481.0683
Internal Work Order
Analysis Code
Run Number
13-07147
UUISO
2
Date
Dept
08/09/13 07:22
PREP
JWOLFE
ALIQUOTED AND ADDED SPIKES AND TRACERS- PRESERVED FRACTIONS WITH HN03 AND DRIED
SAMPLES DOWN
08/12/13 17:28
CHEM
JDEMELAS
columns with 35 ml 8N HCI; Centrifuged samples and loaded onto columns; Rinsed C-Tubes with 20 ml 8N
User
Notes
Printed: 8/13/2013 6:31AM
Page 1 of 1
<ES!;:RL..INE;
SERVICES
Date
Dept
08/09/13 07:22
PREP
o8t1211'31T28- ~HEr;r-
User
JWOLFE
JDEMELAS
08/13/13 06:30
CHEM
601 Scarboro Rd.

Oak Ridge, TN 37830
Voice: 865.481.0683
Internal Work Order
RMARTZ
13-07147
.....
Analysis Code
!~-
Run Number
UUISO
2
Notes
ALl QUOTED AND ADDED SPIKES AND TRACERS- PRESERVED FRACTIONS WITH HN03 AND DRIED
SAMPLES DOWN
..------------------..--.........
.._______.....
columns with 35 mi8N HCI; Centrifuged samples and loaded onto columns; Rinsed C-Tubes with 20 m18N
---~---- --~----------~--------~----~--
____
"~--~-
ADDED 0.1 ML NEODYMIUM CARRIER, 0.3 ML TITANOUS CHLORIDE, & 1 ML HF TO C-TUBES; LET SET
SIT IN ICE BATH FOR ONE HOUR SET UP FILTERS BY ADDING ALCOHOL & CARBON SUBSTRATE
THEN ADDED SAMPLES; WHEN SAMPLES WERE THROUGH FILTERS, ADDED 10 ML Dl H20 RINSES
FROM C-TUBES, REMOVED FILTERS, LET DRY IN DESSICATOR, THEN SENT SET TO COUNT ROOM.
Eberline Analytical
Printed: 8/13/2013 6:32AM
Page 1 of 1
Internal Work Order
13-07147
Analysis Code
UUISO

Reagent
ID
Reagent
Name
Reagent
Concentration
Analyst
ID
014109P
Nitric Acid
JWOLFE
8/9/2013
014164P
JDEMELA5
8/12/2013 I
JDEMELA5
8/12/2013
t-~~~--l~-~
HCI - HF
6.5N - 0.04N
Ir"~" 014142001
Hydrochloric Acid
JDEMELA5
" . . . "-~"~~-~~~~~---~~~---~~--~~~~---~----~"~---~--. . "~~~~-+---~--,..---~~-~~+~-,.---1
1
0141995
0142375
Hydrochloric Acid
014142P
Hydrochloric Acid
0142485
HCI - NH41
+-
Hydrochloric Acid
JDEMELA5
......~-"}-~-
Reagent Grade
Hydrofluoric Acid
....~....
--~----
! Neodymium Carrier
~---~~~----~!-~~~~~~~~----+
Reagent Alcohol
itanous Chloride
agent Grade
agent Grade
27
--------- ------------
~+-------
-~---------------~----
---~~~----------
-------~
---
-~-
-~--~~~~~--
---~------1--------
"----------~--~-------f------~-
--------
----~-------- ---'---------,-----------1----~-
-------~~--
-----
----l-------~---
--
------~---~------------~-~-~
-------------- __________,__--------!
~~---------
---------------
-----
---------
~-
--~~-----------
---
--------------~~- --------~----
________________
-------
-,
-----------1---
----------------------------- -------
--------- -
------~----~
------~--
-------~
-- -------------
-----------~-~
--~---
----------
--------------- - - - -
ISOTHNOTES
Printed: 8/2/2013 8:38AM
Page 1 of 1
~
E B E;~R.~J ~ E;
~
SERVICES
# 1
Date
Dept
08/02/13 08:38
PREP
User
JWOLFE

601 Scarboro Rd.
Oak Ridge, TN 37830
Voice: 865.481.0683
Internal Work Order
Analysis Code
Run Number
13-07147
ThiSO
1
Notes
Printed: 8/8/2013 6:36PM
Page 1 of 1
~ E13E;:Rl_IN !==
SERVICES

601 Scarboro Rd.
Oak Ridge, TN 37830
Voice: 865.481.0683
Analysis Code
Run Number
13-07147
ThiSO
1
Date
Dept
08/02/13 08:38
PREP
JWOLFE
08/08/13 18:36
CHEM
JDEMELAS
Added concentrated HN03 to sample beakers and heated to dryness; Added 20 ml 8N HN03 to samples and
transferred to new, labeled C-Tubes, adding 8N HN03 to bring volume to -35 ml; Preconditioned resin
columns with 50 ml 8N HN03; Centrifuged samples as needed, and passed through columns; Rinsed C-Tubes
with 20 ml 8N HN03; Centrifuged rinsates and loaded onto columns; Rinsed columns with 40 ml 8N HN03;
Eluted Thorium with 50 ml of 8N HCI into clean, labeled 100-ml beakers; Dried-down samples on hotplate;
Dissolved samples in -10 ml of concentrated HCI; Transferred to new, labeled C-Tubes with deiononized
water brinaina volume to -15ml. Set samoles aside for later orecioitation and filterina.
User
Notes
fllfl76
Printed: 8/9/2013 6:54AM
Page 1 of 1
~
#
-=:::. e
r::::: F.!. I.- .,....... .;;;:
601 Scarboro Rd.

Oak Ridge, TN 37830
Voice: 865.481.0683
SERVICES
Date
08/02/13 08:38
""2" .
08/08/13 18:36
Dept
PREP
User
JWOLFE
13-07147
ThiSO
In
A
r-m-~
Run Number
Notes
Adcie<i.conceillr"aieci"HNo3 iosami)iebeakersand heatecfto dfiness; Addeci"2'on1i 8N iiNo3 io5arrii)le5"ai1d

transferred to new, labeled C-Tubes, adding 8N HN03 to bring volume to -35 ml; Preconditioned resin
columns with 50 ml BN HN03; Centrifuged samples as needed, and passed through columns; Rinsed C-Tubes
with 20 ml 8N HN03; Centrifuged rinsates and loaded onto columns; Rinsed columns with 40 ml 8N HN03;
Eluted Thorium with 50 ml of 8N HCI into clean, labeled 100-ml beakers; Dried-down samples on hotplate;
Dissolved samples in -10 ml of concentrated HCI; Transferred to new, labeled C-Tubes with deiononized
ll---::-!--;,==~~-:--r~=-:--+--:::::::":':':=~-~4~w~a~te~r,~b~ri~n~gii~ng~vo~~lu~m~e~to~~-:...!1_':'5;ml. Set samples aside for later precipitation and filtering.
3
08/09/13 06:54
CHEM
RMARTZ
ADDED 0.75 ML 0.1 MG/ML CERIUM CARRIER & 1 ML HF TO C-TUBES & LET SET SIT IN ICE BATH FOR
ONE HOUR; SET UP FILTERS BY ADDING ALCOHOL & CARBON SUBSTRATE THEN ADDED SAMPLES;
WHEN SAMPLES WERE THROUGH FILTERS, ADDED 10 ML Dl H20 RINSES FROM C-TUBES,
REMOVED FILTERS LET DRY IN DESSICATOR THEN SENT SET TO COUNT ROOM.
CHEM
JDEMELAs
Eberline Analytical
Printed: 8/9/2013 6:54AM
Page 1 of 1
Internal VVorkOrder
13-07147
Reagent
ID
Reagent
Name
Analysis Code
Run
ThiSO
Reagent
Concentration
Analyst
ID
Reagent Grade
"~~-
~.~~~.mm~~
Hydrochloric Acid
8/8/2013
i 8/8/2013
8/8/2013
8/8/2013
Nitric Acid
Carbon substrate
Solution
Cerrium Carrier
0.1mg/ml
~~--,~~~~
013221P
Hydrofluoric Acid
Reagent Grade
013574P
Reagent Alcohol
Reagent Grade
8/9/2013
49
---------------r--- ----------i!l------------------------1---------------- -------

--------------jr------------l----------~----------1------------~----- ---~--- ------
-----J------------------------------1
------------- --r---------------11------------
--------1-
-----------1------~- ------ - -----1--
------ -------1--------- ------------------------------
------------~------1----~--~--+-
----ii
~1-----------
------~. ___________,_____ ~-----t-----------------1----------------------+----------l-----------l----------+-----'"
."'
103)
i
_,...._
RA-226 NOTES
Printed: 7/31/2013 12:33 PM
Page 1 of 1
jfJ E;e~;;~Ra,.,l N~E

~
SERVICES
#
1
Date
Dept
07/31/13 12:33
PREP
User
JWOLFE

601 Scarboro Rd.
Oak Ridge, TN 37830
Voice: 865.481.0683
Internal Work Order

Analysis Code
Run Number
13-07147
Ra226
1
Notes
ALIQUOTED AND ADDED SPIKES AND TRACERS- PH'D SAMPLES- PRECIPITATED WITH BA AND PB
CARRIERS AND AMMONIUM SULFATE- DECANTED SAMPLES AND CENTRIFUGED- SUBMITIED
RADIUM PRECIP TO SEPARATIONS
~~~
'-::/-(3/ w
Printed: 8/5/2013 3:41PM
Page 1 of 1
~
E; B r:;:_RJ,~J ,.._.. E
~
SERVICES
Date
Dept
07/31/13 12:33
PREP
08/02/13 12:57
PREP- :-- LWALKER
08/05/13 15:41
PREP
1
-
2
3
User
JWOLFE
LWALKER

601 Scarboro Rd.
Oak Ridge, TN 37830
Voice: 865.481.0683
Internal Work Order
Analysis Code
Run Number
13-07147
Ra226
1
Notes
ALIQUOTED AND ADDED SPIKE S AND TRACERS- PH'D SAMPLES- PRECIPITATED WITH BA AND PB
CARRIERS AND AMMONIUM SULFATE- DECANTED SAMPLES AND CENTRIFUGED- SUBMITTED
ADDED EDTA TO PRECIP-VORTEX-LET SIT OVERNIGHT TO DIGEST.
FOLLOWED STEPS 12.1 TO 12.81N AP-006 REV 12 FOR RA 226 ANALYSIS-(SYRINGE FILTERED
PRECIP-FIL TERED-DRIED-OBTAIN FINAL WEIGHT)-SUBMIT TO COUNT ROOM.
Printed: 8/6/2013 2:33 PM
Page 1 of 1
Eberline Analytical
13-07147
1
Ra226

Reagent
'N'iiune
Grade
Ammonium Sulfate
014007002
Barium Carrier
1 mg/ml
014008002
Lead Carrier
166 mg/ml
014109P
Nitric Acid
Reagent Grade
JWOLFE
014212S
EOTA
0.25M
LWALKER
Acetic Acid
Reagent Grade
LWALKER
Ammonium Sulfate
200 mg/ml
11383P
013575005
8/5/2013
~ 'flf'dtJ
.
. -)_
v u.~
_____
.c~
=t-,-'-1~
-~-~~-'2_nY~~'(t_'f, 1- \..-t~~ __ _q_~crr
t--L.~ ~:ll._l\tr
._}--:El.L~lf'l___ L'}~f--\~t!.\:(\1\ . . \..A-~~
1~2~
1.-1\orb~- __ "::h- .--- ~~
-P\<>)2_ J:2~'L'\I'l y -1) >"\.\) "',_
!)._21 -- <--~,;., _""[1-- .. . ICCl >
-r-~)_~_t') ___\_')~'=!\'\~~(._\-'}) . 6 M;, _ l~~~ -- -~h~~-- --~ ____ J~ ___ :
-1-'--
-~~--~
- - -~-~----~---------------------- -- - -
-~l~()____ J.~t>:l~~n.Cr>:\4~ _ f::t)'\-)_ _

I l - (o
'i\~JJJ~ __ l~~=l~ ~Jl(~-\.- \:S} -~\t~-1 _J liJ ~
Cl_Ys:h~--- . \.~ o3.J}-IA- G~i 1 ~- _u.\Al(L -- __ J u \3..
'
~LkfJ7--~ ----D~~'--(2~( ________ -~

or'-- Y
~k/L2~-- ----~~?.JJ~-:?lUfl-lt1 __ ;(}15 ____ -~-PriX?
~~tt--'J-- --~ _____ l'Jo_'-f___f_2o.A_(_lf_) _ L!t..;k"'L,.,
~~ ~Et-~-~~~--- --~- ...t.']J21L'1Yt~u~ .. cr~,~-c"'t,._

~~~~~~-? _-~---!1.t?._rtJr.4lk _ __L!//~;'o~-7t
~tP/1'7-~- -~-~____LL_o_'2_1_A;;_4:JJ. - tl~-t, ~~....
~- -~J t')_~-- J~~J>3J"!~"!_L~.:t '-\)__ ___ &~-~

.
~J~\1~ __ J'3o-a:JY3J.~-:-1lJ_ __6 rYl ~ ___ _
~=~4--~LwJ_]___ ~-TJ~.~ly/tt ----cj~----- __()L_~y'_ ___ t_~---~------4$L{JJL')
_ L'? C2-:lL7tALIJ,
- ____ j___!l_" h~
j_) 0 7 _!_~ (f J+( ---=-~}_
___
____\..cL~--~ _(21_J~-- ----~t:'~ _ -~? --~=-----

___ __}{6-lldq- --l--'3~_\'_pt?_~Alt~tt) __h_LC:>~ ----0-C::Z-?--~--- _-=t-L -bt~_________ -tG/J.eit'").. _____/ "Jl2:J_L 1o.41l-J ~--U.t--.;~1- ____ -~")-!'_____ -~~-:k~r---4k~--=-_,
___ 4-Jl!tJL:l \'!Jo l~l_tl- (~-t \c)_______ \.A.L)_{L____ JJ--~:('_ _ l-~~-~ __A)-fL---1---'---'-1~
. --- -~~_2_____ {_?-~:!_~------- _;;. ~y So~-~---- "t'h.

Jro
_:_ ____~_ita_\tL l ~q1JJ-.].Ji{:r'1:t_ ----~U) ~----- J~3_'f-~---- ~~~ ___ ((.w~-- ') ____
____jt il~t1 JJ__a~L'-t1'8_u ~:t~- ---~-6_m~-------LlD0~---- __ h~-~~-- -~~---J~----:------,'---------t-----------------
~-----------~---------------------------
------
__________.___ ~----If-------~----~------
------~~----------
--
----------------------
---------- -- ---- --------
--~---------
---------------~---
~--------
-----
-~-
------~---------- --~-----~--+--
.. ------------------- ----------------
---~---
----------------
~-----~;---- ----~-------------------
------------------------------------- -- -----------------
-------~-
---
- - - - - - - - + - - - ----~-------------------
---~-------------------
-------->----~---1-----~-----~---------------- -~~---
-----
---------------~----
-------"----+----------------
---
-~-------------
----
-------------------------- -------------------- ----------------
---------------------------- ------------~- --------
------------;----------1-~-------
-----------'------+------------- ~---------~-- -------~---
RA-228 NOTES
Printed: 7/31/2013 12:33 PM
Page 1 of 1
)!JEBERLtN~
~
SERVICES
Date
Dept
07/31/13 12:33
PREP
User
JWOLFE

601 Scarboro Rd.
Oak Ridge, TN 37830
Voice: 865.481.0683
Internal Work Order
Analysis Code
Run Number
13-07147
Ra228
1
Notes
CARRIERS AND AMMONIUM SULFATE- DECANTED SAMPLES ANO CENTRIFUGED- SUBMITTED
~u:11.~
11
Printed: 8/9/2013 5:46PM
Page 1 of 1
~
EE;u;:R--..II'JE
~
SERVICES
Date
Dept
07/31/13 12:33
PREP
08/07/13 12:18
PREP
08/09/13 17:46
PREP
User
JWOLFE
LWALKER
LWALKER

601 Scarboro Rd.
Oak Ridge, TN 37830
Voice: 865.481.0683
Internal Wor1< Order
Analysis Code
Run Number
13-07147
Ra228
1
Notes
RECEIVED FILTERS BACK FROM COUNT ROOM-PUT BACK INTO C-TUBES-ADDED EDTA AND
SWIRLED-LET SIT OVERNIGHT TO DIGEST.
FOLLOWED STEPS 12.1 TO 12.7 IN AP-007 REV 18 (CHEMCAL CLEANUP FOR RA 228)
)~
Printed: 8/14/2013 9:05AM
}tJ E
~
Page 1 of 1
~.I::R.LI Nl::
SERVICES

601 Scarboro Rd.
Oak Ridge, TN 37830
Voice: 865.481.0683
Internal Work Order
Analysis Code
13-07147
Ra228
1
Date
Dept
07/31/13 12 33
PREP
JWOLFE
08/07/13 12:18
PREP
LWALKER
08/09/13 17:46
PREP
LWALKER
FOLLOWED STEPS 12.1 TO 12.71N AP-007 REV 18 (CHEMCAL CLEANUP FOR RA 228)
08/14/13 09:05
CHEM
TSMITH
Followed steps 12.7 to 12.15 in AP-007 rev. 17 . ( Precipitated samples, hot bathed, centrifuged, and
discarded supernate. Dissolved precip, precipitated samples, hot bathed, centrifgued, and discarded
supernate. Dissolved precip, precipitated and filtered samples, obtained final weights, covered with aluminum
foil and took to count room l
User
Notes
RECEIVED FILTERS BACK FROM COUNT ROOM-PUT BACK INTO C-TUBES-ADDED EDTAAND
SWIRLED-LET SIT OVERNIGHT TO DIGEST.
Eberline Analytical
Printed: 8/14/2013 10:16 AM
Page 1 of 1
Internal Work Order
13-07147
E:ee:: e~ ~-e::
SERVICES
Analysis Code
Run
Ra228
G.~,.JJ76P
Ammonium Hydroxide
Reagent Grade
JWOLFE
G.~,.JS30003
Ammonium Sulfate
200 mg/ml
JWOLFE
014007002
Barium Carrier
1 mg/ml
JWOLFE
7/31/2013
014008002
Lead Carrier
166 mg/ml
JWOLFE
17/31/2013
014109P
Nitric Acid
Reagent Grade
JWOLFE
7/31/2013
011504032
Ammonium Sulfide
2%
LWALKER
8/9/2013
014008003
Lead Carrier
1.5 mg/ml
LWALKER
8/9/2013
014109P
Nitric Acid
Reagent Grade
LWALKER
s;9;2o13
Sodium Hydroxide
10M
LWALKER
8/9/2013
014060S
Yttrium Carrier
9 mg/ml
LWALKER
013763002
Ammonium Oxalate
5%
Reagent
ID
013065006
Reagent
Name
10
'
7/31/2013
8/9/2013
TSMITH
IS/14/2013
ITH
8/14/2013
TSMITH
8/14/2013
Nitric Acid
6N
Sodium Hydroxide
10M
TSMITH
8/14/2013
18M
TSMITH
8/14/2013
Nitric Acid
014110004
013065010
Ani'ifySt
I
I
013910007
013065009
'Reagent
c:on~entratio n
Sodium Hydroxide
1N
-;-::;;
L(JL{t t o(L~
0~,~'
;.
'
,,;_,-,-";
---
L 0 "'l
-4nu
~:tt;
nPD_,<.':jf~.-
;;o?;;'f#/Jn-r\
~/1?11?
~~/I 'tit
t7v~tt7dA1
It l'i
1Jr''
I /"'1
..,
~(lft{t)
~ll'tt;1
~lllflt.J
if?ltvtt1 I~ 0'1-1'11 Slf t.. j ~\
~ h"l \I'!> 106i\ '4~ (LA ( <1-l&l
I1
tOOl...
nt'\..
eM~
u A tt}--~
Lh>
t1ttv
/'1 o?tvtfl.l <tJ -trJ ~/2-u- OtFr
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, t7 7 lifo 5Y{t. ..,,{,)
OK,("1
( .1 [J)rL
I"?, fY71-:tL.~ It {, '7 - (,/_,(~)
_.::__:::_-:__
/1.-I~""J
....
-~10::&<:._
't11~u-,
"
l b,:f\~Jt.A--
/!tc...r>,oM"'
..
-:L,.A,~ (;,(__OTt~
Q_2~
Blt3tn
\\.0\
"1-L-
"7.--l-
;;
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1.
A'.4.
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.:p ~L
c.__
c.
,/lA
,, .
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'--'
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(_~
Sflfp_(tL
....
~,.~
~f~y
~"'L...
<Jlfd(v
:).-~
-,
29
-- -
(_
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\c.,)
------
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1----------
.
1-----
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'
--~-.--
'o}. : >, ; . _ '
;.. ,':f'?r--;.;,c-;;
"'0
. 'i
...
----~---------
..
SECTION VIII
ANALYTICAL DATA (ISOTOPIC URANIUM)
RUNl
Eberline Services
Analysis Sheet
Printed: 8/8/2013 6:07AM

Page 1 of 3
13-07147
UUISO
Run 1
Work Order
13-07147
Internal
Fraction
Sample
Desc
UUISO
01
LCS
Client
ID
Login
CPM
Sample
Date
Sample
Aliquot
Analysis Code
Run
Date Received
LCS
07/23/13 00:00
1.ooooE+ooj
BLANK
07/23/13 00:00
1.0000E+OO'
---
02
7/22/2013
03
MBL
--
DUP
D-12
TOT
46
07/15/13 15:27
1.0000E+OO
D-12
TOT
46
07/15/13 15:27
1.0000E+OO
D-12 DIS
46
07/15/13 15:27
1.0000E+OO
lab Deadline
8/13/2013
Client I Engineering Management Support, Inc.
04
DO
05
TRG
---
Project I
West lake OU-1
06
TRG
TOT
45
07/15/13 00:00
1.0000E+OO
DUP05 DIS
45
07/15/13 00:00
1.0000E+OO
DUP05
--
Report level
07
TRG
---
Activity Units
08
TRG
PZ-208-SS
TOT
43
07/16/13 09:25
1.0000E+OO
09
TRG
PZ-208-SS DIS
43
07/16/13 09:25
1.0000E+OO
WA
10
TRG
TOT
46
07/16/13 12:05
1.0000E+OO
HASL 300, 4.5.2
11
TRG
46
07/16/13 12:05
1.0000E+OO
07/16/13 12:34
1.0000E+OO
41
07/16/13 12:34
1.0000E+OO
TOT
41
07/16/13 13:25
1.0000E+OO
MW-104 DIS
41
07/16/13 13:25
1.0000E+OO
pCi
Aliquot Units
Matrix
Method
PZ-304-AI
PZ-304-AI DIS
I
Instrument Type
Alpha Spectroscopy
12
TRG
PZ-304-AS
TOT
41
-----
Radiometric Tracer
U-232
13
TRG
Radiometric Sol#
U-10a
14
TRG
Tracer Act (dpm/g)
19.043
15
TRG
PZ-304-AS DIS
MW-104
----
Carrier
16
TRG
PZ-204A-SS
TOT
40
07/16/13 13:56
1.0000E+OO
Carrier Cone (mg/ml)
17
TRG
PZ-204A-SS DIS
40
07/16/13 13:56
1.0000E+OO
18
TRG
PZ-302-AI
TOT
44
07/16/13 15:18
1.0000E+OO
19
TRG
PZ-302-AI DIS
44
07/16/13 15:18
1.0000E+OO
i
Ci!~
Q,,
* SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only.
Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
Eberline Services
Analysis Sheet
Printed: 8/8/2013 6:07AM

Page 2 of 3
13-07147
UUISO
Run 1
Internal
Fraction
01
Sample I
Desc '
Tracer
Aliquot (g)
Tracer Total
ACT(dpm)
Radiometric
Tracer (pCi)
~ Radiometric
% Rec
0.9113
17.4
0.00
MBL
0.6093
11.6
0.00
DUP,
0.6069
11.6
LCS
Grav Carrier
Added(ml)
Grav Filter
Tare (g)
II
I
Grav Filter
Final(g)
Grav Filter
Net(g)
Grav
%Rec
I
I
Mean
%Rec
SAF
2*
02
SAF
1*
-------
03
0.00
I
--
04
DO
0.6056
11.5
0.00
05
TRG
0.6054
11.5
0.00
06
TRG
0.6067
11.6
0.00
07
TRG
0.6048
11.5
--~-
-
I
0.00
I
I
08
TRG
0.6031
11.5
09
TRG
0.6014
11.5
10
TRG
0.6035
11.5
0.00
11
TRG
0.6044
11.5
0.00
12
TRG
0.6020
11.5
0.00
13
TRG
0.6030
11.5
0.00
14
TRG
0.6018
11.5
0.00
15
TRG
0.6027
11.5
0.00
16
TRG
0.6018
11.5
0.00
17
TRG
0.6021
11.5
0.00
18
TRG
0.6007
11.4
0.00
19
TRG
0.6019 I
11.5
0.001
0.00
I
0.00
-
I
I
II
--
---
t.1rlli
;:~
....U~~
Actual mass exceeded the calibration curve range. Results should be qualified as appropriate .
Eberline Services
Analysis Sheet
Printed: 8/8/2013 6:07AM

Page 3 of3
13-07147
UUISO
Run 1
Internal
Fraction
Sample
Desc
Rough Prep
Date
RoughPrep
By
Prep
Date
Prep
Sep tO
Date/Time
By
Sep tO
By
01
LCS
08/02/13 08:15
JWOLFE
MBL
08/02/13 08:15
JWOLFE
03
DUP
08/02/13 08:15
JWOLFE
04
DO
JWOLFE
05
TRG
08/02/13 08:15
JWOLFE
06
TRG
08/02/13 08:15
JWOLFE
07
TRG
08/02/13 08:15
JWOLFE
~-
08/02/13 08:15
By
02
Sept1
Sept1
Date/Time
--~
I
..
--~----
-,
I
--
08
TRG
09
TRG
10
TRG
08/02/13 08:15
11
TRG
08/02/13 08:15
JWOLFE
12
TRG
08/02/13 08:15
JWOLFE
13
TRG
08/02/13 08:15
JWOLFE
14
TRG
08/02/13 08:15
JWOLFE
15
TRG
08/02/13 08:15
JWOLFE
16
TRG
08/02/13 08:15
JWOLFE
17
TRG
08/02/13 08:15
JWOLFE
18
TRG
I 08/02/13 08:15
JWOLFE
19
TRG
08/02/13 08:15
JWOLFE
08/02/13 08:15
JWOLFE
08/02/13 08:15
JWOLFE
1
JWOLFE
t
'i
!-------
I
!
I
I
~~
'";!li
**Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
Eberline Services
.~
~
.,
s::
C(
LCS
Flag
112.34
OK
MDA
Flag
RPD
Flag
Activity
Units
U-234
LCS
LCS
pCi/1
9.09E+OO
1.32E+OO
1.10E-01
02
U-234
MBL
BLANK
pCi/1
2.05E-01
1.11E-01
9.10E-02
03
U-234
DUP
D-12 TOT
pCI/1
6.71E-01
2.17E-01
1.15E-01
U-234
DO
D-12 TOT
pCI/1
5.84E-01
2.04E-01
6.80E-02
OK
05 i
06 I -
U-234
TRG
D-12 DIS
pCi/1
3.38E-01
1.86E-01
1.02E-01
OK
U-234
TRG
DUPOS TOT
pCi/1
6.65E-01
2.49E-01
1.00E-01
OK
07
U-234
TRG
DUPOS DIS
pCi/1
4.55E-01
1.80E-01
1.09E-01
OK
U-234
TRG
PZ-208-SS TOT
pCI/1
1.81E+OO
4.13E-01
1.09E-01
OK
09
U-234
TRG
PZ-208-SS DIS
pCi/1
1.58E+OO
3.76E-01
9.63E-02
OK
10
U-234
TRG
PZ-304-AI TOT
pCi/1
7.25E-01
3.63E-01
1.70E-01
OK
U-234
TRG
PZ-304-AI DIS
pCi/1
6.34E-01
3.45E-01
1.78E-01
OK
U-234
TRG
PZ-304-AS TOT
pCi/1
3.28E-02
2.13E-01
5.79E-01
OK
U-234
TRG
PZ-304-AS DIS
pCi/1
1.60E+OO
1.97E+OO
2.09E+OO
INV
U-234
TRG
MW-104 TOT
pCi/1
2.89E+OO
5.92E-01
1.20E-01
OK
U-234
TRG
MW-104 DIS
pCi/1
2.21E+OO
4.96E-01
1.02E-01
OK
U-234
TRG
PZ-204A-SS TOT
pCi/1
1.98E+OO
6.51E-01
2.05E-01
OK
Results
Error Estimate
MDA
8.09E+OO
0
en
::l
::l
OK
OK
OK
I
~----------- ----
04
---
r---
Blank
Flag
~---
--
LCS
%R
Client
Identification
01
.g
LCS
Known
Sample
Oesc
~~-
0::
Work Order: 13-07147-UUIS0-1
Nuclide
Lab
Fraction
Printed: 8/8/2013 1:15 PM
Page 1 of 3
Preliminary Data Report & Analytical Calculations
Ii
i
OK
OK
------
08
-
1 - - - - - ---
11
-j--
12
d
.E
~
0
Q.
Q.
::s
...s:::
CJ)
Cll
0.~I
13
-----~-
14
-
15
r------
17
1-----+----
Cll
Cll
Cll
s:::
;::
Cll
Cll
s:::
s:::
c;,
w
-----~----
18 I
j-----+ -
19 I
11..0
!JO
U-234
TRG
PZ-204A-SS DIS
pCI/1
2.41E+OO
6.17E-01
1.13E-01
OK
U-234
TRG
PZ-302-AI TOT
pCi/1
3.60E+OO
5.96E-01
6.66E-02
OK
TRG
PZ-302-AI DIS
pCi/1
5.18E+OO
1.25E+OO
2.27E-01
OK
----
U-234
r--------+-- ------
I
I
g~
16
Cll
s:::
-------
r--~-
Cll
:a:
l.li::!\1
--
--'------
L.__
L_
'
1::
::s
a::
.!!!
~
ii
1::
Sample
Date
01
U-234
LCS
07/23/13 00:00
1.00E+OO
72.66
0.00
0.00
02
U-234
MBL
07/23/13 00:00
1.00E+OO
99.04
0.00
0.00
U-234
CUP
07/15/13 15:27
1.00E+OO
88.83
0.00
0.00
1.00E+OO
79.47
0.00
0.00
"(
SAF
SeptO
Date/Time
Sept1
Daterrime
~---~-----
t----~-
-::::::
Mean
%Rec
Grav
%Rec
Sample
Desc
04
Radiometric
%Rec
Nuclide
03
en
Sample
Aliquot
Lab
Fraction
--
1-------- e---
.g
Printed: 8/8/20131:15 PM
Page 2 of 3
Eberline Services
U-234
DO
I--
05
07/15/13 15:27
--~--
U-234
TRG
07/15/13 15:27
1.00E+OO
54.56
0.00
0.00
U-234
TRG
07/15/13 00:00
1.00E+OO
67.67
0.00
0.00
U-234
TRG
07/15/13 00:00
1.00E+OO
90.44
0.00
0.00
U-234
TRG
07/16/13 09:25
1.00E+OO
103.51
0.00
0.00
07/16/13 09:25
1.00E+OO
84.14
0.00
0.00
07/16/13 12:05
1.00E+OO
35.19
0.00
0.00
07/16/13 12:05
1.00E+OO
34.02
0.00
0.00
07/16/13 12:34
1.00E+OO
13.55
0.00
0.00
--
06
f------~
07
c----~-
08
r----~--
---~-
09
10
r------
----
U-234
TRG
U-234
TRG
--
11
--~-~
U-234
TRG
U-234
TRG
r-------- 1--
12
f--------~
cJ
.5
~
0
c.
c.
:::1
en
....s:::
Q)
~I
E
Q)
Cl
CIS
s:::
CIS
::!
Cl
s:::
;:
Q)
Q)
s:::
a,
s:::
w
~~
.....
~
~:!ll
-----
-~--
13
U-234
TRG
07/16/13 12:34
1.00E+OO
3.53
0.00
0.00
U-234
TRG
07/16/13 13:25
1.00E+OO
70.94
0.00
0.00
U-234
TRG
07/16/13 13:25
1.00E+OO
71.86
0.00
0.00
16
U-234
TRG
07/16/13 13:56
1.00E+OO
35.51
0.00
0.00
17
U-234
TRG
07/16/13 13:56
1.00E+OO
54.80
0.00
0.00
18
U-234
TRG
07/16/13 15:18
1.00E+OO
104.63
0.00
0.00
19
U-234
TRG
07/16/13 15:18
1.00E+OO
41.84
0.00
0.00
- - - - f-
14
!----~--~
------
15
- - - - - -1--
f - - - - - - I-
I
I
Eberline Services
Lab
Fraction
---.
I
'
s::~ iI
ll:!
--+ -
03
Count
Time
Bkg
CPM
Counts
Eff
Detect
Carrier
08/08/13 09:06
A_Spec
Alpha_003
170 4.34 E+02
3.00 E-03
17.5
MBL
08/08/13 09:06
A_Spec
Alpha_004
170 1.48 E+01
7.00 E-03
19.4
08/08/13 09:06
A_Spec
Alpha_010
170 4.41 E+01
1.10 E-02
-------
U-234
DUP
19.7
04
U-234
08/08/13 09:06
DO
A_Spec
Alpha_011
1.00 E-03
170 3.58 E+01
20.5
r-
05
U-234
TRG
06
U-234
TRG
08/08/13 09:06
A_Spec
Alpha_012
170.02 1.38 E+01
1.00 E-03
19.9
08/08/13 09:06
A_Spec
Alpha_013
170.02 3.17 E+01
2.00 E-03
18.7
07
U-234
TRG
08/08/13 09:06
A_Spec
Alpha_014
170.02 2.86 E+01
8.00 E-03
18.5
08
U-234
TRG
08/08/13 09:06
A_Spec
Alpha_015
170.02 1.04 E+02
6.00 E-03
14.8
09
U-234
TRG
08/08/13 09:08
A_Spec
Alpha_033
170 9.23 E+01
4.00 E-03
18.5
10
U-234
TRG
08/08/13 09:08
A_Spec
Alpha_034
170 1.78 E+01
1.00 E-03
18.6
11
U-234
TRG
08/08/13 09:08
A_Spec
Alpha_035
170 1.48 E+01
1.00 E-03
18.3
12
U-234
TRG
08/08/13 09:08
A_Spec
Alpha_036
170 3.20 E-01
4.00 E-03
19.1
c..i
13
U-234
TRG
08/08/13 09:08
A_Spec
Alpha_038
170 3.66 E+OO
2.00 E-03
17.2
t:
14
U-234
TRG
08/08/13 09:08
A_Spec
Alpha_039
170 1.52 E+02
6.00 E-03
19.7
15
U-234
TRG
08/08/13 09:08
A_Spec
Alpha_040
170 1.13 E+02
3.00 E-03
19
08/08/13 09:08
A_Spec
Alpha_045
170 5.05 E+01
3.00 E-03
19.1
0
0..
0..
::l
(/)
~I
ol
U-234
LCS
Halflife
(days)
- -
en
..E
... ,
02
Counting
Date/Time
::J
~I ::J
]. I
U-234
Desc
Sample
----
~~ 0
oi
0
'
,., I
Nuclide
01
Printed: 8/8/2013 1:15PM
Page 3 of 3
....c
Q)
Q)
Ol
Cl$
c
Cl$
:i!i
""-
16
U-234
17
U-234
TRG
08/08/13 09:08
A_Spec
Alpha_046
170 8.88 E+01
1.00 E-03
17.9
18
U-234
TRG
08/08/13 09:08
A_Spec
Alpha_047
170 2.59 E+02
2.00 E-03
18.2
19
U-234
TRG
08/08/13 09:08
A_Spec
Alpha_048
170 1.37 E+02
0.00 E+OO
16.8
TRG
r----
I
!
I
IC!!!l!
..".'
1:;!1
'"...
--
Eberline Services
Lab
0.:
.g
0
.(!!
~
ca
1::
":t
120.39
OK
MDA
Flag
RPD
Flag
Client
Identification
Activity
Units
01
U-238
LCS
LCS
pCi/1
9.SOE+OO
1.37E+OO
8.69E-02
02
U-238
MBL
BLANK
pCi/1
1.8SE-01
1.07E-01
9.78E-02
DUP
D-12 TOT
pCi/1
2.29E-01
1.22E-01
9.06E-02
DO
D-12 TOT
pCi/1
4.00E-01
1.66E-01
7.75E-02
U-238
TRG
D-12 DIS
pCI/1
1.18E-01
1.08E-01
1.02E-01
U-238
TRG
DUPOS TOT
pCi/1
2.58E-01
1.52E-01
1.18E-01
TRG
DUPOS DIS
pCI/1
2.64E-01
1.32E-01
7.57E-02
t---
OK
TRG
PZ-208-SS TOT
pCi/1
1.43E+OO
3.55E-01!
9.07E-02
OK
TRG
PZ-208-SS DIS
pCi/1
9.80E-01
2.81E-01
8.13E-02
---r
Results
Error Estimate
MOA
7.89E+OO
OK
05
I OK
ToK
-----
06
--
-----~-
---------
07
U-238
--------- --
..
- -------
08 I
OK
OK
INV
------~---
r------
Blank
Flag
OK
r------ ---------
---
::J
::J
LCS
Flag
Sample
Desc
03
U-238
~---t----04
U-238
CJ)
LCS
%R
LCS
Known
Nuclide
Fraction
Printed: 8/8/2013 1:15PM
Page 1 of 3
OK
---
U-238
--------- '--- -----------
09
U-238
~-----
10
TRG
PZ-304-AI TOT
pCi/1
8.03E-01
3.83E-01
1.69E-01
___l _______
OK
U-238
TRG
PZ-304-AI DIS
pCi/1
3.33E-01
2.44E-01
1.78E-01
OK
U-238
TRG
PZ-304-AS TOT
pCi/1
-5.41 E-02
2.25E-01
7.26E-01
OK
U-238
TRG
PZ-304-AS DIS
pCi/1
1.30E+OO
1.88E+OO
2.60E+OO
INV
U-238
TRG
MW-104 TOT
pCi/1
2.39E+OO
5.17E-01
7.91E-02
TRG
MW-104 DIS
pCi/1
1.65E+OO
4.11E-01
1.16E-01
OK
TRG
PZ-204A-5S TOT
pCi/1
1.27E+OO
4.94E-01
1.86E-01
OK
TRG
PZ-204A-5S DIS
pCi/1
1.86E+OO
5.19E-01
1.13E-01
OK
U-238
TRG
PZ-302-AI TOT
pCi/1
3.10E+OO
5.34E-01
6.63E-02
OK
U-238
TRG
PZ-302-AI DIS
pCi/1
4.06E+OO
1.04E+OO
1.57E-01
OK
12
---
~----~--
~
0
c.
c.
:I
...c
~I
13
14
0)
--------
Cl>
Cl>
ftS
ftS
:E
---
18
~
I
J'>,,~
OK
U-238
U-238
I
I
---r--
-----
17 _________
____i
-------
!1::1!i!ll
U-238
-- r----
--------
-------+--
19
,.,......
------r
-------r
---+-----
15
------
16
(/)
---
--------------
11
U-238
------
.E
OK
r--- ------------
r-
------
'
--
Eberline Services
a:
Printed: 8/8/2013 1:15PM
Page 2 of 3
Lab
Fraction
Nuclide
Sample
Desc
Sample
Date
01
U-238
LCS
07/23/13 00:00
02
U-238
03
U-238
Sample
Aliquot
Radiometric
%Rec
Grav
%Rec
Mean
%Rec
SAF
1.00E+OO
72.66
0.00
0.00
1.00E+OO
99.04
0.00
0.00
1.00E+OO
88.83
0.00
0.00
SeptO
Date/Time
Sep t1
Date/Time
- ----------
MBL
07/23/13 00:00
r-------- r----
07/15/13 15:27
DUP
----
.g
8
.~
~
ii
.li
en
:::J
04
U-238
DO
07/15/13 15:27
1.00E+OO
79.47
0.00
0.00
05
U-238
TRG
07/15/13 15:27
1.00E+OO
54.56
0.00
0.00
----
:::J
06
U-238
TRG
07/15/13 00:00
1.00E+OO
67.67
0.00
0.00
07
U-238
TRG
07/15/13 00:00
1.00E+OO
90.44
0.00
0.00
--
1-
r--
.E
~
0
Q.
Q.
:I
(/)
(J
s::
( I)
E
(I)
Cl
111
s::
111
:E
Cl
s::
;:
(I)
(I)
.5
Cl
s::
w
112!1
li"""
l:il!~
t,.,)t
08
U-238
TRG
07/16/13 09:25
1.00E+OO
103.51
0.00
0.00
09
U-238
TRG
07/16/13 09:25
1.00E+OO
84.14
0.00
0.00
10
U-238
TRG
07/16/13 12:05
1.00E+OO
35.19
0.00
0.00
11
U-238
TRG
07/16/13 12:05
1.00E+OO
34.02
0.00
0.00
12
U-238
TRG
07/16/13 12:34
1.00E+OO
13.55
0.00
0.00
13
U-238
TRG
07/16/13 12:34
1.00E+OO
3.53
0.00
0.00
14
U-238
TRG
07/16/13 13:25
1.00E+OO
70.94
0.00
0.00
07/16/13 13:25
1.00E+OO
71.86
0.00
0.00
1.00E+OO
35.51
0.00
0.00
1.00E+OO
54.80
0.00
0.00
-~
15
U-238
--1-
TRG
16
U-238
TRG
r-----
07/16/13 13:56
-----
17
U-238
TRG
07/16/13 13:56
--------
18
U-238
TRG
07/16/13 15:18
1.00E+OO
104.63
0.00
0.00
U-238
TRG
- - - --~------+
1.00E+OO
41.84
0.00
0.00
r-- -
19
--------
r-
07/16/13 15:18
- - - L__
------
Eberline Services
a::
Lab
Fraction
01
--
{l
.!!!
~
~
"(
Sample
Desc
Counting
Datemme
U-238
LCS
U-238
Halflife
(days)
Count
Time
Counts
Bkg
Eft
Detect
Carrier
08/08/13 09:06
A_Spec
Alpha_003
170 4.56 E+02
1.00 E-03
17.5
MBL
08/08/13 09:06
A_Spec
Alpha_004
170 1.35 E+01
9.00 E-03
19.4
DUP
08/08/13 09:06
A_Spec
Alpha_010
170 1.52 E+01
5.00 E-03
19.7
DO
08/08/13 09:06
A_Spec
Alpha_011
170 2.47 E+01
2.00 E-03
20.5
U-238
TRG
08/08/13 09:06
A_Spec
Alpha_012
170.02 4.83 E+OO
1.00 E-03
19.9
U-238
TRG
08/08/13 09:06
A_Spec
Alpha_013
170.02 1.23 E+01
4.00 E-03
18.7
U-238
---
--
04
Nuclide
CPM
---~-------
03
--~-
r-
02
Printed: 8/8/2013 1:15 PM
Page 3 of 3
---
U-238
-
en
-::::>
::::>
05
06
-F- -
r------
--------
07
c 08
U-238
TRG
08/08/13 09:06
A_Spec
Alpha_014
170.02 1.67 E+01
2.00 E-03
18.5
U-238
TRG
08/08/13 09:06
A_Spec
Alpha_015
170.02 8.25 E+01
3.00 E-03
14.8
Qg
-~ U-238 -~--
I TRG
08/08/13 09:08
A_Spec
Alpha_033
170 5.77 E+01
2.00 E-03
18.5
TRG
08/08/13 09:08
A_Spec
Alpha_034
170 1.98 E+01
1.00 E-03
18.6
TRG
08/08/13 09:08
A_Spec
Alpha_035
170 7.83 E+OO
1.00 E-03
18.3
TRG
08/08/13 09:08
A_Spec
Alpha_036
170 -5.30 E-01
9.00 E-03
19.1
TRG
08/08/13 09:08
A_Spec
Alpha_038
170 3.00 E+OO
0.00 E+OO
17.2
TRG
08/08/13 09:08
A_Spec
Alpha_039
170 1.26 E+02
1.00 E-03
19.7
10
~-r---~
U-238
~---------
11
--~---~----t
U-238
r--------- - - - - - - - - - -
12
r-------~-~
.E
~
0
c.
c.
:I
(/)
....c:
~I
Cll
E
Cll
0'1
ns
ns
c:
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il'.:l!!li
......
a~
.~:,,.,
13
-----~
U-238
---------
U-238
------------r-
14
U-238
15
U-238
TRG
08/08/13 09:08
A_Spec
Alpha_040
170 8.50 E+01
0.00 E+OO
19
16
U-238
TRG
08/08/13 09:08
A_Spec
Alpha_045
170 3.27 E+01
2.00 E-03
19.1
17
U-238
TRG
08/08/13 09:08
A_Spec
Alpha_046
170 6.88 E+01
1.00 E-03
17.9
18
U-238
TRG
08/08/13 09:08
A_Spec
Alpha_047
170 2.24 E+02
2.00 E-03
18.2
19
U-238
TRG
08/08/13 09:08
A_Spec
Alpha_048
170 1.08 E+02
1.00 E-03
16.8
~-
Eberline Services
T"'"
e::
~
0
.!!!
~
Ill
t:
<t
LCS
Known
LCS
%R
LCS
Flag
RPD
Flag
MDA
Flag
Nuclide
Sample
Oesc
Client
Identification
Activity
Units
01
U-235
LCS
LCS
pCi/1
1.75E+OO
4.61E-01
1.08E-01
OK
BLANK
pCi/1
1.93E-01
1.18E-01
9.61E-02
OK
D-12 TOT
pCi/1
2.15E-01
1.30E-01
9.84E-02
------
U-235
----~------------
03
---
--
Lab
Fraction
02
t:
::s
Printed: 8/8/2013 1:15PM
Page 1 of 3
U-235
------~------
MBL
---
Error Estimate
MDA
NA
OK
--
U-235
DO
D-12 TOT
pCi/1
3.78E-01
1.78E-01
8.39E-02
OK
en
05
U-235
TRG
D-12 DIS
pCi/1
2.21E-01
1.71E-01
1.70E-01
OK
::J
::J
06
U-235
TRG
DUP05TOT
pCi/1
2.15E-01
1.56E-01
1.46E-01
OK
07
U-235
TRG
DUP05 DIS
pCUI
2.78E-01
1.53E-01
1.17E-01
OK
08
------
U-235
TRG
PZ-208-SS TOT
pCi/1
3.21E-01
1.72E-01
1.28E-01
OK
09
U-235
TRG
PZ-208-SS DIS
pCi/1
4.84E-01
2.11E-01
1.26E-01
OK
10
U-235
TRG
PZ-304-AI TOT
pCi/1
4.93E-01
3.24E-01
2.09E-01
OK
11
U-235
TRG
PZ-304-AI DIS
pCi/1
1.58E-01
2.09E-01
3.16E-01
OK
12
U-235
TRG
PZ-304-AS TOT
pCi/1
1.46E-01
3.66E-01
7.58E-01
OK
U-235
TRG
PZ-304-AS DIS
pCi/1
1.72E-01
1.12E+OO
3.04E+OO
INV
U-235
TRG
MW-104 TOT
pCi/1
7.40E-01
2.77E-01
1.23E-01
OK
e.i
.5
t:
0
Q.
Q.
::s
14
- - - - - - -----
15
U-235
TRG
MW-104 DIS
pCi/1
3.60E-01
1.94E-01
1.44E-01
OK
16
U-235
TRG
PZ-204A-SS TOT
pCi/1
3.78E-01
2.77E-01
2.02E-01
OK
17
U-235
TRG
PZ-204A-SS DIS
pCi/1
4.01E-01
2.44E-01
2.00E-01
OK
18
U-235
TRG
PZ-302-AI TOT
pCi/1
7.33E-01
2.36E-01
8.22E-02
OK
pCUI
8.39E-01
4.24E-01
2.79E-01
OK
<II
Cl
ns
c
ns
Cl
<II
<II
c
c,
c
w
'~'
u~
----
c
<II
E
;:
~.,
13
c------
en
:E
........
OK
04
--
1:
Blank
Flag
---------------
DUP
--
Results
r------ -
19
------
U-235
~-----------~----
TRG
PZ-302-AI DIS
----
II
Lab
Fraction
Nuclide
01
Sample
Date
Sample
Desc
Sample
Aliquot
Radiometric
%Rec
Grav
%Rec
Mean
%Rec
SAF
U-235
LCS
07/23/13 00:00
1.00E+OO
72.66
0.00
0.00
U-235
MBL
07/23/13 00:00
1.00E+OO
99.04
0.00
0.00
U-235
DUP
07/15/13 15:27
1.00E+OO
88.83
0.00
0.00
04
U-235
DO
07/15/13 15:27
1.00E+OO
79.47
0.00
0.00
05
U-235
TRG
07/15/13 15:27
1.00E+OO
54.56
0.00
0.00
U-235
TRG
07/15/13 00:00
1.00E+OO
67.67
0.00
0.00
U-235
TRG
07/15/13 00:00
1.00E+OO
90.44
0.00
0.00
U-235
TRG
07/16/13 09:25
1.00E+OO
103.51
0.00
0.00
------ --
~~.~
~I
Sep t1
Date/Time
r-
03
r-----
Septo
Date/Time
---
- - - - -----
~I ~
~I :::l
~
02
1------
Printed: 8/8/2013 1:15PM
Page 2 of 3
Eberline Services
:::l
06
---
!-----~------
07
f---------
08
r-------- --
09
U-235
TRG
07/16/13 09:25
1.00E+OO
84.14
0.00
0.00
U-235
TRG
07/16/13 12:05
1.00E+OO
35.19
0.00
0.00
11
U-235
TRG
07/16/13 12:05
1.00E+OO
34.02
0.00
0.00
12
'
U-235
TRG
07/16/13 12:34
1.00E+OO
13.55
0.00
0.00
U-235
TRG
07/16/13 12:34
1.00E+OO
3.53
0.00
0.00
14
U-235
TRG
07/16/13 13:25
1.00E+OO
70.94
0.00
0.00
15
U-235
TRG
07/16/13 13:25
1.00E+OO
71.86
0.00
0.00
U-235
TRG
07/16/13 13:56
1.00E+OO
35.51
0.00
0.00
U-235
TRG
07/16/13 13:56
1.00E+OO
54.80
0.00
0.00
U-235
TRG
07/16/13 15:18
1.00E+OO
104.63
0.00
0.00
U-235
TRG
07/16/13 15:18
1.00E+OO
41.84
0.00
0.00
-------
10
----
~-
r----
;-----
c.i
.E
~
0
Q.
Q.
:I
(/)
~I
oi
c::
Q)
E
Q)
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co
c::
Cl
c::
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Q)
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w
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~--
13
1------- -
f-----
16
1-----
17
1------ ---
18
1-
19
f---------- I
'
Lab
Fraction
01
r--~
02
a::
8
.!I,!
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03
04
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05
06
Nuclide
U-235
Sample
Oesc
Counting
Date/Time
LCS
08/08/13 09:06
U-235
A_Spec
Carrier
Alpha_003
Count
Time
Counts
170 6.78 E+01
Bkg
CPM
1.00 E-03
Eft
!
17.5
08/08/13 09:06
TRG
-+--
Alpha_004
170 1.13 E+01
4.00 E-03
19.4
I
08/08/13 09:06
A_Spec
Alpha_010
170 1.15 E+01
3.00 E-03
19.7
08/08/13 09:06
A_Spec
Alpha_011
170 1.88 E+01
1.00 E-03
20.5
08/08/13 09:06
A_Spec
Alpha_012
170.02 7.32 E+OO
4.00 E-03
19.9
08/08/13 09:06
A_Spec
Alpha_013
170.02 8.32 E+OO
4.00 E-03
18.7
A_Spec
Alpha_014
170.02 1.41 E+01
5.00 E-03
18.5
---
I TRG
U-235
A_Spec
f- -
07
Detect
I
I
MBL
-~--=r~~::: 1--"a:
U-235
Halflife
(days)
---
1----~-----
U-235
Printed: 8/8/2013 1:15PM
Page 3 of 3
Eberline Services
08/08/13 09:06
TRG
---
08
U-235
TRG
08/08/13 09:06
A_Spec
Alpha_015
170.02 1.50 E+01
0.00 E+OO
14.8
09
U-235
TRG
08/08/13 09:08
A_Spec
Alpha_033
170 2.30 E+01
0.00 E+OO
18.5
10
U-235
TRG
08/08/13 09:08
A_Spec
Alpha_034
170 9.83 E+OO
1.00 E-03
18.6
11
U-235
TRG
08/08/13 09:08
A_Spec
Alpha_035
170 3.00 E+OO
0.00 E+OO
18.3
08/08/13 09:08
A_Spec
Alpha_036
170 1.15 E+OO
5.00 E-03
19.1
08/08/13 09:08
A_Spec
Alpha_038
170 3.20 E-01
4.00 E-03
17.2
TRG
08/08/13 09:08
A_Spec
Alpha_039
170 3.15 E+01
3.00 E-03
19.7
TRG
08/08/13 09:08
A_Spec
Alpha_040
170 1.50 E+01
0.00 E+OO
19
08/08/13 09:08
A_Spec
Alpha_045
170 7.83 E+OO
1.00 E-03
19.1
08/08/13 09:08
A_Spec
Alpha_046
170 1.20 E+01
0.00 E+OO
17.9
08/08/13 09:08
A_Spec
Alpha_047
170 4.27 E+01
2.00 E-03
18.2
A_Spec
Alpha_048
170 1.80 E+01
0.00 E+OO
16.8
12
c.i
.5
~
0
a.
a.
::l
U)
...c:
....c:
Cll
Cll
Cl
"'c:
"'
::!!
Cl
c:
;:
Cll
Cll
.5
Cl
c:
13
!-----
14
15
U-235
U-235
+~
TRG
~---------+---- --
U-235
U-235
--
16
U-235
I TRG
1------ 1------~t---
17
j-----
18
j------
19
r----~
U-235
---------+
~~I
!:a
JI
TRG
~----~~-+~~
U-235
TRG
r-------- __ j _________
I
I
II"'"'"
--
f-------
08/08/13 09:08
'
Count Room Report

Client: Engineering Management Su
13-07147-UUIS0-1 (pCi/1) in WA
TraceriD: U-10a
~~
/'"\,
Internal
Fraction
01 "")
Sample
Desc
Printed: 8/8/2013 6:07AM

Page 1 of 1
\,"
i
Client
ID
Sample
Date
LCS
07/23/13 00:00
1.0000
0.9113
17.3539 !
0.00
BLANK
07/23/13 00:00
1.0000
0.6093
11.6029
0.00
0.6069
11.5572
0.00
LCS
I
I
Sample
Aliquot
Tracer
Aliquot(g)
Tracer
ACT(dpm)
Radiometric
Tracer (pCi)
SAF
1*
Radiometric
%Rec
SAF
2*
----
02
MBL
--.
\1
\)
..a
03
DUP
04
DO
D-12 TOT
07/15/13 15:27
05
TRG
D-12 DIS
07/15/13 15:27
D-12 TOT
07/15/1315:~1.0000
1.0000
0.6056
11.5324
0.00
1.0000
0.6054
11.5286
0.00
06
TRG
DUP05 TOT
07/15/13 00:00
1.0000
0.6067
11.553~
0.00
0.00
-~
\)\
07
TRG
DUP05 DIS
07/15/13 00:00
1.0000
0.6048
11.5172
08 \"~
TRG
PZ-208-SS TOT
07/16/13 09:25
1.0000
0.6031
11.4848
0.00
09 _/'j ~ TRG
PZ-208-SS DIS
07/16/13 09:25
1.0000
0.6014
11.4525
0.00
10
TRG
PZ-304-AI TOT
07/16/13 12:05
1.0000
0.6035
11.4925
0.00
11
TRG
PZ-304-AI DIS
07/16/13 12:05
1.0000
0.6044
11.5096
0.00
12
TRG
PZ-304-AS TOT
07/16/13 12:34
1.0000
0.6020
11.4639 I
0.00
0.00 I
I
I
I
----t--~
13
TRG
PZ-304-AS DIS
07/16/13 12:34
1.0000
0.6030
11.4829
14
TRG
MW-104 TOT
07/16/13 13:25
1.0000
0.6018
11.4601
0.00
I
15
TRG
MW-104 DIS
07/16/13 13:25
1.0000
0.6027
11.4772
16
TRG
PZ-204A-SS TOT
07/16/13 13:56
1.0000
0.6018
11.4601
0.00
17
TRG
PZ-204A-SS DIS
07/16/13 13:56
1.0000
0.6021
11.4658
o.oo
18
TRG
PZ-302-AI TOT
07/16/13 15:18
1.0000
0.6007
11.4391
19\!,<J " TRG
PZ-302-AI DIS
07/16/13 15:18
1.0000
0.6019
11.4620
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-r
I
I
I
I
0.00
0.00
0.00
I
l!it!ll
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l2lt
()()
Eberline Services
Page 1 of 1
Printed: 8/2/2013 8:15AM
Spike and Tracer Worksheet
UUISO
Isotope
Sol#
Activity
dpmlg
Solution
Date
Approx
Addition
JWOLFE
LCS
MS
Volume
Used(g)
Volume
Used(g)
LC~[);.;.
LCS
MSD
Known
pCi
LCSD
E"or
Estimate
Added
pCi
Error
Estimate
Known
pCi
35.240
8/2/2013
0.500
0.5098
0.00
0.000
0.00
34.3501
8/2/2013
0.500
0.5098
0.00
0.000
o.oo[
Trac~r-:::
.. .
Activity
dpmlg
...
. .
..
Solution
Date
Volume
Used(g)
Approx
Addition
fraction
Isotope
Sol#
01
U-232
U-10a
19.043
8/2/2013
0.9113
0.6300
02
U-232
U-10a
19.043
8/2/2013
0.6093
0.6300
03
U-232
U-10a
19.043
8/2/2013
0.6069
0.6300
04
U-232
U-10a
19.043
8/2/2013
0.6056
0.6300
05
U-232
U-10a
19.043
8/2/2013
0.6054
0.6300
06
U-232
U-10a
19.043
8/2/2013
0.6067
0.6300
07
U-232
U-10a
19.043
8/2/2013
0.6048
0.6300
08
U-232
U-10a
19.043
8/2/2013.
0.6031
0.6300
09
U-232
U-10a
19.043
8/2/2013
0.6014
0.6300
10
U-232
U-10a
19.043
8/2/2013
0.6035
0.6300
11
U-232
U-10a
19.043
8/2/2013
0.6044
0.6300
12
U-232
U-10a
19.043
8/2/2013 .:
0.6020
0.6300
13
U-232
U-10a
19.043
8/2/2013
0.6030
0.6300
19.043
8/2/2013
r.. . \. ......
MSo
Error
Estimate
Tracer
Error
Estimate
0.000
0.00
0.000
-~ooo
0.00
0.000
l:latane Pri.Pter T.-pes
*?.... ....
Added
pCi
..........
LCS
-~
14
U-232
U-10a
0.6018
0.6300
15
U-232
U-10a
19.043
8/2/2013
0.6027
0.6300
16
U-232
U-10a
19.043
8/2/2013
0.6018
0.6300
17
U-232
U-10a
19.043
8/2/2013
0.6021
0.6300
18
U-232
U-10a
19.043
8/2/2013
0"6007
0.6300
19
U-232
U-10a
19.043
8/2/2013
Q;6019
0.6300
.
::_
~~~
j ...~llt
l.!!t!\l
Uli
Version 2.0 08/99
...
'
.. . .
'
Matrix Spike
I
I
h!-<
,.,,.,,,,,,,,,
Eberline Analytical
Printed: 8/2/2013 8:15AM
Page 1 of 1
Aliquot Worksheet
JWOLFE
lab
Fraction 1
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17 ]
18
19
ClientiD
LCS
BLANK
D-12 TOT
D-12 TOT
D-12 DIS
DUP05TOT
DUP05 DIS
PZ-208-SS TOT
PZ-208-SS DIS
PZ-304-AI TOT
PZ-304-AI DIS
PZ-304-AS TOT
PZ-304-AS DIS
MW-104 TOT
MW-104 DIS
PZ-204A-SS TOT
PZ-204A-SS DIS
PZ-302-AI TOT
PZ-302-AI DIS
Comments
i:l~
!1!..!111
"""'
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Technician:
1
l
TRG
T
I
No of on~
Aliquot
Ratio
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.: :.
);
.,
....
..
'
..
.}
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::'
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,:
. . i
..
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..
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.
.......
~
...... r: .
.._
Aliquot
H-3 Solids Only

Water Added
(ml)
Net Equiv _
H3 Dist
Aliq
1.0000E+OO .... 1.0000E+OO

1.0000E+OO .: 1.0000E+00
1.0000E+OO
.1 :OOOOE+OO
1.0000E+OO , HlOQOE+ool
1.0000E+OO
.1:ooOOE+oo
1 OOOOF+OO : .1'0000F+00
.'.. .
I" ~1!4: Equiv
MS Aliquot Data
1.0000E+OO 1tOOOOE+ooi
1.0000E+OO .... it .9QOOE+OO
1.0000E+OO
l.OOOOE+OO
1.0000E+OO 1:: 1.0000E+OO
1.0000E+OO
J.OOOOE+OO
1.0000E+OO
i]OOOOE+OO
1.0000E+OO I' 't,O{J()OE+OO
..... : . ......
::
DltFactor
:.
'
,.
..
: :.
. I''.
...
Aliquot Data
:>'
Ratio
Post/Pre
Type
LCS
MBL
DUP
DO
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
----~
TRG
TRG
Dilution Data
Muffle Data
Sample
:.
...
1.UUUUc+UU
1.;000Ut+UQ
1.0000E+OO UlOOOE+OO
1.0000E+OO
1.0000E+OO
----
--1
'"----
--1
1.0000E+OO .,1.0000E+OO
1.0000E+OO ::. t!)OOOE+OO
'1';00oOE+OO
1.0000E+OO
1:
r'
-Date
l3
Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:
SPIKE
\\OR-ALPHA1\Canberra\ApexAlpha\Root\Data\00000655
1307147A-UU
01
Shelf 2
U iso
Detector Name:
Alpha_003
Chamber Serial Number:
Detector Serial Number:

3
Env. Background:
System Bkgd 64034

Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:
1.000E+000 +/- O.OOOE+OOO liter
8/8/2013
7:05:56 AM
9:06:44 AM
8/8/2013
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chern. Recovery Factor:
U232 UU-10A
0.911 mL
0.1269 +/- 0.0072
0.1746 +/- 0.0033 on 12/15/2012 11:26:47 AM
0.7266 +/- 0.0434
Control Certificate Name:

NatU U-SA
Chern. Recov. of Control:

U-238
Peak Match Tolerance:
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.256
4.735
4.394
4.158
T
Net
Pk Area
1.173603 +/-
AREA
REPORT
Pk Area
Error %
372.15
434.49
67.83
455.83
0.093290
10.17
9.41
23.83
9.18
Ambient
Backgnd
0.85
0.51
0.17
0.17
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
18.9
28.3
5.2
59.2
Tracer Peak used for Effective Efficiency
NUCLIDE ANALYSIS RESULTS
Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.985
0.995
1.000
0.995
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
7.79E+000 +/
9.09E+000 +!
1.75E+000 +/
9.50E+000 +!
8.67E-001
1.32E+000
4.61E-001
1.37E+000
MDA
(pCi/liter
1.25E-001
1.10E-001
1.08E-001
8.69E-002
+!
+!
+1
+!
1.39E-002
1.22E-002
1.20E-002
9.68E-003
J\-6
rtf'sltJ
8111
0000065563.CNF
Live Time 10200.000 sec

Rea1 Time 10200.000 sec
start:
1 3498.4(kev)
stop : 1024 6549. 5(kev)
Acq. start Thu Aug 08 09:06:44 2013
60
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4-'
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'lli!I\IID'lll!J!l!!I!IJU\IIJ!fn!IImlyl/ll\l!fl!l!!llli!I
3500
~
......
......
I'>Y!
ROI Type: 1
4000
IJ!D!Will!C 1 :pll!i!:.! '(iU1J!IIII/
4500
!!'< !fl!lNfVI!I\ID/111l!V!UJ/
\m'fl'i'
5000
Energy(kev)
l!
6116
61
5500
Bfi
16
6000
6 I
6500
Channel Data Report
Page
8/8/2013
*******************************************************
*****
S P E C T R A L
DATA
R E P 0 R T
*****
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Sample Title:
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1
G113
Channel Data Report

369:
8/S/2013
3
Sample Title:
Page
12:~ij"
2
01
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~114
Channel Data Report

801:
8/8/2013
0
Sample Title:
12:l.i:ij
0
Page
0
01
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8115
Sample Description:
Spectrum File:
Sample Geometry:
BLANK
1307147A-UU
02
Shelf 2
U iso
Detector Name:
Alpha_004

4
Env. Background:
System Bkgd 64035

Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:

8/8/2013
7:05:56 AM
8/8/2013
9:06:45 AM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-10A
0.609 mL
0.1922 +/- 0.0109
0.1940 +/- 0.0036 on 12/15/2012 11:26:46 AM

0.9904 +/- 0.0588
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.275
4. 719
4.413
4.127
Net
Pk Area
AREA
REPORT
Pk Area
Error %
376.81
14.81
11.32
13.47
10.12
53.27
60.27
56.84
Ambient
Backgnd
1.19
1.19
0.68
1. 53
Reagent
Backgnd
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
10.2
2.9
2.9
2.9
Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.995
0.987
0.995
0. 977
5302.50*
4761. 50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.21E+000 +/
2.05E-001 +I
1.93E-001 +!
1.85E-001 +!
5.77E-001
1.11E- 001
1.18E-001
1.07E-001
MDA
(pCi/liter
9.10E-002
9.10E-002
9.61E-002
9.78E-002
+I
+I
+I
+!
1.01E-002
1.01E-002
1. 06E- 002
1.08E-002
AG
~I C6/r)
fi116
0000065508.CNF

Real Time 10200.000 sec
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Acq. Start Thu Aug 08 09:06:45 2013
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ROI Type: 1
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6500
Channel Data Report
8/8/2013
12:16:fll
Page
iW
*******************************************************
s P E C T R A L DATA R E P 0 R T *****
*****
*******************************************************
Sample Title:
02
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801:
8/8/2013
0
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1307147A-UU
03
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10
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<not performed>
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7/15/2013
7:05:56 AM
8/8/2013
9:06:37 AM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-10A
0.607 mL
0.1747 +/0.1967 +/0.8883 +/-
0.150 MeV
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Energy
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Nuclide
Net
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0.0103
0.0036 on 12/15/2012 11:26:40 AM
0.0548
AREA
REPORT
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
FWHM
(keV)
1. 70
1. 87
0.51
0.85
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
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2.9
4.4
2.9
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U-234
U-235
U-238
5.280
4.729
4.403
4.176
341.30
44.13
11.49
15.15
10.64
30.23
59.30
51.98

Nuclide
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Conf.
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(pCi/liter )
MDA
(pCi/liter
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U-234
U-235
U-238
0.996
0.993
0.998
0.999
5302.50*
4761.50*
4385.50*
4184.40*
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1.15E-001 +/- 1.33E-002
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Channel Data Report

801:
8/8/2013
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8125
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Sample Geometry:
D-12 TOT
1307147A-UU
04
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Alpha_011
11
System Bkgd 64037
<not performed>
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7:05:56 AM
8/8/2013
9:06:38 AM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-10A
0.606 mL
0.1630 +/0.2051 +/0.7947 +/-
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
Net
Pk Area
0.0099
0.0035 on 7/20/2013
0.0501
AREA
2:50:46 PM
REPORT
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
11.00
32.83
45.41
39.79
0.34
0.17
0.17
0.34
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
FWHM
(keV)
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U-234
U-235
U-238
5.272
4.724
4.419
4.126
317.66
35.83
18.83
24.66
3.9
3.1
3.9
3.3

Nuclide
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Conf.
Energy
(keV)
Activity
(pCi/liter )
MDA
(pCi/liter
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U-234
U-235
U-238
0.993
0.990
0.992
0.976
5302.50*
4761.50*
4385.50*
4184.40*
5.18E+000
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4.00E-001
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7.79E-002
6.80E-002
8.39E-002
7.75E-002
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04
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Channel Data Report

369:
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1
Sample Title:
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Channel Data Report

801:
8/8/2013
0
Sample Title:
fi.ge
12:lillj
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7/15/2013
7:05:56 AM
8/8/2013
9:06:39 AM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-10A
0.605 mL
0.1085 +/ 0.0079
0.1989 +/ 0.0034 on 12/11/2011
0.5456 +/ 0.0407
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.268
4. 716
4.408
4.170
T
Net
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AREA
REPORT
Pk Area
Error %
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13.83
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2:21:56 PM
Ambient
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1. 71E-001
1. 08E-001
AG
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Channel Data Report

801:
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&135
Sample Description:
Spectrum File:
Sample Geometry:
DUP05 TOT
1307147A-UU
06
Shelf 2
u iso
Detector Name:
Alpha_013

13
Env. Background:
System Bkgd 64039

Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:

7/15/2013
7:05:56 AM
8/8/2013
9:06:40 AM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-10A
0.607 mL
0.1265 +/- 0.0086
0.1869 +/- 0.0035 on 12/15/2012 11:26:45 AM

0.6767 +/- 0.0477
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.272
4.733
4.406
4.106
T
Net
Pk Area
246.96
31.66
8.32
12.32
AREA
REPORT
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
FWHM
(keV)
12.53
35.05
71.13
57.62
2.04
0.34
0.68
0.68
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
8.2
2.8
2.8
2.8

Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.993
0.994
0.997
0.957
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.19E+000
6.65E-001
2.15E-001
2.58E-001
+!+I+!+I-
6.91E-001
2.49E-001
1.56E-001
1.52E-001
MDA
(pCi/liter
1.64E-001
1. OOE-001
1.46E-001
1.18E-001
+I+!+!+!-
2.18E-002
1.34E-002
1.95E-002
1.57E-002
AG
~( l<(r~
1i136
0000065540.CNF
Live Time :10201.000 sec

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Channel Data Report
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12;l"'M
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B139
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801:
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Sample Description:
Spectrum File:
Sample Geometry:
DUPOS DIS
1307147A-UU
07
Shelf 2
U iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_014
14
System Bkgd 64040
<not performed>
Sample Size:
Sample Date/Time:

7/15/2013
7:05:56 AM
8/8/2013
9:06:41 AM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-10A
0.605 mL
0.1669 +/
0.0101
0.1846 +/
0.0034 on 12/15/2012 11:26:44 AM
0.9044 +/
0.0571
0.150 MeV
PEAK
Energy
{MeV)
Nuclide
U-232
U-234
U-235
U-238
5.269
4.720
4.401
4.113
T
Net
Pk Area
324.94
28.64
14.15
16.66
AREA
REPORT
Pk Area
Error %'
Ambient
Backgnd
Reagent
Backgnd
FWHM
{keV)
10.93
37.63
53.91
48.59
3.06
1. 36
0.85
0.34
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
8.8
2.9
8.8
2.9

Nuclide
Id
Conf.
Energy
{keV)
U-232
U-234
U-235
U-238
0.992
0.988
0.998
0.964
5302.50*
4761.50*
4385.50*
4184.40*
Activity
{pCi/liter )
5.17E+000
4.55E-001
2.78E-001
2.64E-001
+!
+I
+!
+!
~
6.12E-001
1. 80E-001
1.53E-001
1.32E-001
~( ~ (_)
MDA
{pCi/liter
1.42E-001
1.09E-001
1.17E-001
7.57E-002
+!
+I
+I
+!
1. 68E-002
1.29E-002
1.39E-002
8.95E-003
0000065541.CNF

Rea1 Time :10201. 000 sec
start:
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Stop : 1024:6512.2(kev)
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8/8/2013
Page
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Ci_iU~
Channel Data Report

369:
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8144
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801:
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Sample Geometry:
PZ-208-SS TOT
1307147A-UU
08
Shelf 2
U iso
Detector Name:

Env. Background:
Reagent Blank:
Alpha_015
15
System Bkgd 64041
<not performed>
Sample Size:
Sample Date/Time:
7/16/2013
7:05:56 AM
8/8/2013
9:06:43 AM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-10A
0.603 mL
0.1529 +/0.1477 +/1.0351 +/-
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
Net
Pk Area
0.0096
0.0027 on 7/20/2013
0.0673
AREA
6:27:27 PM
REPORT
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
FWHM
(keV)
11.38
19.33
52.27
21.66
0.17
1. 02
0.00
0.51
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
18.5
4.1
3.0
6.0
-------------------------------------------------------------------------------U-232
U-234
U-235
U-238
5.279
4.732
4.409
4.147
296.83
103.98
15.00
82.49

Nuclide
Id
Conf.
Energy
(keV)
Activity
(pCi/liter )
MDA
(pCi/liter
-------------------------------------------------------------------------------U-232
U-234
U-235
U-238
0.996
0.994
0.996
0.990
5302.50*
4761.50*
4385.50*
4184.40*
5.16E+000
1.81E+000
3.21E-001
1.43E+000
+I+!+I+I-
6.31E-001
4.13E-001
1. 72E-001
3.55E-001
t(f4e,
7.25E-002 +/- 8.88E-003

1.09E-001 +/- 1.34E-002
1.28E-001 +/- 1.57E-002
9.07E-002 +!- 1.11E-002
0000065542.CNF

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Channel Data Report
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Sample Description:
Spectrum File:
Sample Geometry:
PZ-208-SS DIS
1307147A-UU
09
Shelf 2
U iso
Detector Name:
Alpha_033
04026479A
91132
Env. Background:
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Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:

7/16/2013
7:05:56 AM
8/8/2013
9:08:28 AM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-10A
0.601 mL
0.1555 +/- 0.0097
0.1848 +/- 0.0032 on 7/20/2013

0.8414 +/- 0.0543
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.278
4.733
4.396
4.151
Net
Pk Area
301.00
92.32
23.00
57.66
AREA
2:31:30 PM
REPORT
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
11.32
20.49
41.75
25.90
0.00
0.68
0.00
0.34
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
FWHM
(keV)
38.3
9.9
3.0
3.7

Nuclide
Id
Conf.
Energy
(keV)
Activity
(pCi/liter )
MDA
(pCi/liter
-------------------------------------------------------------------------------U-232
U-234
U-235
U-238
0.996
0.994
0.999
0.992
5302.50*
4761.50*
4385.50*
4184.40*
5.14E+000
1.58E+000
4.84E-001
9.80E-001
+I+!+!+!-
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3.76E-001
2.11E-001
2.81E-001
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1.02E-001
9.63E-002
1.26E-001
8.13E-002
+I+I+!+I-
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1.17E-002
1.54E-002
9.90E-003
0000065543.CNF

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Channel Data Report

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S155
Sample Description:
Spectrum File:
Sample Geometry:
PZ-304-AI TOT
1307147A-UU
10
Shelf 2
u iso
Detector Name:
Alpha_034
04026479B
91136
Env. Background:
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Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:
7/16/2013
7:05:56 AM
8/8/2013
9:08:29 AM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-10A
0.604 mL
0.0653 +/- 0.0060
0.1856 +/- 0.0032 on 12/16/2012
0.3519 +/- 0.0329
0.150 MeV
PEAK
Energy
{MeV)
Nuclide
U-232
U-234
U-235
U-238
5.254
4.705
4.374
4.139
Net
Pk Area
126.83
17.83
9.83
19.83
AREA
5:49:43 PM
REPORT
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
17.42
46.68
63.14
44.23
0.17
0.17
0.17
0.17
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
FWHM
{keV)
6.1
3.0
3.0
4.5
Nuclide
Id
Conf.
Energy
{keV)
Activity
{pCi/liter )
MDA
{pCi/liter
-------------------------------------------------------------------------------U-232
U-234
U-235
U-238
0.984
0.977
0.999
0.986
5302.50*
4761.50*
4385.50*
4184.40*
5.16E+000
7.25E-001
4.93E-001
8.03E-001
+!
+I
+I
+I
9.28E-001
3.63E-001
3.24E-001
3.83E-001
~{f)
1. 70E-001
1. 70E-001
2.09E-001
1. 69E- 001
+I+!+I+!-
3.05E-002
3.05E-002
3.77E-002
3.04E-002
0000065544.CNF

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Sample Description:
Spectrum File:
Sample Geometry:
Shelf 2
U iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_035
04026477A
58771
System Bkgd 64053
<not performed>
PZ-304-AI DIS
1307147A-UU
11
Sample Size:
Sample Date/Time:
7/16/2013
7:05:56 AM
8/8/2013
9:08:31 AM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-10A
0.604 mL
0.0621 +/0.1826 +/0.3402 +/-
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
Net
Pk Area
0.0059
0.0032 on 12/16/2012
0.0326
AREA
5:49:42 PM
REPORT
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
FWHM
(keV)
-------------------------------------------------------------------------------U-232
U-234
U-235
U-238
5.294
4.738
4.420
4.165
120.81
14.83
3.00
7.83
17.93
51.24
130.67
70.93
1.19
0.17
0.00
0.17
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
4.4
2.9
2.9
2.9

Nuclide
Id
Conf.
Energy
(keV)
Activity
(pCi/liter )
MDA
(pCi/liter
-------------------------------------------------------------------------------U-232
U-234
U-235
U-238
0.999
0.996
0.992
0.997
5302.50*
4761.50*
4385.50*
4184.40*
5.17E+000
6.34E-001
1.58E-001
3.33E-001
+I+!+!+!-
9.56E-001
3.45E-001
2.09E-001
2.44E-001
2.82E-001
1. 78E- 001
3 .16E-001
1. 78E-001
+I+I+I+!-
5.21E-002
3.30E-002
5.85E-002
3.29E-002
A:-G
~~~(tJ
B161
0000065545.CNF

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C-<i
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J;!i,ib,j
Channel Data Report

369:
8/S/2013
1
Sample Title:
12:lttl
0
..
0
Pa~e
11
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"mts4
Channel Data Report

801:
8/8/2013
0
Sample Title:
Page
12:19:1J 9N
0
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8.165
Sample Description:
Spectrum File:
Sample Geometry:
MW-104 TOT
1307147A-UU
14
Shelf 2
u iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_039
06027396A
83109
System Bkgd 64056
<not performed>
Sample Size:
Sample Date/Time:
1.000E+000 +/
O.OOOE+OOO liter
7/16/2013
7:05:56 AM
8/8/2013
9:08:37 AM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-10A
0.602 mL
0.1394 +/
0.0091
0.1965 +/
0.0034 on 4/20/2013
0.7094 +/
0.0478
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.276
4.728
4.421
4.152
T
Net
Pk Area
270.00
151.98
31.49
125.83
AREA
2:01:25 PM
REPORT
FWHM
(keV)
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
11.95
15.96
35.26
17.49
0.00
1. 02
0.51
0.17
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
42.0
14.3
3.0
6.3

Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.995
0.992
0.991
0.993
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.15E+000 +!
2.89E+000 +!
7 .40E-001 +I
2.39E+000 +/
6.57E-001
5.92E-001
2.77E-001
5.17E-001
MDA
(pCi/liter
1.14E-001
1.20E-001
1.23E-001
7.91E-002
+I
+I
+!
+!
1.46E-002
1.53E-002
1.57E-002
1. 01E-002
Jr.6
8( cg{t 3
81
0000065548.CNF

start:
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Channel Data Report
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8/8/2013
*******************************************************
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"*
Channel Data Report

369:
8/8/201~
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fJ169
Channel Data Report

801:
8/8/2013
0
Sample Title:
12:20~
..
0
Page
0
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Sample Description:
Spectrum File:
Sample Geometry:
MW-104 DIS
1307147A-UU
15
Shelf 2
U iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_040
06027396B
91135
System Bkgd 64057
<not performed>
Sample Size:
Sample Date/Time:
7/16/2013
7:05:56 AM
8/8/2013
9:08:38 AM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-10A
0.603 mL
0.1365 +/0.1900 +/0.7186 +/-
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
Net
Pk Area
0.0090
0.0033 on 12/16/2012
0.0488
AREA
5:49:33 PM
REPORT
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
FWHM
(keV)
-------------------------------------------------------------------------------U-232
U-234
U-235
U-238
5.272
4.737
4.402
4.158
264.83
113.49
15.00
85.00
12.05
18.45
52.27
21.38
0.17
0.51
0.00
0.00
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
6.9
4.1
3.0
4.0

Nuclide
Id
Conf.
Energy
(keV)
Activity
(pCi/liter )
MDA
(pCi/liter
-------------------------------------------------------------------------------U-232
0.993
5302.50*
5.15E+000 +I- 6.63E-001
8.12E-002 +1- 1.04E-002
U-234
0.996
4761.50*
2.21E+000 +I- 4.96E-001
1.02E-001 +!- 1.31E-002
U-235
0.998
4385.50*
3.60E-001 +I- 1. 94E-001
1. 44E- 001 +I- 1. 85E- 002
U-238
0.995
4184.40*
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801:
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Sample Description:
Spectrum File:
Sample Geometry:
PZ-204A-SS TOT
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Detector Name:
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91131
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<not performed>
Sample Size:
Sample Date/Time:

7/16/2013
7:05:56 AM
9:08:40 AM
8/8/2013
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-10A
0.602 mL
0.0678 +/- 0.0061
0.1909 +/- 0.0033 on 7/20/2013

0.3551 +/- 0.0327
0.150 MeV
PEAK
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U-234
U-235
U-238
5.272
4.738
4.397
4.135
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50.49
7.83
32.66
2:31:26 PM
17.16
27.75
70.93
34.50
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0.51
0.17
0.34
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0.994
0.996
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3.78E-001
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Channel Data Report

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Sample Description:
Spectrum File:
Sample Geometry:
PZ-204A-SS DIS
1307147A-UU
17
Shelf 2
U iso
Detector Name:
Alpha_046
04026482B
58762
Env. Background:
System Bkgd 64061

Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:

7/16/2013
7:05:56 AM
8/8/2013
9:08:43 AM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-10A
0.602 mL
0.0981 +1- 0.0075
0.1789 +/- 0.0031 on 12/16/2012

0.5480 +/- 0.0429
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.268
4.729
4.418
4.141
T
Net
Pk Area
190.00
88.83
12.00
68.83
AREA
5:49:23 PM
REPORT
FWHM
(keV)
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
14.26
20.82
58.89
23.66
0.00
0.17
0.00
0.17
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
7.8
4.4
3.0
4.4

Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.992
0.992
0.993
0.986
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.15E+000 +1
2.41E+000 +1
4. 01E-001 +/
1.86E+000 +!
7.70E-001
6.17E-001
2.44E-001
5.19E-001
MDA
(pCi/liter
1. 62E-001
1.13E-001
2.00E-001
1.13E-001
+!
+1
+I
+I
2.43E-002
1.69E-002
2.99E-002
1.68E-002
4-Y
g(<;s(tJ
m1s1
0000065551.CNF

start:
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Acq. Start :Thu Aug 08 09:08:43 2013
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Channel Data Report
8/S/2013
12:~~~
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Channel Data Report

369:
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Channel Data Report

801:
8/8/2013
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12:~Jt
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Sample Description:
Spectrum File:
Sample Geometry:
PZ-302-AI TOT
1307147A-UU
18
Shelf 2
U iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_047
02030596A
91086
System Bkgd 64062
<not performed>
Sample Size:
Sample Date/Time:
1.000E+000 +/
O.OOOE+OOO liter
7/16/2013
7:05:56 AM
8/8/2013
9:08:45 AM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-10A
0.601 mL
0.1906 +/
0.0109
0.0032 on 12/16/2012
0.1822 +/
1.0463 +/
0.0624
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.270
4.720
4.417
4.140
Net
Pk Area
AREA
REPORT
Pk Area
Error %
368.49
258.66
42.66
223.66
5:49:21 PM
10.22
12.20
30.15
13.12
Ambient
Backgnd
0.51
0.34
0.34
0.34
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
16.8
16.3
3.4
16.1

Nuclide
Id
Conf.
Energy
(keV)
Activity
(pCi/liter )
MDA
(pCi/liter
-------------------------------------------------------------------------------U-232
U-234
U-235
U-238
0.992
0.988
0.993
0.986
5302.50*
4761.50*
4385.50*
4184.40*
5.14E+000
3.60E+000
7.33E-001
3.10E+000
+!+I+I+I-
5.74E-001
5.96E-001
2.36E-001
5.34E-001
7.31E-002
6.66E-002
8.22E-002
6.63E-002
+I+!+!+I-
8.17E-003
7.44E-003
9.18E-003
7.41E-003
~I rs{{J
i1
0000065552.CNF

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8/8/2013
1~:2J4f'l
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18
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1
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3
2
2
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10
16
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!11 ""~
Channel Data Report

801:
8/8/2013
0
Sample Title:
121~., . .
0
w
0
Page
0
18
809:
817:
825:
833:
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921:
929:
937:
945:
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0
0
0
0
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0
0
0
0
0
0
0
0
0
0
0
0
0
0
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Sample Description:
Spectrum File:
Sample Geometry:
PZ-302-AI DIS
1307147A-UU
19
Shelf 2
u iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_048
02030596B
83111
System Bkgd 64063
<not performed>
Sample Size:
Sample Date/Time:

7/16/2013
7:05:56 AM
9:08:47 AM
8/8/2013
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-10A
0.602 mL
0.0703 +/ 0.0063
0.1680 +/ 0.0030 on 12/16/2012
0.4184 +/ 0.0380
0.150 MeV
PEAK
Energy
{MeV)
Nuclide
U-232
U-234
U-235
U-238
5.283
4.730
4.421
4.147
T
Net
Pk Area
AREA
REPORT
Pk Area
Error %
136.15
137.00
18.00
107.83
5:49:20 PM
16.86
16.81
47.46
18.89
Ambient
Backgnd
0.85
0.00
0.00
0.17
Reagent
Backgnd
FWHM
{keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
19.2
4.6
3.0
3.9

Nuclide
Id
Conf.
Energy
{keV)
U-232
U-234
U-235
U-238
0.997
0.993
0.991
0.990
5302.50*
4761.50*
4385.50*
4184.40*
Activity
{pCi/liter )
5.15E+000
5.18E+000
8.39E-001
4.06E+000
+!+!+!+!-
8.98E-001
1.25E+000
4.24E-001
1.04E+000
A;q
r( ~r(j
MDA
{pCi/liter
2.26E-001
2.27E-001
2.79E-001
1.57E-001
+I+!+!+!-
3.95E-002
3.95E-002
4.88E-002
2.74E-002
0000065553.CNF

Start:
1:3453 .O(kev)
stop : 1024:6472 .l(kev)
Acq. Start :Thu Aug 08 09:08:47 2013
60
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V'l
+-'
8 30
25
20
15
10
5
0
3500
4000
4500
S:r.ll
5000
Energy(kev)
5500
6000
J!<.....
~~ron
~~.jl
ROI Type: 1
ROI Type: 3
Channel Data Report
8/8/2013
12:22:1t
..
Page
*******************************************************
*****
*******************************************************
Sample Title:
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Q193
Channel Data Report

369:
8/8/2013
1
Sample Title:
14tJt~
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~194
Channel Data Report

801:
8/S/201:3
0
Sample Title:
l~tiiIW
W
0
Page
0
19
809:
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833:
841:
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953:
961:
969:
977:
985:
993:
1001:
1009:
1017:
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:3
Page 1 of 2
8/8/2013
7:55:58 AM
QA SUMMARY REPORT
Review Of QA Results - Pulser Check
Date
Time
: 8/8/2013
: 7:55:58 AM
CHAMBER
Alpha 001
Alpha 002
Alpha 003
Alpha 004
Alpha 005
Alpha 006
Alpha 007
AlQha 008
Alf>ha 009
Alpha 010
Alpha 011
Alpha 012
Alpha 013
Alpha 014
Alpha 015
Alpha 016
Alpha 017
Alpha 018
Alpha 019
Alpha 020
Alpha 021
Alpha 022
Alpha 023
Alpha 024
Alpha 025
Alpha 026
Alpha 027
Alpha 028
Alpha 029
Alpha 030
Alpha 031
Alpha 032
Alpha 033
Alpha 034
Alpha 035
Alpha 036
Alpha 037
Alpha 038
Alpha 039
Alpha 040
Alpha 041
Alpha 042
DEVICE
2lf
21f
2lf
2lf
21f
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
21f
2lf
21f
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
Alpha Analystl OODC
Alpha Analyst 1OODC
Alpha Analystl OODC
Alpha Analystl OODC
Alpha Analystl OODC
Alpha Analyst 1OODC
Alpha AnalystlOODC
Alpha Analystl OODC
Alpha Analyst 1OODC
Alpha AnalystlOODC
PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
Peak Energy
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
PeakFWHM
ALL
ALL
ALL
ALL
FLAG
Not Done
Not Done
Passed
Passed
Not Done
Not Done
Not Done
Not Done
Not Done
Passed
Passed
Passed
Passed
Passed
Action
Not Done
Not Done
Passed
Passed
Passed
Not Done
Passed
Passed
Passed
Passed
Not Done
Passed
Not Done
Passed
Not Done
Passed
Not Done
Passed
Passed
Passed
Passed
Not Done
Action
Passed
Passed
Passed
Passed
DATE
8/8/2013 5:38:35 AM
8/8/2013 5:38:36 AM
8/8/2013
8/8/2013
8/8/2013
8/8/2013
8/8/2013
8/8/2013
5:38:37 AM
5:38:38 AM
5:38:39 AM
5:38:40 AM
5:38:40 AM
5:38:41 AM
8/8/2013 5:38:42 AM
8/8/2013 5:38:43 AM
8/2/2013 5:14:08 AM
8/8/2013
8/8/2013
8/8/2013
8/8/2013
5:38:44 AM
5:38:45 AM
5:38:45 AM
5:38:46 AM
8/8/2013 5:38:47 AM
8/8/2013 5:38:48 AM
8/8/2013 5:38:49 AM
8/8/2013
8/8/2013
8/8/2013
8/8/2013
5:38:50 AM
5:38:51 AM
5:38:52 AM
5:38:54 AM
8/8/2013
8/8/2013
8/8/2013
8/8/2013
8/8/2013
5:38:55 AM
5:38:57 AM
5:38:58 AM
5:39:00 AM
5:39:02 AM
81
Page 2 of 2
Review of QA Results - Pulser Check
8/8/2013
CHAMBER
Alpha 043
Alpha 044
Alpha 045
Alpha 046
Alpha 047
Alpha 048
DEVICE
Alpha Analystl OODC
Alpha AnalystlOODC
Alpha AnalystlOODC
Alpha AnalystlOODC
Alpha AnalystlOODC
Alpha Analyst I OODC
PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
FLAG
Not Done
Not Done
Passed
Passed
Passed
Passed
APPROVED BY:
APPROVAL DATE:
~/lf!t)
7:55:58 AM
DATE
8/8/2013
8/8/2013
8/8/2013
8/8/2013
5:39:03
5:39:05
5:39:06
5:39:08
AM
AM
AM
AM
6/12/12
Library Listing Report
Page
12:17:04 PM
*************************************************************************
*****
L I B R A R Y L I S T I N G R E P 0 R T
*****
*************************************************************************
Nuclide Library Title:
Uranium
Nuclide Library Description:

Nuclide
Name
Half-Life
(Seconds)
U-232
U-234
U-235
U-238
2.174E+009
7.731E+012
2.221E+016
1. 410E+017
Energy
(keV )
U-232,-234,-235,-238
Energy
Uncert. (keV
0.000
0.000
0.000
0.000
5302.500*
4761.500*
4385.500*
4184.400*
key line
TOTALS:
Nuclides
Energy Lines
Yield
(%)
99.8000
99.8000
80.9000
100.2300
Yield
Uncert . (Abs . +- )
0.0000
0.0000
0.0000
0.0000
RUN2
Eberline Services
Analysis Sheet
Printed: 8/13/2013 6:32AM

Page 1 of 3
13-07147
UUISO
Run 2
Internal
Fraction
13-07147
Work Order
UUISO
2
Analysis Code
Run
01
-t
LCS
Login
CPM
Client
ID
Sample
Desc
Sample
Aliquot
Sample
Date
LCS
07/23/13 00:00
1.0000E+OO
07/23/13 00:00
1.0000E+OO
07/16/13 12:34
2.5000E-01
..
02
MBL
BLANK
i
Date Received I
7/22/2013
03
DUP
PZ-304-AS TOT
41
8/13/2013
12
DO
PZ-304-AS TOT
41
07/16/13 12:34
2.5000E-01
TRG
PZ-304-AS DIS
41
07/16/13 12:34
2.5000E-01
Lab Deadline

Project I
13
West Lake OU-1
Report Level
Activity Units
pCi
Aliquot Units
Matrix
Method
WA
HASL 300, 4.5.2

.
Instrument Type
---
Alpha Spectroscopy
-
Radiometric Tracer
U-232
Radiometric Sol#
U-10a
Tracer Act (dpm/g)
19.04
Carrier
..
--
l>i1~
I'\)
~~~
ijl!~
Eberline Services
Analysis Sheet
Printed: 811312013 6:32AM

Page 2 of 3
13-07147
UUISO
Run 2
Internal
Fraction
Sample
Desc
Tracer
Aliquot{g)
Radiometric
Tracer (pCi)
11.7
0.00
11.6
0.00
11.6
0.001
0.6034 .
11.5
0.00
0.6099
11.6
~--
. LCS
0.6134
02
MBL
0.6087
DUP
0.6070
12
DO
13
TRG
Grav Filter
Tare (g)
Radiometric I Grav Carrier

% Rec
Added {ml)
t-
01
:-o3
Tracer Total
ACT{dpm)
Grav Filter
Final{g)
GravFilter
Net(g)
Grav
%Rec
Mean
%Rec
SAF
1*
SAF
2*
~-
t
-+---r---~--~-~
1-
f-----~------~----~-------
~r----------+----------~------~--------
---+---+----- -+--------+------+----+-------+
--4
l
I;~~
t"Z!I
H-~
SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only.
--+-
Eberline Services
Analysis Sheet
Printed: 8/13/2013 6:32AM

Page 3 of 3
13-07147
UUISO
Run 2
Internal
Fraction
Sample
Desc
01
LCS
Rough Prep
Date
03
DUP
08/09/13 07:17
JWOLFE
Sep tO
Date/Time
By
SeptO
By
Sep t1
Date/Time
Sep t1
By
-------
08/09/13 07:17
MBL
-
Prep
By
-~-
02
Prep
Date
Rough Prep
r-
JWOLFE
--
I
08/09/13 07:17
JWOLFE
-----~--
12
DO
08/09/13 07:17
JWOLFE
13
TRG
08/09/13 07:17
JWOLFE
i
I
I
i
-~-----
i
I
I
I
I
I
I
---.-~-
--
I
I
!
--
I
I
~~~~
il'>,jl
~
r-.::n
Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
Eberline Services
Lab
Fraction
01
Sample
Nuclide
U-234
&
U-234
MBL
03
U-234
DUP
.!!!
en
::l
::l
12
U-234
13
U-234
RPD
MDA
Blank
Flag
Flag
Flag
85.66
OK
LCS
pCi/1
7.03E+OO
9.87E-01
8.28E-02
BLANK
pCi/1
1.92E-01
1.13E-01
9.87E-02
PZ-304-AS TOT
pCI/1
5.94E-01
6.83E-01
8.93E-01
PZ-304-AS TOT
pCi/1
4.56E-01
6.87E-01
1.11E+OO
j_
PZ-304-AS DIS
pCi/1
1.27E+OO
9.10E-01
8.91E-01
Results
Error Estimate
MDA
8.20E+OO
OK
1--
.g
LCS
Flag
Activity
Units
LCS
02
LCS
%R
LCS
Known
Client
Identification
Oesc
-~-
Printed: 8/13/2013 12:56 PM
Page 1 of 3
+~~
OK
NA
OK
OK
INV
OK
---~-
---
---~--
_J
-----
1-----
I
~~---
.5
~
0
Q.
Q.
--==1
-------
~~-~---
r-
:l
Cl)
- -
1:
Q)
~I
E
Q)
---
Ol
Ill
1:
Ill
:e
Ol
1:
;:
Q)
Q)
1:
g.,
--
1:
w
tit:ll
I'''~
~~
~,;;,11
-----
--
Eberline Services
Lab
Sample
Aliquot
Radiometric
%Rec
Grav
%Rec
Mean
%Rec
Nuclide
Sample
Desc
Sample
Date
01
U-234
LCS
07/23/13 00:00
1.00E+OO
115.92
0.00
0.00
02
_______ -----
U-234
MBL
07/23/13 00:00
1.00E+OO
115.72
0.00
0.00
U-234
DUP
07/16/13 12:34
2.50E-01
36.47
0.00
0.00
DO
07/16/13 12:34
2.50E-01
31.56
0.00
0.00
TRG
07/16/13 12:34
2.50E-01
43.25
0.00
0.00
Fraction
Printed: 8/13/2013 12:56 PM
Page 2 of 3
Sep to
Date/Time
SAF
Sept1
Date/Time
------
0::
1--
--
.g
0
.!/!
"'
c:
"'(
--~---------------
03
----------
--
12
U-234
--
-en
::J
::J
--
13
U-234
----
----------
r--~-------
f-------
------------~-
r-------- -
- - - - - -----
---
c.i
.5
~
0
c.
c.
II)
i:
--r
-------
c
Ql
E
Ql
Cl
ftl
ftl
:e
---- ----
I
f-------+-----
r-~-l----I
t,t~
#~gliu
----+ ---
r----~---r-
~~:~
f\~
---~-------
- ~-----+----::I
------~
-----------t
I
---~-------:
La~
Nuclide
01
U-234
Fractoon
03=t
~ ~0 l13~-
:::~
a::
12

I
Count~ng
Sample
Desc
Date/Tome
LCS
08/13/13 09:05
~2---- U-234---1-~~--;:---1----
c::
:::J
~ ~I
U-234
I DUP
U-234
U-234
Printed: 8/13/2013 12:56 PM
Page 3 of 3
Eberline Services
TRG
08/13/13 09:05
Halflife
(days)
I
I
08/13/13 09:06
08/13/1309:06
08113/13 . .,..
Detect
Carrier
C~unt
Tome
Counts
Bkg
CPM
Eff
A_Spec
IA1pha_019I
17015.09 E+02
10.00 E+OO
16.6
A_Spec
/Alpha_0221
17011.28 E+01
17.00 E-03
A_Spec
IA1pha_0231
17013.49 E+OO
13.00 E-03
A_Spec
IA1pha_024I
170I2.32E+OO
I4.00E-03
17.1
A_Spec
IA1ph_025I
17018.98 E+OO
16.00 E-03
17.4
15.3
17.1
[-I--~-~-1~-1-----+
1--------
+-
~~
1-------+-
----t-----1
.5
t!
0
a.
a.
:I
(/)
....
c
Gl
E
Gl
0)
ns
c
ns
::!E
1-------+-- -
+----------+-------+------+------+---+-----+----+---------1
1---t--
0)
-~
I 1--------t-
-l
Gl
-~
w
t~~
f',,.~
tit~
~;.J"il
I 1------------+---
-+ ~-----t---
Lab
Desc
Client
Identification
Activity
Units
Sample
Nuclide
Fraction
Printed: 8/13/2013 12:56 PM
Page 1 of 3
Eberline Services
Results
Error Estimate
MDA
01
U-238
LCS
LCS
pCi/1
8.61E+OO
1.16E+OO
7.21E-02
02
U-238
MBL
BLANK
pCi/1
8.70E-02
7.25E-02
6.23E-02
LCS
Known
7.99E+OO
LCS
%R
LCS
Flag
107.70
OK
RPD
Flag
MDA
Flag
Blank
Flag
OK
--
c:
&!
OK
OK
-- 1----
-------- 1---
03
U-238
DUP
PZ-304-AS TOT
pCi/1
-1.73E-01
3.61E-01
1.07E+OO
12
U-238
DO
PZ-304-AS TOT
pCi/1
4.54E-01
6.84E-01
1.10E+OO
NA
INV
------------
.g
c3
.~
13
(/)
::J
::J
INV
-1----
1-- .
PZ-304-AS DIS
TRG
U-238
pCi/1
5.40E-01
5.62E-01
5.88E-01
OK
-----
-----
-- -
---
--~-
---------~
1---
~-
---
.E
- -
-~---
Q.
Q.
-----~
:s
r---
U)
c:
.9!
c
E
Ql
--
Ql
Cl
ns
ns
::::E
Cl
;:
Ql
Ql
----~~----
---
- - 1--
a,
c
w
~~:~
I'~)
---------- - - - - - - - - 1----
~---------
Eberline Services
Lab
Fraction
11::
-~-~~--
12
~
.,
::J
::J
c::
C(
r-----~------
en
LCS
07/23/13 00:00
1.00E+OO
115.92
0.00
0.00
MBL
07/23/13 00:00
1.00E+OO
115.72
0.00
0.00
U-238
DUP
07/16/13 12:34
2.50E-01
36.47
0.00
0.00
U-238
DO
07/16/13 12:34
2.50E-01
31.56
0.00
0.00
07/16/13 12:34
2.50E-01
43.25
0.00
0.00
U-238
~-
----~---
03
.g
8
Sample
Date
13
Radiometric
o/o Rec
Mean
%Rec
Sep tO
Date/Time
SAF
----
--------
------------------- [---
U-238
TRG
f-----
----------------
-------
-----~ --~----+---
-------
t---
~~=-=t=
------~- -- -+
=-=~==-r
----1-------t
-----
1---------
~--~~-
d
.E
t!
0
Cl.
Cl.
::II
-
---1-- .... -~
Cl)
c
E
Ql
.!!!
(j
Ql
0"1
----~-
-------------
nl
nl
:E
- - - r--------~--
0"1
;::
------
Ql
Ql
c
c
w
c,
~-----
- - L____________
~;~
~"~
J!lr~
"l<lllt~
Sept1
Date/Time
----------~-
02
-----
.!/l
t---
Sample
Aliquot
Grav
'IoRee
Sample
Desc
U-238
-~
Nuclide
01
Printed: 8/13/2013 12:56 PM
Page 2 of 3
L__
~
1:
~~
Lab
Fraction
Nuclide
Sample
Desc
01
U-238
LCS
U-238
MBL
U-238
DUP
02
N
~----~-
03
Printed: 8/13/2013 12:56 PM
Page 3 of 3
Eberline Services
Counting
Date/Time
Halflife
(days)
Detect
Carrier
Count
Time
Counts
Bkg
CPM
Eff
08/13/13 09:05
A_Spec
Alpha_019
170 6.26 E+02
3.00 E-03
16.6
08/13113 09:05
A_Spec
Alpha_022
170 5.83 E+OO
1.00 E-03
15.3
A_Spec
Alpha_023
170 -1.02 E+OO
6.00 E-03
17.1
08/13/13 09:06
A_Spec
Alpha_024
170 2.32 E+OO
4.00 E-03
17.1
08/13/13 09:06
A_Spec
Alpha_025
170 3.83 E+OO
1.00 E-03
17.4
~~------~--~-~t---------~--------t
08/13/13 09:06
-~
---
.g
8
.!Q
12
U-238
DO
en
-
13
U-238
TRG
------- 1--
----
::::l
::::l
-
-~
-~
1---------
--------------
1---
- r----
1--
t----
c.i
.5
- 1---
t:
0
Q.
Q.
1-------- 1---~~~---
----~
~~----
::s
...c
U)
-----
-~
ell
1:1
0~I
r----------
ell
Cl
1-------- -
-- - - - - - - - - - - - - -
CG
CG
:IE
-----~
c___
- t----
Cl
ell
ell
.5
Cl
c
w
f--
1------
---- t----
----
~~!!!
Eberline Services
Printed: 8/13/2013 12:56 PM
Page 1 of 3
Lab
Fraction
.
Nuclide
Sample
Desc
Client
Identification
01
U-235
LCS
LCS
U-235
MBL
U-235
II
Activity
Units
Results
.
Error Estimate
MDA
LCS
Known
LCS
%R
LCS
Flag
RPD
Flag
MDA
Flag
pCi/1
9.54E-01
2.73E-01
1.02E-01
OK
BLANK
pCi/1
6.41E-02
8.34E-02
1.31E-01
OK
DUP
PZ-304-AS TOT
pCi/1
4.87E-01
7.32E-01
1.18E+OO
Blank
Flag
f----------
02
03
NA
INV
----~-1----------------
.!!l
en
:J
:J
OK
12
U-235
DO
PZ-304-AS TOT
pCi/1
7.23E-01
9.82E-01
1.53E+OO
INV
13
U-235
TRG
PZ-304-AS DIS
pCi/1
3.49E-01
5.95E-01
1.05E+OO
INV
----~ ~---~---------
'
+-
--
1-----~--------------~---t-----J------------t-------+----+-----+----+-----+---+----+-----i-----f--------l
~-~--r--------------~---+-------------~-j------+------j----+----~----~---+---~-----+---~-----j
1-----
-~~-
-+---~--------------------~------4------4------~-----~----~----~-----+-----+-----+--------
c.i
.5
- - -----------
--~r----
c..
c..
--
--~----t----J------------+------+----1-----+-~--+---+----+----+------,I----+------l
:I
en
.....
c
Q)
~I
E
Q)
Cl
ns
c
ns
:E
Cl
c
;:
Q)
Q)
c
a,
c
w
11::!~1
11\:ll
~lf!li
~j(jl
1-------+--------~--~----
r---t--~--
f-----r-- ---r
+----+---+----+--~----+---t---+---+---+----1-------l
I
~--~
-~
-f- ~
I
Eberline Services
Oesc
Sample
Date
U-235
LCS
07/23/13 00:00
U-235
I MBL
Lab
Fraction
Nuclide
01
Printed: 8/13/2013 12:56 PM
Page 2 of 3
Sample
Sample
Aliquot
Radiometric
%Rec
Grav
'IoRee
Mean
%Rec
1.00E+OOI
115.921
0.001
0.00
1.00E+OOI
115.721
0.001
0.00
2.50E-011
36.471
0.001
0.00
2.50E-011
31.561
0.001
0.00
2.50E-011
43.251
0.001
0.00
SAF
Sep tO
DatefTime
I
I
Sept1
Date/Time
~------
a:
u
.!!!
~
IV
c:
"(
02 I
.~~i- ~:;;: --G::
t
13-l . ---
en
U-235
TRG
07/23/13 00:00
07/16/13 12:34
07/16/13 12:34
07/16/13 12:34
::J
::J
---------+-----+-----------------+---------~---------+-----------b----------1-------4------------------r----------------~
t-------+--------+----t--
I
c..i
.E
c.
c.
-+
-------+----
:I
II)
c:
.sa
0
....r::
E
Cl)
C)
cu
cu
r::
::i
C)
r::
;::
Cl)
Cl)
=r::
C)
w
t::!~
1\'>,:Ji
~"""'
~~'
t------1
Cl)
:~3~- __-j_-1~=-~ ~+=r~-t--+--t-+------t====l

---r-!---+--__J
-r---t----------____j______---+----

a:
-----
~
.!!!
~
<II
I:
<;(
Nuclide
Sample
Desc
Counting
Date/Time
01
U-235
LCS
U-235
12
Halflife
(days)
Count
Time
Bkg
CPM
Counts
Eft
Detect
Carrier
08/13/13 09:05
A_Spec
Alpha_019
170 5.60 E+01
0.00 E+OO
16.6
MBL
08/13/13 09:05
A_Spec
Alpha_022
170 3.47 E+OO
9.00 E-03
15.3
U-235
DUP
08/13/13 09:06
A_Spec
Alpha_023
170 2.32 E+OO
4.00 E-03
17.1
U-235
DO
08/13/13 09:06
A_Spec
Alpha_024
170 2.98 E+OO
6.00 E-03
17.1
TRG
08/13/13 09:06
A_Spec
Alpha_025
170 2.00 E+OO
0.00 E+OO
17.4
en ~
-
::l
::l
Lab
Fraction
=~:I-
Printed: 8/13/2013 12:56 PM
Page 3 of 3
Eberline Services
.... U-235
~~~~
----~~~----
---t
--~~----r
---
--~-
t.i
.E
~
0
Q.
Q.
::J
-~~----~
~----L
(/)
c:
~----
Cll
1:
~
(.,)
Cll
Cl
10
c:
10
:i
-~--~
~-~
Cl
c:
;::
Cll
Cll
.5
Cl
c:
w
Gil~~
r',ll
~
.....
~M~
~----~
t-~
Count Room Report

13-07147-UUIS0-2 (pCi/1) in
Tracer 10: U-1 Oa
Printed: 811312013 6:32AM

Page 1 of 1
/l'
Internal
Fraction
~,
'\..~
()
Sample
Desc
01
r------
i LCS
02
MBL
ho
'c-
~
LCS
H-~~
0
Sample
Aliquot
Tracer
ACT(dpm)
Radiometric
Tracer (pCi)
IRadiometric
,
%Rec
0.6134
11.6791
0.00
07/23/13 00:00
1.0000
0.6087
11.5896
0.00
PZ-304-AS T0!-~~16/13 12:34
0.2500
0.6070
11.5573
0.00
PZ-304-AS TOT
0.2500
0.6034
11.4887
0.00
0.6099
11.6125
0.00
07/16/13 12:34
---
~-
PZ-304-AS DIS
I TRG
Tracer
Aliquot(g)
1.0000
I,
~-
Sample
Date
i 07/23/13 00:00
--
BLANK
13
Client
ID
07/16/13 12:34
0.2500
-- -t
___L
----t-~--
--
I
--
i
\
I
I
I
..L
I
~lel
1\J
'"'""'
I'IJ!
II
II
SAF
1*
SAF
2*
Eberline Services
Page 1 of 1
Printed: 8/9/2013 7:17AM
JWOLFE
Sol#
U-8a
U-8a
I
I
Activity
dpmlg
Solution
Date
Volume
Used(g)
Approx
Addition
Volume
Used(g)
35.240
8/9/2013
0.500
0.5167 . ';.
34.350
8/9/2013
0.500
0.51-67
',:
Activity
dpm/g
Solution
Date
Volume
Used(g)
Approx
Addition
Isotope
Sol#
01
U-232
U-10a
19.040
8/9/2013
0.6134
0.6300
02
U-232
U-10a
19.040
8/9/2013
0.6087
0.6300
03
U-232
U-10a
19.040
8/9/2013
0,6070
0.6300
12
U-232
U-10a
19.040
8/9/2013
0.6034
0.6300
13
U-232
U-10a
19.040
8/9/2013
0.6099
0.6300
..
t~~
!~<-"'
(.yi
Version 2.0 08/99
~-
MS
u::~
Known
pCi
Error
Estimate
Added
pCi
-.J~
8.20
0.295
0.00
0.000
7.99
0.288
0.00
0.000
_L
;.
-----
Tracer
MSD
LCSO
Error
Estimate
Known
pCi
I Estimate
Error
00~+
o.oo,
Added
pCi
I Estimate
E"or
0.000
0.~~--0~-~00
0.000
0.00.
li
Balance Pri.'nter "fa pes
fraction
MSD
Volume
Used(g)
"'fracers
...
W,,)
'.
LCSD
Volume
Used(g}
LCS
Matrix Spike
0.000
Eberline Analytical
Printed: 8/9/2013 7:17AM
Page 1 of 1
Aliquot Worksheet
JWOLFE
Lab
Fraction
01
02
03
12
13
ClientiD
LCS
BLANK
PZ-304-AS TOT
PZ-304-AS TOT
PZ-304-AS DIS
~~
Sample
Type
LCS
MBL
DUP
DO
TRG
Dilution Data
Muffle Data
Ratio
PO$tiPre
Aliquot Data
No of Oils
Oil Factor
Aliquot
R~tio
~ ~ ~ ~ ..
~ ~~ ~..
.~
1 ~DOOOE+OO
1.0000E+OO
2.5000E-01
2.5000E-01
2.5000E-01
~~
....
~
~~
;~
~~
~_,
..
NetEquiv
1.0000E+OO
1.0000E+OO
2.5000E-01
2.5000E-01
2.5000E-01
Aliquot
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Sample Description:
Spectrum File:
Sample Geometry:
SPIKE
1307147B-UU
01
Shelf 2
u iso
Detector Name:
Alpha_019

19
Env. Background:
System Bkgd 64773

Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:
1.000E+000 +I- O.OOOE+OOO liter

8/13/2013
7:05:52 AM
8/13/2013
9:05:58 AM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-10A
0.613 mL
0.1923 +/- 0.0108
0.1659 +/- 0.0029 on 2/17/2013

1.1592 +/- 0.0684

NatU U-8A

U-238
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.256
4.722
4.414
4.153
T
Net
Pk Area
1.049880 +/-
AREA
0.079014
REPORT
Pk Area
Error %
379.66
509.00
56.00
626.49
10:45:23 AM
Ambient
Backgnd
10.06
8.70
26.42
7.83
0.34
0.00
0.00
0.51
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
6.1
36.8
3.3
33.7

Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.985
0.989
0.994
0.993
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.24E+000 +I
7.03E+000 +/
9.54E-001 +/
8.61E+000 +I
5.78E-001
9.87E-001
2.73E-001
1.16E+000
MDA
(pCi/liter
6.60E-002
8.28E-002
1.02E-001
7.21E-002
+I
+I
+I
+!
7.28E-003
9.13E-003
1.13E-002
7.95E-003
-AG
o/t0(c
215
0000066026.CNF

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1219
Sample Description:
Spectrum File:
Sample Geometry:
BLANK
1307147B-UU
02
Shelf 2
U iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_022
22
System Bkgd 64774
<not performed>
Sample Size:
Sample Date/Time:

8/13/2013
7:05:52 AM
8/13/2013
9:05:59 AM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-lOA
0.609 mL
0.1772 +/- 0.0104
0.1531 +/0.0029 on 12/15/2012
1.1572 +I- 0. 0713
0.150 MeV
PEAK
Energy
{MeV)
Nuclide
U-232
U-234
U-235
U-238
5.302
4.687
4.446
4.106
Net
Pk Area
AREA
REPORT
Pk Area
Error %
347.13
12.81
3.47
5.83
1:57:26 PM
Ambient
Backgnd
10.55
57.66
129.55
82.55
1. 87
1.19
1. 53
0.17
Reagent
Backgnd
FWHM
{keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
25.3
0.0
3.1
3.1

Nuclide
Id
Con.
Energy
{keV)
U-232
U-234
U-235
U-238
1. 000
0.961
0.974
0.957
5302.50*
4761.50*
4385.50*
4184.40*
Activity
{pCi/liter )
5.20E+000
1.92E-001
6.41E-002
8.70E-002
+I+!+!+I-
5.97E-001
1.13E-001
8.34E-002
7.25E-002
~3(0
MDA
{pCi/liter
1.13E- 001
9.87E-002
1.31E-001
6.23E-002
+I+I+I+!-
1.30E-002
1.13E-002
1. 51E- 002
7.14E-003
0000066027.CNF

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8/13/2013
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6223
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801:
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!224
Sample Description:
Spectrum File:
Sample Geometry:
PZ-304-AS TOT-DUP
1307147B-UU
03
Shelf 2
u iso
Detector Name:
Alpha_023

23
Env. Background:
System Bkgd 64775

Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:
2.500E-001 +/- O.OOOE+OOO liter

7/16/2013
7:05:52 AM
8/13/2013
9:06:00 AM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-lOA
0.607 mL
0.0624 +/- 0.0058
0.1710 +/- 0.0030 on 7/20/2013

0.3647 +/- 0.0347
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
Net
Pk Area
AREA
6:18:25 PM
REPORT
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
FWHM
(keV)
0.17
0.51
0.68
1. 02
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
-------------------------------------------------------------------------------U-232
U-234
U-235
U-238
5.283
4.782
4.430
4.132
121.83
3.49
2.32
-1.02
17.77
113.53
149.12
208.15
13.9
3.1
3.1
0.0

Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.997
0.997
0.986
0.980
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
2.08E+001
5.94E-001
4.87E-001
-1. 73E-001
+I
+I
+!
+!
3.81E+000
6.83E-001
7.32E-001
3.61E-001
AG
<6((31 (3
MDA
(pCi/liter
7.11E-001
8.93E-001
1.18E+000
1.07E+000
+!
+I
+I
+I
1.30E-001
1. 64E- 001
2.17E-001
1.96E-001
0000066028.CNF

1 3403.0(kev)
Start:
Stop : 1024 6588.3(kev)
Acq. Start Tue Aug 13 09:06:00 2013
60+
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---------
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m2
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Sample Description:
Spectrum File:
Sample Geometry:
PZ-304-AS TOT
1307147B-UU
12
Shelf 2
U iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_024
24
System Bkgd 64776
<not performed>
Sample Size:
Sample Date/Time:
2.500E-001 +/
O.OOOE+OOO liter
7/16/2013
7:05:52 AM
8/13/2013
9:06:01 AM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-10A
0.603 mL
0.0540 +/
0.0055
0.0032 on 12/15/2012
0.1710 +/
0.3156 +/
0.0324
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.283
4.685
4.418
4.098
T
Net
Pk Area
AREA
REPORT
Pk Area
Error %
104.81
2.32
2.98
2.32
2:02:15 PM
19.27
149.12
134.36
149.12
Ambient
Backgnd
1.19
0.68
1. 02
0.68
Reagent
Backgnd
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
5.4
3.1
3.1
3.1

Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.997
0.959
0.992
0.948
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
2.06E+001
4.56E-001
7.23E-001
4.54E-001
+1
+1
+1
+1
4.08E+000
6.87E-001
9.82E-001
6.84E-001
MDA
(pCi/liter
1.30E+000
1.11E+000
1.53E+000
1.10E+000
+1
+I
+I
+I
2.57E-001
2.20E-001
3.03E-001
2.19E-001
A-G
<t/rJ(a
S2
0000066029.CNF

start:
1 3411.6(kev)
Stop : 1024 6597 .O(keV)
Acq. Start rue Aug 13 09:06:01 2013
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!(,.,)
.....
ROI Type: 1
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Energy(kev)
5500
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Channel Data Report
8/13/2013
Page
12:08:05 PM
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8233
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0
Sample Description:
Spectrum File:
Sample Geometry:
PZ-304-AS DIS
1307147B-UU
13
Shelf 2
u iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_025
25
System Bkgd 64777
<not performed>
Sample Size:
Sample Date/Time:
2.500E-001 +/ O.OOOE+OOO liter

7/16/2013
7:05:52 AM
8/13/2013
9:06:02 AM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-10A
0.610 mL
0.0751 +/ 0.0064
0.1736 +/ 0.0032 on 12/15/2012
0.4325 +/ 0.0380
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.266
4.740
4.438
4.167
Net
Pk Area
AREA
REPORT
Pk Area
Error %
147.32
8.98
2.00
3.83
1:57:27 PM
16.19
69.62
169.74
102.72
Ambient
Backgnd
Reagent
Backgnd
FWHM
(keV)
0.68
1. 02
0.00
0.17
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
11.8
4.7
3.1
3.1

Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.991
0.997
0.980
0.998
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
2.09E+001
1.27E+000
3.49E-001
5.40E-001
+I
+I
+1
+!
3.51E+000
9.10E-001
5.95E-001
5.62E-001
MDA
(pCi/liter
7.99E-001
8.91E-001
1.05E+000
5.88E-001
+I
+I
+I
+I
1.34E-001
1.50E-001
1.76E-001
9.88E-002
AC4
<t/rJf3
8235
0000066030.CNF

1 3405. 9(kev)
Start:
Stop : 1024 6615. S(kev)
60+
55
50
45
40
35
Vl
.f-J
s::::
::::l
8 30
25
20
15
10
5
0
3500
4000
4500
N
t..~
ROI Type: 1
5000
Energy(kev)
5500
6000
ROI Type: 3
6500
Channel Data Report
8/13/2013
Page
12:08:14 PM
*******************************************************
*****
*******************************************************
Sample Title:
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8239
Page 1 of 2
8/13/2013 5:41:01 AM
QA SUMMARY REPORT
Date
Time
: 8/13/2013
: 5:41 :01 AM
CHAMBER
Alpha 001
Alpha 002
AfiJ_ha 003
Alpha 004
Alpha 005
Alpha 006
Alpha 007
Alpha 008
Alpha 009
Alpha 010
Alpha 011
Alpha 012
Alpha 013
Alpha 014
Alpha 015
Alpha 016
Alpha 017
Alpha 018
Alpha 019
Alpha 020
Alpha 021
Alpha 022
Alpha 023
Alpha 024
Alpha 025
Alpha 026
Alpha 027
Alpha 028
Alpha 029
Alpha 030
Alpha 031
AfiJ_ha 032
Alpha 033
Alpha 034
Alpha 035
Alpha 036
Alpha 037
Alpha 038
Alpha 039
Alpha 040
Alpha 041
Alpha 042
DEVICE
21f
21f
21f
21f
21f
21f
21f
21f
21f
21f
21f
21f
21f
21f
21f
21f
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
Alpha AnalystlOODC
AlQha AnalystlOODC
AlQha AnalystlOODC
Alpha Analyst! OODC
Alpha AnalystlOODC
AlQ_ha AnalystlOODC
Alpha Analyst I OODC
Alpha AnalystlOODC
Alpha Analyst! OODC
Alpha Analyst 1OODC
PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
Peak Energy
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
FLAG
Not Done
Not Done
Passed
Passed
Not Done
Not Done
Not Done
Not Done
Not Done
Passed
Passed
Passed
Passed
Passed
Action
Not Done
Not Done
Passed
Passed
Not Done
Not Done
Passed
Passed
Passed
Passed
Not Done
Passed
Not Done
Passed
Not Done
Passed
Not Done
Passed
Passed
Passed
Passed
Passed
Passed
Passed
Passed
Passed
Passed
DATE
8/13/2013 5:25:16 AM
8/13/2013 5:25:17 AM
8/13/2013
8113/2013
8/13/2013
8/13/2013
8113/2013
8/13/2013
5:25:18 AM
5:25:18 AM
5:25:19 AM
5:25:20 AM
5:25:21 AM
5:25:22 AM
8/10/2013 11:23:01 AM
8/13/2013 5:25:22 AM
8/13/2013
8/13/2013
8/13/2013
8/13/2013
5:25:23 AM
5:25:24 AM
5:25:25 AM
5:25:26 AM
8/13/2013 5:25:26 AM
8113/2013 5:25:27 AM
8/13/2013 5:25:28 AM
8/13/2013
8113/2013
8/13/2013
8/13/2013
8/13/2013
8113/2013
8/13/2013
8/13/2013
8/13/2013
8113/2013
5:25:29 AM
5:25:30 AM
5:25:31 AM
5:25:33 AM
5:25:34 AM
5:25:35 AM
5:25:37 AM
5:25:38 AM
5:25:40 AM
5:25:41 AM
Page 2 of 2

8/13/2013 5:41 :01 AM
CHAMBER
Alpha 043
Alpha 044
Alpha 045
Alpha 046
Alpha 047
Alpha 048
DEVICE
Alpha AnalystlOODC
Alpha Analystl OODC
Alpha Analyst100DC
Alpha AnalystlOODC
Alpha Analyst100DC
Alpha Analyst100DC
PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
FLAG
Passed
Passed
Passed
Passed
Passed
Passed
DATE
8/13/2013 5:25:42 AM
8/13/2013 5:25:44 AM
8/13/2013 5:25:46 AM
8/13/2013 5:25:47 AM
8113/2013 5:25:49 AM
8/13/2013 5:25:50 AM
APPROVED BY:
APPROVAL DATE:
1:2:41
6/12/12
Page
12:17:04 PM
*************************************************************************
*****
*****
*************************************************************************
Uranium
U-232,-234,-235,-238

Nuclide
Name
Half-Life
(Seconds)
U-232
U-234
U-235
U-238
2.174E+009
7.731E+012
2.221E+016
1.410E+017
Energy
Uncert. (keV
Energy
(keV )
0.000
0.000
0.000
0.000
5302.500*
4761.500*
4385.500*
4184.400*
* = key line
TOTALS:
Nuclides
Energy Lines
Yield
( %)
99.8000
99.8000
80.9000
100.2300
Yield
Uncert. (Abs. +-)
0.0000
0.0000
0.0000
0.0000
SECTION IX
ANALYTICAL DATA (ISOTOPIC THORIUM)
&243
Eberline Services
Oak Ridge laboratory
Analysis Sheet
Printed: 81912013 6:54AM

Page 1 of3
13-07147
ThiSO
Run 1
13-07147
Work Order
Analysis Code
ThiSO
Run
7/22/2013
Lab Deadline I
8/13/2013
Date Received
Internal i Sample
Fraction . Desc
01
02
r-------
03
i LCS
I MBL
I
I
Client
ID
LCS
Login
CPM
Sample
Date
I
I
07/23/13 00:00
BLANK
Sample
Aliquot
1.0000E+OO
07/23/13 00:00
1.0000E+OO
--------
DUP
D-12 TOT
46
07/15/13 15:27
1.0000E+OO
--
04
DO
D-12 TOT
46
07/15/13 15:27
05
TRG
D-12 DIS
46
07/15/13 15:27
1.0000E+OO
1.0000E+OO
-
Project I
West Lake OU-1
06
TRG
DUP05 TOT
45
07/15/13 00:00
1.0000E+OO
Report Level
07
TRG
DUP05 DIS
45
07/15/13 00:00
1.0000E+OO
Activity Units
pCi
08
TRG
PZ-208-SS TOT
43
07/16/13 09:25
1.0000E+OO
09
TRG
PZ-208-SS DIS
43
07/16/13 09:25
1.0000E+OO
TRG
PZ-304-AI TOT
46
07/16/13 12:05
--~
Aliquot Units
WA
10
HASL 300, 4.5.2
11
TRG
PZ-304-AI DIS
46
07/16/13 12:05
1.0000E+OO
Alpha Spectroscopy
12
TRG
PZ-304-AS TOT
41
07/16/13 12:34
1.0000E+OO
Radiometric Tracer
Th-229
13
TRG
PZ-304-AS DIS
41
07/16/13 12:34
1.0000E+OO
Radiometric Sol#
Th-18a
14
TRG
MW-104 TOT
41
07/16/13 13:25 !
1.0000E+OO
Tracer Act (dpm/g)
22.466
15
TRG
MW-104 DIS
41
07/16/13 13:25
1.0000E+OO
Matrix
Method
Instrument Type
1.0000E+OO
Carrier
16
TRG
PZ-204A-SS TOT
40
07/16/13 13:56
1.0000E+OO
17
TRG
PZ-204A-SS DIS
40
07/16/13 13:56
1.0000E+OO
-------
18
19
TRG
PZ-302-AI TOT
44
07/16/13 15:18
1.0000E+OO
TRG
PZ-302-AI DIS
44
07/16/13 15:18
1.0000E+OO
til~~~
II',J!
~:c.
,~::~
..
Eberline Services
Analysis Sheet
Printed: 81912013 6:54AM

Page 2 of3
13-07147
ThiSO
Run 1
Internal j Sample
Fraction , Desc
LCS
01
Tracer
Aliquot(g)
03
, DUP
Radiometric
Tracer (pCi)
I Radiometric
I
%Rec
0.4801
10.~
0.2401
5.4
0.00
0.2373
5.3
0.00
0.2358
5.3
0.00
--
' _o: I ::~
Tracer Total
ACT(dpm)
Grav Carrier
Added(ml)
Grav Filter
Tare (g)
Grav Filter
Final(g)
Grav Filter
Net (g)
I
1
0.00
Mean
%Rec
Grav
% Rec
SAF
1*
SAF
2*
I
I
04
DO
--
05
I TRG
0.2356
5.3
TRG
0.2368
5.3
0.00
TRG
0.2341
5.3
0.00
---
0.00
Ii
---
06
f-------
07
TRG
08
'
i
!
0.2345
5.3
0.00
I
----
09
TRG
0.2353
5.3
0.00
10
TRG
0.2354
5.3
0.00
11
r-----------
12
TRG
0.2351
5.3
0.00
TRG
0.2332
5.2
0.00
i
I
I
-
13
TRG
0.2350
5.3
0.00
14
TRG
0.2339
5.3
0.00
15
TRG
0.2331
5.2
16
TRG
0.2340
5.3
17
TRG
0.2345
5.3
0.00
18
TRG
0.2352
5.3
0.00
19
TRG
0.2356
5.3
0.00
1
I
--
0.00
0.00
(if1!li
~"~~
4~:.,
Lllil
Eberline Services
Analysis Sheet
Printed: 8/9/2013 6:54AM

Page 3 of 3
13-07147
ThiSO
Run 1
Internal
Fraction
Sample
Desc
Rough Prep
Date
Rough Prep
By
Prep
Date
Prep
By
Sep tO
Date/Time
SeptO
By
Sep t1
Date/Time
Sep t1
By
01
!
I
LCS
08102113 08:16 I
'
JWOLFE
. -
02
MBL
08/02/13 08:161
JWOLFE
----
03
04
05
DUP
08/02/13 08:161
DO
08/02/13 08:16
TRG
08/02/13 08:16
JWOLFE
'
---~-----
JIIVOLFEl
JWOLFE
--
I
---
TRG
08/02/13 08:16
JWOLFE
JWOLFE
07
TRG
08/02/13 08:16
08
TRG
08/02/13 08:16
09
TRG
10
11
----~~
i
-
06
I
I
JWOLFE
08/02/13 08:16
JWOLFE
TRG
08/02/13 08:16
JWOLFE
TRG
08/02/13 08:16
JWOLFE
I
I
"-----
---1---------~
12
TRG
08/02/13 08:16
JWOLFE
13
TRG
08/02/13 08:16
JWOLFE
14
TRG
08/02/13 08:16
JWOLFE
15
TRG
08/02/13 08:16
JWOLFE
16
TRG
08/02/13 08:16
JWOLFE
17
TRG
08/02/13 08:16
JWOLFE
18
TRG
o8/o2/13 o8:16 I
JWOLFE
I
"------
"
---
19
TRG
08/02/13 08:16
I
JWOLFE
I
(i:J
it'.:ll
Actual mass exceeded the calibration curve range" Results should be qualified as appropriate.
Lab
Fraction
j
03~- ~-
.(!!
~
ii
c::
"(
en
-..c:
1
_
TH-2;;,
Q4
TH-228
--OS06
TH-228
08
TH-228
-t
0
c.
c.
::I
t::
Ql
i:
Ql
.S!
Cl
Ill
(3
t::
Ill
::!:
Cl
t::
'i:
Ql
Ql
.!:
Cl
t::
w
tli111!
11".:~
~:~
..
pCi/1
4.58E+OO!
7.22E-011
BLANK
pCi/1
1.19E-03
5.61E-02
----;;:;-2 TOT
pCUI
8.45E-02
1.85E-01
3.50E-01
D-12 TOT
pCi/1
1.05E-01
1.01E-01
1.22E-01
OK
D-12 DIS
pCi/1
-2.64E-021
6.54E-02
1.86E-01
OK
DUP05 TOT
pCi/1
2.92E-02
7.05E-02
1.41E-01
OK
DUP05 DIS
pCi/1
-1.75E-02
6.13E-02
1.61E-01
OK
PZ-208-SS TOT
pCi/1
2.09E-01
1.38E-01
1.14E-01
OK
7 .....21
,_,...2
7.36E-02
~0
TR~
i--:;RG
TH-228
TRG: ----
___ TH-22~---
15
TH-228
8_ J__ _ _
93.51
OK
OK
OK
1.29E-01
1.03E-01
8.68E-021
PZ-304-AI DIS
pCi/1
6.57E-02
7.80E-Ot- 1.14E-01
PZ-304-AS TOT
pCUI
2.85E.021
6.19E-021
1.22E-011
OK
PZ-304-AS DIS
pCUI
9.25E.021
9.66E-021
1.21E.011
OK
TRG
MW-104 TOT
pCi/1
7.10E-011
2.49E-01
9.47E-02I
TRG
MW-104DIS
pCi/1
2.81E-03
3.93E-02
1.12E-01
PZ-204A-SS TOT
pCi/1
3.72E-01
2.08E-01
1.47E-011
PZ-204A-S~
pCi/1
4.02E-02
6.04E-02
9.78E-02
OK
TRG
__
__
DIS
oK
OK
--1
--1
OK
1
OK
OK
OK
OK
TH-228
TRG
PZ-302-AI TOT
pCi/1
1.18E-01
9.25E-02
7.24E-02
OK
TH-228
TRG
PZ-302-AI DIS
pCi/1
-2.69E-03
3.15E-02
6.62E-02
OK
---+--------~---r
OK
NA
pCi/1
[_~?~ ~~:28 t~~~1----------1------

19
,__ -
4.89E+OOI
PZ-304-AI TOT
-:--.;H-228
1.18E-011
TRG
_'"1<:228---r
--~~ _1
.c.. ,_,...
MDA
ez-2oa-ss Dis
TH-228
IError Estimate I
I TRG
--11-t ---:;:H-2;~-- --:;~G

--~~-~~~~-TH;;-t-TR-;,1~-1
-
-16
C/)
LCS
---~-=p~
TH-228
TRG
<.i
LC~-
--~U-;
~ oil .=-,:;;:~"
1 t
.=
Activity
Units
Results
Blank
Flag
MDA
Flag
RPD
Flag
Client
Identification
~BL
-------;H-228
1------
07
LCS
Flag
LCS
%R
LCS
Known
Oesc
Sample
-~~-~----~~~~~-02
Work Order: 13-07147-ThiS0-1
Nuclide
Printed: 8/12/2013 8:47AM

Page 1 of 3
Eberline Services
Eberline Services
a::
~
0
u
.!!!
q;
Lab
Fraction
01
Sample
Desc
Nuclide
Sample
Date
~I -~H-228 --~ --~~/23/13 00:00
-~~--- --~~:~---t~~L- ~7/23/13

03
TH-228
DUP
05
-..c: --os -r
1
C/)
TH-228
TRG
rH-228
0.00
0.00
103.211
0.00
0.00
34.56
0.00
0.00
0.00
0.00
o.oo
o.oo
1.00~
1.ooe+oo[
44.04
TRG
TH-228
07/15/13 00:00
1.00E+OOi
90.78
0.00
0.00
--+
1.ooe+ool
90.941
o.ool
o.oo
1.00E+OO
94.22
0.00
0.00
1.00E+OO
83.12
0.00
0.00
09:25
-+-----+- - - - - -
TRG
07/16/13 09:25
~-228~fTRG
07/16113 ,,,..
0.00
0.00
12
TH-228
TRG
07/16/13 12:34
1.00E+OO
65.84
0.00
0.00
.E
13
TH-228
TRG
07/16/13 12:34
1.00E+OO
71.24
0.00
0.00
t::
0
14
TH-228
TRG
07/16/13 13:25
1.00E+OO
94.06
0.00
0.00
15
TH-228
TRG
07/16/13 13:25
1.00E+OO
73.83
0.00
0.00
16
TH-228
07/16/13 13:56
1.00E+OO
58.20
0.00
0.00
-
I
c:
Q)
E
Q)
"'c:
"'
Cl
c:
;::
Q)
Q)
c:
Cl
TRG
c:
TH-228
TRG
17
---- ------+-------------+------
TH-228
TRG
18
19
-----
----t
Cl
::!:
o.oo
86.31
:::1
----r=-~~~--------+--+-----------1
o.oo
1.00E+OO
(/)
73.35
07/16/13 12:05
c..
c..
Sept1
DatefTime
Sep tO
OatefTime
-~-------
1.ooe+ool
TRG
11
-
-+-
07/15/13 oo:oo
TH-228
()(~
SAF
--t------+
t--~-1
~~~
Mean
% Rec
1.00E+00+----~~4
I 1.00E+oo[
07/15/13 15:27
--01 -tT;~-QS-t---TH-228~- -T-;~- -~7~~6/13

09
i"Ji
t!!l!ll
Grav
%Rec
---t-----
TH-228
07/15/13 15:27
Radiometric
% Rec
'
___
...c:
00:00
Sample
Aliquot
:o.;__[-~":,,.--1-;; ~;,~,,;~;;-1 ,.;,-r---~4.88
Printed: 8/12/2013 8:47AM
Page 2 of 3
TH-228
TRGJ
-~------ --------~--
07/16/13 13:56
1.00E+OO
82.16
0.00
0.00
07/16/13 15:18
1.00E+OO I
87.62
0.00
0.00
1.ooE+oo\
94.15
0.00
0.00
07/16/13 15:18
----------
-+
-----+----------~
(
~
TSample
TH-228
I LCS
08/10/1314:55
~~~~~;--~!~-;~
I
!
01
02
Nuclide
Lab
Fraction
"""""
TH-228
------
8
.!!,!
~
;;
c:
"(
I DUP
I
DO
Count
Time
~~228 ~
05
en
Alpha_OO~
170~3.54 E+02
,1.90 E-02
17.5
08/10/1314:55
A_Spec
Alpha_Oo4G-7o.o2[8.97 E-02
12.30 E-02
19.4
08/10/13 14:55
A_Spec
Alpha_010
1.70 E-02
19.7
170 2.11 E+OO
CPM
08/10/13 14:55
A_Spec
Alpha_011
17015.15 E+OO
5.00 E-03
A_Spec
Alpha_012
1701-8.50 E-01
5.00 E-03
TRG
08/10/1314:55
A_Spec
Alpha_od
17011.47 E+OO
19.00 E-03
18.7
TRG
08/10/13 14:55
A_Spec
Alpha_014
~-:_~i _j -~-~~~~~-----~-;~~
08/10/1314:55
A_Spec
Alpha_015
17011.03 E+01
koo E-03
08/10/13 15:01
A_Spec
Alpha_033
17015.49 E+OO
3.00 E-03
~~07
_ --~~_:~_J
I
__ 12__ J_ ____
c..
c..
:I
...
en
c
Q)
1:
E
Q)
Cl
Cll
c
Cll
::!!:
Cl
;:
Q)
Q)
TH-228
TH-228
1 TRG
I TRG
1s--- --~~~;28 ----~-TRG-
---16~~-- ---~~-22-8~--17--~~----;H~;-;8-~
14.8
18.5
Alpha_034
170 5.83 E<OO
11.00 E-03
18.6 -I
08/10/1315:02
A_Spec
Alpha_035
170 3.81 E+OO
17.00 E-03
18.3
A_Spec
1Aipha_036I
17011.32 E+OO
14.00 E-03
19.1
A_Spec
Alpha_037
17014.32 E+OO
14.00 E-03
17.8
A_Spec
Alpha_038
170 4.23 E+01
4.00 E-03
17.2
A_spec
Alpha_o39
110 1.50 E-01
5.oo E-03
19.7
-~
A_Spoe
Alph'-040
170 1.51 E<01
5.00 E-03
19
-I
A_Spec
jAipha_0451
17012.32 E+OO
14.00 E-03
19.1
A._Sp"
IAIPh'-04<1
17016.83 E<
11.00 E-03
17.9
A_Spec
1Aipha_0471
170j1.70 E-01
11.00 E-03
18.2
_-c-_
08/10/13 15:02
08/10/13 15:02
08110113 16o02
TRG
08/10/1315:02
1----~~--J ----~~~-~-----~ TRG
18.5
A._Spo<
TRG
~1~_:_l~i"="--~l TRG
r~:~-=~-----1-TRG_ -~~~~~1315:~-~
TH-228
170.0211.08 E+OO ,2.40 E-02
08/1011315o02
1----~-~--t _--~H--~:~----+--~R~ ----0~/10/13 15:02

14
~--
--
_.8/1011316o02___f
08/10/1315:02
+
I
Cl
c
w
t::
0
20.5
1
08/10/13 14:55
! ____
to
Counts
TRG
-..c:
<.i
.E
Eff
A_Spec
II
19.9
~~- TH-22~-- t:;;~

--~-!__
rH:2~~---J _:"~<:>__
~;JI
~:tiJo,
Bkg
Carrier
!til~
Detect
. --------------------+-------
09
.!!!
Halflife
(days)
Counting
Date/Time
Desc
~-----r--
TH-228
Printed: 8/12/2013 8:47AM

Page 3 of 3
Eberline Services
1
!
I'
Eberline Services
,:
~
.!!!
~
~
I:
q:
en
..c:
1
+-
Lab
Fraction
Nuclide
01
TH-230
02
Sample
Desc
1-===-~- -~ __
I--~-~-- --------~H-2~----~---~-~~-+04
l-05-
TH-230t--
,___
TH-230
TH-230
TH-230
Oe
TH-230
_.._o_
---
11--l
TH-230
TRG
TH-230
TRG
TH-230
TRG
MDA
Flag
Flag
Blank
Flag
S.OOE+OO
7.73E-01
8.15E-02
pCi/1
4.55E-01
1.72E-01
9.74E-02
-~---12 TOT
pCi/1
8.32E-01
4.29E-01
2.87E-01
D-12 TOT
pCi/1
5.35E-01
2.27E-01
8.33E-02
pCi/1
5.40E-01
2.81E-01
1.26E-01
pCi/1
5.36E-01
2.25E-01
9.26E-02
pCi/1
5.44E-01
2.06E-01
8.94E-02
-1
I ~
~------+
pCI/1
6.98E-01
2.68E-01
1.11E-01
Tli----1-----1--0-K-+--
pCi/1
4.27E-01
1.76E-01
9.14E-02
-r--~-~
-;;_;;-8--S-S ;OT
~G ~
TH-230
RPD
pCi/1
-~~~ -----;Z-208-SS DIS
r----1-21~--
f--
LCS
Flag
LCS
~- --.;RG___ --- --~UPOS TOT

TR~- --- ---- ---- DUPOS DIS
~R~-
LCS
%R
LCS
Known
Activity
Units
.TR~------ --- ---~~;2-D-IS-
l--08--
DO
Client
Identification
- - ~-'=-~~~
~TH~30 -1-~~~--
TH-230
Printed: 8/12/2013 8:47AM
Page 1 of 3
IError Estimate
Results
MDA
-~.46E+O~-~~--~~J
OK
~~~----~--
OK
-+--+---
I
._,....,
2.33E-01
1.03E-01
PZ-304-AI DIS
pCi/1
2.47E-01
1.35E-01
8.05E-02
pCi/1
6.44E-01
2.63E-01
1.11E-01
pCi/1
4.88E-01
2.38E-01
1.35E-01
OK
OK
--
OK
OK
OK
r: :
,c.,
-----1
OK
INV
PZ-304-AI TOT
~-------;Z-304-AS TOT
OK
OK
OK
:
1
OK
1
OK
.::
~
0
Q.
Q.
:::1
...
en
c:
Cll
~l!~l
f\Jf
(.,!'~
G:ll!
16
Cll
C)
ca
ca
c:
______
:i
-----~--23_'>____
C)
TH-230
c:
;:::
C)
c:
TRG
!~-20-~~~~ DIS_
>--
--I ---
TH-230
-t"'" - -
PZ-302-AI TOT
--~--+----~-----------
Cll
Cll
.!:
1_rR:_
_____
PZ-204A-SS TOT
_'_":'02-AI DIS
-r
X-
--
pCi/1
4.17E-011
1.82E-01
8.09E-02
pCi/1
5.93E-011
2.25E-01
1.02E-01
pCI/1
5.70E-01:
2.08E-O'>
6.46E~-----I
OK
OK
---------1
OK
-OK--+---
Lab
Fract1on
-,-----1
---~~--J___
~
---
~~-
.!!!
~
ii
c::
oq:
Sample
Desc
___
Lcs
-~H~2~~- - ___ J
t'
------~--
(.)
-t
0
c.
c.
::::s
"'
01
c:
;::
(1)
(1)
.5
01
c:
w
f.!~l
~''ll
11:.1~
...J.Ibt
17
34.56
0.00
0.00
07/15/1315:27
1.00E+ooL 44.o4[
o.oo
o.oo
: : : : : : ' :::::t__ ::::1

07/16/1312:05
1.00E+OOi
90.94
0.00
0.00
1.00E+OOf
94.22
0.00
0.00
83.12
0.00
0.00
r -~-OOE+00 1
I
----I
--------~
'
Lrf<G__
j_~~G
II TRG
1.00E+OOI
:::: ---+
- .. -
1--~~~-
'
"I
-(-~~~'
I
--1-
_j__
07/16/13 12:34
0711611313,25
07/16/13 13:56
....
1.00E+oof
58.20
o.oo
o.oo
1.00E+OO!I
82.16
0.00
0.00
1.00E+OO
87.62
0.00
0.00
94.15
0.00
0.00
I 1.00E+OO
II
--1
0.00
--------
73.83
__
- 1.00E+ool
07/16/13 13:56
07/16/1315:18
1.00E+oo[
0.00
:::
:::
TH-230
07/16/13 12:05
j'
::::~_ -tt~.;~ j:::::~: : : :- J:::~::~j - 2::!
_rH-230
TRG
07/16/13 09:25
-----j---------------------1
o.oo
--~! ----- TH-230

I
'
0.00
TRG
18+~-;_,;-~l-;..;;~0;~16/1315:18
I
0.00
o.oo
E
(1)
"'c:
103.21
65.84
-- - --
c:
:!:
0.00
I
I
0.00
07/16/13 09:25
_-------~
__J_
0.00
(1)
01
1.00E+OO
Sep 11
Date/Time
SeptO
Datemme
0.00
-
-~ 1---~~~2~~
(/)
...
~-:
. -.il
__15_ -
-I
86.31
--~~__j__ ---~H-230
c:
o.oo
64.88
---r~;~~i
-i
o.oo
SAF
1.00E+OOj
TH-230
117.53[
Mean
% Rec
07/15/13 15:27
J TH-230
TRG
---09--~---- -;~-~;~ .-t~RG
'
I 1.00E+oof
Grav
% Rec
DO
~it~::~;;--[_;~
i
Radiometric
% Rec
1.~0E~~+
.....
10-_t:--~~-~~~--
sa.mple
Ahquot
07/15/1315:27
TH-230
08
07123113 00:00
-.--. TH-230
11
07/23/13 oo:oo
MBL
~~-~~~~ _-:-~:~-;~~~~:o:~ _j
-..c:
Sample
Date
en
i ----
---~~--~.
04
Nuclide
TH-230
'
Printed: 8/12/2013 8:47AM

Page 2 of 3
Eberline Services
---1
---------1
Eberline Services
Lab
.
Fractoon
[
i
uc
I'd
1
[
'I
Sa;,~;~--Desc
~~-~-----~H-2-~~------i~--~-:_~
a::
-~~--J----p--~~=~~----+-~~-L-
--~3___ ,_________ T_H-230----+~~

04
~
0
(,)
.!!!
~
iii
1::
"(
TH-230
'
- -o6-l
1
..c:
Counting
.
Date/Tome
_
_
DO
~~~;-o-1-;R~-~
~
0
c.
c.
::s
-~=~30
__
I ~-G
Cl
s:::
;:
Q.l
Q.l
s:::
c;,
s:::
170/3.87 E+02
U11
l!">,l!
Eff
6.00 E-03
17.~
170.0~~3.43 E+01
1.00 E-02
19.4
08/10/1314:55
A_Spec
Alpha_0101
170:2.13 E+01
1.00 E-02
19.7
08/10/1314:55
A_Spec
Alpha_0111
170[2.68 E+01
08/10/13 14:55
A_spec
1Aipha_o12i
17~+o1
A_Spec
Alpha_013
17012.77 E+01
08/10/13 14:55
_L
___08/10/13
15:~J
~:::
20.5
19.9
2.00 E-03
18.7
:::
A_Spec
Alpha_033f
170 2.80 E+01
0.00 E+OO
18.5
A_Spec
Alpha_0341
170 3.60 E+01
0.00 E+OO
18.6
A_Spec
1Aipha_0351
170 1.47 E+01
2.00 E-03
18.3
I TRG
08/10/13 15:02
14
TH-230
TRG
08/10/13 15:02
A_Spec
Alpha_038
17017.00 E+01
0.00 E+OO
17.2
TH-230
TRG
08/10/13 15:02
A_Spec
1Aipha_0391
17012.53 E+01
4.00 E-03
19.7
TH-230
TRG
08/10/13 15:02
A_Spec
Alpha_04ol
17012.03 E+01
4.00 E-03
19
TH-230
TRG
--~~;~,~;~5:02
I
i
A_Spec
Alpha_045
17012.47 E+01
2.00 E-03
19.1
A_Spec
Alpha_046f
170 3.50 E+01
0.00 E+OO
17.9
A_Spec
Alpha_0471
170 3.68 E+01
1.00 E-03
18.2
15
-+-
17
------
--~--
18
TH-230
19
TH-230
TRG
08/10/13 15:02
-+
1---------+----------~+----+-------------r---
1 - - ___ j
-----1-
TRG
08/10/13 15:02
---+- ------- __________.___
--t
-+----r---
1
tl~!
Bkg
CPM
,..,)
t
oun s
TH-230
16 '
--- + -
1--------t---------
s:::
Alpha_~
1
1
1
E
Q.l
I'll
A_Spec
Count
.
Tome
13
Q.l
:2::
Alpha_004f
08/10/1315:02
----1---
Cl
I'll
arr1er
-~T- TH-2-~~12
TH-230
I TRG I 08110/1315o02
'~---------- -----~ --+
---- - - - - - - + - - - - - + - - - - - + - - - - - + - - - + - - - - + - - - - + - - - - - 1
...s:::
en
...
~
__
A_Spec
.:~~~-~~~-~-;H-230
~rr -~:=J :~~- --~~~~~;~:;~. j
I _'BJ'"~-1
----~
0 etect
08/10/13 14:55
I TRG
.E
Halflife
(days)
_o_8,_1~1: 14:55
0
en 1---os--T ---:;:H-23~~---~~~-;
1
Printed: 8/12/2013 8:47AM
Page 3 of 3
I
-
Lab
Fraction
N
uc
01
0::
-u~~u-~
03
r1d
--
-I ..
Sample
Desc
TH-232
Client
Identification
Lcs
~H-23~----~_13-~--TH-232
!!1
iii
t1~~1
M
Ul
t.1r
U)
.J:
DUP
R
It5
esu
pCi/1
I 4.93E+OO
TH-232
s.ne-02
pCi/1
6.39E-02
1.38E-01
2.67E-01
D-12 TOT
p~
1.16E-01
9.83E-02
8.31E-02
D-12 DIS
pCifl
-t---'"E-02
1.23E-01
1.81E-01
~Ci/1
I 1.71E-01
1.18E-01
8.07E-02
I -1.08E-02
3.28E-02
8.92E-02
2.53E-01
1.48E-01
8.23E-02
PZ-208-SS TOT
pCi/1
11
TH-232
TRG
PZ-304-AI DIS
pCi/1
13
TH-232
TRG
PZ-304-AS DIS
pCi/1
14 ----------
TH-232
pCi/1
15
TH-232
pCUI
TR~
c.
c.
:l
C/)
s:::
Ql
E
Ql
01
CIS
s:::
CIS
::!:
01
s:::
;::
Ql
Ql
=s:::
01
TRG
------
--~~ J ----~~~-~- .I. TRG17
18
TH-232
T.RG
-~---t--------------+-----
I TRG
TH-232
~=~T":"'
__
!-""'-
M~~104 TOT
MW-104 DIS
____
4.89E+ool
LI
10
7.92E-02
09
.E
7.05E-02
DUP05 TOT
TRG
7.63E-01
LCS
Known
8.14E-02
~- __ --~~~-~RG_ -------~-u~~s DIS-----~
MDA
---+I
.-- -:=-- :~=~=~--l : :

08
Error Estimate
pCi/1
D-12 TOT
05- - - TH-232
TRG
- -~-~---t----~~-~~--~RG
Activity
Units
----~
BLANK
---------l--------r---07 _
lI
Lcs
--<>4___ - - - -TH~;;---~~
~
0
u
Printed: 8/12/2013 8:4 7 AM
Page 1 of 3
Eberline Services
_.':_~=~~-55 TOT
PZ-204A-SS DIS
- ----------
PZ-302-AI TOT
_PZ-302-AIIliS____
pCi/1
.
I
pCi/1
I ::::::: ::::::: :::::::
LCS
1~0.65
OK
OK
OK
NA
OK
T_
OK
OK
-+
OK
1.01 E-01
9.38E-02
8.71 E-02
6.03E-01
2.22E-01
6.83E-02
4.86E-02
6.32E-02
8.73E-02
1.84E-01
1.39E-01
1.15E-01
1.15E-01
9.01E-02
7.05E-02
OK
1.52E-01
1.08E-01
1.01E-01
OK
7.20E-02
6.92E-02
7.39E-02
I_pC~
OK
pCi/1
j j
=
I I1:: I l
+--j_
7.02E-02
OK
OK
6.71E-02
OK
6.44E-02
Blank
Flag
MDA
Flag
RPD
Flag
LCS
Flag
%R
r----t
TI
I
I
I1 I I
OK
OK
-l
OK
OK
OK
Lab

I Sample
Nuclide
Fraction
01
0::
or
02
---------- .
03
u
.!(!
~
c:
<t
iij
--
04
-----------
en
c.
c.
:I
...
en
c:
Cll
Cl
Cll
res
c:
res
::E
Cl
c:
;::
Cll
Cll
c:
c,
c:
w
~~I
h:ll
~J1
J:~h
o.ooJ
64.88
0.00
0.00
1.00E+OO
44.04
0.00
1.00E+OO
73.35
0.00
1.00E+OO
90.78
0.00
1.00E+OO
90.94
0.00
1.00E+OO
94.22
0.00
07/16/13 12:05
1.00E+OO
83.12
0.00
0.00
07/16/13 12:05
1.00E+OO
86.31
0.00
0.00
07/16/13 12:34
1.00E+OO
65.84
0.00
0.00
07/16/13 12:34
1.00E+OO
71.24
0.00
0.00
07/16/13 13:25
1.00E+OO
94.06
0.00
0.00
07/16/13 13:25
1.00E+OO
73.83
0.00
0.00
34.56
1.00E+OO
07/15/13 15:27
07/15/13 00:00
07/15/13 15:27
TRG
06
TH-232
TRG
07
TH-232
TRG
07/15/13 00:00
-
-- --------.
08
TRG
07/16/13 09:25
09
TH-232
TRG
07/16/13 09:25
11
TH-232
TRG
13
TH-232
TRG
TH-232
TRG
TH-232
TRG
TH-232
TRG
-~
---
-------
----
-------
15
-----
--
I
-~--
j---
14
II
0+
--
TRG
--------
TH-232
Sep t1
Date/Time
-----------~-----
TH-232
10
SeptO
Datemme
SAF
----------
--
0.00
1.00E+OO
---------------
--
----
o.ool
103.21
07/15/13 15:27
----
c..i
0.001
1.00E+OO
--
12
Mean
%Rec
- -------
TH-232
--------- ----
.E
Grav
%Rec
o.oo/
07/23/13 00:00
DO
----- --------
05
-.J:
....
----- !--
TH-232
-----------.
DUP
--------
0.00
117.53
07/23/13 00:00
-------
TH-232
--- -------
_______ ______________
Radiometric
%Rec
---------~----
MBL
TH-232
-
--
Sample
Aliquot
1.00E+OO
LCS
TH-232
- -
Sample
Date
Oesc
--------
Printed: 8/12/2013 8:47AM
Page 2 of 3
Eberline Services
----------~-----
.. --
16
TH-232
17
TH-232
---------- - - - - - - -
TRG
07/16/13 13:56
1.00E+OO
58.201
i
0.00
o.ot
07/16/13 13:56
1.00E+OO
82.16
0.00
o.ool
1.00E+OO
87.62
0.00
1.00E+OO
94.15
0.00
-------- f--------------- -- - - - - ----.
TRG
------
18
TRG
TH-232
19
TH-232
TRG
----
- - [------
- - - - - - !----
07/16/13 15:18
07/16/13 15:18
II
I
1
i
- -1------------------
Eberline Services
0::
.g
8
.!2
~
iii
c:
q:
Lab
01
Sample
Oesc
Nuclide
Fraction
t' LCS
TH-232
-~~t :~;-03
en
.c
TH-232
06
DUP
TH-232
09
TH-232
10
TH-232
-------
12
-=~
170 3.81 E.02
A_spec
Alpha_oo4
110.02 6.15 e+oo
A_Spec
Alpha_010
170\1.64 E+OO
13.00 E-o3
5.oo
Eft
J__17.5
e-a~J~~
8.00 E-03
19.7
~:= :::~:::
: : : : :: ::::: i :::
A_Spec
Alpha_013
170 8.83 E+OO
1.00 E-03
TRG
08/10/13 14:55
A_Spec
Alpha_015
170 1.28 E+01
1.00 E-03
08/10/13 15:01
A_Spec
Alpha_033
17015.83 E+OO
11.00 E-03
18.5
08/10/13 15:02
A_Spec
Alpha_034
170 2.83 E+OO
1.00 E-03
18.6
08/10/1315:02
A_Spec
Alpha_035
170 3.83 E+OO
1.00 E-03
18.3
A_Spec
Alpha_036
170 6.98 E+OO
6.00 E-03
18.7
13
,_ _ _
Q.
Q.
:I
-
---~~15
rn
TRG
] TRG
-- ----------08/10/13 15:02
TRG
08/10/13 15:02
-------- ---------------~-
A_Spec
Alpha_037
170 4.83 E+OO
1.00 E-03
19.1
r-------------1
17.8
08/10/13 15:02
A_Spec
Alpha_038
170 3.68 E+01
1.00 E-03
17.2
A_Spe<
Alpha_039
1702.66E+OO
2.00E-o3
19_.7~
A_Spec
Alpha_040
170,7.66 E+OO
2.00 E-03
08/10/13 15:02
A_Spec
Alpha_045
17016.83 E+OO
1.00 E-03
08/10/13 15:02
A_Spec
Alpha_046
170 19.00 E+OO
O.OOE+O~~~
'1
TH-232
TH-232
(I TRG
-----~-+-
----~-----------+-------
---~;;;~-~ ;RG~--~101~'."'"
Q)
Cl
c:
;:
Q)
Q)
.!:
Cl
c:
--
TRG
TH-232
__
J~~-- ---~~10/~~15:02_]
TH-232
Cl
::iiE
14.8
------
------~---~-+---
c:
Q)
E
co
c:
co
[,~~
Alpha_003
I
I
08/10/13 14:55
---1--~------~~~;;---T;;~-
u11
A_Spe<
Time
TRG
,_____________________________ !______
r.Jr
08/10/1314:55
Bkg
CPM
Counts
Carrier
--
~----~--
it;!~
__
Count
Detect
08
L
_:~:~~~~r
!
08/10113 1.,55
r : : -
TH-232
Halflife
(days)
Counting
Date/Time
----o21- ------~H-2~----- -~~= ~~~~~~~~~4:55
oc
Printed: 8/12/2013 8:47AM
Page 3 of 3
~:-r-
-19=L
TH-232
TH-232
I T~GTRG
TH-232 __}G
!
r----~--~-,-1-0/-13_1_5-:0_2_---l~lf-------+---A-_-S-pe-c-I--A-Ip_h_a_-0-4----j71--17-0+114-.6-6_E_+_OO-+
~--
19
19.1
12-.0-0_E_-0_3-+-1-18-.2---1
Count Room Report

Internal
Fraction
Sample
Desc
Client
ID
j
1
,_ 01 L L~S I
02-l MBL T
03
l~
.I
04
ouP
DO
Sample
Date
Sample
Aliquot
07/23/13 00:00
1.0000
BLANK_07/23/13 oo:oo
1.oooo
I
10.7859_1
0.2401~ 5.3941
LCS
Tracer
Aliquot (g)
0.4801
[
j
Tracer
ACT (dpm)
jl
_I
D-12 TOT
07~15/13 15:27
1.oooo
0.2373
D-12 TOT
0711_5113_15:27
1.0000
0.2358
5.~312
5.2975
Radiometric
Tracer (pCi)
I Radiometric
% Rec
i
j
'
0.00 ~
_o.oo
TRG
D-12 DIS
07/15/1~ 15:27
1.0000
0.2356
5.2930 I
'
06
TRG
DUP05 TOT
07/15/1300:00
1.0000
0.2368
5.3199
07
TRG
DUP05 DIS
I 07/15/13 00:00
1.0000
0.23411_
5.2593
08
TRG
09:25
1.0000
0.2345
5.2683
09
~7/16/13 09:25
1.0000
0.2353
5.2862
0.00 i
10
TRG
07/16/1312:05
1.0000
0.2354
5.2885
0.00
07/16/1312:05
1.oooo
0.2351
5.2818
o.oOT
PZ-304-AS TOT
I 07/16/1312:34
1.0000
0.2332
5.2391
0.00 I
PZ-304-AS DIS
07/16/1312:34
1.0000
0.2350 .
5.2795
0.00
MW-104 TOT
07/16/13 13:25
1.0000
0.~
5.2548
MW-104 DIS
07/16/1313:25
1.0000
0.2331 '
07/16/13 13:56
1.0000
0.234~ I
5.2368
1.0000
0.2345
1.0000
1.0000
\}.._()
12
~~'
I
1
TRGJ
PZ-208-sS TOT
PZ-208-SS DIS
PZ-304-AI TOT
PZ-304-AI DIS
13
TRG
14
TRG
'
15
TRG
16
TRG
'
PZ-204A-SS TOT
17
TRG
PZ-204A-5S DIS
18
TRG
19
TRG
~ .:
~S;.('
~07/1-6/13
I
1
-~-07/16/13 13:56
PZ-302-AI TO~ 07/16/1315:18
PZ-302-AI DIS
I 07/16/1315:18
5.2570
'!
I
I
'
0.00
j_
0.00 !
0.00 ]:
0.00
0.00
0.00
.
.
0.00 I
SAF
2*
0.00+--1-~
05
-~
o.oo_!
SAF
1*
L_
TRG
W<>.:JI
1.
~
~\,-
tlr!!
Printed: 81912013 6:54AM

Page 1 of 1
13-07147-ThiS0-1 {pCi/1) in WA
Tracer 10: Th-18a
.
-
I
-t-----
I __
+-I I
i
f
I
I
5.2683 I
0.001
0.2352
5.2840 I
0.00 !
0.2356
5.2930
0.00 I
.l
'
_
'
,
1
Eberline Services
Page 1 of 1
Printed: 8/2/2013 8:16AM
JWOLFE
ftiJ$'
LCS
Isotope
Activity
dpm!g
Sol#
' ,:\!1 ''';, '~
Known
pCi
'
Sol#
Tracers.. ,'
''
Activity
dpmlg
;!
'r
'
.'",,,,
',
Solution
Date
Volume
Used(g)
Approx
Addition
fraction
Isotope
01
Th-229
Th-18a
22.466
8/2/2013
0.4801
0.2200
02
Th-229
Th-18a
22.466
8/2/2013
0;2401
0.2200
03
Th-229
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22.466
8/2/2013
0.2373
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04
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22.466
8/2/2013 ' ..
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05
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8/2/2013
0.2358
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06
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22.466
8/2/2013
0.2368
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07
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22.466
8/2/2013
0.2341'
0.2200
08
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22.466
8/2/2013
0:2345
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09
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22.466
8/2/2013
0.2353
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10
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8/2/2013
0;2354
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11
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Sample Description:
Spectrum File:
Sample Geometry:
SPIKE
1307147A-TH
01
Shelf 2
Th iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_003
3
System Bkgd 64764

<not performed>
Sample Size:
Sample Date/Time:

7:27:05 AM
8/9/2013
2:55:07 PM
8/10/2013
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.480 mL
0.2052 +/- 0.0124
0.1746 +/- 0.0033 on 12/15/2012 11:26:47 AM
1.1753 +/- 0.0741
Control Certificate Name: NatTh Th-8

TH-232
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.855
5.347
4.883
4.610
3.948
Net
Pk Area
34.79
353.77
376.32
386.98
381.49
1.006466 +/-
AREA
0.085100
REPORT
FWHM
(keV)
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
34.44
10.48
10.11
9.98
10.04
2.21
3.23
0.68
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0.51
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20.7
5.1
36.0
13.6
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Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
1. 000
0.985
0.999
0.980
0.987
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
4.61E-001
4.58E+000
4.88E+000
5.00E+000
4.93E+000
+I+I+I+I+I-
1.68E-001
7.22E-001
5.76E-001
7.73E-001
7.63E-001
MDA
(pCi/liter
1.06E-001 +11.18E- 001 +I7.32E-002 +!8.15E-002 +!6.77E-002 +/-
1.25E-002
1.39E-002
8.63E-003
9.61E-003
7.99E-003
8/ ld-/d
ti259
0000065790.CNF

start:
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Channel Data Report
8/11/2013
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2
0
2
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0
0
0
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0
0
1
0
0
1
0
0
0
1
0
0
0
0
0
1
2
1
2
3
0
0
1
0
0
0
0
0
1
0
2
0
0
0
1
0
0
0
0
1
1
1
1
2
2
2
1
0
0
0
0
0
0
1
0
1
2
0
2
0
0
0
1
0
1
0
1
0
1
1
2
0
2
4
0
0
0
1
1
1
0
2
0
3
1
0
1
0
0
2
0
0
0
1
0
0
1
1
2
5
0
0
0
0
1
0
0
1
1
0
0
0
0
2
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1
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0
Sample Description:
Spectrum File:
Sample Geometry:
BLANK
1307147A-TH
02
Shelf 2
Th iso
Detector Name:

Env. Background:
Reagent Blank:
Alpha_004
System Bkgd 64765
<not performed>
Sample Size:
Sample Date/Time:
8/9/2013
7:27:05 AM
8/10/2013
2:55:08 PM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.240 mL
0.2003 +/- 0.0161
0.1940 +/- 0.0036 on 12/15/2012 11:26:46 AM
1. 0321 +I- 0.0851
0.175 MeV
PEAK
AREA
REPORT
--------------------------------------------------
Energy
(MeV)
Nuclide
Net
Pk Area
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
0.85
3.91
1. 36
1.70
0.85
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
FWHM
(keV)
-------------------------------------------------------------------------------TH-227
TH-228
TH-229
TH-230
TH-232
5.747
5.318
4.870
4.625
3.973
1.15
0.09
183.64
34.30
6.15
249.60
4720.2
14.53
34.42
85.19
2.9
2.9
6.8
3.7
2.9
-------------------------------------------------NUCLIDE ANALYSIS RESULTS
--------------------------------------------------
Nuclide
Id
Conf.
Energy
(keV)
Activity
(pCi/liter )
MDA
(pCi/liter
-------------------------------------------------------------------------------TH-227
TH-228
TH-229
TH-230
TH-232
0.946
0.965
1. 000
0.988
0.997
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
1.56E-002
1.19E-003
2.44E+000
4.55E-001
8.14E-002
+I+!+I+I+I-
3.90E-002
5.61E-002
3.84E-001
1. 72E-001
7.05E-002
-A(o
8/ li}/(j
8.13E-002 +/- 1.28E-002

1.29E-001 +!- 2.03E-002
9.12E-002 +I- 1.44E-002
9.74E-002 +!- 1.53E-002
7.92E-002 +I- 1.25E-002
0000065791.CNF

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8/11/2013
Page
10:16:41 AM
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Sample Description:
Spectrum File:
Sample Geometry:
D-12 TOT-DUP
1307147A-TH
03
Shelf 2
Th iso
Detector Name:

Env. Background:
Reagent Blank:
Alpha_010
10
System Bkgd 64766
<not performed>
Sample Size:
Sample Date/Time:
7/15/2013
7:27:05 AM
8/10/2013
2:55:01 PM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.237 mL
0.0680 +/- 0.0091
0.1967 +/- 0.0036 on 12/15/2012 11:26:40 AM
0.3456 +/- 0.0467
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
Net
Pk Area
AREA
REPORT
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
1302.3
217.67
25.53
44.41
214.83
2.72
2.89
2.38
1. 70
1. 36
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
FWHM
(keV)
-------------------------------------------------------------------------------TH-227
TH-228
TH-229
TH-230
TH-232
5.824
5.387
4.854
4.554
3.959
0.28
2.11
61.62
21.30
1. 64
2.9
2.9
3.4
5.9
2.9

Nuclide
Id
Conf.
Energy
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Activity
(pCi/liter )
MDA
(pCi/liter
-------------------------------------------------------------------------------TH-227
TH-228
TH-229
TH-230
TH-232
0.997
0.999
0.998
0.930
0.993
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
1.12E-002
8.45E-002
2.41E+000
8.32E-001
6.39E-002
+1+I+I+!+1-
1.46E-001
1.85E-001
6.33E-001
4.29E-001
1.38E-001
llG
~fr.J,{f~
3.44E-001 +!3.50E-001 +!3.21E-001 +!2.87E-001 +!2.67E-001 +/-
9.01E-002
9.20E-002
8.42E-002
7.53E-002
7.01E-002
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Channel Data Report
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8273
Sample Description:
Spectrum File:
Sample Geometry:
D-12 TOT
1307147A-TH
04
Shelf 2
Th iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_011
11
System Bkgd 64767
<not performed>
Sample Size:
Sample Date/Time:

7/15/2013
7:27:05 AM
8/10/2013
2:55:02 PM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.236 mL
0.1331 +/0.0128
0.2051 +/- 0.0035 on 7/20/2013
0.6488 +/- 0.0636
0.175 MeV
2:50:46 PM
-------------------------------------------------PEAK
AREA
REPORT
--------------------------------------------------
Energy
(MeV)
Nuclide
Net
Pk Area
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
FWHM
(keV)
-------------------------------------------------------------------------------TH-227
TH-228
TH-229
TH-230
TH-232
5.855
5.390
4.860
4.591
3.960
3.15
5.15
119.83
26.83
5.83
126.67
94.34
17.92
37.98
82.55
0.85
0.85
0.17
0.17
0.17
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
2.6
2.6
4.7
2.6
2.6
--------------------------------------------------
Nuclide
Id
Conf.
Energy
(keV)
Activity
(pCi/liter )
MDA
(pCi/liter
-------------------------------------------------------------------------------TH-227
TH-228
TH-229
TH-230
TH-232
1. 000
1. 000
0.999
0.966
0.993
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
6.45E-002
1.05E-001
2.40E+000
5.35E-001
1.16E-001
+1+I+I+I+I-
8.26E-002
1.01E-001
4.54E-001
2.27E-001
9.83E-002
AG
iJ.J/5
1.23E-001
1.22E-001
8.35E-002
8.33E-002
8.31E-002
+!+!+I+!+1-
2.32E-002
2.32E-002
1. 58E-002
1.58E-002
1.57E-002
0000065785.CNF
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&278
Sample Description:
Spectrum File:
Sample Geometry:
D-12 DIS
1307147A-TH
OS
Shelf 2
Th iso
Detector Name:
Alpha_012

12
Env. Background:
System Bkgd 64768

Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:

7/15/2013
7:27:05 AM
2:55:03 PM
8/10/2013
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.236 mL
0.0876 +/- 0.0102
0.1989 +/- 0.0034 on 12/11/2011

0.4404 +/- 0.0521
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
Net
Pk Area
5.702
5.314
4.859
4.613
3.983
0.83
-0.85
78.83
17.83
3.15
AREA
2:21:56 PM
REPORT
Pk Area
Error %
FWHM
(keV)
Ambient
Backgnd
Reagent
Backgnd
0.17
0.85
0.17
0.17
0.85
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
239.53
246.69
22.10
46.68
126.67
3.0
0.0
5.9
5.2
3.0
Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.892
0.962
0.999
0.982
0.999
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
2.58E-002
-2.64E-002
2.40E+000
5.40E-001
9.53E-002
+I
+I
+I
+I
+I
6.21E-002
6.54E-002
5.49E-001
2.81E-001
1.23E-001
MDA
(pCi/liter
1. 30E- 001
1. 86E-001
1.27E-001
1.26E-001
1.81E-001
+!
+!
+!
+I
+I
2.97E-002
4.26E-002
2.91E-002
2.90E-002
4.15E-002
AG
gltJtlt3
6279
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fi!282
Channel Data Report

801:
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Sample Title:
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0
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Sample Description:
Spectrum File:
Sample Geometry:
DUP05 TOT
1307147A-TH
06
Shelf 2
Th iso
Detector Name:

Env. Background:
Reagent Blank:
Alpha_Ol3
13
System Bkgd 64769
<not performed>
Sample Size:
Sample Date/Time:
7/15/2013
7:27:05 AM
8/10/2013
2:55:04 PM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.237 mL
0.1371 +/- 0.0131
0.1869 +/- 0.0035 on 12/15/2012 11:26:45 AM
0.7335 +/- 0.0713
0.175 MeV
-------------------------------------------------PEAK AREA REPORT

--------------------------------------------------
Energy
(MeV)
Nuclide
Net
Pk Area
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
1. 70
1.53
1. 02
0.34
0.17
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
FWHM
(keV)
-------------------------------------------------------------------------------TH-227
TH-228
TH-229
TH-230
TH-232
5.816
5.327
4.870
4.609
3.969
4.30
1.47
123.98
27.66
8.83
114.31
240.74
17.69
37.53
66.70
2.8
2.8
4.1
2.8
2.8

--------------------------------------------------
Nuclide
Id
Conf.
Energy
(keV)
Activity
(pCi/liter )
MDA
(pCi/liter
-------------------------------------------------------------------------------TH-227
TH-228
TH-229
TH-230
TH-232
0.994
0.972
1.000
0.980
0.996
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
8.54E-002 +12.92E-002 +I2.41E+000 +I5.36E-001 +I1.71E-001 +/-
9.90E-002
7.05E-002
4.50E-001
2.25E-001
1.18E-001
1.46E-001
1.41E-001
1.22E-001
9.26E-002
8. 07E- 002
~/fj
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2.73E-002
2.64E-002
2.29E-002
1. 73E-002
1.51E-002
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Sample Description:
Spectrum File:
Sample Geometry:
DUP05 DIS
1307147A-TH
07
Shelf 2
Th iso
Detector Name:
Alpha_014

14
Env. Background:
System Bkgd 64770

Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:

7/15/2013
7:27:05 AM
2:55:05 PM
8/10/2013
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.234 mL
0.1675 +/- 0.0147
0.1846 +/- 0.0034 on 12/15/2012 11:26:44 AM

0.9078 +/- 0.0814
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.797
5.390
4.862
4.630
3.969
Net
Pk Area
1.28
-1.08
149.81
34.32
-0.68
AREA
REPORT
Pk Area
Error %
323.53
348.68
16.09
33.84
304.42
Ambient
Backgnd
2.72
4.08
1.19
0.68
0.68
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
2.9
2.9
5.1
3.4
0.0
Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.985
1. 000
1. 000
0.991
0.996
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
2.08E-002
-1. 75E-002
2.38E+000
5.44E-001
-1. 08E-002
+I+I+!+I+I-
6.74E-002
6.13E-002
4.09E-001
2.06E-001
3.28E-002
MDA
(pCi/liter
1. 39E-001
1.61E-001
1.05E-001
8.94E-002
8.92E-002
+I+I+!+I+I-
2.40E-002
2.76E-002
1.80E-002
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:f1292
Channel Data Report

801:
8/11/2013
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Sample Title:
Page
10:25:02 AM
0
07
Channe 1 I- - - - - - I - - - - - - - I - - - - - - - I - - - - - - - I - - - - - - - I - - - - - - - I - - - - - - - I - - - - - - - I
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Sample Description:
Spectrum File:
Sample Geometry:
PZ-208-SS TOT
1307147A-TH
08
Shelf 2
Th iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_015
15
System Bkgd 64771
<not performed>
Sample Size:
Sample Date/Time:

7/16/2013
7:27:05 AM
8/10/2013
2:55:06 PM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.235 mL
0.1343 +/- 0.0130
0.1477 +/- 0.0027 on 7/20/2013
0.9094 +1- 0.0893
0.175 MeV
6:27:27 PM
-------------------------------------------------PEAK AREA REPORT

--------------------------------------------------
Energy
(MeV)
Nuclide
Net
Pk Area
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
0.85
0.68
0.68
0.68
0.17
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
FWHM
(keV)
-------------------------------------------------------------------------------TH-227
TH-228
TH-229
TH-230
TH-232
5.739
5.305
4.864
4.611
3.943
2.15
10.32
120.32
35.32
12.83
161.66
63.32
17.93
33.35
55.14
3.0
3.0
6.2
4.5
3.0
-------------------------------------------------
-------------------------------------------------
Nuclide
Id
Conf.
Energy
(keV)
Activity
(pCi/liter )
MDA
(pCi/liter
-------------------------------------------------------------------------------TH-227
TH-228
TH-229
TH-230
TH-232
0.938
0.954
1. 000
0.981
0.985
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
4.36E-002 +!- 7.09E-002

2.09E-001 +1- 1.38E-001
2.38E+000 +I- 4.51E-001
6.98E-001 +/- 2.68E-001
2.53E-001 +I- 1.48E-001
fG
g/rJfrJ
1. 21E- 001 +I- 2.30E-002

1.14E- 001 +/- 2.16E-002
1.12E-001 +!- 2.12E-002
l.llE-001 +I- 2.11E-002
8.23E-002 +/- 1.56E-002
0000065789.CNF

1 3490. S(kev)
Start:
Stop : 1024 6558. S(kev)
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Channel Data Report
8/11/2013
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m2
Channel Data Report

801:
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Page
10:17:38 AM
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Sample Description:
Spectrum File:
Sample Geometry:
PZ-208-SS DIS
1307147A-TH
09
Shelf 2
Th iso
Detector Name:
Alpha_033
04026479A
91132
Env. Background:
System Bkgd 64781

Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:

7/16/2013
7:27:05 AM
8/10/2013
3:01:59 PM
170.0 minutes
173.6 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.235 mL
0.1741 +/- 0.0150
0.1848 +/- 0.0032 on 7/20/2013

0.9422 +1- 0.0826
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.874
5.343
4.876
4.604
3.960
Net
Pk Area
-0.85
5.49
156.49
28.00
5.83
AREA
2:31:30 PM
REPORT
Pk Area
Error %
246.69
88.08
15.70
37.70
82.55
Ambient
Backgnd
0.85
0.51
0.51
0.00
0.17
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
0.0
3.0
6.3
4.5
3.0
Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.997
0.983
1. 000
0.976
0.993
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
-1.33E-002
8.57E-002
2.39E+000
4.27E-001
8.87E-002
+1
+1
+1
+I
+I
3.29E-002
7.69E-002
4.03E-001
1.76E-001
7.47E-002
MDA
(pCi/liter
9.36E-002
8.19E-002
8.02E-002
9.14E-002
6.35E-002
+!+1+!+1+I-
1.58E-002
1.38E-002
1.35E-002
1. 54E- 002
1. 07E-002
~{I)
1 299
0000065795.CNF

Start:
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Channel Data Report
8/11/2013
Page
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Sample Description:
Spectrum File:
Sample Geometry:
PZ-304-AI TOT
1307147A-TH
10
Shelf 2
Th iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_034
04026479B
91136
System Bkgd 64782
<not performed>
Sample Size:
Sample Date/Time:

7/16/2013
7:27:05 AM
8/10/2013
3:02:01 PM
170.0 minutes
173.6 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.235 mL
0.1542 +/- 0.0140
0.1856 +/- 0.0032 on 12/16/2012
0.8312 +/- 0.0766
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
Net
Pk Area
AREA
5:49:43 PM
REPORT
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
0.17
0.17
0.34
0.00
0.17
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
FWHM
(keV)
-------------------------------------------------------------------------------TH-227
TH-228
TH-229
TH-230
TH-232
5. 771
5.351
4.853
4.612
3.945
1. 83
5.83
138.66
36.00
2.83
152.56
82.55
16.67
33.12
120.53
3.0
3.0
5.0
3.0
3.0

Nuclide
Id
Con.
Energy
(keV)
Activity
(pCi/liter )
MDA
(pCi/liter
-------------------------------------------------------------------------------TH-227
TH-228
TH-229
TH-230
TH-232
0.968
0.987
0.998
0.982
0.986
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
3.23E-002
1.03E-001
2.39E+000
6.20E-001
4.86E-002
+I+I+I+!+I-
4.96E-002
8.68E-002
4.25E-001
2.33E-001
5.92E-002
AG
s/rJ-/13
7.37E-002
7.36E-002
8.25E-002
1.03E-001
7.17E-002
+I+I+!+!+!-
1.31E-002
1.31E-002
1.46E-002
1.83E-002
1. 27E- 002
0000065796.CNF

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Channel Data Report
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0
0
0
0
0
Sample Description:
Spectrum File:
Sample Geometry:
PZ-304-AI DIS
1307147A-TH
11
Shelf 2
Th iso
Detector Name:
Alpha_035
04026477A
58771
Env. Background:
System Bkgd 64783

Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:

7/16/2013
7:27:05 AM
3:02:02 PM
8/10/2013
170.0 minutes
173.6 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.235 mL
0.1576 +/- 0.0141
0.1826 +/- 0.0032 on 12/16/2012

0.8631 +/- 0.0789
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.754
5.378
4.883
4.644
3.935
Net
Pk Area
AREA
REPORT
Pk Area
Error %
1. 32
3.81
141.49
14.66
3.83
215.97
117.34
16.51
51.88
102.72
5:49:42 PM
Ambient
Backgnd
0.68
1.19
0.51
0.34
0.17
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
2.9
2.9
3.9
2.9
2.9

Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.953
0.997
0.999
0.996
0.980
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
2.28E-002 +I- 4.94E-002
6.57E-002 +I- 7.80E-002
2.39E+000 +I- 4.21E-001
2.47E-001 +/- 1.35E-001
6.44E-002 +I- 6.71E-002
A-G
~/r.>(~
MDA
(pCi/liter
9.75E-002 +!- 1.72E-002
1.14E-001 +!- 2.00E-002
8.87E-002 +/- 1.56E-002
8.05E-002 +!- 1.42E-002
7.02E-002 +!- 1.23E-002
0000065797.CNF

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Sample Description:
Spectrum File:
Sample Geometry:
PZ-304-AS TOT
1307147A-TH
12
Shelf 2
Th iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_036
04026477B
84167
System Bkgd 64784
<not performed>
Sample Size:
Sample Date/Time:

7/16/2013
7:27:05 AM
8/10/2013
3:02:04 PM
170.0 minutes
173.6 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.233 mL
0.1257 +/- 0.0126
0.1910 +/- 0.0033 on 7/20/2013

0.6584 +/- 0.0668
0.175 MeV
PEAK
AREA
2:31:37 PM
REPORT
--------------------------------------------------
Energy
(MeV)
Nuclide
Net
Pk Area
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
0.51
0.68
1. 02
0.51
1. 02
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
FWHM
(keV)
-------------------------------------------------------------------------------TH-227
TH-228
TH-229
TH-230
TH-232
5.827
5.226
4.835
4.621
3.932
0.49
1. 32
111.98
30.49
6.98
416.98
215.97
18.62
35.84
80.28
3.0
3.0
4.4
3.0
3.0
--------------------------------------------------
Nuclide
Id
Conf.
Energy
(keV)
Activity
(pCi/liter )
MDA
(pCi/liter
-------------------------------------------------------------------------------TH-227
TH-228
TH-229
TH-230
TH-232
0.997
0.854
0.993
0.986
0.978
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
1.06E-002
2.85E-002
2.37E+000
6.44E-001
1.47E-001
+I+!+!+!+I-
4.43E-002
6.19E-002
4.64E-001
2.63E-001
1.22E-001
11<4
8/rJ/3
1.14E-001 +!- 2.23E-002

1. 22E- 001 +!- 2.39E-002
1.33E-001 +I- 2.61E-002
l.llE-001 +/- 2.17E-002
1.33E-001 +!- 2.60E-002
0000065798.CNF

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8317
Channel Data Report

801:
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10:20:16 AM
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Spectrum File:
Sample Geometry:
PZ-304-AS DIS
1307147A-TH
13
Shelf 2
Th iso
Detector Name:
Alpha_037
04026478A
91133
Env. Background:
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Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:

7/16/2013
7:27:05 AM
8/10/2013
3:02:06 PM
170.0 minutes
173.6 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.235 mL
0.1270 +/0.0126
0.1783 +/0.0033 on 1/26/2013

0.7124 +/- 0.0718
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
50 813
5.360
4.877
4.581
3.927
Net
Pk Area
AREA
REPORT
Pk Area
Error %
2.83
4.32
114 000
30.66
4.83
3:28:25 PM
120.53
102.62
18.44
35.63
91.00
Ambient
Backgnd
Reagent
Backgnd
FWHM
(keV)
0.17
0.68
0.00
0.34
0.17
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
2.9
2.9
3.2
5.9
2.9

Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.993
0.992
1. 000
0.958
0.975
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
6.07E-002
9.25E-002
2.39E+000
6.41E-001
1.01E-001
+!
+I
+I
+!
+I
7.41E-002
9.66E-002
4.64E-001
2.60E-001
9.38E-002
MDA
(pCi/liter
8.95E-002 +I1.21E-001 +I1. 26E- 001 +!9.99E-002 +!8. 71E-002 +/-
1. 74E-002
2.34E-002
2.44E-002
1.94E-002
1.69E-002
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tJ1322
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801:
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11:17:48 .lM
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Sample Description:
Spectrum File:
Sample Geometry:
MW-104 TOT
1307147A-TH
14
Shelf 2
Th iso
Detector Name:
Alpha_038
04026478B
91134
Env. Background:
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Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:

7/16/2013
7:27:05 AM
8/10/2013
3:02:07 PM
170.0 minutes
173.6 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.234 mL
0.1619 +/0.0144
0.1722 +/0.0030 on 5/11/2013

0.9406 +!- 0.0852
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.888
5.381
4.889
4.628
3.951
Net
Pk Area
AREA
REPORT
Pk Area
Error %
5.00
42.32
144.66
70.00
36.83
5:13:35 PM
96.02
30.41
16.32
23.59
32.38
Ambient
Backgnd
0.00
0.68
0.34
0.00
0.17
Reagent
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O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
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3.0
5.5
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Nuclide
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Conf.
Energy
(keV)
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TH-228
TH-229
TH-230
TH-232
0.993
0.998
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2.38E+000
1.15E+000
6.03E-001
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2.22E-001
AG
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Channel Data Report
8/11/2013
Page
10:26:SI .tJt
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mJ27
Channel Data Report

801:
8/11/2013
0
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Sample Description:
Spectrum File:
Sample Geometry:
MW-104 DIS
1307147A-TH
15
Shelf 2
Th iso
Detector Name:
Alpha_039
06027396A
83109
Env. Background:
System Bkgd 64786

Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:

7/16/2013
7:27:05 AM
8/10/2013
3:02:09 PM
170.0 minutes
173.6 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.233 mL
0.1451 +/- 0.0136
0.1965 +/- 0.0034 on 4/20/2013

0.7383 +/- 0.0703
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.842
5.347
4.851
4.602
4.035
Net
Pk Area
AREA
REPORT
Pk Area
Error %
0.49
0.15
129.15
25.32
2.66
2:01:25 PM
416.98
1397.8
17.31
39.56
128.85
Ambient
Backgnd
Reagent
Backgnd
FWHM
(keV)
0.51
0.85
0.85
0.68
0.34
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
3.0
3.0
4.5
3.7
3.0

Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
1.000
0.986
0.998
0.975
0.993
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
9.20E-003
2.81E-003
2.37E+000
4.63E-001
4.86E-002
+I
+I
+I
+I
+I
3.84E-002
3.93E-002
4.35E-001
2.02E-001
6.32E-002
MDA
(pCi/liter
9.85E-002 +1
1.12E-001 +/
1.10E-001 +1
1.03E-001 +1
8.73E-002 +/
1.81E-002
2.06E-002
2.02E-002
1. 89E-002
1.60E-002
1\G
g{rJ-{f!l
8329
0000065801.CNF

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8/11/2013
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Channel Data Report

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S3.33
Sample Description:
Spectrum File:
Sample Geometry:
PZ-204A-SS TOT
1307147A-TH
16
Shelf 2
Th iso
Detector Name:
Alpha_040
06027396B
91135
Env. Background:
System Bkgd 64787

Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:

7:27:05 AM
7/16/2013
3:02:10 PM
8/10/2013
170.0 minutes
173.6 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.234 mL
0.1106 +/0. 0117
0.1900 +/- 0.0033 on 12/16/2012

0.5820 +!- 0.0621
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
Net
Pk Area
5.839
5.345
4.867
4.619
3.910
AREA
REPORT
Pk Area
Error %
2.66
15.15
98.83
20.32
7.66
128.85
51.98
19.74
44.32
72.63
5:49:33 PM
Ambient
Backgnd
0.34
0.85
0.17
0.68
0.34
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
3.0
3.0
7.9
3.7
3.0
Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.999
0.984
1. 000
0.986
0.961
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
6.55E-002 +/- 8.55E-002
3.72E-001 +I- 2.08E-001
2.38E+000 +I- 4.91E-001
4.88E-001 +I- 2.38E-001
1.84E-001 +!- 1.39E-001
1\G
&/t~/0
MDA
(pCi/liter
1.18E- 001
1.47E-001
1.00E-001
1.35E-001
1.15E- 001
+!+I+!+I+!-
2.43E-002
3.04E-002
2.07E-002
2.80E-002
2.37E-002
0000065802.CNF

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Channel Data Report
8/11/2013
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Channel Data Report

369:
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Channel Data Report

801:
8/11/2013
0
Sample Title:
Channel I - - - - - 809:
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10:27:17 AM
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I - - - - - - - I - - - - - - - I - - - - - - - I - - - - - - - I - - - - - - - I - - - - - - - I - - - - - - - 'I
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Sample Description:
Spectrum File:
Sample Geometry:
PZ-204A-SS DIS
1307147A-TH
17
Shelf 2
Th iso
Detector Name:
Alpha_045
04026482A
91131
Env. Background:
System Bkgd 64789

Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:

7/16/2013
7:27:05 AM
8/10/2013
3:02:13 PM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.235 mL
0.1569 +/- 0.0141
0.1909 +/- 0.0033 on 7/20/2013

0.8216 +/- 0.0754
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.838
5.346
4.885
4.604
3.968
Net
Pk Area
AREA
REPORT
Pk Area
Error %
2.66
2.32
140.49
24.66
6.83
2:31:26 PM
128.85
149.12
16.57
39.79
76.08
Ambient
Backgnd
0.34
0.68
0.51
0.34
0.17
Reagent
Backgnd
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
3.0
3.0
4.5
5.9
3.0
Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.999
0.985
0.999
0.976
0.996
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
4.62E-002
4.02E-002
2.38E+000
4.17E-001
1.15E-001
+!
+I
+I
+I
+I
6.01E-002
6.04E-002
4.21E-001
1.82E-001
9.01E-002
MDA
(pCi/liter
8.30E-002
9.78E-002
8.91E-002
8.09E-002
7.05E-002
+!+!+!+!+!-
1.47E-002
1.73E-002
1.57E-002
1.43E-002
1.24E-002
AG
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6339
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G342
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0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
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0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
Sample Description:
Spectrum File:
Sample Geometry:
PZ-302-AI TOT
1307147A-TH
18
Shelf 2
Th iso
Detector Name:
Alpha_046
04026482B
58762
Env. Background:
System Bkgd 64790

Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:
1.000E+000 +/O.OOOE+OOO liter

7:27:05 AM
7/16/2013
3:02:14 PM
8/10/2013
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.235 mL
0.1568 +/0.0141
0.1789 +/- 0.0031 on 12/16/2012

0.8762 +/0.0802
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.882
5.350
4.859
4.608
3.939
Net
Pk Area
AREA
REPORT
Pk Area
Error %
5.83
6.83
140.83
35.00
9.00
5:49:23 PM
Ambient
Backgnd
0.17
0.17
0.17
0.00
0.00
82.55
76.08
16.53
33.60
68.87
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
3.0
3.0
8.2
3.7
3.0
Nuclide
Id
Con.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.995
0.987
0.999
0.979
0.983
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
1. 01E-001
1.18E-001
2.39E+000
5.93E-001
1.52E-001
+I
+!
+I
+I
+I
8.55E-002
9.25E-002
4.21E-001
2.25E-001
1. 08E-001
Jt;
gfr.ttr:;
MDA
(pCi/liter
7.25E-002 +!7.24E-002 +17.09E-002 +11.02E-001 +!1.01E-001 +/-
1.28E-002
1.27E-002
1.25E-002
1.79E-002
1.78E-002
0000065793.CNF

start:
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ROI Type: 1
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Channel Data Report
8/11/2013
Page
10:27:33 AM
*******************************************************
S P E C T R A L
R E P 0 R T
DATA
*****
*****
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18
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Channe 1
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I- - - - - - I- - - - - - - I- -- - - - - I- - - - - - - I- - - - - - - I- - - - - - - I- - - - - - - I- - - - -- - I
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&3
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801:
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1
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Sample Description:
Spectrum File:
Sample Geometry:
PZ-302-AI DIS
1307147A-TH
19
Shelf 2
Th iso
Detector Name:
Alpha_047
0203 0596A
91086
Env. Background:
System Bkgd 64791

Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:

7/16/2013
7:27:05 AM
8/10/2013
3:02:16 PM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.236 mL
0.1715 +/- 0.0148
0.1822 +/- 0.0032 on 12/16/2012

0.9415 +/- 0.0831
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.709
5.300
4.856
4.639
3. 971
Net
Pk Area
0.66
-0.17
154.32
36.83
4.66
AREA
5:49:21 PM
REPORT
Pk Area
Error %
305.43
1169.4
15.82
32.38
94.59
Ambient
Backgnd
Reagent
Backgnd
FWHM
(keV)
0.34
0.17
0.68
0.17
0.34
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
2.9
0.0
8.1
2.9
2.9

Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.901
0.949
0.999
0.994
0.996
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
1.05E-002
-2.69E-003
2.40E+000
5.70E-001
7.20E-002
+I
+I
+I
+I
+I
3.21E-002
3.15E-002
4.06E-001
2.08E-001
6.92E-002
AG
s(tJtr3
MDA
(pCi/liter
7.59E-002 +1- 1.29E-002
6.62E-002 +1- 1.12E-002
8.76E-002 +/- 1.48E-002
6.46E-002 +1- 1.09E-002
7.39E-002 +1- 1.25E-002
0000065794.CNF

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1o:;r~.;jj
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*****
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19
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Channel Data Report

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0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
2
3
4
5
0
2
0
1
1
0
0
0
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
2
0
0
1
1
2
6
5
2
3
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
1
0
2
1
0
2
2
2
5
2
2
3
2
0
1
0
0
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
1
1
1
0
1
1
2
4
2
1
3
0
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
fi.352
Channel Data Report

801:
8/11/2013
0
Sample Title:
10:27:43
0
w
0
Page
0
19
809:
817:
825:
833:
841:
84 9:
857:
865:
873:
881:
889:
8 97:
905:
913:
921:
929:
937:
94 5:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
-S353
Page 1 of 2
8/10/2013 11:44:26 AM
QA SUMMARY REPORT
Date
Time
: 8/10/2013
: 11 :44:26 AM
CHAMBER
Alpha 001
Alpha 002
Alpha 003
Alpha 004
Alpha 005
Alpha 006
Alpha 007
Alpha 008
Apha 009
Alpha 010
Alpha 011
Alpha 012
Alpha 013
Alpha 014
Alpha 015
Alpha 016
Alpha 017
Alpha 018
Alpha 019
Alpha 020
Alpha 021
Alpha 022
Alpha 023
Alpha 024
Alpha 025
Alpha 026
Alpha 027
Alpha 028
Alpha 029
Alpha 030
Alpha 031
Alpha 032
Alpha 033
Alpha 034
Alpha 035
Alpha 036
Alpha 037
Alpha 038
Alpha 039
Alpha 040
Alpha 041
Alpha 042
DEVICE
2lf
2lf
21f
21f
21f
21f
2lf
21f
2lf
2lf
21f
21f
21f
21f
21f
21f
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
Alpha Analyst100DC
Alpha AnalystlOODC
Alpha AnalystlOODC
Alpha AnalystlOODC
Alpha Analyst 1OODC
Alpha Analyst100DC
Alpha Analyst! OODC
Alpha Analyst 1OODC
Alpha AnalystlOODC
Alpha Analyst! OODC
PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
Peak CPS
ALL
ALL
ALL
ALL
ALL
PeakFWHM
ALL
FLAG
Not Done
Not Done
Passed
Passed
Not Done
Not Done
Not Done
Not Done
Not Done
Passed
Passed
Passed
Passed
Passed
Passed
Not Done
Not Done
Passed
Passed
Not Done
Not Done
Passed
Passed
Passed
Passed
Not Done
Passed
Not Done
Passed
Not Done
Passed
Not Done
Passed
Passed
Action
Passed
Passed
Passed
Passed
Passed
Action
Passed
DATE
8/10/2013 11:22:54 AM
8/10/2013 11:22:55 AM
8/10/2013
8/10/2013
8/10/2013
8/10/2013
8/10/2013
8/10/2013
11:22:55 AM
11:22:56 AM
11:22:57 AM
11 :22:58 AM
11:22:59 AM
11:25:06 AM
8/10/2013 11:23:01 AM
8/10/2013 11:23:01 AM
8/10/2013
8/10/2013
8/10/2013
8/10/2013
11 :23:02 AM
11:23:03 AM
11:23:04 AM
11:23:05 AM
8/10/2013 11:23:06 AM
8/10/2013 11 :23:06 AM
8/10/2013 11 :23:07 AM
8/10/2013 11 :23:08 AM
8/10/2013 11:23:10 AM
8/9/2013 5:06:44 AM
8/10/2013 11:23:12 AM
8/10/2013 11:23:14 AM
8/10/2013 11:23:16 AM
8/10/2013 11:23:17 AM
8/10/2013 11:23:19 AM
8/10/2013 11:23:20 AM
8/10/2013 11:23:22 AM
Page 2 of 2

8/10/2013 11:44:26AM
CHAMBER
Alpha 043
Alpha 044
Alpha 045
Alpha 046
Alpha 047
Alpha 048
DEVICE
Alpha Analystl OODC
Alpha Analyst100DC
Alpha Analyst 1OODC
Alpha Analyst 1OODC
Alpha Analyst100DC
Alpha Analyst100DC
PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
FLAG
Not Done
Not Done
Passed
Passed
Passed
Passed
APPROVED BY:
~_,_]_/O__,_/I=C3-
APPROVAL DATE: _ _
DATE
8/10/2013
8/10/2013
8/10/2013
8/10/2013
11:23:24 AM
11:23:25 AM
11:23:27 AM
11 :23:28 AM
6/12/12
Page
12:16:29 PM
*************************************************************************
*****
*****
*************************************************************************
Thorium

Nuclide
Name
Half-Life
(Seconds)
TH-227
TH-228
TH-229
TH-230
TH-232
6.873E+008
6.034E+007
2.487E+011
2.379E+012
4.434E+017
Energy
(kev )
Th-227,-228,-229,-230,-232
Energy
Uncert. (keV
0.000
0.000
0.000
0.000
0.000
5850.000*
5400.000*
4872.000*
4672.000*
3997.000*
* = key line
TOTALS:
Nuclides
Energy Lines
Yield
(%)
97.5000
99.9400
99.5200
99.8200
100.0000
Yield
Uncert . (Abs . +- )
0.0000
0.0000
0.0000
0.0000
0.0000
SECTION X
ANALYTICAL DATA (RADIUM-226)
Eberline Services
Analysis Sheet
Printed: 81612013 2:33PM

Page 1 of 3
13-07147
Ra226
Run 1
Internal
Fraction
Sample
Desc
Client
ID
Ra226
1
01
LCS
LCS
07/23/13 00:00
1.0000E+OO
02
MBL
BLANK
07/23/13 00:00
1.0000E+OO
7/22/2013
03
DUP
D-12 TOT
46
07/15/13 15:27
1.0000E+OO
Lab Deadline I
8/13/2013
04
DO
D-12 TOT
46
07/15/13 15:27
1.0000E+OO
05
TRG
D-12 DIS
46
07/15/13 15:27
1.0000E+OO
West Lake OU-1
06
TRG
DUP05 TOT
45
07/15/13 00:00
1.0000E+OO
Analysis Code
Run
Date Received

Project I
Login
CPM
Sample
Date
Sample
Aliquot
13-07147
Work Order
Report Level
07
TRG
DUP05 DIS
45
07/15/13 00:00
1.0000E+OO
Activity Units
pCi
08
TRG
PZ-208-SS TOT
43
07/16/13 09:25
1.0000E+OO
09
TRG
PZ-208-SS DIS
43
07/16/13 09:25
1.0000E+OO
WA
10
TRG
PZ-304-AI TOT
46
07/16/13 12:05
1.0000E+OO
E903.0
11
TRG
PZ-304-AI DIS
46
07/16/13 12:05
1.0000E+OO
Alpha Spectroscopy
12
TRG
PZ-304-AS TOT
41
07/16/13 12:34
1.0000E+OO
Ba-133
13
TRG
PZ-304-AS DIS
41
07/16/13 12:34
1.0000E+OO
Radiometric Sol#
Ba-6a
14
TRG
MW-104 TOT
41
07/16/13 13:25
1.0000E+OO
Tracer Act (dpm/g)
991.479
15
TRG
MW-104 DIS
41
07/16/13 13:25
1.0000E+OO
Carrier
16
TRG
PZ-204A-SS TOT
40
07/16/13 13:56
1.0000E+OOI
17
TRG
PZ-204A-SS DIS
40
07/16/13 13:56
1.0000E+OOI
18
TRG
PZ-302-AI TOT
44
07/16/13 15:18
1.0000E+OO
19
TRG
PZ-302-AI DIS
44
07/16/13 15:18
1.0000E+OO
Aliquot Units
Matrix
Method
Instrument Type
Radiometric Tracer
Q!!il
Jl,~
Uil
00
** Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
Eberline Services
Analysis Sheet
Printed: 81612013 2:33PM

Page 2 of 3
13-07147
Ra226
Run 1
SAF
1*
SAF
2*
93.67
2.23
1.00
0.0055
93.77
1.95
1.00
0.0297
0.0065
98.48
2.34
1.00
0.0229
0.0294
0.0065
88.76
2.34
1.00
95.69
0.0224
0.0291
0.0067
95.69
2.40
1.00
380.7
93.28
0.0230
0.0294
0.0064
93.28
2.31
1.00
905.0
385.0
94.44
0.0224
0.0294
0.0070
94.44
2.50
1.00
0.9113
903.5
366.7
90.10
0.0226
0.0287
0.0061
90.10
2.20
1.00
TRG
0.9122
904.4
406.4
99.75
0.0228
0.0293
0.0065
99.75
2.34
1.00
10
TRG
0.9115
903.7
372.5
91.50
0.0223
0.0358
0.0135
91.50
5.02
1.oo
11
TRG
0.9100
902.2
395.5
97.31
0.0226
0.0317
0.0091
97.31
3.04
1.00
12
TRG
0.9079
900.2
383.4
94.55
0.0232
0.0351
0.0119
94.55
4.00
1.00
13
TRG
0.9121
904.3
357.3
87.71
0.0223
0.0352
0.0129
87.71
4.58
1.00
14
TRG
0.9090
901.3
356.2
87.74
0.0225
0.0321
0.0096
87.74
3.17
1.00
15
TRG
0.9091
901.4
394.5
97.16
0.0225
0.0298
0.0073
97.16
2.58
1.00
16
TRG
0.9109
903.1
377.2
92.72
0.0228
0.0296
0.0068
92.72
2.44
1.00
17
TRG
0.9061
898.4
406.4
100.43
0.0226
0.0297
0.0071
100.43
2.53
1.00
18
TRG
0.9064
898.7
436.4
107.80
0.0225
0.0295
0.0070
107.80
2.50
1.00
TRG
0.9104
902.6
351.8
86.52
0.0226
0.0296
0.0070
86.52
2.50
1.00
Internal
Fraction
Sample
Desc
01
LCS
0.9234
915.5
386.3
93.67
0.0230
0.0292
0.0062
02
MBL
0.9145
906.7
383.0
93.77
0.0231
0.0286
03
DUP
0.9149
907.1
402.4
98.48
0.0232
04
DO
0.9109
903.1
361.1
88.76
05
TRG
0.9102
902.4
389.0
06
TRG
0.9138
906.0
07
TRG
0.9128
08
TRG
09
Tracer
Aliquot(g)
Tracer Total
ACT(dpm)
Radiometric
Tracer (pCi)
Radiometric GravCarrier
%Rec
Added(ml)
Grav Filter
Tare (g)
Grav Filter
Final (g)
Grav Filter
Net(g)
Grav
%Rec
Mean
%Rec
19
-
~~'
t...Jt
U'11
~.<tll
Eberline Services
Analysis Sheet
Printed: 8/6/2013 2:33 PM

Page 3 of 3
13-07147
Ra226
Run 1
Internal
Fraction
Sample
Desc
01
Prep
Date
Prep
By
Sep tO
Date/Time
Sep tO
By
LCS
07/31/13 12:40
JWOLFE
08/05/13 13:55
LWALKER
02
MBL
07/31/13 12:40
JWOLFE
08/05/13 13:55
LWALKER
03
DUP
07/31/13 12:40
JWOLFE
08/05/13 13:55
LWALKER
-t
Rough Prep
Date
Rough Prep
By
DO
07/31/13 12:40
JWOLFE
08/05/13 13:55
LWALKER
05
. TRG
07/31/13 12:40
JWOLFE
08/05/13 13:55
LWALKER
06
TRG
07/31/13 12:40
JWOLFE
08/05/13 13:55
LWALKER
07
TRG
07/31/13 12:40
JWOLFE
08/05/13 13:55
LWALKER
08
TRG
07/31/13 12:40
JWOLFE
08/05/13 13:55
LWALKER
04
Sep t1
By
Sep t1
Date/Time
-
-
09
07/31/13 12:40
TRG
JWOLFE
08/05/13 13:55
LWALKER
-
10
TRG
07/31/13 12:40
JWOLFE
08/05/13 13:55
LWALKER
11
TRG
07/31/13 12:40
JWOLFE
08/05/13 13:55
LWALKER
12
TRG
07/31/13 12:40
JWOLFE
08/05/13 13:55
LWALKER
13
TRG
07/31/13 12:40
JWOLFE
08/05/13 13:55
LWALKER
14
TRG
07/31/13 12:40
JWOLFE
08/05/13 13:55
LWALKER
15
TRG
07/31/13 12:40
JWOLFE
08/05/13 13:55
LWALKER
16
TRG
07/31/13 12:40
JWOLFE
08/05/13 13:55
LWALKER
17
TRG
07/31/13 12:40
JWOLFE
08/05/13 13:55
LWALKER
18
TRG
07/31/13 12:40
JWOLFE
08/05/13 13:55
LWALKER
19
TRG
07/31/13 12:40
JWOLFE
08/05/13 13:55
LWALKER
L_
------
~:!II
Eberline Services
a::
Lab
8
.!!!
"'(
N
N
ca
0:::
Desc
Client
Identification
Activity
Units
Results
Error Estimate
MDA
LCS
Known
LCS
%R
LCS
Flag
107.32
OK
RPD
Flag
OK
LCS
LCS
pCi/1
1.10E+01
1.39E+OO
2.59E-01
02
RA-226
MBL
BLANK
pCi/1
3.64E-02
1.15E-01
2.44E-01
DUP
D-12 TOT
pCi/1
1.15E-01
1.66E-01
2.79E-01
DO
D-12 TOT
pCi/1
2.95E-01
2.25E-01
2.27E-01
OK
TRG
D-12 DIS
pCi/1
4.67E-01
2.86E-01
2.91E-01
OK
1.03E+01
Blank
Flag
MDA
Flag
RA-226
OK
OK
-""---f--"
03
CD
Sample
01
~--
Work Order: 13-07147-Ra226-1
Nuclide
Fraction
Printed: 8/7/2013 9:57AM
Page 1 of 3
RA-226
NA
OK
-1----
f---
04
RA-226
05
RA-226
06
RA-226
TRG
DUP05 TOT
pCi/1
3.60E-01
2.20E-01
1.61E-01
OK
07
RA-226
TRG
DUP05 DIS
pCi/1
4.43E-01
3.27E-01
3.85E-01
OK
PZ-208-5S TOT
pCUI
7.11E-01
3.16E-01
1.97E-01
OK
PZ-208-5S DIS
pCi/1
4.46E-01
2.47E-01
1.89E-01
OK
TRG
PZ-304-AI TOT
pCi/1
1.64E+OO
6.37E-01
2.65E-01
OK
TRG
PZ-304-AI DIS
pCi/1
1.15E+OO
4.53E-01
2.97E-01
OK
08
RA-226
I TRG
09
RA-226
TRG
-
10
RA-226
11
RA-226
-
12
RA-2~~~:- -
PZ-304-AS TOT
pCi/1
2.00E+OO
7.28E-01
4.46E-01
OK
13
RA-226
PZ-304-AS DIS
pCi/1
1.68E+OO
6.55E-01
4.52E-01
OK
14
RA-226
MW-104 TOT
pCUI
9.82E-01
4.44E-01
2.64E-01
OK
MW-104 DIS
pCi/1
2.41E-01
2.14E-01
2.84E-01
OK
!-------------- ______
c..i
.5
t:
0
a.
a.
:I
TRG
--r---- -
TRG
----"
15
RA-226
TRG
16
RA-226
! TRG
PZ-204A-SS TOT
pCi/1
1.82E+OO
5.23E-01
2.26E-01
Ql
OK
01
1---"--
ftS
17
RA-226
TRG
PZ-204A-SS DIS
pCi/1
1.07E+OO
3.85E-01
1.84E-01
OK
18
RA-226
TRG
PZ-302-AI TOT
pCi/1
8.02E-01
3.42E-01
1.77E-01
OK
19
RA-226
PZ-302-AI DIS
pCi/1
6.86E-01
3.42E-01
2.37E-01
OK
en
c
Ql
~I
01
ftS
:E
01
;:
Ql
Ql
a,
c
w
~~~~
t..~
()til
U..
--"--"-----t---
I
TRG
- - - - f-----"--~--~-----
-""--
(
c::
ci!
(0
N
N
.!!!
ns
r.t:
Work Order: 13-07147-Ra226-1
Lab
Fraction
Nuclide
Sample
Desc
Sample
Date
01
RA-226
LCS
07/23/13 00:00
02
RA-226
MBL
07/23/13 00:00
03
RA-226
DUP
07/15/13 15:27
Sample
Aliquot
Radiometric
%Rec
Mean
%Rec
Grav
% Rec
SeptO
Date/Time
SAF
1.00E+OO
93.67
0.00
93.67
8/5/2013 13:55
1.00E+OO
93.77
0.00
93.77
8/5/2013 13:55
1.00E+OO
98.48
0.00
98.48
8/5/2013 13:55
RA-226
8/5/2013 13:55
DO
07/15/13 15:27
1.00E+OO
88.76
0.00
88.76
1.00E+OO
95.69
0.00
95.69
8/5/2013 13:55
1.00E+OO
93.28
0.00
93.28
8/5/2013 13:55
8/5/2013 13:55
-----
05
RA-226
TRG
07/15/13 15:27
06
RA-226
TRG
07/15/13 00:00
07
RA-226
TRG
07/15/13 00:00
1.00E+OO
94.44
0.00
94.44
08
RA-226
--+~RG
07/16/13 09:25
1.00E+OO
90.10
0.00
90.10
09
10
RA-226
TRG
- - - - - - - 1--
RA-226
TRG
8/5/2013 13:55
-
f-----
07/16/13 09:25
1.00E+OO
99.75
0.00
99.75
8/5/2013 13:55
07/16/13 12:05
1.00E+OO
91.50
0.00
91.50
8/5/2013 13:55
1.00E+OO
97.31
0.00
97.31
8/5/2013 13:55
1.00E+OO
94.55
0.00
94.55
8/5/2013 13:55
1.00E+OO
87.71
0.00
87.7t=+~
8/5/2013 13:55
1.00E+OO
87.74
0.00
87.74
8/5/2013 13:55
.E
t:
0
Q.
Q.
::l
...c::
.!!!
11
RA-226
TRG
07/16/13 12:05
12
RA-226
TRG
07/16/13 12:34
RA-226
TRG
0711611312o34
RA-226
TRG
07/16/13 13:25
13
-~-----
14
-t
r.n
15
RA-226
TRG
07/16/13 13:25
cQ)
E
Q)
16
RA-226
TRG
07/16/13 13:56
17
RA-226
TRG
07/16/13 13:56
18
RA-226
TRG
07/16/13 15:18
19
RA-226
TRG
C)
;:;
Q)
Q)
c
c
c,
0.00
97.16
1.00E+OO
92.72
0.00
92.72
8/5/2013 13:55
1.00E+OO
100.00
0.00
100.43
8/5/2013 13:55
1.00E+OO
100.00
0.00
107.80
8/5/2013 13:55
07/16/13 15:18 TOE+OO
86.52
0.00
86.52
8/5/2013 13:55
~11
(ll']
~J
97.16
UJ
t.,Jr
1.00E+OO
C)
"'c
"'
::iE
Sept1
Date/Time
04
Printed: 8/7/2013 9:57AM
Page 2 of 3
Eberline Services
8/5/2013 13:55
I
I
I
I
~
1:
Lab
Fraction
Nuclide
01
RA-226
02
~
Work Order: 13-07147-Ra226-1
Sample
Desc
Counting
Date/Time
LCS
08/06/13 16:35
Halflife
(days)
Detect
Carrier
J
A_Spec
Count
Time
Counts
Bkg
CPM
Eff
Alpha_022
170.02 2.68 E+02
6.00 E-03
15.3
---
~-------
Printed: 8/7/2013 9:57AM
Page 3 of 3
Eberline Services
RA-226
MBL
08/06/13 16:35
A_Spec
Alpha_023
170 1.13 E+OO
1.10 E-02
17.1
RA-226
DUP
08/06/13 16:35
A_Spec-+Aipha_024
170 3.13 E+OO
1.10 E-02
17.1
RA-226
DO
08/06/13 16:35
A Spec
Alpha 025
170 7.32 E+OO
4.00 E-03
17.4
05
RA-226
TRG
08/06/13 16:35
A_Spe~pha_027
170.02 1.21 E+01
1.10 E-02
17.3
06
RA-226
TRG
08/06/13 16:35
A_Spec
1Alpha_029
170 1.07 E+01
2.00 E-03
19.5
07
RA-226
TRG
08/06/13 16:35
A_Spec
1Aipha_031
170 8.96 E+OO
1.20 E-02
14.2
08
RA-226
TRG
08/06/13 16:35
A_Spec
Alpha_033
170 2.03 E+01
4.00 E-03
18.5
RA-226
TRG
08/06/13 16:35
A_Spec
Alpha_034
170 1.33 E+01
4.00 E-03
18.6
RA-226
TRG
08/06/13 16:35
A_Spec
1Aipha_035
170 2.58 E+01
1.00 E-03
18.3
RA-226
TRG
08/06/13 16:35
A_Spec
1Aipha_036
170 2.66 E+01
8.00 E-03
19.1
RA-226
TRG
08/06/13 16:35
A_Spec
Alpha_038
170 3.06 E+01
8.00 E-03
17.2
RA-226
TRG
A_Spoo
t:lp'"-'''
170 2.73 E+01
1.00 E-02
19.7
-----
03
-------- ---
{l
(0
8
-!!!
N
N
0::
cu
04
~------
r------
---
1--
1------
---~~-
09
1-----
10
r-------
11
r----------
,--
12
1-------------
c.i
-=~
0
Q.
Q.
:I
en
c:
Q)
~I
E
Q)
C)
10
c:
10
:E
C)
c:
;:
Q)
Q)
.5
C)
c:
UJ
~-~
!tJ,JI
[jtjl
~l!
13
14
08/06/13 16:35
-
~-
---~--
RA-226
TRG
08/06/13 16:35
A_Spec
Alpha_040
170 1.95 E+01
3.00 E-03
19
RA-226
TRG
08/06/13 16:36
A_Spec
1Aipha_041
170 6.79 E+OO
1.30 E-02
19.8
RA-226
TRG
08/06/13 16:36
A_Spec
1Aipha_042
170 4.82 E+01
5.00 E-03
18.5
RA-226
TRG
08/06/13 16:36
A_Spec
Alpha_045
170 3.05 E+01
3.00 E-03
19.1
RA-226
TRG
08/06/13 16:36
A_Spec
Alpha_046
170 2.17 E+01
2.00 E-03
17.9
RA-226
TRG
08/06/13 16:36
-1-----------------
A_Spec
Alpha_047
170 1.63 E+01
4.00 E-03
18.2
---------
15
t------~-
-----
16
f---~--
17
---.
18
1-------
19
1-------~--
Count Room Report

~K~l
Printed: 8/6/2013 2:33PM

Page 1 of 1
13-07147-Ra226-1 (pCi/1) in WA
Tracer 10: Ba-6a
~~
SAF
1*
SAF
2*
93.67
2.23
1.00
383.0000
93.77
1.95
1.00
907.1041
402.4000
98.48
2.34
1.00
0.9109
903.1382
361.1000
88.76
2.34
1.00
1.0000
0.9102
902.4442
389.0000
95.69
2.40
1.00
07/15/13 00:00
1.0000
0.9138
906.0135
380.7000
93.28
2.31
1.00
DUP05 DIS
07/15/13 00:00
1.0000
0.9128
905.0220
385.0000
94.44
2.50
1.00
TRG
PZ-208-SS TOT
07/16/13 09:25
1.0000
0.9113
903.5348
366.7000
90.10
2.20
1.00
09
TRG
PZ-208-SS DIS
07/16/13 09:25
1.0000
0.9122
904.4271
406.4000
99.75
2.34
1.00
10
TRG
PZ-304-AI TOT
07/16/13 12:05
1.0000
0.9115
903.7331
372.5000
91.50
5.02
Internal
Fraction
Sample
Desc
Client
ID
Sample
Date
Sample
Aliquot
01
LCS
LCS
07/23/13 00:00
1.0000
0.9234
915.5317
386.3000
02
MBL
BLANK
07/23/13 00:00
1.0000
0.9145
906.7075
03
DUP
D-12 TOT
07/15/13 15:27
1.0000
0.9149
04
DO
D-12 TOT
07/15/13 15:27
1.0000
05
TRG
D-12 DIS
07/15/13 15:27
06
TRG
DUP05 TOT
07
TRG
/~')r r--- 08
Tracer
Aliquot (g)
Tracer
ACT(dpm)
Radiometric
Tracer (pCi)
Radiometric
%Rec
--
--
1.00
,~::,.,.,
11
TRG
PZ-304-AI DIS
07/16/13 12:05
1.0000
0.9100
902.2459
395.5000
97.31
3.04
12
TRG
PZ-304-AS TOT
07/16/13 12:34
1.0000
0.9079
900.1638
383.4000
94.55
4.00 I 1.00
13
TRG
PZ-304-AS DIS
07/16/13 12:34
1.0000
0.9121
904.3280
357.3000
87.71
4.58
1.00
14
TRG
MW-104 TOT
07/16/13 13:25
1.0000
0.9090
901.2544
356.2000
87.74
3.17
1.00
15
TRG
MW-104 DIS
07/16/13 13:25
1.0000
0.9091
901.3536
394.5000
97.16
2.58
1.00
16
TRG
PZ-204A-SS TOT
07/16/13 13:56
1.0000
0.9109
903.1382
377.2000
92.72
2.44
1.00
17
TRG
PZ-204A-SS DIS
07/16/13 13:56
1.0000
0.9061
898.3791
406.4000
100.43
2.53
1.00
18
TRG
PZ-302-AI TOT
07/16/13 15:18
1.0000
0.9064
898.6766
436.4000
107.80
2.50
1.00
19
TRG
PZ-302-AI DIS
07/16/13 15:18
1.0000
0.9104
902.6425
351.8000
86.52
2.50
1.00
1.00
Eberline Services
Page 1 of 1
Printed: 7/31/2013 12:40 PM
Ra226
Activity
dpmlg
Solution
Date
Ra-5b
Ra-226
t----t-----+---44_._06_6~
7/31/20131
,>c
:,r;
fraction
Tracers
Activity
dpm/g
LCS
MS
LCSD
Volume
Used(g)
Volume
Used(g)
Volume
Used(g)
o.5ool
o.5t811
..,
::::,:c.
Approx
Addition
Isotope
Sol#
01
Ba-133 I
Ba-6a
991.479 7/31/2013
.... 0.9234
1.0200
02
Ba-133
Ba-6a
991.479 7/31/2013 . . a:9145
1.0200
03
Ba-133
Ba-6a
991.479 7/31/2013
0.9149.
1.0200
04
Ba-133
Ba-6a
991.479 7/31/2013
. 0.9109
1.0200
05
Ba-133
Ba-6a
991.479 7/31/2013
0;91:02
1.0200
06
Ba-133 I
Ba-6a
1.0200
07
Ba-133
Ba-6a
~ .. 0.9138
991.479 7/31/2013 . 0.9128
08
Ba-133
Ba-6a
991.479 7/31/2013 !;~
: 0.9113
1.0200
09
Ba-133
Ba-6a
991.479 7/31/2013
0.9122
1.0200
10
Ba-133
Ba-6a
991.479 7/31/2013:.
0.91'15
1.0200
11
Ba-133
Ba-6a
991.479 7/31/2013
} 0.91'00
1.0200
12
Ba-133
Ba-6a
991.479 7/31/2013
0:9079.
1.0200
13
Ba-133
Ba-6a
991.479 7/31/2013
0.9121
1.0200
14
Ba-6a
991.479 7/31/2013
0.9090
1.0200
15
Ba-133 I
Ba-133 I
Ba-6a
991.479 7/31/2013
0.9091
1.0200
16
Ba-133
Ba-6a
991.479 7/31/2013 .
: 0.9109
1.0200
17
Ba-133
Ba-6a
991.479 7/31/2013
0;90&1
1.0200
18
Ba-133
Ba-6a
991.479 7/31/2013
(1~90&4
1.0200
19
Ba-133 I
Ba-6a
991.479 7/31/2013
Ol91.04
1.0200
991.479 7/31/2013
..
~;it~l
Version 2.0 08/99
LCS
MS
Error
Estimate
c,l
Volume
Used(g)
Solution
Date
. ::
I!J'II
JWOLFE
10.281
:,;.:,,,'.:/
:-:.
0.473
0.00
Error
Estimate
Known
pCi
0.000
Error
Estimate
0.00
0.000
Tracer
LCS
;;:
'!'
1.0200
Matrix Spike
.;!<' " ' l
... "
Added
pCi
0.00
Error
Estimate
0.000
Balance Printet.la.,. .:' .
';
Added
pCi
,.~-'
,.,.
.j
.. "1
c
-
Eberline Analytical
Printed: 7/31/2013 12:34 PM

Page 1 of 1
Aliquot Worksheet
JWOLFE
Lab
sample
Muffle Data
Type
Ratio
Post/Pre
Fraction
ClientiD
01 I
02
03
04
05
06
07
08
09
10 I
11
12
13
14
15
~f-.
17
18 I
19 I
LCS
BLANK
-D-12 TOT
D-12 TOT
D-12 DIS
DUP05 TOT
DUP05 DIS
PZ-208-SS TOT
PZ-208-SS DIS
PZ-304-AI TOT
PZ-304-AI DIS
PZ-304-AS TOT
PZ-304-AS DIS
MW-104 TOT
MW-104 DIS
PZ-204A-SS TOT
PZ-204A-SS DIS
PZ-302-AI TOT
PZ-302-AI DIS
Comments
~~I
Teohnidan
I LCS I
MBL I >
DUP
DO
TRG
..
TRG
TRG
TRG
TRG
I TRG I
I
I
TRG
TRG
TRG
TRG
TRG
TRG
TRG
MS Aliquot Data
No of Oils .
'
'
'
;
-~
'"Jli: ~ .. ,, .
'
<
f {i!\}ii;, i'i.;
; "; .
..
I?
!.
..,.
L'
. '
Aliquot
1.0000E+OOI
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.OOOOE+OO
1.0000E+OO
1.0000E+OOI
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OOI
1.0000E+OOI
; ,. ~
.' ~, .:
Aliquot
Net Equiv
H-3 Solids Only

Water Added
(ml)
H3 Dist
Aliq
1.0000E+OO
1.0QOOE+OOI
1.0000E+OOI
1.00QOE+OOI
1.0000E+00.
1.0000E+OO
1.QOOOE+OO
1.0000E+OO
1.0000E+00
1.0000E+OO
1.0000E+OO
1.0000Et00
1.oooOE~OO
1.00QOE+o(}
1:0000Et00
1.0000E+OO
1.0000Et00
1.000012+09
1.00QOE+OO
__j1 ~.DateU 1 /~
\
Eberline Services - Oak Ridge

Version 1.0 9/1999
Printed: 8/5/2013 3:40 PM

Page 1 of 1
Gravimetric Worksheet
Gravimetric
Carrier
Analysis
Work Order
Code
Carrier Cone
(mg/ml)
Technician
Ra226
TRetec
Fraction
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
Client ID
LCS
BLANK
DUP
D-12 TOT
D-12 DIS
DUP05 TOT
DUP05 DIS
PZ-208-SS TOT
PZ-208-SS DIS
PZ-304-AI TOT
PZ-304-AI DIS
PZ-304-AS TOT
PZ-304-AS DIS
MW-104 TOT
MW-104 DIS
PZ-204A-SS TOT
PZ-204A-SS DIS
PZ-302-AI TOT
PZ-302-AI DIS
Sample
Type
LCS
MBL
DUP
DO
TRG
TRG
.
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
.
TRG
TRG
TRG
TRG
TRG
c-
Technician:./c
, "
- - .......
Filter Data
Carrier Data
Carrier Added
(ml)
Date:
Gravimetric
Filter Tare
Filter Final
Filter Net
(g)
(g)
(g)
..
~-
!I>!~~
LWALKER
0.0230
0.0231
0.0232
0.0229
0.0224
0.0230
0.0224
0.0226
0.0228
0.0223
0.0226
0.0232
0.0223
0.0225
0.0225
0.0228
0.0226
0.0225 '
0.0226
( ; 1(3
- 1-
0.0292
0.0286
0.0297
0.0294
0.0291
0.0294
0.0294
0.0287
0.0293
0.0358
0.0317
0.0351
0.0352
0.0321
0.0298
0.0296
0.0297
0.0295
0.0296
%
Recovery
'
a~ooGi
O;,oo5s
.0~0065;.
O.OO.c5
o~oo67
Q.0064
0.0070.
0.0061
0.0065;
.
o~o1.~s
0.0091
0.0119.
0,01.~9
0~0096
..
0;007~
0.0068.
0.00.71
..
O.QO'lt
.
o.;ooto ...
..
..
Sample Description:
Spectrum File:
Sample Geometry:
SPIKE
1307147A-RA
01
Shelf 2
Ra
Detector Name:
Alpha_022

22
Env. Background:
System Bkgd 64044

Reagent Blank:
<not performed>
Sample Size:
Generic Mult. Factor:
Sample Date/Time:
1.000E+000 +/O.OOOE+OOO liter

2.230E+000
Generic Div. Factor:
8/6/2013
2:34:11 PM
8/6/2013
4:35:16 PM
170.0 minutes
170.0 minutes
0.9367 +/0.1531 +/0.1435 +/-
0.0000
0.0029 on 12/15/2012
0.0027

Ra226 Ra-5b

RA-226
0.481241 +/Peak Match Tolerance:
0.350 MeV
PEAK
Nuclide
Energy
(MeV)
Net
Pk Area
AREA
1.000E+000
1:57:26 PM
0.034067
REPORT
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
FWHM
(keV)
-------------------------------------------------------------------------------RA-224
RA-226
5.526
4. 712
484.45
267.98
8.93
12.00
2.55
1.02
O.OOE+OOO
O.OOE+OOO
10.9
11.4
Nuclide
Id
Conf.
Energy
(keV)
Activity
(pCi/liter )
MDA
(pCi/liter
-------------------------------------------------------------------------------RA-224
RA-226
0.967
0.993
5685.50*
4785.00*
2.10E+001 +/- 2.03E+000

1.10E+001 +/- 1.39E+000
3.63E-001 +/- 1.36E-002

2.59E-001 +/- 9.69E-003
0000065373.CNF

start:
1:3421.5 (kev)
stop : 1024:6608.8(kev)
Acq. start :Tue Aug 06 16:35:16 2013
60
55
50
45
40
35
Vl
+-'
s:::
8 3o
25
20
15
:::i
~
10
5
0
~~~ll
3500
4000
ROI Type: 1
4500
5000
Energy(kev)
5500
6000
6500
Channel Data Report
8/7/2013
Page
5:36:08 AM
*******************************************************
*****
*******************************************************
Sample Title:
01
Elapsed Live time:

Elapsed Real Time:
10201
10201
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:
10201
3
1
1
1
1
2
1
1
1
1
0
1
1
2
2
4
2
1
4
2
2
1
1
2
2
1
1
2
2
2
2
6
2
4
5
3
4
2
3
4
6
2
2
6
2
10201
1
1
4
1
1
3
1
2
1
0
2
3
0
1
1
2
4
3
3
1
0
5
1
3
4
1
1
3
2
4
0
2
0
0
4
3
3
3
1
3
0
6
3
4
7
0
3
0
3
2
0
3
1
1
0
2
1
1
4
2
0
4
4
2
3
1
3
1
2
5
4
4
4
0
4
2
2
5
3
5
0
6
4
0
2
0
2
3
3
3
4
0
0
1
1
1
2
3
0
1
2
1
0
4
2
3
1
3
0
1
2
1
2
4
0
1
2
1
1
1
0
2
2
2
2
1
2
6
2
2
5
2
2
2
2
5
5
0
2
2
2
1
0
0
1
3
1
0
2
1
2
2
0
2
3
2
2
1
1
2
0
2
3
6
3
3
2
1
3
1
2
2
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R!
"'"
Channel Data Report

801:
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Sample Title:
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5:36:08 AM
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1
&372
Sample Description:
Spectrum File:
Sample Geometry:
BLANK
1307147A-RA
02
Shelf 2
Ra
Detector Name:
Alpha_023

23
Env. Background:
System Bkgd 64045

Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:

1.950E+000
7/16/2013
2:34:11 PM
8/6/2013
4:35:17 PM
170.0 minutes
170.0 minutes
0.9377 +/0.1710 +/0.1603 +/-
Energy
(MeV)
6:18:25 PM
0.350 MeV
PEAK
Nuclide
0.0000
0.0030 on 7/20/2013
0.0028
1.000E+000
Net
Pk Area
AREA
REPORT
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
FWHM
(keV)
-------------------------------------------------------------------------------RA-224
RA-226
5.533
4.654
0.45
1.13
806.99
315.93
2.55
1. 87
O.OOE+OOO
O.OOE+OOO
3.1
3.1

Nuclide
Id
Conf.
Energy
(keV)
Activity
(pCi/liter )
MDA
(pCi/liter
-------------------------------------------------------------------------------RA-224
RA-226
0.970
0.978
5685.50*
4785.00*
1.54E-002 +/- 1.24E-001

3.64E-002 +/- 1.15E-001
2.86E-001 +/- 9.91E-003

2.44E-001 +/- 8.43E-003
0000065322.CNF
If-

start:
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Acq. Start rue Aug 06 16:35:17 2013
60-f
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35
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.......
:::::s
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It
10-lt-
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Channel Data Report

801:
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5:36:14 AM
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02
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fi1377
Sample Description:
Spectrum File:
Sample Geometry:
D-12 TOT DUP

1307147A-RA
03
Shelf 2
Ra
Detector Name:
Alpha_024

24
Env. Background:
System Bkgd 64046

Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:

2.340E+000
7/15/2013
2:34:11 PM
4:35:18 PM
8/6/2013
170.0 minutes
170.0 minutes
0.9848 +/0.1710 +/0.1684 +/-
Energy
(MeV)
RA-224
RA-226
2:02:15 PM
0.350 MeV
PEAK
Nuclide
0.0000
0.0032 on 12/15/2012
0.0031
1.000E+000
Net
Pk Area
5.491
4.628
AREA
REPORT
Pk Area
Error %
3.64
3.13
Ambient
Backgnd
123.16
144.40
1. 36
1.87
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
3.1
3.1
Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.952
0.968
5685.50*
4785.00*
Activity
(pCi/liter )
1.42E-001 +/- 1.75E-001
1.15E-001 +/- 1.66E-001
g{1/f3
MDA
(pCi/liter
2.67E-001 +/- 9.81E-003
2.79E-001 +/- 1.02E-002
0000065323.CNF

1 3411.6(kev)
Start:
Stop : 1024 6597. O(kev)
Acq. start Tue Aug 06 16:35:18 2013
60+
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IF.!~~
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ROI Type: 1
6500
Channel Data Report
8/7/2013
Page
5:36:20 AM
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03
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Channel Data Report

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Sample Description:
Spectrum File:
Sample Geometry:
D-12 TOT
1307147A-RA
04
Shelf 2
Ra
Detector Name:
Alpha_025

25
Env. Background:
System Bkgd 64047

Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:

2.340E+000
7/15/2013
2:34:11 PM
8/6/2013
4:35:19 PM
170.0 minutes
170.0 minutes
0.8876 +/0.1736 +/0.1541 +/-
Energy
(MeV)
RA-224
RA-226
1:57:27 PM
0.350 MeV
PEAK
Nuclide
0.0000
0.0032 on 12/15/2012
0.0029
1.000E+000
Net
Pk Area
5.540
4.583
AREA
REPORT
Pk Area
Error %
2.13
7.32
191.21
76.28
Ambient
Backgnd
Reagent
Backgnd
FWHM
(keV)
1. 87
0.68
O.OOE+OOO
O.OOE+OOO
3.1
6.3

Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.973
0.948
5685.50*
4785.00*
Activity
(pCi/liter )
9.08E-002 +/- 1.74E-001
2.95E-001 +/- 2.25E-001
MDA
(pCi/liter
3.23E-001 +/- 1.18E-002
2.27E-001 +/- 8.29E-003
0000065324.CNF

Start:
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Sample Description:
Spectrum File:
Sample Geometry:
D-12 DIS
1307147A-RA
05
Shelf 2
Ra
Detector Name:
Alpha_027

27
Env. Background:
System Bkgd 64048

Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:

2.400E+000
7/15/2013
2:34:11 PM
8/6/2013
4:35:20 PM
170.0 minutes
170.0 minutes
0.9569 +!0.1728 +/0.1653 +/-
Energy
(MeV)
RA-224
RA-226
2:27:41 PM
0.350 MeV
PEAK
Nuclide
0.0000
0.0032 on 12/15/2012
0.0031
1.000E+000
Net
Pk Area
5.501
4.595
6.96
12.13
AREA
REPORT
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
86.10
61.14
2.04
1. 87
O.OOE+OOO
O.OOE+OOO
FWHM
(keV)
3.2
6.4

Nuclide
Id
Conf.
Energy
(keV)
Activity
(pCi/liter )
MDA
(pCi/liter
-------------------------------------------------------------------------------RA-224
RA-226
0.956
0.954
5685.50*
4785.00*
2.84E-001 +/- 2.44E-001

4.67E-001 +/- 2.86E-001
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Sample Description:
Spectrum File:
Sample Geometry:
DUP05 TOT
1307147A-RA
06
Shelf 2
Ra
Detector Name:
Alpha_029

29
Env. Background:
System Bkgd 64049

Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:

2.310E+000
7/15/2013
2:34:11 PM
8/6/2013
4:35:21 PM
170.0 minutes
170.0 minutes
0.9328 +/0.1945 +/0.1815 +/-
Energy
(MeV)
2:30:02 PM
0.350 MeV
PEAK
Nuclide
0.0000
0.0036 on 12/15/2012
0.0033
1.000E+000
Net
Pk Area
AREA
REPORT
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
FWHM
(keV)
-------------------------------------------------------------------------------RA-224
RA-226
5.534
4.536
3.96
10.66
124.69
61.14
2.04
0.34
O.OOE+OOO
O.OOE+OOO
3.1
3.1

Nuclide
Id
Conf.
Energy
(keV)
Activity
(pCi/liter )
MDA
(pCi/liter
-------------------------------------------------------------------------------RA-224
RA-226
0.970
0.922
5685.50*
4785.00*
1.41E-001 +/- 1.76E-001

3.60E-001 +/- 2.20E-001
2.78E-001 +/- 1.00E-002
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5397
Sample Description:
Spectrum File:
Sample Geometry:
DUP05 DIS
1307147A-RA
07
Shelf 2
Ra
Detector Name:
Alpha_031

31
Env. Background:
System Bkgd 64050

Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:

2.500E+000
2:34:11 PM
7/15/2013
8/6/2013
4:35:22 PM
170.0 minutes
170.0 minutes
0.9444 +/0.1418 +/0.1340 +/-
Energy
(MeV)
RA-224
RA-226
3:23:29 PM
0.350 MeV
PEAK
Nuclide
0.0000
0.0034 on 6/13/2013
0.0032
1.000E+000
Net
Pk Area
5.444
4.665
AREA
REPORT
Pk Area
Error %
4.32
8.96
102.62
73.69
Ambient
Backgnd
0.68
2.04
Reagent
Backgnd
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
3.1
4.7

Nuclide
Id
Con.
Energy
(keV)
RA-224
RA-226
0.927
0.981
5685.50*
4785.00*
Activity
(pCi/liter )
2.26E-001 +/- 2.32E-001
4.43E-001 +/- 3.27E-001
MDA
(pCi/liter
2.95E-001 +/- 1.41E-002
3.85E-001 +/- 1.83E-002
0000065327.CNF

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Acq. Start :Tue Aug 06 16:35:22 2013
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8/7/2013
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Sample Description:
Spectrum File:
Sample Geometry:
PZ-208-SS TOT
1307147A-RA
08
Shelf 2
Ra
Detector Name:
Alpha_033
04026479A
91132
Env. Background:
System Bkgd 64051

Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:

2.200E+000
7/16/2013
2:34:11 PM
8/6/2013
4:35:48 PM
170.0 minutes
170.0 minutes
0.9010 +/0.1848 +/0.1665 +/-
Energy
(MeV)
2:31:30 PM
0.350 MeV
PEAK
Nuclide
0.0000
0.0032 on 7/20/2013
0.0029
1.000E+000
Net
Pk Area
AREA
REPORT
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
FWHM
(keV)
-------------------------------------------------------------------------------RA-224
RA-226
5.522
4.557
11.15
20.32
61.26
44.32
0.85
0.68
O.OOE+OOO
O.OOE+OOO
4.5
3.0

Nuclide
Id
Conf.
Energy
(keV)
Activity
(pCi/liter )
MDA
(pCi/liter
-------------------------------------------------------------------------------RA-224
RA-226
0.966
0.934
5685.50*
4785.00*
4.13E-001 +/- 2.54E-001

7.11E-001 +/- 3.16E-001
2.22E-001 +/- 7.65E-003

1.97E-001 +/- 6.79E-003
0000065330.CNF

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ROI Type: 1
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Energy(kev)
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Channel Data Report
8/7/2013
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5:36:51 AM
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Sample Geometry:
PZ-208-SS DIS
1307147A-RA
09
Shelf 2
Ra
Detector Name:
Alpha_034
04026479B
91136
Env. Background:
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<not performed>
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Sample Date/Time:

2.340E+000
7/16/2013
2:34:11 PM
8/6/2013
4:35:49 PM
170.0 minutes
170.0 minutes
0.9975 +/0.1856 +/0.1851 +/-
Energy
(MeV)
RA-224
RA-226
5:49:43 PM
0.350 MeV
PEAK
Nuclide
0.0000
0.0032 on 12/16/2012
0.0032
1.000E+000
Net
Pk Area
5.493
4.567
AREA
REPORT
Pk Area
Error %
7.83
13.32
70.93
55.28
Ambient
Backgnd
0.17
0.68
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
3.0
3.0
Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.953
0.940
5685.50*
4785.00*
Activity
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2.78E-001 +/
4.46E-001 +/
1.97E-001
2.47E-001
MDA
(pCi/liter
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8/7/2013
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Sample Description:
Spectrum File:
Sample Geometry:
PZ-304-AI TOT
1307147A-RA
10
Shelf 2
Ra
Detector Name:
Alpha_035
04026477A
58771
Env. Background:
System Bkgd 64053

Reagent Blank:
<not performed>
Sample Size:
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4.000E+000
7/16/2013
2:34:11 PM
8/6/2013
4:35:51 PM
170.0 minutes
170.0 minutes
0.9150 +/0.1826 +/0.1671 +/-
Energy
(MeV)
5:49:42 PM
0.350 MeV
PEAK
Nuclide
0.0000
0.0032 on 12/16/2012
0.0029
1.000E+000
Net
Pk Area
AREA
REPORT
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
FWHM
(keV)
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RA-226
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4.604
5.66
25.83
85.23
38.71
0.34
0.17
O.OOE+OOO
O.OOE+OOO
2.9
2.9

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Id
Conf.
Energy
(keV)
Activity
(pCi/liter )
MDA
(pCi/liter
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RA-226
0.963
0.958
5685.50*
4785.00*
3.80E-001 +/- 3.24E-001

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46
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J(.!:io,
!lu~lolitlt
""'~'
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8/7/2013
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G-417
Sample Description:
Spectrum File:
Sample Geometry:
Shelf 2
Ra
Detector Name:
Env. Background:
Reagent Blank:
Alpha_036
04026477B
84167
System Bkgd 64054
<not performed>
PZ-304-AI DIS
1307147A-RA
11
Sample Size:
Sample Date/Time:
3.040E+000
Generic Div. Factor: 1.000E+000
7/16/2013
2:34:11 PM
8/6/2013
4:35:53 PM
170.0 minutes
170.0 minutes

0.9731 +/0.1910 +/0.1858 +/-
Energy
(MeV)
2:31:37 PM
0.350 MeV
PEAK
Nuclide
0.0000
0.0033 on 7/20/2013
0.0032
Net
Pk Area
AREA
REPORT
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
FWHM
(keV)
-------------------------------------------------------------------------------RA-224
RA-226
5.575
4.596
9.32
26.64
66.89
39.09
0.68
1. 36
O.OOE+OOO
O.OOE+OOO
3.0
3.0

Nuclide
Id
Conf.
Energy
(keV)
Activity
(pCi/liter )
MDA
(pCi/liter
-------------------------------------------------------------,-----------------
RA-224
RA-226
0.984
0.954
5685.50*
4785.00*
4.28E-001 +/- 2.86E-001

1.15E+000 +/- 4.53E-001
A-G
gf1(()
2.59E-001 +/- 8.84E-003

2.97E-001 +/- 1.01E-002
0000065333.CNF

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Sample Description:
Spectrum File:
Sample Geometry:
PZ-304-AS TOT
1307147A-RA
12
Shelf 2
Ra
Detector Name:
Env. Background:
Reagent Blank:
Alpha_038
04026478B
91134
System Bkgd 64055
<not performed>
Sample Size:
Sample Date/Time:
1.000E+000 +/
O.OOOE+OOO liter
4.000E+000
7/16/2013
2:34:11 PM
4:35:55 PM
8/6/2013
170.0 minutes
170.0 minutes

0.9455 +/
0.1722 +/
0.1628 +/
Energy
(MeV)
RA-224
RA-226
5:13:35 PM
0.350 MeV
PEAK
Nuclide
0.0000
0.0030 on 5/11/2013
0.0029
1.000E+000
Net
Pk Area
5.479
4.601
AREA
REPORT
Pk Area
Error %
10.15
30.64
64.46
36.32
Ambient
Backgnd
0.85
1. 36
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
5.9
3.0
Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.946
0.957
5685.50*
4785.00*
Activity
(pCi/liter )
7.00E-001 +/- 4.52E-001
2.00E+000 +/- 7.28E-001
MDA
(pCi/liter
4.13E-001 +/- 1.42E-002
4.46E-001 +/- 1.54E-002
1\-G
~I1{ 1 J
1423
0000065334.CNF

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Channel Data Report

801:
8/7/2013
1
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Page
5:37:18 AM
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Spectrum File:
Sample Geometry:
PZ-304-AS DIS
1307147A-RA
13
Shelf 2
Ra
Detector Name:
Alpha_039
06027396A
83109
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<not performed>
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4.000E+000
2:34:11 PM
7/16/2013
8/6/2013
4:35:57 PM
170.0 minutes
170.0 minutes
0.8771 +/0.1965 +/0.1724 +/-
Energy
(MeV)
RA-224
RA-226
2:01:25 PM
0.350 MeV
PEAK
Nuclide
0.0000
0.0034 on 4/20/2013
0.0030
1.000E+000
Net
Pk Area
5.530
4.611
AREA
REPORT
Pk Area
Error %
6.66
27.30
78.18
38.85
Ambient
Backgnd
0.34
1. 70
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
3.0
3.0
Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.969
0.961
5685.50*
4785.00*
Activity
(pCi/liter )
4.34E-001 +/- 3.39E-001
1.68E+000 +/- 6.55E-001
MDA
(pCi/liter
3.11E-001 +/- 1.06E-002
4.52E-001 +/- 1.53E-002
0000065335.CNF

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Channel Data Report
8/7/2013
Page
5:37:24 AM
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G~~~
Channel Data Report

801:
8/7/2013
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Sample Description:
Spectrum File:
Sample Geometry:
MW-104 TOT
1307147A-RA
14
Shelf 2
Ra
Detector Name:
Env. Background:
Reagent Blank:
Alpha_040
06027396B
91135
System Bkgd 64057
<not performed>
Sample Size:
Sample Date/Time:

3.170E+000
7/16/2013
2:34:11 PM
8/6/2013
4:35:59 PM
170.0 minutes
170.0 minutes

0.8774 +/0.1900 +/0.1667 +/-
Energy
(MeV)
RA-224
RA-226
5:49:33 PM
0.350 MeV
PEAK
Nuclide
0.0000
0.0033 on 12/16/2012
0.0029
1.000E+000
Net
Pk Area
5.488
4.608
AREA
REPORT
Pk Area
Error %
11.15
19.49
61.26
45.07
Ambient
Backgnd
0.85
0.51
Reagent
Backgnd
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
3.0
3.0

Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.950
0.960
5685.50*
4785.00*
Activity
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5.95E-001 +/- 3.65E-001
9.82E-001 +/- 4.44E-001
MDA
(pCi/liter
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2.64E-001 +/- 8.99E-003
9433
0000065336.CNF

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Acq. Start :Tue Aug 06 16:35:59 2013
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8/7/2013
Page
5:37:31 AM
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64
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15
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Alpha_041
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91087
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7/16/2013
2:34:11 PM
8/6/2013
4:36:02 PM
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170.0 minutes
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RA-226
5:49:31 PM
0.350 MeV
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0.0000
0.0034 on 12/16/2012
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6.79
190.02
88.39
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Backgnd
0.51
2.21
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1.07E-001
2.14E-001
MDA
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2.84E-001 +/
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9.63E-003
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mA~l
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801:
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Sample Description:
Spectrum File:
Sample Geometry:
PZ-204A-SS TOT
1307147A-RA
16
Shelf 2
Ra
Detector Name:
Alpha_042
05026930B
84185
Env. Background:
System Bkgd 64059

Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:

2.440E+000
7/16/2013
2:34:11 PM
8/6/2013
4:36:04 PM
170.0 minutes
170.0 minutes
0.9272 +/0.1846 +/0.1712 +/-
Energy
(MeV)
RA-224
RA-226
5:49:29 PM
0.350 MeV
PEAK
Nuclide
0.0000
0.0032 on 12/16/2012
0.0030
1.000E+000
Net
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5.509
4.618
AREA
REPORT
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Error %
25.81
48.15
39.61
28.54
Ambient
Backgnd
1.19
0.85
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
4.5
3.7

Nuclide
Id
Con.
Energy
(keV)
RA-224
RA-226
0.960
0.964
5685.50*
4785.00*
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1.82E+000 +/- 5.23E-001
MDA
(pCi/liter
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2.26E-001 +/- 7.71E-003
0000065337.CNF

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Acq. Start Tue Aug 06 16: 36:04 2013
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4Y446
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Sample Description:
Spectrum File:
Sample Geometry:
PZ-204A-SS DIS
1307147A-RA
17
Shelf 2
Ra
Detector Name:
Alpha_045
04026482A
91131
Env. Background:
System Bkgd 64060

Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:

2.530E+000
2:34:11 PM
7/16/2013
4:36:07 PM
8/6/2013
170.0 minutes
170.0 minutes
1.0000 +/0.1909 +/0.1909 +/-
Energy
(MeV)
RA-224
RA-226
2:31:26 PM
0.350 MeV
PEAK
Nuclide
0.0000
0.0033 on 7/20/2013
0.0033
1.000E+000
Net
Pk Area
5.481
4.587
AREA
REPORT
Pk Area
Error %
12.49
30.49
56.77
35.84
Ambient
Backgnd
0.51
0.51
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
3.0
4.5
Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.947
0.950
5685.50*
4785.00*
Activity
(pCi/liter )
4.64E-001 +/- 2.64E-001
1.07E+000 +/- 3.85E-001
MDA
(pCi/liter
1.95E-001 +/- 6.67E-003
1.84E-001 +/- 6.28E-003
0000065329.CNF

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Acq. Start Tue Aug 06 16: 36:07 2013
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8/7/2013
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1451
Channel Data Report

801:
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1
Sample Description:
Spectrum File:
Sample Geometry:
PZ-302-AI TOT
1307147A-RA
18
Shelf 2
Ra
Detector Name:
Alpha_046
04026482B
58762
Env. Background:
System Bkgd 64061

Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:

2.500E+000
7/16/2013
2:34:11 PM
8/6/2013
4:36:09 PM
170.0 minutes
170.0 minutes
1.0000 +/0.1789 +/0.1789 +/-
Energy
(MeV)
RA-224
RA-226
5:49:23 PM
0.350 MeV
PEAK
Nuclide
0.0000
0.0031 on 12/16/2012
0.0031
1.000E+000
Net
Pk Area
5.540
4.579
5.83
21.66
AREA
REPORT
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
FWHM
(keV)
82.55
42.50
0.17
0.34
O.OOE+OOO
O.OOE+OOO
3.0
3.0

Nuclide
Id
Con.
Energy
(keV)
RA-224
RA-226
0.973
0.946
5685.50*
4785.00*
Activity
(pCi/liter )
2.29E-001 +/
8.02E-001 +/
1.89E-001
3.42E-001
MDA
(pCi/liter
1.64E-001 +/
1.77E-001 +/
5.64E-003
6.09E-003
0000065328.CNF

Start:
1:3453.7(kev)
Stop : 1024:6515.4(kev)
Acq. Start :Tue Aug 06 16: 36: 09 2013
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s:::::
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~~~
ROI Type: 1
4000
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Energy(kev)
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6500
Channel Data Report
8/7/2013
5:37:5~
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'-M
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18
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Channel Data Report

801:
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0
Sample Title:
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Sample Description:
Spectrum File:
Sample Geometry:
PZ-302-AI DIS
1307147A-RA
19
Shelf 2
Ra
Detector Name:
Alpha_047
02030596A
91086
Env. Background:
System Bkgd 64062

Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:

2.500E+000
2:34:11 PM
7/16/2013
4:36:11 PM
8/6/2013
170.0 minutes
170.0 minutes
0.8652 +/0.1822 +/0.1576 +/-
Energy
(MeV)
RA-224
RA-226
5.594
4.618
5:49:21 PM
0.350 MeV
PEAK
Nuclide
0.0000
0.0032 on 12/16/2012
0.0028
1.000E+000
Net
Pk Area
AREA
REPORT
Pk Area
Error %
4.83
16.32
91.00
49.69
Ambient
Backgnd
0.17
0.68
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
2.9
2.9
Nuclide
Id
Con.
Energy
(keV)
RA-224
RA-226
0.989
0.964
5685.50*
4785.00*
Activity
(pCi/liter )
2.15E-001 +/- 1.96E-001
6.86E-001 +/- 3.42E-001
MDA
(pCi/liter
1.86E-001 +/- 6.39E-003
2.37E-001 +/- 8.14E-003
0000065339.CNF

Rea1 Time 10200 .100 sec
start:
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Channel Data Report
8/7/2013
Page
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Channel Data Report

801:
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5:38:05 AM
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Page 1 of 2
8/6/2013
5:51:01 AM
QA SUMMARY REPORT
Date
Time
8/6/2013
: 5:51 :01 AM
CHAMBER
Alpha 001
Alpha 002
Alpha 003
Alpha 004
Alpha 005
Alpha 006
Alpha 007
Alpha 008
Alpha 009
Alpha 010
Alpha 011
Alpha 012
Alpha 013
Alpha 014
Alpha 015
Alpha 016
Alpha 017
Alpha 018
Alpha 019
Alpha 020
Alpha 021
Alpha 022
Alpha 023
AlJ:lha 024
Alpha 025
Alpha 026
Alpha 027
Alpha 028
Alpha 029
Alpha 030
Alpha 031
Alpha 032
Alpha 033
Alpha 034
Alpha 035
Alpha 036
Alpha 037
Alpha 038
Alpha 039
Alpha 040
Alpha 041
Alpha 042
DEVICE
2lf
21f
21f
21f
21f
21f
21f
2lf
21f
2lf
21f
2lf
21f
21f
21f
21f
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
Alpha Analyst! OODC
Alpha Analyst100DC
Alpha Analyst100DC
Alpha AnalystlOODC
Alpha AnalystlOODC
Alpha AnalystlOODC
Alpha Analyst100DC
Alpha AnalystlOODC
Alpha Analyst! OODC
Alpha Analyst 1OODC
PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
PeakFWHM
ALL
ALL
ALL
ALL
FLAG
Not Done
Not Done
Passed
Passed
Not Done
Not Done
Not Done
Not Done
Not Done
Passed
Passed
Passed
Passed
Passed
Passed
Not Done
Not Done
Passed
Passed
Passed
Not Done
Passed
Passed
Passed
Passed
Not Done
Passed
Not Done
Passed
Not Done
Passed
Not Done
Passed
Passed
Passed
Passed
Not Done
Action
Passed
Passed
Passed
Passed
DATE
8/6/2013 5:29:13 AM
8/6/2013 5:29:14 AM
8/6/2013
8/6/2013
8/6/2013
8/6/2013
8/6/2013
8/6/2013
5:29:14 AM
5:29:15 AM
5:29:16 AM
5:29:17 AM
5:29:18 AM
5:29:18 AM
8/6/2013 5:29:19 AM
8/6/2013 5:29:20 AM
8/2/2013 5:14:08 AM
8/6/20 13
8/6/2013
8/6/2013
8/6/2013
5:29:21 AM
5:29:22 AM
5:29:22 AM
5:29:23 AM
8/6/2013 5:29:24 AM
8/6/2013 5:29:25 AM
8/6/2013 5:29:26 AM
8/6/2013
8/6/2013
8/6/2013
8/6/2013
5:29:27 AM
5:29:28 AM
5:29:30 AM
5:29:31 AM
8/6/2013
8/6/2013
8/6/2013
8/6/2013
8/6/2013
5:29:32 AM
5:29:34 AM
5:29:35 AM
5:29:37 AM
5:29:38 AM
-m
Page 2 of 2
8/6/2013
CHAMBER
Alpha 043
Alpha 044
AJpha 045
Alpha 046
Alpha 047
Alpha 048
DEVICE
Alpha AnalystlOODC
Alpha AnalystlOODC
Alpha AnalystlOODC
Alpha AnalystlOODC
Alpha Analyst! OODC
Alpha AnalystlOODC
PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
APPROVED BY:
APPROVAL DATE:
FLAG
Not Done
Not Done
Passed
Passed
Passed
Passed
5:51:01 AM
DATE
8/6/2013
8/6/2013
8/6/2013
8/6/2013
5:29:40 AM
5:29:42 AM
5:29:43 AM
5:29:45 AM
6/12/12
Page
12:16:17 PM
*************************************************************************
*****
*****
*************************************************************************
Radium
Ra-226, Po-218, Rn-222
Nuclide
Name
Half-Life
(Seconds}
P0-218
RN-222
RA-226
5.049E+010
5.049E+010
5.049E+010
Energy
Uncert. (keV
Energy
(keV )
6003.000*
5490.000*
4785.000*
0.000
0.000
0.000
key line
TOTALS:
Nuclides
Energy Lines
Yield
(%}
99.9800
99.9200
100.0000
Yield
Uncert . (Abs . +-}
0.0000
0.0000
0.0000
SECTION XI
ANALYTICAL DATA (RADIUM-228)
Eberline Services
Analysis Sheet
Printed: 8/14/2013 10:16 AM

Page 1 of 3 ,
13-07147
Ra228
I ~''''li
Run 1
Work Order
Analysis Code
-
Internal
Fraction
Sample
Desc
01
LCS
Ra228
Client
ID
Login
CPM
LCS
02
MBL
Sample
Date
07/23/13 00:00
Sample
Aliquot
1.0000E+OOi
'
~-~~---
Run
BLANK
07/23/13 00:00
1.0000E+OO
07/15/13 15:27
1.0000E+OO
-107/15/13 15:27
1.0000E+OO
-----
Date Received
Lab Deadline
r---
Client
Project
03
7/22/2013
DUP
D-12
TOT
46
!
i
04
DO
05
TRG
West Lake OU-1
06
TRG
8/13/2013
TOT
46
D-12 DIS
46
D-12
r----
DUP05
TOT
I
I
45
1--
07/15/13 15:27
1.0000E+OO
07/15/13 00:00
1.0000E+OO
------
Report Level
07
TRG
Activity Units
pCi
08
TRG
PZ-208-SS
Aliquot Units
09
WA
Matrix
DUP05 DIS
--
45
07/15/13 00:00
1.0000E+OO
TOT
43
07/16/13 09:25
1.0000E+OO
TRG
PZ-208-SS DIS
43
07/16/13 09:25
1.0000E+OO
10
TRG
PZ-304-AI
TOT
46
07/16/13 12:05
1.0000E+OO
E904.0
11
TRG
PZ-304-AI DIS
46
07/16/13 12:05
1.0000E+OO
Alpha/Beta GPC
12
TRG
PZ-304-AS
TOT
41
07/16/13 12:34
1.0000E+OO
Ba-133
13
TRG
PZ-304-AS DIS
41
07/16/13 12:34
1.0000E+OO
14
TRG
MW-104 TOT
41
07/16/13 13:25
1.0000E+OO
MW-104 DIS
41
07/16/13 13:25
1.0000E+OO
Method
Instrument Type
Radiometric Tracer
Radiometric Sol#
Ba-6a
Tracer Act (dpm/g)
991.479
15
TRG
Carrier
Yttirum
16
TRG
PZ-204A-SS
TOT
40
07/16/13 13:56
1.0000E+OO
34
17
TRG
PZ-204A-SS DIS
40
07/16/13 13:56
1.0000E+OO
18
TRG
PZ-302-AI
TOT
44
07/16/13 15:18
1.0000E+OO
19
TRG
PZ-302-AI DIS
44
07/16/13 15:18
1.0000E+OO
Carrier Cone {mg/ml)
r---
1----
t~
-~~~
Of1t
....~
SAF1
is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only.
**Actual mass exceeded the calibration curve range. Results should be qualified as appropriate .
Eberline Services
Analysis Sheet
Printed: 8/1412013 10:16 AM

Page 2 of3
13-07147
Ra228
Run 1
Internal
Fraction
Sample
Desc
Tracer
Aliquot (g)
I Tracer Total
ACT (dpm)
Radiometric
Tracer (pCi)
Radiometric Grav Carrier

%Rec
Added(ml)
Grav Filter
Tare (g)
GravFilter
Final (g)
Grav Filter
Net(g)
01
LCS
0.9234 I
915.5
386.3
93.67
2.000
0.0911
0.15141
0.0603
02
MBL
0.9145
906.7
383.0
93.77
2.000
0.0916
0.1498
0.0582
DUP
0.9149
Grav
%Rec
1
Mean
%Rec
SAF
SAF
1*
2*
1.00
88.68
83.06
1.00
85.59
80.26
1.00 I 1.00
I
03
04
DO
0.9109
907.1
903.1
402.4
361.1
98.48
88.76
2.000
I
2.000'
0.1486,
0.0572
84.12
82.84
1.00
0.0912
0.1468
0.0556
81.76
72.58
1.00
------
05
TRG
0.9102 I
0.0914
902.4
389.0
95.69
2.000
0.0922
0.1490
1.00
---
---
1.00
------
0.0568
83.53
79.93
1.00
1.00
0.0585
86.03
80.25
1.00
1.00
0.0557
81.91
77.36
1.00
1.00
06
TRG
0.9138
906.0
380.7
93.28
2.000
0.0922
0.1507
07
TRG
0.9128
905.0
385.0
94.44
2.000
0.0919
0.1476
TRG
0.9113 I
08
903.5
366.7
90.10
2.000
0.0923
0.1482
0.0559
82.21
74.07
1.oo
09
TRG
0.9122
904.4
406.4
99.75
2.000
0.0923
0.14801
0.0557
81.91
81.71
1.oo
1
1.00
1.00
10
TRG
0.9115
903.7
372.5
91.50
2.000
0.0923
0.1472
0.0549
80.74
73.88
1.00
1.00
11
TRG
0.9100
902.2
395.5
97.31
2.000
0.0923
0.1461
0.0538
79.12
76.99
1.00
1.00
12
TRG
0.9079
900.2
383.4
94.55
2.000
0.0925
0.1472
0.0547
80.44
76.06
10~ 1~
13
TRG
0.9121
904.3
357.3
87.71
2.000
0.0922
0.1487
0.0565
83.09
72.88
1.00 I 1.00
14
TRG
0.9090
901.3
356.2
87.74
2.000
0.0921
0.1486
0.0565
83.09
72.90
1.00
1.00
15
TRG
0.9091
901.4
394.5
97.16
2.000
0.0921
0.1485
0.0564
82.94
80.59
1.00
1.00
0.0559
82.21
76.22
1.00
1.00
0.0561
82.50
82.85
16
TRG
0.9109
903.1
377.2
92.72
2.000
0.0918
0.1477
898.4
406.4
100.43
2.000
0.0921
0.1482
---
17
TRG
0.9061
1.00
I
1.00
-
18
TRG
0.9064
898.7
436.4
107.80
2.000
0.0920
0.1494
0.0574
84.41
91.00
1.00
1.00
19
TRG
0.9104
902.6
351.8
86.52
2.000
0.0918
0.1483
0.0565
83.09
71.89
1.00
1.00
il:iii'~
Eberline Services
Analysis Sheet
Printed: 8/14/2013 10:16 AM

Page 3 of 3
13-07147
Ra228
Run 1
Internal
Fraction
Sample
Desc
01
02
Rough Prep
Date
Rough Prep
By
Prep
Date
Prep
By
Septo
Date/Time
LCS
07/31/13 12:41
JWOLFE
08/05/13 13:55 I LWALKER
MBL
07/31/13 12:41
JWOLFE
08/05/13 13:55
JWOLFE
08/05/13 13:55
Sep to
By
Sep t1
Date/Time
Sep t1
By
TSMITH
LWALKER
08/14/13 06:531
TSMITH
LWALKER
08/14/13 o6:53 I
08114113 06:53
--
-----
03
DUP
I 07/31/13 12:41
-
04
DO
07/31/13 12:41
TSMITH
-
08/05/13 13:55
JWOLFE
LWALKER
08/14/13 06:53
TSMITH
- ---
05
TRG
' 07/31/13 12:41
JWOLFE
08/05/13 13:55
LWALKER
08/14/13 06:53 '
TSMITH
06
TRG
07/31/13 12:41
JWOLFE
08/05/13 13:55
LWALKER
08/14/13 06:53
TSMITH
07
TRG
07/31/13 12:41
JWOLFE
08/05/13 13:55
LWALKER
08/14/13 06:53
TSMITH
08
TRG
07/31/13 12:41
JWOLFE
08/05/13 13:55
LWALKER
08/14/13 06:53
'
TSMITH
09
TRG
I 07/31/13 12:41
JWOLFE
08/05/13 13:55
LWALKER
08/14/13 06:53
TSMITH
10
TRG
07/31/13 12:41
JWOLFE
08/05/13 13:55
LWALKER
08/14/13 06:53
TSMITH
11
TRG
07/31/13 12:41
JWOLFE
08/05/13 13:55
LWALKER
08/14/13 06:53
TSMITH
12
TRG
07/31/13 12:41
JWOLFE
08/05/13 13:55
LWALKER
08/14/13 06:53
TSMITH
13
TRG
07/31/13 12:41
JWOLFE
08/05/13 13:55
LWALKER
08/14/13 06:53
TSMITH
14
TRG
07/31/13 12:41
JWOLFE
08/05/13 13:55
LWALKER
08/14/13 06:53
TSMITH
I
15
TRG
07/31/13 12:41
JWOLFE
08/05/13 13:55
LWALKER
08/14/13 06:53
TSMITH
16
TRG
07/31/13 12:41
JWOLFE
08/05/13 13:55
LWALKER
08/14/13 06:53
TSMITH
17
TRG
07/31/13 12:41
JWOLFE
08/05/13 13:55
LWALKER
08/14/13 06:53
TSMITH
18
TRG
07/31/13 12:41
JWOLFE
08/05/13 13:55
LWALKER
08114/13 06:53
TSMITH
19
TRG
07/31/13 12:41
JWOLFE
08/05/13 13:55
LWALKER
08/14/13 06:53
TSMITH
~~:!li
(J()
Eberline Servic~s
a::
or
--
{;
0
.!!!
~
as
c:
<:(
co
N
N
cu
0:::
Work Order: 13-07147 -Ra228-1
LCS
Known
LCS
%R
LCS
Flag
92.87
OK
RPD
Flag
MDA
Flag
Nuclide
Sample
Desc
Client
Identification
Activity
Units
01
RA-228
LCS
LCS
pCi/1
8.18E+OO
9.14E-01
1.17E+OO
02
RA-228
MBL
BLANK
pCi/1
1.01E+OO
5.67E-01
1.08E+OO
03
RA-228
DUP
D-12 TOT
pCi/1
3.76E-01
5.83E-01
1.21E+OO
04
RA-228
DO
D-12 TOT
pCi/1
1.13E+OO
6.70E-01
1.30E+OO
OK
05
RA-228
TRG
D-12 DIS
pCi/1
1.74E+OO
6.83E-01
1.26E+OO
OK
RA-228
TRG
DUPOS TOT
pCi/1
9.66E-01
7.01E-01
1.39E+OO
OK
RA-228
TRG
DUPOS DIS
pCi/1
1.44E+OO
7.15E-01
1.37E+OO
OK
08
RA-228
TRG
PZ-208-SS TOT
pCi/1
2.37E+OO
8.03E-01
1.46E+OO
OK
09
RA-228
TRG
PZ-208-SS DIS
pCi/1
1.10E+OO
6.98E-01
1.37E+OO
OK
10
RA-228
TRG
PZ-304-AI TOT
pCi/1
2.52E+OO
7.57E-01
1.33E+OO
11
RA-228
TRG
PZ-304-AI DIS
pCi/1
2.43E+OO
7.96E-01
1.44E+OO
OK
12
RA-228
TRG
PZ-304-AS TOT
pCi/1
1.79E+OO
6.98E-01
1.28E+OO
OK
13
RA-228
TRG
PZ-304-AS DIS
pCi/1
1.93E+OO
7.95E-01
1.49E+OO
OK
14
RA-228
TRG
MW-104 TOT
pCi/1
1.72E+OO
7.86E-01
1.49E+OO
OK
15
RA-228
TRG
MW-104 DIS
pCi/1
8.48E-01
7.24E-01
1.46E+OO
OK
RA-228
TRG
PZ-204A-SS TOT
pCi/1
5.73E-01
7.32E-01
1.50E+OO
OK
17
RA-228
TRG
PZ-204A-SS DIS
pCi/1
1.59E+OO
7.23E-01
1.37E+OO
OK
18
RA-228
TRG
PZ-302-AI TOT
19
RA-228
TRG
PZ-302-AI DIS
Lab
Fraction
Printed: 8/14/2013 2:47PM
Page 1 of 3
Results
Error Estimate
MDA
8.81E+OO
Blank
Flag
OK
OK
OK
----
r-
NA
OK
r------
!------------
06
---
07
---
C--------
OK
r-------
.5
;::
-----~--
Q.
Q.
:I
!/)
~I
r--------
....c:
1------'
16
Cl>
Cl>
Cl
r--
res
c:
res
:!:
Cl
c:
;:
Cl>
Cl>
1:::
c;,
c:
w
,1!1!
.~~
..
r--
pCi/1
8.53E-01
7.57E-01
1.53E+OO
OK
pCi/1
1.34E+OO
8.83E-01
1.74E+OO
OK
"
Eberline Services
Lab
Fraction
Nuclide
01
RA-228
Printed: 8/14/2013 2:47PM
Page 2 of 3
Work Order: 13-07147 -Ra228-1
Sample
Sample
Aliquot
Grav
%Rec
Radiometric
%Rec
Mean
%Rec
Sep tO
Date/Time
Sep 11
Date/Time
Desc
Sample
Date
LCS
07/23/13 00:00
1.00E+OO
93.67
88.68
83.06
1.00
8/5/2013 13:55
8/14/2013 6:53
MBL
07/23/13 00:00
1.00E+OO
93.77
85.59
80.26
1.00
8/5/2013 13:55
8/14/2013 6:53
07/15/13 15:27
1.00E+OO
98.48
84.12
82.84
1.00
8/5/2013 13:55
8/14/2013 6:53
SAF
a:
02
RA-228
- -------
T"'"
03
RA-228
DUP
---
.g
8
00
N
N
'iV
0::
.!!!
~
c:
"'(
ca
04
RA-228
DO
07/15/13 15:27
1.00E+OO
88.76
81.76
72.58
1.00
8/5/2013 13:55
8/14/2013 6:53
05
RA-228
TRG
07/15/13 15:27
1.00E+OO
95.69
83.53
79.93
1.00
8/5/2013 13:55
8/14/2013 6:53
06
RA-228
TRG
07/15/13 00:00
1,00E+OO
93.28
86.03
80.25
1.00
8/5/2013 13:55
8/14/2013 6:53
07
RA-228
07/15/13 00:00
1.00E+OO
94.44
81.91
77.36
1.00
8/5/2013 13:55
8/14/2013 6:53
,_
I
TRG
.
08
RA-228
TRG
07/16/13 09:25
1.00E+OO
90.10
82.21
74.07
1.00
8/5/2013 13:55
8/14/2013 6:53
09
RA-228
TRG
07/16/13 09:25
1.00E+OO
99.75
81.91
81.71
1.00
8/5/2013 13:55
8/14/2013 6:53
10
RA-228
TRG
07/16/13 12:05
1.00E+OO
91.50
80.74
73.88
1.00
8/5/2013 13:55
8/14/2013 6:53
11
RA-228
TRG
07/16/13 12:05
1.00E+OO
97.31
79.12
76.99
1.00
8/5/2013 13:55
8/14/2013 6:53
12
RA-228
TRG
07/16/13 12:34
1.00E+OO
94.55
80.44
76.06
1.00
8/5/2013 13:55
8/14/2013 6:53
07/16/13 12:34
1.00E+OO
87.71
83.09
72.88
1.00
8/5/2013 13:55
8/14/2013 6:53
07/16/13 13:25
1.00E+OO
87.74
83.09
72.90
1.00
8/5/2013 13:55
8/14/2013 6:53
07/16/13 13:25
1.00E+OO
97.16
82.94
80.59
1.00
8/5/2013 13:55
8/14/2013 6:53
--..--
c..i
.E
t:
0
c..
c..
::s
en
....c
c:
~
Q)
E
Q)
Cl
cG
c
:E
cG
Cl
;:
Q)
Q)
.5
Cl
w
(d~
~.
~.,,J
11<....
13
RA-228
TRG
-- ----
14
RA-228
---
15
RA-228
TRG
- --
TRG
- ------
16
RA-228
TRG
07/16/13 13:56
1.00E+OO
92.72
82.21
76.22
1.00
8/5/2013 13:55
8/14/2013 6:53
17
RA-228
TRG
07/16/13 13:56
1.00E+OO
100.43
82.50
82.85
1.00
8/5/2013 13:55
8/14/2013 6:53
18
RA-228
TRG
07/16/13 15:18
1.00E+OO
107.80
84.41
91.00
1.00
8/5/2013 13:55
8/14/2013 6:53i
RA-228
TRG
07/16/13 15:18
1.00E+OO
86.52
83.09
71.89
1.00
8/512013 13:55
8/14/2013 6:53
--
19
!
1
(
c:
~
Printed: 8/14/2013 2:47PM
Page 3 of 3
Eberline Services
Work Order: 13-07147-Ra228-1
Lab
Fraction
Nuclide
Sample
Desc
Counting
Date/Time
01
RA-228
LCS
02
RA-228
03
Halflife
(days)
Count
Time
Counts
Bkg
CPM
Eff
Detect
Carrier
08/14/13 11:08
L84110R
A1
120
606 1.083333333
0.4776
M8L
08/14/13 11:08
L84110R
A2
120
156 0.833333333
0.4699
RA-228
DUP
08/14113 11:08
L84110R
A3
120
162 1.166666667
0.4809
04
RA-228
DO
08/14/1311:08
L84110R
A4
120
177
0.4732
05
RA-228
TRG
08/14/13 11 :08
L84110R
81
120
237 1.166666667
0.4754
n:s
06
RA-228
TRG
08/14/13 11 :08
L84110R
82
120
219 1.383333333
0.4658
07
RA-228
TRG
08114/13 11 :08
L84110R
83
120
229 1.266666667
0.4713
08
RA-228
TRG
08/14/13 11:08
L84110R
84
120
287 1.366666667
0.4773
09
RA-228
TRG
08/14/13 11 :09
L84110A
81
120
225 1.366666667
0.4626
10
RA-228
TRG
08/14/13 11:09
L84110A
82
120
256 1.066666667
0.4691
11
RA-228
TRG
08/14/13 11:09
LB4110A
83
120
273
1.25
0.449
12
RA-228
TRG
08/14/13 11:09
LB4110A
84
120
214 1.016666667
0.4619
c.i
13
RA-228
TRG
08/14113 11:09
LB4110A
C1
120
252
1.3
0.4667
14
RA-228
TRG
08/14/13 11 :09
LB4110A
C2
120
234
1.25
0.4578
15
RA-228
TRG
08/14/13 11:09
LB4110A
C3
120
233
1.55
0.4699
16
RA-228
TRG
08/14/1311:09
LB4110A
C4
120
206 1.466666667
0.4692
17
RA-228
TRG
08/14/13 12:03
LB4110R
C1
120
222 1.166666667
0.4705
18
RA-228
TRG
08/14/13 12:03
LB4110R
C2
120
260 1.766666667
0.4676
19
RA-228
08/14/13 12:03
L84110R
C3
120
225 1.383333333
0.4614
'f"'"
co
.g
8
.!!!
.E
0
Q,
Q,
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1:
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1:
Cll
Cl
<
1:
<
:E
TRG
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'
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~:~
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--
Printed: 8/14/2013 10:16 AM

Page 1 of 1
13-07147-Ra228-1 (pCi/1) in WA
Tracer 10: Ba-6a
Count Room Report

Internal
Fraction
Sample
Desc
Client
ID
01
LCS
LCS
Sample
Date
Sample
Aliquot
07/23/13 00:00
1.0000
MBL
03
DUP
BLANK
-1
07/23/13 00:00
D-12 TOT
04
DO
D-12 TOT
05
TRG
D-12 DIS
06
TRG
DUP05 TOT
07
TRG
DUP05 DIS
08
TRG
09
I
I
Tracer
ACT(dpm)
Radiometric
Tracer (pCi)
Radiometric
% Rec
SAF
1*
SAF
2*
0.9234
915.5317
386.3000
93.67
1.00
1.00
1.0000
0.9145
906.7075
383.0000
93.77
1.00
1.00
07/15/13 15:27
1.0000
0.9149
907.1041
402.4000
98.48
1.00
1.00
07/15/13 15:27
1.0000
0.9109
903.1382
361.1000
88.76
1.00
1.00
07/15/13 15:27
1.0000
0.9102
902.4442
389.0000
95.69
1.00
1.00
07/15/13 00:00
1.0000
0.9138
906.0135
380.7000
93.28
1.00
1.00
0.9128
905.0220
385.0000
94.44
1.00
1.00
02
Tracer
Aliquot (g)
I
'
07/15/13 00:00
1.0000
PZ-208-SS TOT
07/16/13 09:25
1.0000
0.9113
903.5348
366.7000
90.10
1.00
1.00
TRG
PZ-208-SS DIS
07/16/13 09:25
1.0000
0.9122
904.4271
406.4000
99.75
1.00
1.00
10
TRG
PZ-304-AI TOT
07/16/13 12:05
1.0000
0.9115
903.7331
372.5000
91.50
1.00
1.00
11
TRG
PZ-304-AI DIS
07/16/13 12:05
1.0000
0.9100
902.2459
395.5000
97.31
1.00
1.00
12
TRG
PZ-304-AS TOT
07/16/13 12:34
1.0000
0.9079
900.1638
383.4000
94.55
1.00
1.00
13
TRG
PZ-304-AS DIS
07/16/13 12:34
1.0000
0.9121
904.3280
357.3000
87.71
1.00
1.00
14
TRG
MW-104 TOT
07/16/13 13:25
1.0000
0.9090
901.2544
356.2000
87.74
1.00
1.00
15
TRG
MW-104 DIS
07/16/13 13:25
1.0000
0.9091
901.3536
394.5000
97.16
1.00
1.00
16
TRG
PZ-204A-SS TOT
07/16/13 13:56
1.0000
0.9109
903.1382
377.2000
92.72
1.00
1.00
17
TRG
PZ-204A-SS DIS
07/16/13 13:56
1.0000
0.9061
898.3791
406.4000
100.43
1.00
1.00
18
TRG
PZ-302-AI TOT
07/16/13 15:18
1.0000
0.9064
898.6766
436.4000
107.80
1.00
1.00
19
TRG
PZ-302-AI DIS
07/16/13 15:18
1.0000
0.9104
902.6425
351.8000
86.52
1.00
1.00
- -- -
----
ll:l~
~.~~!fl.
"~I
(,1\J!
- ---------
'
Eberline Services
Page 1 of 1
Printed: 7/31/2013 12:41 PM
JWOLFE
Isotope
Sol#
Ra-228
Activity
dpmlg
Solution
Date
37.7151
7/31/2013
Approx
Addition
0.530
LCS
MSD
Volume
Used(g)
Volume
Used(g)
. .
.; ."t~aQ'er,s
Solution
Date
Volume
Used(g)
Approx
Addition
fraction
Isotope
Sol#
01
Ba-133
Ba-6a
991.479 7/31/20131
0.92$4
1.0200
02
Ba-133
Ba-6a
991.479 7/31/2013
0.9145
1.0200
03
Ba-133
Ba-6a
991.479 7/31/2013
0.9149
1.0200
04
Ba-133
Ba-6a
991.479 7/31/2013
0.9109
1.0200
05
Ba-133
Ba-6a
991.479 7/31/2013
0.9102
1.0200
06
Ba-133
Ba-6a
991.479 7/31/2013
0.9138
1.0200
07
Ba-133
Ba-6a
991.479 7/31/2013
0.9128
1.0200
Ba-133
Ba-6a
991.479 7/31/2013
0.9113
1.0200
Ba-133
Ba-6a
991.479 7/31/2013
0.912~
1.0200
Ba-133
Ba-6a
991.479 7/31/2013
0.9115
1.0200
Ba-133
Ba-6a
991.479 7/31/2013
0.910()
1.0200
12
I Ba-133
Ba-6a
991.479 7/31/2013
o:90r9
1.0200
13
Ba-133
Ba-6a
991.479 7/31/20131
0.9121
1.0200
14
Ba-133
Ba-6a
991.479 7/31/2013
0.9090
1.0200
15
Ba-133
Ba-6a
991.479 7/31/2013 '
0.9091
1.0200
16
Ba-133
Ba-6a
991.479 7/31/2013
0.910~
1.0200
17
Ba-133
Ba-6a
991.479 7/31/2013
o;9os1 .
1.0200
18
Ba-133
Ba-6a
991.479 7/31/2013
0.9064
1.0200
19
Ba-133
Ba-6a
991.479 7/31/2013
0.9104 i
1.0200
08
09
I
I
10
11
lti!t!li
~~:.,
~~
Activity
dpm/g
8.81
0.5184
..hJ
,ft::y,,
Version 2.0 08/99
MS
LCS
Known
pCi
Error
Estimate
0.449
Added
pCi
0.00
Error
Estimate
0.000
Known
pCi
0.00
0.000
Balance Printer Tapes
0.00
>::.:;."_':: :+
Tracer
LCS
Matrix Spike
Eberline Analytical
Printed: 7/31/2013 12:34 PM
Page 1 of 1
Aliquot Worksheet
JWOLFE
lab
Fraction
01
02
03
04
05
06
07
08
09
10
11
12
-
13
14
15
16
17
18
19
-
ClientiD
LCS
BLANK
D-12TOT
D-12TOT
D-12 DIS
DUP05TOT
DUP05 DIS
PZ-208-SS TOT
PZ-208-SS DIS
PZ-304-AI TOT
PZ-304-AI DIS
PZ-304-AS TOT
PZ-304-AS DIS
MW-104TOT
MW-104 DIS
PZ-204A-SS TOT
PZ-204A-SS DIS
PZ-302-AI TOT
PZ-302-AI DIS
-
Comments
1Ji1~
.r:rno
Techn;oano
Sample
Dilution Data
Muffle Data
Ratid'"
Post/Pre
..
Type
LCS
MBL
DUP
DO
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
'
\,
,;~!; :~; it Oils
:, '
;/.'
~~
.
~
,v
.'~. ... , :l~il~ ~ ;;:, :...
. '.:
,,
.
,,,'i! ~"";;,
....;p
Aliquot Data
RaU<l ;
Oil Factor
.,..
..
pP;
., ' ,,
'
,.,.
'~
;; P,,,,
.;.
.
"; ,1,:.. ,
......... ,:;:: ... '
;:.; . . t
...
,., ,,....; .
..
,,
.,
. :'' .;;,.
;:
. .
,,
' i ....
\ .'.
ii-'
...
,,, . P
. f l .
';
...v,,
.....,
...
,.
..
':i .
"
., f:
~
~~._c~t'
':
..
.; ...
.;
'---....
',
.,
''.
.'
-
.;
. ,.,,,
'
.,.
Aliquot
.
1.0000E+OO
1.0000E+OO .
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO I
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
H-3 Solids Only
MS Aliquot Data
NetEquiv
1..ooooE+OO
1.QOQOE+OO
Aliquot
Water Added
(ml)
NetEquiv
H3 Dist
Aliq
....:.
1.0QOOE+OO
1':oOOOE+OO
1.0000E+OO
1.0000E+OO
1.0~E+OO
{OOooJ;+OO
1.0000E+OO
1.QOQOE+OO
1.0000E+00
1.0000E+OO
fooooE+OO
:4_
.,
\
1.oooee+ao
1.ooQoE+OO.
1:oooOE+OO
1.QOOOE+OQ
'1.0000E+OO
1.ooooe+oo
..
-----
L__~
...
--
--'
L__ ..
I
'J ~
Date '-:{
2J 1~
Eberline Services - Oak Ridge

Version 1.0 9/1999
Work Order
TRetec
Fraction
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
Client ID
LCS
BLANK
DUP
D-12 TOT
D-12 DIS
DUP05 TOT
DUP05 DIS
PZ-208-SS TOT
PZ-208-SS DIS
PZ-304-AI TOT
PZ-304-AI DIS
PZ-304-AS TOT
PZ-304-AS DIS
MW-104 TOT
MW-104 DIS
PZ-204A-SS TOT
PZ-204A-SS DIS
PZ-302-AI TOT
PZ-302-AI DIS
Sample
Type
LCS
MBL
DUP
DO
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
Analysis
Code
Gravimetric
Carrier
Carrier Cone
(mgfml)
Technician
Ra228
Yttirum
34.0000
TSMITH
Filter Data
Carrier Data
Carrier Added
(ml)
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
~~
...,JI
~~
Technician:-----------------
Date:
Gravimetric
Filter Tare
Filter Final
Filter Net
(g)
(g)
(g)
0.0911
0.0916
0.0914
0.0912
0.0922
0.0922
0.0919
0.0923
0.0923
0.0923
0.0923
0.0925
0.0922
0.0921
0.0921
0.0918
0.0921
0.0920
0.0918
f.",.,
Printed: 8/14/2013 10:16 AM

Page 1 of 1
Gravimetric Worksheet
Sr'1___l_!i!__fj_
0.1514
0.1498
0.1486
0.1468
0.1490
0.1507
0.1476
0.1482
0.1480
0.1472
0.1461
0.1472
0.1487
0.1486
0.1485
0.1477
0.1482
0.1494
0.1483
%...
R~qy~!:y
0.0603
0.0582
0.0.572
.... if8.6~ !
i~' ;J5.s9
. ' . 84.12
o~o556
..
0.0568
0~0585
0.0557
0.0559
0..0557
.0.0549.
0.0538
0.0547
. :l
...
.
80.74
; . . ;f9.12 ;
' . so;.#
0~0565
0.0565
0.0564
0.0559
0.0561
o.o$:t4
O.Q$65
81.76
..$3~53
86.03
8'1.91
8.2.21
IJ1.91 i
;
.
..... < .
... ...
.
... ~
; ..
......
.8$;.09
83;09
.82.94
82.21
,2.50
84)41
83.09
Sheet1
Detector ID Sample ID Alpha

Beta Count Time
Voltage
A1
1307147-01
12
606
120
1400
A2
1307147-02 19
156
120
1400
A3
1307147-03 18
162
120
1400
A4
1307147-04 16
177
120
1400
81
1307147-05 12
237
120
1400
82
1307147-06
7
219
120
1400
83
1307147-07 10
229
120
1400
84
1307147-08
7
287
120
1400
Ci~
f.;~Rt,
Page 1
Bfrr~:;
((g
TOO
8/14/13 13:08
8/14/13 13:08
8/14/13 13:08
8/14/13 13:08
8/14/13 13:08
8/14/13 13:08
8/14/13 13:08
8/14/13 13:08
C..-
~~:
Sheet1
Detector ID Sample ID Alpha

Beta Count Time
Voltage
81
1307147-09 12
225
120
1400
82
1307147-10
7
256
120
1400
83
1307147-11
10
273
120
1400
84
1307147-12 11
214
120
1400
C1
1307147-13 18
252
120
1400
C2
1307147-14 18
234
120
1400
C3
1307147-15 16
233
120
1400
C4
1307147-16 19
206
120
1400
G'l
Jt,~.
Page 1
TOO
8/14/13 13:09
8/14/13 13:09
8/14/13 13:09
8/14/13 13:09
8/14/13 13:09
8/14/13 13:09
8/14/13 13:09
8/14/13 13:09
Sheet1
Detector 10 Sample 10 Alpha Beta Count Time Voltage

TOO
C1
1307147-17 14
222
120
1400 8/14/13 14:03
C2
1307147-18
9
260
120
1400 8/14/13 14:03
C3
1307147-19 12
225
120
1400 8/14/13 14:03
'~
t;'...
....J
u;~
Page 1
~~
Eberline Analytical
Printed: 8/14/2013 6:53AM
Page 1 of 1
GPC Detector Report

(ALL Backgrounds)
C
Detector
Calibration Date
Count Date
Bkg CPM
PFW
LCL
Mean
UCL
-2.13E+01
2.82E-01
2.19E+01
1.86E+01
LB4110A- A1
Alpha
11/18/2007
8/14/2013
S.OOE-02
LB4110A- A2
Alpha
11/18/2007
8/14/2013
8.33E-02
-1.81E+01
2.54E-01
LB4110A- A3
Alpha
11/18/2007
8/14/2013
l.OOE-01
-1.76E+01
2.16E-01
1.80E+01
LB4110A- A4
Alpha
11/18/2007
8/14/2013
6.67E-02
-1.87E+01
2.36E-01
1.92E+01
LB4110A- 81
Alpha
11/18/2007
8/14/2013
8.33E-02
-9.68E-02
7.51E-02
2.47E-01
6.67E-02
-7.81E-02
7.22E-02
2.22E-01
LB4110A- 82
Alpha
11/18/2007
8/14/2013
LB4110A- 83
Alpha
11/18/2007
8/14/2013
6.67E-02
-6.29E-02
5.34E-02
1. 70E-01
LB4110A- 84
Alpha
11/18/2007
8/14/2013
1.67E-02
-1.40E-01
7.88E-02
2.98E-01
LB4110A- C1
Alpha
11/18/2007
8/14/2013
S.OOE-02
-1.49E-01
8.86E-02
3.26E-01
I
I
LB4110A- C2
Alpha
11/18/2007
8/14/2013
8.33E-02
-1.77E-01
8.67E-02
3.50E-01
LB4110A- C3
Alpha
11/18/2007
8/14/2013
l.OOE-01
-1. 72E-01
l.OOE-01
3.72E-01
LB4110A- C4
Alpha
11/18/2007
8/14/2013
1.33E-01
-6.27E-02
6.83E-02
1.99E-01
I
I
LB4110A- 01
Alpha
11/18/2007
8/14/2013
1.67E-02
-5.36E-02
8.33E-02
2.20E-01
LB4110A- 02
Alpha
11/18/2007
8/14/2013
S.OOE-02
-6.98E-02
6.06E-02
1.91E-01
LB4110A- 03
Alpha
11/18/2007
8/14/2013
6.67E-02
-4.85E-02
7.07E-02
1.90E-01
LB4110A- 04
Alpha
11/18/2007
8/14/2013
6.67E-02
-5.72E-02
7.03E-02
1.98E-01
LB4110R- A1
Alpha
11/24/2006
8/14/2013
S.OOE-02
-9.81E-02
1.01E-01
3.00E-01
LB4110R- A2
Alpha
11/24/2006
8/14/2013
3.33E-02
-8.92E-02
7.63E-02
2.42E-01
LB4110R- A3
Alpha
11/24/2006
8/14/2013
8.33E-02
-7.32E-02
7.73E-02
2.28E-01
LB4110R- A4
Alpha
11/24/2006
8/14/2013
1.17E-01
-5.27E-02
7.09E-02
1.94E-01
LB4110R- 81
Alpha
11/24/2006
8/14/2013
S.OOE-02
-9.41E-02
6.16E-02
2.17E-01
11/24/2006
8/14/2013
S.OOE-02
-6.94E-02
6.33E-02
1.96E-01
-6.49E-02
6.99E-02
2.05E-01
LB4110R- 82
Alpha
LB4110R- 83
Alpha
11/24/2006
8/14/2013
6.67E-02
LB4110R- 84
Alpha
11/24/2006
8/14/2013
6.67E-02
-6.38E-02
7.02E-02
2.04E-01
LB4110R- C1
Alpha
11/24/2006
8/14/2013
6.67E-02
-7.67E-02
7.36E-02
2.24E-01
LB4110R- C2
Alpha
11/24/2006
8/14/2013
6.67E-02
-7.54E-02
7.10E-02
2.17E-01
LB4110R- C3
Alpha
11/24/2006
8/14/2013
1.67E-02
-8.79E-02
8.43E-02
2.57E-01
LB4110R- C4
Alpha
11/24/2006
8/14/2013
6.67E-02
-6.18E-02
8.12E-02
2.24E-01
LB4110R- 01
Alpha
11/24/2006
8/14/2013
O.OOE+OO
-1.03E-01
7.01E-02
2.43E-01
LB4110R- 02
Alpha
11/24/2006
8/14/2013
O.OOE+OO
-7.79E-02
6.96E-02
2.17E-01
LB4110R- 03
Alpha
11/24/2006
8/14/2013
O.OOE+OO
-8.29E-02
6.93E-02
2.22E-01
LB4110R- 04
Alpha
11/24/2006
8/14/2013
O.OOE+OO
-7.53E-02
7.41E-02
2.23E-01
S.OOE-02
-1.56E-02
9.58E-02
2.07E-01
LB5100- 1
fJl/!11
Alpha/Beta
Alpha
7/10/2006
10/26/2007
fJttlfl-L--
Eberline Analytical
!1:!~
""'"'
Printed: 8/14/2013 6:53AM
Page 1 of 1
GPC Detector Report

(ALL Backgrounds)
c..
Detector
Alpha/Beta
Calibration Date
Count Date
Bkg CPM
PFW
LCL
Mean
UCL
LB4110A- A1
Beta
11/18/2007
8/14/2013
8.53E+00
-2.89E+02
7.63E+OO
3.04E+02
LB4110A- A2
Beta
11/18/2007
8/14/2013
3.42E+00
-3.03E+01
2.59E+OO
3.55E+01
LB4110A- A3
Beta
11/18/2007
8/14/2013
1.32E+OO
-5.01E+01
2.63E+OO
5.54E+01
LB4110A- A4
Beta
11/18/2007
8/14/2013
7.37E+00
-3.24E+01
3.22E+OO
3.88E+01
LB4110A- B1
Beta
11/18/2007
8/14/2013
1.37E+00:
-1.04E+01
3.23E+OO
1.68E+01
LB4110A- B2
Beta
11/18/2007
8/14/2013
1.07E+00
-7.62E+00
2.00E+OO
1.16E+01
2.60E+OO
LB4110A- B3
Beta
11/18/2007
8/14/2013
1.25E+OO.
1.16E-01
1.36E+OO
LB4110A- B4
Beta
11/18/2007
8/14/2013
1.02E+00.
-7.61E+OO
1.97E+OO
1.16E+01
LB4110A- C1
Beta
11/18/2007
8/14/2013
1.30E+00
-5.38E+00
2.12E+OO
9.62E+OO
LB4110A- C2
Beta
11/18/2007
8/14/2013
1.25E+00
3.81E-01
1.27E+OO
2.15E+OO
4.72E-01
1.46E+OO
2.45E+OO
LB4110A- C3
Beta
11/18/2007
8/14/2013
l.SSE+OO,
LB4110A- C4
Beta
11/18/2007
8/14/2013
1.47E+00'
-1.75E+00
2.10E+OO
5.95E+OO
LB4110A- D1
Beta
11/18/2007
8/14/2013
2.17E+00
-2.31E+00
2.56E+OO
7.43E+OO
3.76E+OO
LB4110A- D2
Beta
11/18/2007
8/14/2013
1.45E+00
-6.40E-01
1.56E+OO
LB4110A- D3
Beta
11/18/2007
8/14/2013
4.92E+00
1.29E+OO
4.48E+OO
7.66E+OO
LB4110A- D4
Beta
11/18/2007
8/14/2013
1.25E+00
-4.23E-01
1.37E+OO
3.16E+OO
LB4110R- A1
Beta
11/24/2006
8/14/2013
1.08E+00
-6.08E+01
3.66E+OO
6.81E+01
LB4110R- A2
Beta
11/24/2006
8/14/2013
8.33E-01 .
-4.83E+01
2.01E+OO
5.23E+01
LB4110R- A3
Beta
11/24/2006
8/14/2013
1.17E+00-
-4.47E+01
2.73E+OO
5.02E+01
LB4110R- A4
Beta
11/24/2006
8/14/2013
l.OOE+OO
-4.46E+01
1.99E+OO
4.86E+01
LB4110R- B1
Beta
11/24/2006
8/14/2013
1.17E+00
-4.69E+01
2.02E+OO
5.10E+01
LB4110R- B2
Beta
11/24/2006
8/14/2013
1.38E+00
-4.69E+01
2.05E+OO
5.10E+01
LB4110R- B3
Beta
11/24/2006
8/14/2013
1.27E+00
-4.67E+01
2.65E+OO
5.20E+01
5.09E+01
LB4110R- B4
Beta
11/24/2006
8/14/2013
1.37E+OO
-4.70E+01
1.92E+OO
LB4110R- C1
Beta
11/24/2006
8/14/2013
1.17E+OO
-4.68E+01
2.96E+OO
5.27E+01
LB4110R- C2
Beta
11/24/2006
8/14/2013
1.77E+OO.
-4.68E+01
2.71E+OO
5.22E+01
LB4110R- C3
Beta
11/24/2006
8/14/2013
1.38E+OO
-4.72E+01
2.52E+OO
5.23E+01
LB4110R- C4
Beta
11/24/2006
8/14/2013
1.75E+00
-5.33E+01
2.95E+OO
5.92E+01
LB4110R- D1
Beta
11/24/2006
8/14/2013
O.OOE+OO
-4.44E+01
S.SSE+OO
5.55E+01
LB4110R- D2
Beta
11/24/2006
8/14/2013
O.OOE+OO
-4.77E+01
1.87E+OO
5.15E+01
LB4110R- D3
Beta
11/24/2006
8/14/2013
O.OOE+OO
-5.11E+01
5.52E+OO
6.22E+01
LB4110R- D4
Beta
11/24/2006
8/14/2013
O.OOE+OO
-4.74E+01
2.23E+OO
5.19E+01
LB5100- 1
Beta
~1_10/2906-
10/26/2007
-
4.52E+OO
-3.19E-01
1.5_8_E:-f:OO _ __3.4-8E+OO
----------------------
----
'-------
-------
~I fl.ftt---
.....
Eberline Analytical
Detector
Alpha/Beta
Calibration Date
Count Date
Eff
PFW
LCL
Mean
UCL
L84110A- A1
Alpha
11/18/2007
8/14/2013
0.2512
-0.0128
0.2159
0.4446
L84110A- A2
Alpha
11/18/2007
8/14/2013
0.1976
-0.0503
0.1741
0.3986
L84110A- A3
Alpha
11/18/2007
8/14/2013
0.2062
-0.0736
0.1634
0.4004
L84110A- A4
Alpha
11/18/2007
8/14/2013
0.2163
-0.0521
0.1821
0.4162
LB4110A- 81
Alpha
11/18/2007
8/14/2013
0.2161
0.1943
0.2243
0.2543
L84110A- 82
Alpha
11/18/2007
8/14/2013
0.2080
0.1923
0.2213
0.2502
0.2305
0.1279
0.2323
0.3366
0.2088
0.2364
0.2639
L84110A- 83
Alpha
L84110A- B4
Alpha
11/18/2007
8/14/2013
0.2253
L84110A- C1
Alpha
11/18/2007
8/14/2013
0.2185
0.1976
0.2207
0.2439
0.2271
0.1971
0.2252
0.2532
W'!JI
11/18/2007
8/14/2013
L84110A- C2
Alpha
L84110A- C3
Alpha
11/18/2007
8/14/2013
0.2512
0.2234
0.2494
0.2755
L84110A- C4
Alpha
11/18/2007
8/14/2013
0.2224
0.1969
0.2256
0.2544
LB4110A- 01
Alpha
11/18/2007
8/14/2013
0.2246
0.2028
0.2328
0.2628
11/18/2007
8/14/2013
L84110A- 02
Alpha
11/18/2007
8/14/2013
0.2532
0.2277
0.2580
0.2884
L84110A- 03
Alpha
11/18/2007
8/14/2013
0.2557
0.2309
0.2634
0.2958
L84110A- 04
Alpha
11/18/2007
8/14/2013
0.1884
0.1642
0.1992
0.2342
L84110R- A1
Alpha
11/24/2006
8/14/2013
0.2327
0.1983
0.2385
0.2786
L84110R- A2
Alpha
11/24/2006
8/14/2013
0.2088
0.1851
0.2201
0.2551
L84110R- A3
Alpha
11/24/2006
8/14/2013
0.2141
0.1924
0.2243
0.2563
8/14/2013
0.2384
0.2118
0.2453
0.2789
0.1832
0.2257
0.2681
LB4110R- A4
Alpha
L84110R- 81
Alpha
11/24/2006
8/14/2013
0.2190
L84110R- 82
Alpha
11/24/2006
8/14/2013
0.2072
0.1754
0.2169
0.2585
11/24/2006
L84110R- 83
Alpha
11/24/2006
8/14/2013
0.2453
0.2015
0.2438
0.2861
LB4110R- 84
Alpha
11/24/2006
8/14/2013
0.2154
0.1882
0.2312
0.2742
LB4110R- C1
Alpha
11/24/2006
8/14/2013
0.2126
0.1833
0.2150
0.2466
0.2208
0.1932
0.2245
0.2558
L84110R- C2
Alpha
L84110R- C3
Alpha
11/24/2006
8/14/2013
0.2345
0.2034
0.2394
0.2754
L84110R- C4
Alpha
11/24/2006
8/14/2013
0.2093
0.1826
0.2222
0.2618
L84110R- 01
Alpha
11/24/2006
8/14/2013
0.0000
0.0035
0.1992
0.3949
L84110R- 02
Alpha
11/24/2006
8/14/2013
0.0000
0.0047
0.2265
0.4484
L84110R- 03
Alpha
11/24/2006
8/14/2013
0.0000
0.0046
0.2225
0.4404
L84110R- 04
Alpha
11/24/2006
8/14/2013
0.0000
0.0023
0.1793
0.3564
0.3368
0.3332
0.3455
0.3578
L85100 - 1
t;l~l
Printed: 8/14/2013 6:53AM
Page 1 of 1
GPC Detector Report

(ALL Efficiencies)
Alpha
11/24/2006
7/10/2006
8/14/2013
10/26/2007
~
I
I
~ f(Cft'-
Eberline Analytical
Detector
Alpha/Beta
Calibration Date
Count Date
Eff
PFW
LCL
Mean
UCL
LB4110A- A1
Beta
11/18/2007
8/14/2013
0.5501
0.2112
0.5625
0.9138
0.1621
0.4648
0.7676
LB4110A- A2
Beta
11/18/2007
8/14/2013
0.4861
LB4110A- A3
Beta
11/18/2007
8/14/2013
0.4623
0.0901
0.4572
0.8243
LB4110A- A4
Beta
11/18/2007
8/14/2013
0.5187
0.1429
0.4892
0.8355
LB4110A- B1
Beta
11/18/2007
8/14/2013
0.5074
0.4634
0.5297
0.5961
0.5085
0.4632
0.5268
0.5904
0.3169
0.5314
0.7459
LB4110A- B2
Beta
11/18/2007
8/14/2013
LB4110A- B3
Beta
11/18/2007
8/14/2013
0.5253
LB4110A- B4
Beta
11/18/2007
8/14/2013
0.5471
0.4918
0.5538
0.6158
0.5013
0.4511
0.5026
0.5542
0.4293
0.5010
0.5728
LB4110A- C1
Beta
LB4110A- C2
Beta
11/18/2007
8/14/2013
0.4973
LB4110A- C3
Beta
11/18/2007
8/14/2013
0.6105
0.5291
0.5907
0.6523
0.5262
0.4578
0.5248
0.5918
0.4784
0.5530
0.6275
LB4110A- C4
Beta
11/18/2007
11/18/2007
8/14/2013
8/14/2013
LB4110A- D1
Beta
11/18/2007
8/14/2013
0.5361
LB4110A- D2
Beta
11/18/2007
8/14/2013
0.5635
0.4887
0.5871
0.6855
0.6122
0.5374
0.6149
0.6924
LB4110A- D3
Beta
11/18/2007
8/14/2013
g(C('
'
LB4110A- D4
Beta
11/18/2007
8/14/2013
0.4431
0.3845
0.4719
0.5592
LB4110R- A1
Beta
11/24/2006
8/14/2013
0.5579
0.4743
0.5672
0.6601
LB4110R- A2
Beta
11/24/2006
8/14/2013
0.5014
0.4158
0.5085
0.6013
8/14/2013
0.5143
0.4503
0.5384
0.6264
0.5032
0.5914
0.6797
I
I
0.5422
0.6380
LB4110R- A3
Beta
LB4110R- A4
Beta
11/24/2006
8/14/2013
0.5879
LB4110R- B1
Beta
11/24/2006
8/14/2013
0.5302
0.4463
11/24/2006
LB4110R- B2
Beta
11/24/2006
8/14/2013
0.5048
0.4247
0.5195
0.6144
LB4110R- B3
Beta
11/24/2006
8/14/2013
0.6049
0.4939
0.5917
0.6895
LB4110R- B4
Beta
11/24/2006
8/14/2013
0.5211
0.4540
0.5489
0.6438
0.4606
0.4159
0.5015
0.5871
0.4440
0.5283
0.6126
Beta
11/24/2006
8/14/2013
LB4110R- C2
Beta
11/24/2006
8/14/2013
0.5183
LB4110R- C3
Beta
11/24/2006
8/14/2013
0.5685
0.4755
0.5706
0.6656
0.4258
0.5249
0.6241
LB4110R- C4
Beta
11/24/2006
8/14/2013
0.4916
11/24/2006
8/14/2013
0.0000
0.0076
0.4763
0.9450
0.0092
0.5352
1.0613
LB4110R- D1
Beta
LB41.10R - D2
Beta
11/24/2006
8/14/2013
0.0000
LB4110R- D3
Beta
11/24/2006
8/14/2013
0.0000
0.0089
0.5198
1.0308
LB4110R- D4
Beta
11/24/2006
8/14/2013
0.0000
0.0044
0.4279
0.8514
LB5100 - 1
Beta
7/10/2006
10/26/2007
0.4428
0.4555
0.4731
0.4906
L........
c__
LB4110R- C1
~f.lll
Printed: 8/14/2013 6:53AM
Page 1 of 1
GPC Detector Report

(ALL Efficiencies)
SECTION XII
BARIUM-133 ANALYTICAL TRACER DATA
1484
e:_
VAX/VMS Peak Search Report Generated
Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
t {,ffJ
DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP_130714701 - GE3 BAFIL 194347.CN

PEAK V16.9 PEAKEFF V2.2
SPIKE
6-AUG-2013 00:00:00.
1307147-01
FILTER
GE3
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
30.83
34.96
52.44
61.75
65.72
81.05
85.15
87.84
92.69
111.79
115.95
161.37
187.85
238.42
276.61
303.09
307.53
311.86
333.74
338.14
356.31
377.05
384.05
387.02
391.34
414.72
418.06
437.26
468.07
473.33
511.29
514.88
911.22
2139
540
59
244
108
806
20
28
29
214
65
17
49
28
56
116
34
11
94
30
548
12
120
222
49
38
16
120
20
10
12
6
8
86
71
129
62
59
55
60
58
55
50
46
72
126
59
37
52
7
15
12
14
21
27
24
19
16
20
26
4
4
1
2
0
0
2
2
0
1
1
3
3
3
3
2
2
0
0
0
0
0
1
1
3
3
0
2
2
2
2
2
2
0
2
2
3
3
0
6-AUG-2013 09:35:33.57
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1.58
1. 57
2.54
1. 51
1.52
1.48
1. 87
1. 88
1. 89
1. 75
1. 76
0.88
7.46
1.13
1. 24
1. 67
1.81
1. 81
1.88
2.22
1. 95
2.05
2.06
1. 85
2.06
2.08
2.09
2.00
2.13
2.13
2.38
1. 97
1. 33
31.15
35.28
52.76
62.06
66.04
81.36
85.47
88.16
93.01
112.10
116.27
161. 68
188.16
238.73
276.91
303.40
307.84
312.16
334.05
338.45
356.62
377.36
384.36
387.32
391.64
415.02
418.36
437.56
468.37
473.63
511.59
515.18
911.50
Left
Pw
26
26
48
57
57
77
77
77
77
107
107
158
182
235
273
298
307
307
329
329
354
374
374
374
374
411
411
434
464
464
507
507
908
13
13
9
17
17
23
23
23
23
13
13
7
12
8
7
9
8
8
15
15
9
23
23
23
23
11
11
7
14
14
11
11
7
6-AUG-2013 09:20:14.
l.OOOOOE+OO filter
0
BAFIL
0 00:15:04.59 0.5%
4096
10.00000
Cts/Sec %Err
2.38E+00
6.00E-01
6.52E-02
2.71E-Ol
1.20E-01
8.95E-01
2.26E-02
3.13E-02
3.24E-02
2.38E-01
7.21E-02
1.84E-02
5.45E-02
3.13E-02
6.26E-02
1.28E-01
3.76E-02
1.26E-02
1. 04E- 01
3.32E-02
6.09E-01
1.29E-02
1.34E-01
2.47E-01
5.40E-02
4.24E-02
1.75E-02
1.33E-01
2.20E-02
1.14E-02
1.32E-02
6.21E-03
8.89E-03
2.3
5.0
37.4
8.3
15.4
3.7
72.6
51.6
49.9
8.6
20.5
88.2
48.3
50.6
22.3
14.7
10.7
65.0
12.3
33.9
4.5
68.2
11.3
7.9
22.1
25.1
65.3
9.5
28.3
44.0
39.5
72.2
35.4
Fit
1. OlE+Ol
5.25E+00
3.32E+00
2.88E+00
8.67E+00
3.66E+00
4.00E+00
2.71E+00
7.27E-01
6.04E-01
!:485
Summary of Nuclide Activity

Sample ID : 1307147-01
Acquisition date
Total number of lines in spectrum

Number of unidentified lines
Number of lines tentatively identified by NID
33
28
5
Page :
2
6-AQG-2013 09:20:14
15.15%
Nuclide Type : FISSION

Nuclide
Hlife
CD-109
464.00D
BA-133
10.50Y
NP-237 2.14E+06Y
Decay
1. 00
1. 00
1. 00
Total Activity
Wtd Mean
Uncorrected
pCi/filter
1.328E+02
3.863E+02
3.838E+01
--------
5.575E+02
Wtd Mean
Decay Corr
pCi/filter
1.329E+02
3.863E+02
3.838E+01
2-Sigma
Decay Corr
2-Sigma Error %Error Flags
103.66
1.378E+02
17.47
0.675E+02
103.65
3.978E+01
--------
5.576E+02
Nuclide Type : NATQRAL

Nuclide
Hlife
TH-234 4.47E+09Y
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
7.277E+02
Total Activity
Grand Total Activity :
--------
Wtd Mean
Decay Corr
pCi/filter
7.277E+02
--------
7.277E+02
7.277E+02
1.285E+03
1.285E+03
Flags: "K" = Keyline not found

"E" = Manually edited
2-Sigma
Decay Corr
17.98
1.308E+02
"M" = Manually accepted

"A" = Nuclide specific abn. limit
Nuclide Line Activity Report

Sample ID : 1307147-01
Acquisition date
Page :
3
6-AUG-2013 09:20:14
Nuclide Type: FISSION

Nuclide
CD-109
Energy
88.03
%Abn
3.72*
Final Mean for

BA-133
81.00
302.84
356.01
NP-237
86.50
1 Valid Peaks =
33.00*
17.80
60.00
Final Mean for
1.899E+01
6.222E+00
5.860E+00
1.749E+01
3.863E+02
3.134E+02
4.679E+02
17.47
35.93
16.37
OK
OK
OK
3.863E+02+/- 6.747E+01 ( 17.47%)
3.838E+01
1 Valid Peaks =
Status
OK
1.329E+02+/- 1.378E+02 (103.66%)
3.863E+02
3.134E+02
4.679E+02
3 Valid Peaks =
12.60*
Final Mean for
Uncorrected Decay Corr 2-Sigma

%Eff
pCi/filter pCi/filter %Error
1.712E+01 1.328E+02
1.329E+02 103.66
3.838E+01 103.65
OK
3.838E+01+/- 3.978E+01 (103.65%)
Nuclide Type: NATURAL

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag: "*"
Keyline

%Eff
2.648E+01 7.277E+02
7.277E+02 17.98
1 Valid Peaks
Status
OK
7.277E+02+/- 1.308E+02 ( 17.98%)
Combined Activity-MDA Report

Sample ID : 1307147-01
Acquisition date
Page :
4
6-AUG-2013 09:20:14
Identified Nuclides
Nuclide
CD-109
BA-133
TH-234
NP-237
Activity
(pCi/filter)
Act error
1.329E+02
3.863E+02
7.277E+02
3.838E+01
1.378E+02
6.747E+01
1.308E+02
3.978E+01
MDA
(pCi/filter)
1.949E+02
1.973E+01
1.265E+02
5.624E+01
MDA error
Act/MDA
1.607E+01
3.017E+00
6.793E+00
4.546E+00
0.682
19.583
5.754
0.683
MDA error
Act/MDA
1.238E+00
4.459E-02
3.985E-02
9.422E-01
0.382
0.792
1.435
1.727
Non-Identified Nuclides
Nuclide
C0-57
PA-231
PA-234
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
4.144E+00
2.484E+00
4.020E+00
3.309E+01
Act error
6.242E+00
1.561E+00
1.449E+00
1.000E+01
MDA
(pCi/filter)
1.083E+01
3.135E+00
2.802E+00
1.916E+01
c_
Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
B/ ~/1-:::.
DKA100: [GAMMA.SCUSR.ARCHIVE]SMP_130714702 GE3 BAFIL 194349.CN

BLANK
6-AUG-2013 00:00:00.
1307147-02
FILTER
GE3
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
6
6
6
3
3
3
3
2
2
0
4
4
0
0
4
4
4
0
0
0
1
1
0
0
0
0
0
27.81
30.88
34.95
53.23
61.74
65.75
69.82
80.98
84.63
94.08
111. 8 8
116.01
143.05
276.92
303.17
307.44
311.62
333.95
338.84
356.22
384.70
390.70
417.21
437.31
468.19
510.97
609.20
39
1886
546
55
252
114
19
799
19
54
224
57
44
46
161
42
11
81
20
496
92
42
84
103
29
14
12
50
89
129
52
55
72
62
66
54
94
44
37
115
37
16
19
18
17
31
21
11
4
20
13
10
7
2
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
6-AUG-2013 09:53:12.81
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1. 43
1.43
2.33
1. 80
1. 82
1. 83
1.52
1.70
1. 70
1.96
1. 80
2.13
2.79
1.14
1. 74
2.29
2.41
1. 79
1. 63
1. 90
1. 70
1. 71
4.65
1. 83
1.82
1.85
2.06
28.13
31.20
35.27
53.55
62.06
66.07
70.14
81.29
84.95
94.40
112.20
116.32
143.36
277.23
303.48
307.75
311.92
334.25
339.15
356.52
385.00
391.00
417.52
437.61
468.49
511.27
609.49
6-AUG-2013 09:37:50.
1.00000E+00 filter
0
BAFIL
0 00:15:05.58 0.6%
4096
10.00000
Left
Pw
Cts/Sec %Err
27
27
27
49
49
49
49
76
76
89
107
107
138
273
301
301
301
331
337
351
381
381
412
432
462
507
606
14
14
14
25
25
25
25
13
13
10
14
14
13
8
14
14
14
6
6
12
14
14
13
10
9
9
8
4.31E-02 25.3
2.10E+00 2.4
6.06E-01 6.8
6.16E-02 25.8
2.80E-01 7.8
1.27E-01 16.7
2.10E-02 65.1
8.88E-01 3.8
2.16E-02112.2
5.99E-02 36.4
2.49E-01 8.0
6.28E-02 28.3
4.88E-02 52.4
5.14E-02 27.2
1.79E-01 8.4
4.63E-02 31.5
1.21E-02 88.3
9.05E-02 13.6
2.21E-02 48.0
5.51E-01 4.9
1.02E-01 12.9
4.69E-02 28.7
9.31E-02 15.4
1.15E-01 11.7
3.22E-02 26.5
1. 58E- 02 42.3
1.31E-02 36.1
Fit
3.80E+01
4.11E+00
9.71E+00
1.81E+00
6.23E+00
2.55E+01

Sample ID : 1307147-02
Acquisition date

27
22
5
Page :
2
6-AUG-2013 09:37:50
18.52%

Nuclide
Hlife
BA-133
10.50Y
NP-237 2.14E+06Y
Wtd Mean
uncorrected
Decay pCi/filter
1. 00
3.830E+02
1.00 2.654E+01
Total Activity
Nuclide Type
---------
4.095E+02
Wtd Mean
uncorrected
Decay pCi/filter
1.00 7.529E+02
Total Activity
=
=
---------
2-Sigma
Decay Corr
17.54
0.672E+02
224.64
5.962E+01
4.095E+02
NATURAL
Nuclide
Hlife
TH-234 4.47E+09Y
Flags: nKn
nEn
Wtd Mean
Decay Corr
pCi/filter
3.830E+02
2.654E+01
---------
Wtd Mean
Decay Corr
pCi/filter
7.529E+02
---------
7.529E+02
7.529E+02
1.162E+03
1.162E+03
Keyline not found

Manually edited
Decay Corr
2-Sigma
1.284E+02
17.05
liM II
All
II
=
=
Manually accepted
Nuclide specific abn. limit

Sample ID : 1307147-02
Acquisition date
Page :
3
6-AUG-2013 09:37:50

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

NP-237
86.50
3 Valid Peaks
12.60*
Final Mean for

%Eff
1.899E+01 3.830E+02
3.830E+02 17.54
6.222E+00 4.372E+02
4.372E+02 26.56
4.235E+02 16.75
5.860E+00 4.234E+02
1.749E+01
1 Valid Peaks
3.830E+02+/- 6.719E+01 ( 17.54%)
2.654E+01
=
Status
OK
OK
OK
2.654E+01 224.64
OK
2.654E+01+/- 5.962E+01 (224. 64%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag: "*"

%Eff
2.648E+01 7.529E+02
7.529E+02 17.05
1 Valid Peaks
Status
OK
7.529E+02+/- 1.284E+02 ( 17.05%)
Keyline
8491

Sample ID : 1307147-02
----
Acquisition date
Page :
4
6-AUG-2013 09:37:50
Identified Nuclides
Nuclide
BA-133
TH-234
NP-237
Activity
(pCi/filter)
3.830E+02
7.529E+02
2.654E+01
Act error
6.719E+01
1.284E+02
5.962E+01
MDA
(pCi/filter)
1.860E+01
1.225E+02
4.593E+01
MDA error
Act/MDA
2.845E+00
6.579E+00
3.713E+00
20.585
6.147
0.578
MDA error
Act/MDA
9.522E-01
1.333E+01
4.381E-02
4.030E-02
8.915E-01
0.033
0.046
0.761
1.458
1. 576
Nuclide
C0-57
CD-109
PA-231
PA-234
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
2.768E-01
7.425E+00
2.343E+00
4.132E+00
2.858E+01
Act error
5.037E+00
1.118E+02
1.536E+00
1.399E+00
9.064E+00
MDA
(pCi/filter)
8.335E+00
1.617E+02
3.080E+00
2.834E+00
1.813E+01
C
Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
er"fl?
DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP_l30714703 GE3 BAFIL 194350.CN

D-12 TOT
6-AUG-2013 00:00:00.
1307147-03
FILTER
GE3
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
30.84
35.12
52.33
61.88
66.00
76.68
81.26
84.22
111.83
115.89
135.15
246.22
253.29
276.84
303.06
307.37
311.32
333.66
338.27
352.70
356.35
365.62
384.05
387.34
391.59
416.75
422.34
437.24
467.93
511.41
610.71
1960
434
48
259
105
14
839
30
228
37
31
16
19
62
141
25
13
63
22
12
452
9
108
222
42
47
12
125
23
18
14
99
78
114
71
83
23
57
49
43
51
66
9
23
23
17
17
15
26
24
6
15
29
12
14
15
2
0
2
1
14
0
3
3
0
3
3
3
3
3
5
5
0
3
3
0
4
4
4
3
3
3
3
0
2
2
2
5
5
0
0
0
0
6-AUG-2013 10:11:24.77
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1. 54
1.73
2.52
1. 81
1. 83
1.40
1.87
1.87
1. 63
2.34
2.31
2.12
2.13
1.41
1. 76
2.40
2.41
1.94
2.22
1. 68
1.51
1. 34
2.06
2.06
1. 87
2.77
2.09
1. 98
1.79
3.93
2.96
31.16
35.44
52.65
62.19
66.32
77.00
81.58
84.53
112.15
116.20
135.47
246.53
253.60
277.15
303.37
307.67
311.63
333.97
338.57
353.00
356.66
365.93
384.36
387.64
391.90
417.05
422.64
437.54
468.23
511.71
611.00
6-AUG-2013 09:56:04.
l.OOOOOE+OO filter
0
BAFIL
0 00:15:05.25 0.6%
4096
10.00000
Left
Pw
Cts/Sec %Err
26
26
49
58
58
76
76
76
108
108
132
245
245
274
297
297
297
330
330
351
351
362
381
381
381
412
412
434
465
507
607
15
15
8
16
16
12
12
12
24
24
10
13
13
7
18
18
18
16
16
12
12
7
15
15
15
18
18
8
6
11
9
2.18E+00 2.4
4.83E-01 5.9
5.30E-02 41.6
2.87E-01 7.7
1.17E-01 17.6
1.58E-02 45.4
9.33E-01 3.6
3.31E-02 78.0
2.54E-01 7.8
4.14E-02 43.9
3.46E-02 51.7
1.73E-02 28.0
2.07E-02 48.7
6.84E-02 18.1
1. 56E-01 9.3
2.73E-02 49.4
1.48E-02 69.9
7.03E-02 17.7
2.43E-02 50.8
1. 37E-02 40.4
5.02E-Ol 4.8
9.63E-03109.4
1. 20E-01 11.5
2.47E-01 7.6
4.71E-02 21.9
5.22E-02 20.7
1.30E-02 47.7
1.39E-01 9.2
2.51E-02 22.7
1.99E-02 46.6
1. 56E-02 26.7
Fit
9.20E+00
1.72E+00
9.58E+01
1. 21E+00
1.40E+00
1.61E+00
4.85E+00
2.11E+00
2.52E+Ol
4.20E+00

Sample ID : 1307147-03
Acquisition date

31
26
5
Page :
2
6-AUG-2013 09:56:04
16.13%

Nuclide
BA-133
Hlife
10.50Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 4.023E+02
Total Activity
4.023E+02
Wtd Mean
Decay Corr
pCi/filter
4.024E+02
Decay Corr
2-Sigma
17.39
0.700E+02
4.024E+02
Nuclide Type : NATURAL

Nuclide
Hlife
TH-234 4.47E+09Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 7.722E+02
Total Activity
Flags: "K"
"E"
Wtd Mean
Decay Corr
pCi/filter
7.722E+02
7.722E+02
7.722E+02
1.175E+03
1.175E+03
= Keyline not found

= Manually edited
"M"
"A"
Decay Corr
2-Sigma
1.299E+02
16.82
= Manually accepted
= Nuclide specific abn. limit

Sample ID : 1307147-03
Acquisition date
Page :
3
6-AUG-2013 09:56:04

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
1.899E+01 4.023E+02
4.024E+02 17.39
6.222E+00 3.813E+02
3.813E+02 27.80
5.860E+00 3.859E+02
3.859E+02 16.73
3 Valid Peaks =
Status
OK
OK
OK
4.024E+02+/- 6.999E+01 ( 17.39%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag: "*"
Keyline

%Eff
2.648E+01 7.722E+02
7.722E+02 16.82
1 Valid Peaks
Status
OK
7.722E+02+/- 1.299E+02 ( 16.82%)

Sample ID : 1307147-03
----
Acquisition date
Page :
4
6-AUG-2013 09:56:04
Identified Nuclides
Nuclide
BA-133
TH-234
Activity
(pCi/filter)
Act error
MDA
(pCi/filter)
MDA error
Act/MDA
4.024E+02
7.722E+02
6.999E+01
1.299E+02
1.746E+01
1.147E+02
2.670E+00
6.161E+00
23.045
6.732
Act error
MDA
(pCi/ filter)
MDA error
Act/MDA
5.673E+00
1.005E+02
1.586E+00
1.445E+00
2.912E+01
8.952E+00
9.369E+00
1.536E+02
3.188E+00
2.853E+00
5.031E+01
1.729E+01
1.070E+00
1.267E+01
4.534E-02
4.058E-02
4.067E+00
8.502E-01
0.078
-0.297
0.822
1.610
0.320
1. 538
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
7.321E-01
-4.558E+01
2.620E+00
4.592E+00
1.611E+01
2.660E+01
8496

Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
--
'6({r;(r?
D~lOO:
[GAMMA.SCUSR.ARCHIVE]SMP_130714704 GE3 BAFIL 194351. CN

PEAK Vl6.9 PEAKEFF V2.2
D-12 TOT
6-AUG-2013 00:00:00.
1307147-04
FILTER
GE3
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
27.94
30.89
34.80
53.32
61.88
65.86
81.09
84.50
111.71
116.20
267.95
277.07
303.05
307.43
334.06
356.36
365.32
384.70
391.61
410.87
414.87
437.41
468.25
512.20
63
1814
498
78
252
112
753
39
220
43
14
43
121
34
65
495
32
94
44
7
35
83
19
14
74
67
88
109
67
59
63
40
54
51
13
31
16
13
31
34
11
11
4
0
4
15
9
5
4
4
4
0
2
2
9
9
3
3
0
0
4
4
0
0
0
1
1
1
1
0
0
0
6-AUG-2013 10:32:17.92
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1. 87
1.42
1.93
2.76
1.62
1. 67
1. 55
1. 78
1.93
1.93
2.79
1. 31
1. 85
1.93
2.03
1. 93
1. 76
1.70
1.88
1. 89
1. 89
1. 89
1. 43
3.50
28.26
31.21
35.12
53.64
62.20
66.18
81.41
84.82
112.02
116.52
268.26
277.38
303.35
307.74
334.37
356.66
365.63
385.00
391.91
411. 17
415.17
437.71
468.55
512.50
Left
Pw
26
26
26
50
58
58
78
78
108
108
266
274
300
300
331
352
362
381
381
410
410
433
465
507
15
15
15
9
16
16
10
10
22
22
5
7
17
17
7
11
9
15
15
11
11
11
7
9
6-AUG-2013 10:16:58.
l.OOOOOE+OO filter
0
BAFIL
0 00:15:05.13 0.6%
4096
10.00000
Cts/Sec %Err
7.03E-02
2.02E+00
5.54E-01
8.64E-02
2.80E-01
1.24E-01
8.37E-01
4.32E-02
2.44E-01
4.83E-02
1. 56E-02
4.77E-02
1.35E-01
3.74E-02
7.24E-02
5.50E-01
3.58E-02
1.04E-01
4.87E-02
7.84E-03
3.84E-02
9.23E-02
2.16E-02
1.59E-02
21.9
2.4
7.0
27.0
7.9
14.5
4.0
56.3
8.9
32.0
46.4
26.5
10.3
25.7
18.7
5.1
25.7
12.5
20.1
31.7
23.5
14.0
33.8
37.7
Fit
3.23E+Ol
3.70E+00
5.34E+00
2.31E+00
2.08E+00
2.23E+Ol
5.48E+00

Sample ID : 1307147-04
Acquisition date

24
19
5
Page :
2
6-AUG-2013 10:16:58
20.83%

Nuclide
Hlife
BA-133
10.50Y
NP-237 2.14E+06Y
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
3.611E+02
1. 00
5.295E+01
Total Activity
--------
4.140E+02
Wtd Mean
Decay Corr
pCi/filter
3.611E+02
5.295E+01
Decay Corr
2-Sigma
17.68
0.638E+02
112.96
5.981E+01
--------
4.141E+02

Nuclide
Hlife
TH-234 4.47E+09Y
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
7.518E+02
Total Activity
Flags: "K"
"E"
--------
Wtd Mean
Decay Corr
pCi/filter
7.518E+02
--------
7.518E+02
7.518E+02
1.166E+03
1.166E+03
= Keyline not found

= Manually edited
2-Sigma
Decay Corr
17.17
1.291E+02
"A"

Sample ID : 1307147-04
Acq1,1isition date
Page :
3
6-AUG-2013 10:16:58

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

NP-237
86.50
3 Valid Peaks =
12.60*
Final Mean for

%Eff
3.611E+02 17.68
1.899E+01 3.611E+02
6.222E+00 3.283E+02
3.283E+02 29.13
4.225E+02 16.99
5.860E+00 4.224E+02
1.749E+01
3.611E+02+/- 6.385E+01 ( 17.68%)
5.295E+01
1 Valid Peaks =
Status
OK
OK
OK
5.295E+01 112.96
OK
5.295E+01+/- 5.981E+01 (112.96%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag: "*"

%Eff
2.648E+01 7.518E+02
7.518E+02 17.17
1 Valid Peaks
Status
OK
7.518E+02+/- 1.291E+02 ( 17.17%)
Keyline
i499

Sample ID : 1307147-04
Acq1,1isition date
Page :
4
6-AUG-2013 10:16:58
---- Identified Nuclides

Nuclide
BA-133
TH-234
NP-237
Activity
(pCi/filter)
3.611E+02
7.518E+02
5.295E+01
Act error
6.385E+01
1.291E+02
5.981E+01
MDA
(pCi/filter)
1.958E+01
1.184E+02
4.757E+01
MDA error
Act/MDA
2.995E+00
6.358E+00
3.846E+00
18.440
6.351
1.113
MDA error
Act/MDA
1.075E+00
1.359E+01
4.431E-02
3.654E-02
8.227E-01
-0.106
0.000
0.922
0.963
1.558
Nuclide
C0-57
CD-109
PA-231
PA-234
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
-9.929E-01
3.522E-02
2.874E+00
2.473E+00
2.606E+01
Act error
5.481E+00
1.016E+02
1.516E+OO
1.395E+00
8.539E+00
MDA
(pCi/filter)
9.410E+00
1.649E+02
3.116E+00
2.569E+00
1.673E+01
~\~\~

Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level

D-12 DIS
6-AUG-2013 00:00:00.
1307147-05
FILTER
GE3
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
30.80
34.81
52.69
61.83
65.88
77.49
80.98
111.43
116.60
160.83
178.70
276.42
281.35
303.10
333.79
338.14
356.29
383.62
387.13
391.68
414.87
418.87
422.87
437.57
468.96
510.52
1884
422
44
279
127
24
812
161
54
38
13
52
13
125
89
27
465
105
224
44
35
23
10
85
19
24
85
66
101
72
93
33
48
162
67
39
53
16
18
20
9
11
36
12
11
12
7
8
9
13
10
6
1
1
0
4
4
2
2
0
0
1
1
2
2
0
3
3
0
4
4
4
1
1
1
0
0
0
6-AUG-2013 10:50:25.79
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1.44
1.45
1.45
1.64
2.02
1. 69
1. 69
1.36
2.43
1. 66
1. 68
1. 96
1. 96
1. 75
1. 81
2.22
1. 87
1.82
1. 75
1. 95
1. 89
1. 90
1.90
1. 62
2.08
2.02
31.12
35.13
53.01
62.15
66.19
77.81
81.29
111.74
116.91
161.15
179.01
276.73
281.66
303.41
334.09
338.45
356.60
383.92
387.43
391.98
415.17
419.17
423.17
437.87
469.26
510.81
Left
Pw
26
26
49
57
57
76
76
108
115
158
158
272
272
300
328
328
352
381
381
381
411
411
411
434
465
506
15
15
7
15
15
11
11
8
6
24
24
13
13
6
14
14
10
20
20
20
17
17
17
9
7
11
6-AUG-2013 10:35:05.
1.00000E+00 filter
0
BAFIL
0 00:15:05.71 0.6%
4096
10.00000
Cts/Sec %Err
2.09E+00
4.69E-01
4.93E-02
3.10E-01
1.41E-01
2.69E-02
9.02E-01
1. 79E-01
5.96E-02
4.25E-02
1.47E-02
5.83E-02
1.44E-02
1.39E-01
9.88E-02
2.98E-02
5.16E-01
1.16E-01
2.49E-01
4.86E-02
3.87E-02
2.55E-02
1.12E-02
9.47E-02
2.10E-02
2.70E-02
2.5
6.1
40.7
7.5
16.2
36.9
3.7
15.7
28.4
31.3
79.2
19.7
61.7
10.5
11.7
34.9
5.2
11.2
7.6
21.0
21.9
34.4
64.6
13.3
36.5
27.7
Fit
1.42E+01
2.55E+00
5.30E+00
2.41E+00
1. 31E+00
7.33E-01
5.37E+00
5.23E-01

Sample ID : 1307147-05
Acquisition date

26
22
4
Page :
2
6-AUG-2013 10:35:05
15.38%

Nuclide
BA-133
Hlife
10.50Y
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
3.890E+02
---------
Total Activity
3.890E+02
Wtd Mean
Decay Corr
pCi/filter
3.890E+02
Decay Corr
2-Sigma
0.679E+02
17.46
---------
3.890E+02

Nuclide
Hlife
TH-234 4.47E+09Y
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
8.320E+02
---------
Total Activity
Grand Total Activity
Flags: "K"
"E"
=
=
Wtd Mean
Decay Corr
pCi/filter
8.320E+02
---------
8.320E+02
8.320E+02
1.221E+03
1.221E+03
Keyline not found

Manually edited
Decay Corr
2-Sigma
16.43
1.367E+02
"M"
"A"
=
=
Manually accepted

Sample ID : 1307147-05
Acquisition date
Page :
3
6-AUG-2013 10:35:05

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
1.899E+01 3.890E+02
3.890E+02 17.46
6.222E+00 3.394E+02
3.394E+02 29.48
3.970E+02 17.21
5.860E+OO 3.969E+02
3 Valid Peaks
Status
OK
OK
OK
3.890E+02+/- 6.792E+01 ( 17.46%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag:
11
* 11
Keyline

%Eff
2.648E+01 8.320E+02
8.320E+02 16.43
1 Valid Peaks
Status
OK
8.320E+02+/- 1.367E+02 ( 16.43%)

Sample ID : 1307147-05
Acquisition date
4
Page :
6-AUG-2013 10:35:05
Identified Nuclides
Nuclide
BA-133
TH-234
Activity
(pCi/filter)
3.890E+02
8.320E+02
Act error
6.792E+01
1.367E+02
MDA
(pCi/filter)
1.840E+01
1.184E+02
MDA error
Act/MDA
2.814E+00
6.358E+00
21.140
7.029
MDA error
Act/MDA
1.143E+00
1.362E+01
4.612E-02
3.855E-02
3.953E+00
8.776E-01
0.250
0.168
0.915
1. 284
0.161
1. 591
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
2.502E+00
2.772E+01
2.967E+00
3.479E+00
7.882E+00
2.841E+01
Act error
5.862E+00
9.819E+01
1.595E+00
1.420E+00
2.919E+01
9.266E+00
MDA
(pCi/filter)
1.001E+01
1.652E+02
3.243E+00
2.710E+00
4.891E+01
1.785E+01
~\1)

Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level

DUP05 TOT
6-AUG-2013 00:00:00.
1307147-06
FILTER
GE3
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
30.83
35.11
52.25
61.77
66.00
80.93
93.98
111.82
116.17
177.77
276.58
298.21
303.01
307.35
311.04
321.67
334.07
337.91
344.44
351.70
356.29
383.87
386.87
391.55
414.91
418.27
437.23
468.39
473.27
512.01
1940
480
84
267
148
794
32
239
70
25
56
4
139
31
12
9
84
25
11
12
520
106
192
44
46
36
127
25
9
26
100
101
106
78
86
91
75
56
69
48
22
4
8
11
11
12
13
11
11
2
9
32
41
13
8
4
0
2
1
0
3
3
0
3
3
0
0
6
6
0
0
0
2
2
2
2
3
3
3
3
3
1
1
0
3
3
0
0
0
0
6-AUG-2013 11:06:09.27
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1.44
1. 68
3.14
1.58
1. 83
1. 83
1. 74
1.59
2.28
2.83
1. 56
2.19
1. 63
1.99
1. 99
2.00
2.21
2.20
2.22
1. 68
1. 55
1. 87
1. 79
2.58
2.29
1. 94
1. 92
1. 43
1.14
5.88
31.15
35.43
52.57
62.09
66.32
81.25
94.30
112.13
116.49
178.08
276.89
298.52
303.32
307.66
311.35
321.98
334.37
338.22
344.74
352.00
356.60
384.17
387.17
391.85
415.21
418.57
437.54
468.69
473.57
512.31
Left
Pw
26
26
49
58
58
77
90
108
108
176
273
298
300
300
300
300
328
328
328
351
351
381
381
391
410
410
434
466
472
507
15
15
8
12
12
7
9
15
15
6
8
3
26
26
26
26
20
20
20
13
13
10
10
6
12
12
9
6
6
11
6-AUG-2013 10:50:38.
1.00000E+00 filter
0
BAFIL
0 00:15:05.28 0.6%
4096
10.00000
Cts/Sec %Err
2.16E+00
5.34E-01
9.38E-02
2.96E-01
1.65E-01
8.82E-01
3.51E-02
2.65E-01
7.80E-02
2.74E-02
6.20E-02
4.31E-03
1.55E-01
3.44E-02
1.35E-02
9.57E-03
9.30E-02
2.75E-02
1.24E-02
1.38E-02
5.78E-01
1.17E-01
2.13E-01
4.93E-02
5.10E-02
4.04E-02
1.41E-01
2.81E-02
1.03E-02
2.89E-02
2.4
5.7
23.6
7.9
13.0
4.1
52.4
8.0
26.0
48.4
19.8
91.2
8.9
25.2
66.2
71.3
14.0
40.8
56.2
9.6
4.5
14.2
10.0
23.8
20.5
23.2
8.9
21.3
37.8
19.6
Fit
3.87E+00
7.09E-01
1. 32E+00
1.74E+00
1.75E+00
2.91E+00
2.78E+01
2.60E+00
1515

Sample ID : 1307147-06
Acquisition date

30
26
4
Page :
2
6-AUG-2013 10:50:38
13.33%

Nuclide
BA-133
Hlife
10.50Y
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
3.806E+02
Total Activity
Nuclide Type
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 7.956E+02
Total Activity
=
=
2-Sigma
Decay Corr
17.77
0.677E+02
---------
3.807E+02
NATURAL
Nuclide
Hlife
TH-234 4.47E+09Y
Flags: "K"
"E"
---------
3.806E+02
Wtd Mean
Decay Corr
pCi/filter
3.807E+02
---------
Wtd Mean
Decay Corr
pCi/filter
7.956E+02
---------
7.956E+02
7.956E+02
1.176E+03
1.176E+03
Keyline not found

Manually edited
2-Sigma
Decay Corr
17.07
1.358E+02
"W'
"A"
Manually accepted

Sample ID : 1307147-06
Acquisition date
Page :
3
6-AUG-2013 10:50:38

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
3.807E+02 17.77
1.899E+01 3.806E+02
6.222E+00 3.775E+02
3.775E+02 27.20
4.440E+02 16.31
5.860E+OO 4.439E+02
3 Valid Peaks
Status
OK
OK
OK
3.807E+02+/- 6.766E+01 ( 17.77%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag: "*"

%Eff
2.648E+01 7.956E+02
7.956E+02 17.07
1 Valid Peaks
Status
OK
7.956E+02+/- 1.358E+02 ( 17.07%)
Keyline
S5

Sample ID : 1307147-06
Acquisition date
4
Page :
6-AUG-2013 10:50:38
Nuclide
BA-133
TH-234
Activity
(pCi/filter)
Act error
MDA
(pCi/ filter)
MDA error
Act/MDA
3.807E+02
7.956E+02
6.766E+01
1.358E+02
1.885E+01
1.287E+02
2.884E+00
6.912E+00
20.190
6.183
Act error
MDA
(pCi/filter)
MDA error
Act/MDA
1.036E+01
1.183E+00
1.236E+01
5.043E-02
4.164E-02
3.953E+00
9.047E-01
0.175
-0.772
1. 004
1. 305
0.358
1.517
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
1.817E+OO
-1.157E+02
3.558E+00
3.821E+00
1.750E+01
2.791E+01
6.207E+00
1.077E+02
1.756E+00
1.560E+00
3.130E+01
9.742E+00
1. 499E+02
3.546E+00
2.928E+00
4.891E+01
1.840E+01
85

Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
W~l/)

DUP05 DIS
6-AUG-2013 00:00:00.
1307147-07
FILTER
GE3
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
30.76
35.13
52.59
61.77
65.65
81.04
84.13
111. 86
116.43
159.10
276.91
303.19
307.66
333.79
337.73
356.30
384.04
387.23
391.29
414.84
418.87
437.16
468.76
472.79
511.14
609.71
1943
503
55
228
93
803
21
240
80
34
68
124
17
62
23
472
111
178
68
46
19
119
16
11
17
9
109
96
160
78
76
64
56
47
48
89
25
39
24
14
13
40
9
5
4
10
8
7
9
3
5
0
4
4
0
2
2
7
7
5
5
0
0
0
0
1
1
0
3
3
3
3
3
0
0
0
0
0
6-AUG-2013 11:22:17.30
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Ga-ussian
FWHM Channel
1.54
1.56
2.35
1. 66
1. 67
1. 50
1. 51
1. 82
2.34
3.68
1. 60
1. 91
1. 30
1.83
1. 83
1. 89
2.26
1. 92
2.21
2.16
1. 90
2.03
1. 86
1. 83
3.69
1. 67
31.08
35.45
52.91
62.09
65.97
81.36
84.44
112.18
116.74
159.42
277.21
303.50
307.96
334.09
338.04
356.61
384.34
387.53
391.59
415.14
419.17
437.46
469.06
473.09
511.43
610.00
6-AOG-2013 11:06:54.
1.00000E+00 filter
0
BAFIL
0 00:15:04.88 0.5%
4096
10.00000
Left
Pw
Cts/Sec %Err
27
27
48
58
58
76
76
107
107
156
274
300
307
328
328
352
380
380
380
411
411
432
464
471
508
607
13
13
10
12
12
11
11
15
15
9
8
7
5
15
15
9
17
17
17
19
19
10
7
6
9
6
2.16E+00 2.4
5.59E-01 5.4
6.11E-02 45.1
2.53E-01 9.0
1.03E-01 19.4
8.93E-01 3.8
2.34E-02103.7
2.67E-01 7.7
8.91E-02 22.2
3.74E-02 53.2
7.58E-02 17.4
1.38E-01 12.2
1.92E-02 50.3
6.83E-02 16.1
2.55E-02 39.1
5.24E-01 5.2
1.24E-01 13.8
1.97E-01 9.2
7.56E-02 20.0
5.07E-02 17.5
2.16E-02 37.6
1.32E-01 10.1
1.76E-02 40.2
1.22E-02 39.1
1.84E-02 34.2
1.00E-02 33.3
Fit
1.32E+01
4.50E+00
1.92E+00
1.47E+00
1. 96E+00
2.94E+00
2.53E+00

Sample ID : 1307147-07
Acquisition date

26
22
4
Page :
2
6-AUG-2013 11:06:54
15.38%

Nuclide
BA-133
Hlife
10.50Y
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
3.850E+02
Total Activity
---------
3.850E+02
Wtd Mean
Decay Corr
pCi/filter
3.850E+02
Decay Corr
2-Sigma
17.56
0.676E+02
---------
3.850E+02

Nuclide
Hlife
TH-234 4.47E+09Y
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
6.805E+02
Total Activity
---------
Wtd Mean
Decay Corr
pCi/filter
6.805E+02
---------
6.805E+02
6.805E+02
1.065E+03
1.065E+03

Decay Corr
2-Sigma
1.302E+02
19.14


Sample ID : 1307147-07
Acquisition date
Page :
3
6-AUG-2013 11:06:54

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for
Uncorrected Decay Carr 2-Sigma

%Eff
1.899E+01 3.850E+02
3.850E+02 17.56
6.222E+00 3.360E+02
3.360E+02 32.01
5.860E+00 4.027E+02
4.028E+02 17.17
3 Valid Peaks
Status
OK
OK
OK
3.850E+02+/- 6.762E+01 ( 17.56%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag: "*"

%Eff
2.648E+01 6.805E+02
6.805E+02 19.14
1 Valid Peaks
Status
OK
6.805E+02+/- 1.302E+02 ( 19.14%)
Keyline
511

Sample ID : 1307147-07
Acquisition date
4
Page :
6-AUG-2013 11:06:54
Nuclide
BA-133
TH-234
Activity
(pCi/filter)
Act error
3.850E+02
6.805E+02
6.762E+01
1.302E+02
MDA
(pCi/filter)
1.885E+01
1.287E+02
MDA error
Act/MDA
2.884E+00
6.912E+00
20.420
5.288
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
-2.537E+00
-3.784E+01
9.146E-01
2.789E+00
-2.254E+01
2.705E+01
Act error
MDA
(pCi/filter)
MDA error
Act/MDA
5.994E+00
1.112E+02
1.566E+00
1.486E+00
3.308E+01
9.682E+00
9.113E+OO
1.721E+02
2.943E+00
2.848E+00
4.902E+01
1.825E+01
1.041E+00
1.419E+01
4.186E-02
4.051E-02
3.962E+00
8.972E-01
-0.278
-0.220
0.311
0.979
-0.460
1.482
5512
a_

Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
'b((p/13
DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP_130714708 - GE3 BAFIL 194357.CN

PZ-208-SS TOT
6-AOG-2013 00:00:00.
1307147-08
FILTER
GE3
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
30.79
34.81
53.09
61.83
66.10
69.97
80.99
92.76
111.92
116.01
134.82
141.89
159.97
199.16
211.58
276.47
296.59
302.97
323.39
334.00
338.73
356.30
383.87
386.87
391.53
414.78
418.53
437.27
467.86
472.62
512.04
608.83
697.82
1775
399
73
266
124
23
765
26
214
26
29
41
35
82
42
51
15
140
13
73
20
441
112
177
49
31
15
89
21
8
10
10
9
1
1
0
5
5
5
0
0
4
4
6
6
0
0
0
0
5
5
0
2
2
0
1
1
1
1
1
0
1
1
0
0
0
6-AUG-2013 11:37:47.42
Bkgnd
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
72 1. 44
50 1. 45
114 2.56
57 1. 86
58 2.22
54 2.23
135 1.81
50 1.09
47 1. 68
41 2.13
30 2.61
57 2.63
68 1. 90
115 13.20
48 5.23
11 1. 77
12 2.63
24 1. 64
14 2.67
11 2.01
14 2.02
40 1. 92
9 1.87
9 1.87
9 1. 88
11 1.89
14 1. 90
5 1. 93
2 1. 93
5 1. 94
7 2.94
2 1. 90
0 3.22
31.11
35.13
53.41
62.15
66.42
70.29
81.31
93.08
112.23
116.33
135.14
142.21
160.28
199.47
211.89
276.78
296.90
303.28
323.69
334.30
339.03
356.61
384.17
387.17
391.83
415.08
418.83
437.57
468.16
472.92
512.33
609.12
698.11
Left
Pw
26
26
49
58
58
58
76
91
108
108
133
133
158
190
208
275
294
294
320
331
331
352
374
374
374
410
410
434
465
465
509
605
695
15
15
9
16
16
16
11
5
12
12
15
15
7
18
9
5
13
13
7
14
14
11
23
23
23
12
12
8
12
12
6
8
7
6-AUG-2013 11:22:25.
l.OOOOOE+OO filter
0
BAFIL
0 00:15:05.44 0.6%
4096
10.00000
Cts/Sec %Err
1.97E+00
4.44E-01
8.08E-02
2.96E-01
1. 37E-01
2.53E-02
8.50E-01
2.89E-02
2.38E-01
2.88E-02
3.17E-02
4.57E-02
3.90E-02
9.09E-02
4.71E-02
5.63E-02
1.66E-02
1.55E-01
1.44E-02
8.08E-02
2.24E-02
4.90E-01
1. 25E-01
1.97E-01
5.47E-02
3.43E-02
1.72E-02
9.87E-02
2.37E-02
8.81E-03
1.13E-02
1.13E-02
l.OOE-02
2.5
6.0
29.2
7.5
15.6
69.9
4.7
45.3
8.3
58.7
32.9
36.3
41.9
32.9
33.0
17.0
54.3
9.7
55.2
14.3
40.3
5.5
11.5
10.1
18.7
26.1
50.9
11.6
25.4
57.1
52.1
39.3
33.3
Fit
1.52E+Ol
2.23E+00
5.73E-01
9.51E-01
7.33E+00
1.99E+00
2.82E+00
2.49E+00
2.39E-01
9513

Sample ID : 1307147-08
Acquisition date

33
28
5
Page :
2
6-AUG-2013 11:22:25
15.15%

Nuclide
BA-133
Hlife
10.50Y
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
3.667E+02
Total Activity
---------
3.667E+02
Wtd Mean
Decay Corr
pCi/filter
3.667E+02
2-Sigma
Decay Corr
18.35
0.673E+02
---------
3.667E+02

Nuclide
Hlife
TH-234 4.47E+09Y
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
7.945E+02
Total Activity
Flags: "K"
"E"
=
=
---------
Wtd Mean
Decay Corr
pCi/filter
7.945E+02
---------
7.945E+02
7.945E+02
1.161E+03
1.161E+03
Keyline not found

Manually edited
2-Sigma
Decay Corr
1.311E+02
16.50
"M"
"A"
=
=
Manually accepted

Sample ID : 1307147-08
Acquisition date
Page :
3
6-AUG-2013 11:22:25

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
1.899E+01 3.667E+02
3.667E+02 18.35
6.222E+OO 3.783E+02
3.783E+02 28.35
5.860E+00 3.768E+02
3.768E+02 17.56
3 Valid Peaks
Status
OK
OK
OK
3.667E+02+/- 6.729E+01 ( 18.35%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag: "*"
Keyline

%Eff
2.648E+01 7.945E+02
7.945E+02 16.50
1 Valid Peaks
Status
OK
7.945E+02+/- 1.311E+02 ( 16.50%)

Sample ID : 1307147-08
Acquisition date
4
Page :
6-AUG-2013 11:22:25

Nuclide
BA-133
TH-234
Activity
(pCi/filter)
Act error
3.667E+02
7.945E+02
6.729E+01
1.311E+02
MDA
(pCi/filter)
1.915E+01
1.001E+02
MDA error
Act/MDA
2.929E+00
5.375E+00
19.150
7.940
MDA error
Act/MDA
1.111E+00
1.627E+01
4.162E-02
3.950E-02
4.611E+00
8.363E-01
0.308
0.475
0.587
1. 571
0.177
1.732
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
3.000E+00
9.377E+01
1.718E+00
4.363E+00
1.011E+01
2.947E+01
Act error
5.589E+00
1.264E+02
1.487E+OO
1.403E+00
3.906E+01
8.497E+00
MDA
(pCi/filter)
9.726E+00
1.973E+02
2.926E+00
2.777E+00
5.704E+01
1.701E+01
S515

Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
f6!vll?

PZ-208-SS DIS
6-AUG-2013 00:00:00.
1307147-09
FILTER
GE3
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
27.64
30.86
34.92
46.63
52.48
61.66
65.70
81.10
92.41
111. 88
115.97
141.16
160.77
276.68
303.15
307.33
312.16
333.80
338.21
356.29
384.18
387.07
391.31
414.87
418.53
422.86
437.31
468.68
511.65
37
2015
498
39
81
286
97
848
25
237
66
40
32
58
165
40
12
86
18
507
127
227
50
35
16
10
99
13
21
83
73
90
91
95
67
65
123
62
60
56
82
57
21
13
8
4
13
17
26
10
5
4
16
8
4
15
16
5
4
4
4
0
0
2
2
0
0
3
3
0
0
0
4
4
4
4
4
0
4
4
4
1
1
1
0
0
0
6-AUG-2013 11:53:24.62
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1. 90
1.44
1. 93
2.16
2.83
1. 66
1.67
1.91
1. 36
1. 66
1.93
3.99
1. 74
1. 32
1. 75
2.24
2.41
1. 89
2.44
1. 94
1.92
1. 83
2.24
1. 89
1.90
1.90
1. 90
1. 97
2.93
27.96
31.18
35.24
46.94
52.80
61.98
66.02
81.42
92.73
112.20
116.28
141.48
161. 08
276.99
303.46
307.64
312.47
334.10
338.52
356.60
384.48
387.37
391.61
415.17
418.83
423.16
437.61
468.98
511.95
Left
Pw
26
26
26
42
50
58
58
77
90
108
108
138
158
273
299
299
299
329
329
351
382
382
382
409
409
409
432
466
508
15
15
15
8
8
11
11
10
6
16
16
9
6
7
17
17
17
15
15
10
13
13
13
17
17
17
9
7
10
6-AUG-2013 11:37:58.
1.00000E+00 filter
0
BAFIL
0 00:15:05.63 0.6%
4096
10.00000
Cts/Sec %Err
4.13E-02
2.24E+00
5.53E-01
4.36E-02
9.03E-02
3.18E-01
1.08E-01
9.42E-01
2.81E-02
2.64E-01
7.36E-02
4.39E-02
3.55E-02
6.47E-02
1.83E-01
4.45E-02
1.38E-02
9.51E-02
1.95E-02
5.64E-01
1.41E-01
2.52E-01
5.58E-02
3.94E-02
1. 79E-02
1.09E-02
1.10E-01
1.49E-02
2.33E-02
37.7
2.3
7.1
45.1
23.4
7.5
17.0
4.2
52.9
8.0
26.2
44.1
41.6
18.5
8.2
30.7
57.9
13.3
54.1
4.8
13.0
7.6
25.5
23.6
48.9
61.6
12.1
54.7
29.5
Fit
1.67E+01
4.77E+00
1.99E+00
2.84E+00
1. 34E+00
4.22E-01
1. 77E+00
l!l517

Sample ID : 1307147-09
Acquisition date

29
25
4
Page :
2
6-AUG-2013 11:37:58
13.79%

Nuclide
BA-133
Hlife
10.50Y
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
4.063E+02
Total Activity
---------
4.063E+02
Wtd Mean
Decay Corr
pCi/filter
4.064E+02
---------
Decay Corr
2-Sigma
0.728E+02
17.93
4.064E+02

Nuclide
Hlife
TH-234 4.47E+09Y
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
8.543E+02
Total Activity
Flags: "K"
"E"
=
=
---------
Wtd Mean
Decay Corr
pCi/filter
8.543E+02
---------
8.543E+02
8.543E+02
1.261E+03
1.261E+03
Keyline not found

Manually edited
Decay Corr
2-Sigma
1.404E+02
16.44
"M"
"A"
=
=
Manually accepted
fil518

Sample ID : 1307147-09
Acquisition date
Page :
3
6-AUG-2013 11:37:58

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
1.899E+01 4.063E+02
4.064E+02 17.93
6.222E+00 4.461E+02
4.461E+02 26.33
5.860E+00 4.334E+02
4.335E+02 16.69
3 Valid Peaks
Status
OK
OK
OK
4.064E+02+/- 7.284E+01 ( 17.93%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag: "*"

%Eff
2.648E+01 8.543E+02
8.543E+02 16.44
1 Valid Peaks
Status
OK
8.543E+02+/- 1.404E+02 ( 16.44%)
Keyline
!519

Sample ID : 1307147-09
Acquisition date
Page :
4
6-AUG-2013 11:37:58
Identified Nuclides
Nuclide
BA-133
TH-234
Activity
(pCi/filter)
Act error
4.064E+02
8.543E+02
7.284E+01
1.404E+02
MDA
(pCi/filter)
1.840E+01
1.276E+02
MDA error
Act/MDA
2.814E+00
6.852E+00
22.082
6.696
MDA error
Act/MDA
1.101E+00
1.333E+01
4.908E-02
4.266E-02
4.128E+00
9.740E-01
-0.162
0.354
1.106
1. 627
0.588
1.846
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
-1.564E+00
5.719E+Ol
3.815E+00
4.878E+00
3.004E+Ol
3.657E+Ol
Act error
6.187E+00
1.026E+02
1.672E+00
1.540E+00
3.090E+01
1.030E+01
MDA
(pCi/filter)
9.636E+00
1.616E+02
3.451E+00
2.999E+00
5.106E+Ol
1.981E+01
!528
~t.\1)

Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level

PZ-304-AI TOT
6-AUG-2013 00:00:00.
1307147-10
FILTER
GE3
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
30.82
35.07
46.24
52.45
61.82
65.97
81.21
93.01
111.83
115.78
185.97
276.58
299.69
303.04
307.37
311.52
335.13
356.31
366.45
383.81
387.14
391.09
414.90
418.51
421.87
426.71
437.28
468.25
473.46
511. 05
610.15
1980
559
25
64
226
124
777
29
196
44
28
67
11
154
33
13
64
524
26
101
240
47
36
31
12
7
111
21
9
19
12
84
66
72
75
86
122
148
78
53
56
87
42
5
12
16
17
63
21
15
17
13
11
7
3
1
0
3
4
2
7
2
3
3
0
0
6
6
0
0
1
1
0
0
3
3
3
3
0
0
0
4
4
4
2
2
2
2
0
0
0
0
0
6-AUG-2013 12:08:52.50
Acql.).isition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1. so
1. 69
1. 08
2.34
1. 52
2.34
1. 96
2.70
1. 59
1. 60
2.32
1. 55
1. 64
1. 84
2.19
2.19
1. 53
1.96
2.25
2.04
2.04
2.50
2.08
2.09
2.09
2.09
1.88
1. 76
1.19
3.86
2.81
31.14
35.39
46.56
52.77
62.13
66.29
81.52
93.33
112.14
116.10
186.28
276.89
300.00
303.35
307.68
311.83
335.44
356.61
366.76
384.11
387.44
391.39
415.20
418.81
422.17
427.01
437.59
468.55
473.76
511.34
610.45
Left
Pw
26
26
44
50
58
58
76
90
108
108
183
272
299
299
299
299
330
351
362
381
381
381
410
410
410
410
435
464
472
507
606
18
18
6
6
12
12
11
7
13
13
8
10
20
20
20
20
10
12
10
15
15
15
20
20
20
20
6
8
5
9
9
6-AUG-2013 11:53:32.
1.00000E+00 filter
0
BAFIL
0 00:15:05.24 0.6%
4096
10.00000
Cts/Sec %Err
2.20E+00
6.21E-01
2.78E-02
7.07E-02
2.51E-01
1. 37E-01
8.64E-01
3.26E-02
2.17E-01
4.87E-02
3.10E-02
7.41E-02
1.24E-02
1.71E-01
3.70E-02
1.43E-02
7.16E-02
5.82E-01
2.88E-02
1.12E-01
2.67E-01
5.24E-02
3.97E-02
3.49E-02
1.37E-02
7.96E-03
1. 23E- 01
2.32E-02
1.04E-02
2.12E-02
1.33E-02
Fit
2.3 5.44E+00
4.9
57.3
24.9
9.0 2.41E+00
18.0
4.7
53.0
9.5 2.84E+00
30.2
60.6
22.0
39.5 8.11E+00
8.5
34.5
63.0
26.1
4.7
35.6
12.6 7.16E+00
7.8
29.4
21.1 1.31E+00
24.8
51.3
53.6
9.8
27.5
37.9
33.7
36.4
8521

Sample ID : 1307147-10
Acquisition date
Total numoer of lines in spectrum

31
27
4
Page :
2
6-AOG-2013 11:53:32
12.90%

Nuclide
BA-133
Hlife
10.50Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 3.725E+02
Total Activity
3.725E+02
Wtd Mean
Decay Corr
pCi/filter
3.725E+02
Decay Corr
2-Sigma
0.685E+02
18.39
3.725E+02

Nuclide
Hlife
TH-234 4.47E+09Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 6.741E+02
Total Activity
Flags: "K"
"E"
Wtd Mean
Decay Corr
pCi/filter
6.741E+02
6.741E+02
6.741E+02
1.047E+03
1.047E+03
= Keyline not found

= Manually edited
"M"
"A"
=
=
Decay Corr
2-Sigma
1.295E+02
19.22
Manually accepted
1522

Sample ID : 1307147-10
Acquisition date
Page :
3
6-AUG-2013 11:53:32

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
1.899E+01 3.725E+02
3.725E+02 18.39
6.222E+00 4.165E+02
4.165E+02 26.72
5.860E+00 4.477E+02
4.478E+02 16.57
3 Valid Peaks
Status
OK
OK
OK
3.725E+02+/- 6.850E+01 ( 18.39%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag:
11
* 11
Keyline

%Eff
2.648E+01 6.741E+02
6.741E+02 19.22
1 Valid Peaks
Status
OK
6.741E+02+/- 1.295E+02 ( 19.22%)

Sample ID : 1307147-10
Acquisition date
Page :
4
6-AUG-2013 11:53:32
Identified Nuclides
Nuclide
BA-133
TH-234
Activity
(pCi/filter)
Act error
3.725E+02
6.741E+02
6.850E+01
1.295E+02
MDA
(pCi/filter)
1.871E+01
1.409E+02
MDA error
Act/MDA
2.861E+00
7.570E+00
19.914
4.783
MDA error
Act/MDA
1.241E+00
1.371E+01
4.336E-02
4.099E-02
4.193E+00
8.432E-01
0.269
-0.294
0.687
1. 485
0.407
0.960
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
2.923E+00
-4.896E+01
2.093E+00
4.279E+00
2.113E+01
1.646E+01
Act error
6.416E+00
1.249E+02
1.536E+00
1.492E+00
3.315E+01
9.051E+00
MDA
(pCi/filter)
1.086E+01
1.663E+02
3.049E+00
2.882E+00
5.187E+01
1.715E+01
i524
~b\0

Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
DKA100: [GAMMA.SCQSR.ARCHIVE]SMP_130714711 GE3 BAFIL 194362.CN

PZ-304-AI DIS
6-AUG-2013 00:00:00.
1307147-11
FILTER
GE3
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
30.84
35.10
38.55
52.47
61.79
65.66
80.99
92.45
101.40
111.92
115.99
160.47
276.90
303.01
307.24
333.98
338.40
356.24
384.07
387.20
414.72
418.53
422.53
437.41
468.51
511.27
2064
507
23
44
258
135
825
27
24
258
45
14
49
138
33
70
18
471
99
202
35
11
17
94
26
19
83
56
39
134
75
79
155
81
76
63
52
88
32
18
16
16
25
39
40
49
30
43
12
7
16
3
3
3
3
0
2
2
0
0
0
2
2
0
0
3
3
7
7
0
5
5
1
1
0
0
0
0
6-AUG-2013 12:24:42.99
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
6-AUG-2013 12:09:21.
1.00000E+00 filter
0
BAFIL
0 00:15:05.54 0.6%
4096
10.00000
FWHM Channel
Left
Pw
Cts/Sec %Err
31.16
35.42
38.87
52.79
62.11
65.98
81.31
92.76
101.72
112.24
116.30
160.79
277.21
303.31
307.54
334.28
338.70
356.54
384.37
387.50
415.02
418.83
422.84
437.71
468.81
511.57
26
26
26
49
58
58
76
89
99
108
108
157
274
299
299
329
329
352
382
382
411
411
421
433
464
508
17
17
17
9
13
13
10
6
7
15
15
8
8
15
15
15
15
11
9
9
11
11
5
9
9
10
2.29E+00 2.3
5.63E-01 5.1
2.52E-02 57.1
4.92E-02 49.6
2.87E-01 8.1
1.50E-01 14.2
9.17E-01 4.5
2.99E-02 56.6
2.67E-02 63.4
2.86E-01 7.7
4.95E-02 31.0
1.56E-02119.1
5.42E-02 24.3
1.53E-01 9.3
3.71E-02 36.6
7.83E-02 15.3
2.05E-02 58.1
5.24E-01 5.3
1.10E-01 17.8
2.24E-01 9.0
3.90E-02 30.0
1.27E-02 88.4
1.86E-02 40.6
1. 05E-01 11.4
2.88E-02 33.9
2.10E-02 28.2
1. 52
1.70
1.46
2.32
1. 66
1.67
1.89
1.00
2.13
1.69
1. 76
1. 08
1.47
1.65
2.19
2.06
2.22
1. 95
1. 90
1. 78
1. 89
1.90
1. 52
1. 67
1. 67
2.44
'
Fit
1.44E+01
4.34E+00
1.45E+00
5.64E+00
1.48E+00
6.58E+00
7.20E+00

Sample ID : 1307147-11
Acquisition date

26
21
5
Page :
2
6-AUG-2013 12:09:21
19.23%

Nuclide
BA-133
Hlife
10.50Y
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
3.955E+02
Total Activity
--------
3.955E+02
Wtd Mean
Decay Corr
pCi/filter
3.955E+02
Decay Corr
2-Sigma
Q.719E+02
18.17
--------
3.955E+02

Nuclide
Hlife
TH-234 4.47E+09Y
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
7.701E+02
Total Activity
Flags: "K"
"E"
=
=
--------
Wtd Mean
Decay Corr
pCi/filter
7.701E+02
--------
7.701E+02
7.701E+02
1.166E+03
1.166E+03
Keyline not found

Manually edited
"M"
"A"
=
=
Decay Corr
2-Sigma
1.356E+02
17.61
Manually accepted
!15

Sample ID : 1307147-11
Acquisition date
Page :
3
6-AUG-2013 12:09:21

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
1.899E+01 3.955E+02
3.955E+02 18.17
6.222E+00 3.745E+02
3.745E+02 27.73
5.860E+00 4.027E+02
4.027E+02 17.31
3 Valid Peaks
Status
OK
OK
OK
3.955E+02+/- 7.187E+01 ( 18.17%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag: "*"

%Eff
2.648E+01 7.701E+02
7.701E+02 17.61
1 Valid Peaks
Status
OK
= 7.701E+02+/- 1.356E+02 ( 17.61%)
= Keyline
~527

Sample ID : 1307147-11
Acquisition date
4
Page :
6-AUG-2013 12:09:21
Identified Nuclides
Nuclide
BA-133
TH-234
Activity
(pCi/filter)
Act error
3.955E+02
7.701E+02
7.187E+01
1.356E+02
MDA
(pCi/filter)
1.855E+01
1.135E+02
MDA error
Act/MDA
2.838E+00
6.094E+00
21.316
6.787
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
2.042E+00
-2.256E+01
1.569E+00
4.359E+00
-3.333E+00
3.105E+01
Act error
MDA
(pCi/filter)
MDA error
Act/MDA
6.129E+00
1.336E+02
1.522E+00
1.472E+00
3.874E+01
9.232E+00
1.029E+01
1.840E+02
2.959E+00
2.864E+00
5.404E+01
1.804E+01
1.176E+00
1.517E+01
4.209E-02
4.074E-02
4.369E+00
8.871E-01
0.198
-0.123
0.530
1.522
-0.062
1.721
~~\t~

Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level

PZ-304-AS TOT
6-AUG-2013 00:00:00.
1307147-12
FILTER
GE3
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
30.88
35.08
52.67
61.67
65.82
81.08
93.55
111. 72
115.97
161.88
276.50
296.04
303.05
333.77
338.60
356.25
384.14
387.30
414.87
418.53
421. 53
437.17
468.96
510.93
583.01
609.60
1974
462
56
236
97
800
45
202
58
30
57
19
140
78
32
488
108
199
41
28
17
110
20
20
10
9
123
95
121
77
79
151
105
58
50
68
37
20
29
17
16
16
29
39
8
5
4
10
21
2
0
0
4
4
0
1
1
0
0
2
2
0
0
5
5
1
1
0
4
4
1
1
1
0
0
0
0
0
6-AUG-2013 12:40:26.32
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1. 50
1. 60
2.83
1.51
1. 52
1. 91
1. 97
1. 75
1. 76
1. 55
1. 56
2.63
1. 68
1. 71
1. 83
1. 89
1.88
1. 72
1. 89
1. 90
1. 90
1. 91
1. 79
1.44
1.90
2.32
31.20
35.40
52.99
61.99
66.14
81.40
93.86
112.03
116.29
162.20
276.81
296.35
303.36
334.07
338.90
356.56
384.44
387.61
415.17
418.83
421.83
437.47
469.26
511.22
583.30
609.89
Left
Pw
27
27
50
58
58
77
90
108
108
160
272
293
293
330
330
351
382
382
411
411
411
433
464
506
581
607
14
14
7
12
12
10
9
14
14
7
10
14
14
13
13
11
9
9
18
18
18
10
9
9
5
6
6-AUG-2013 12:24:59.
1.00000E+00 filter
0
BAFIL
0 00:15:05.27 0.6%
4096
10.00000
Cts/Sec %Err
2.19E+00
5.13E-01
6.25E-02
2.62E-01
1.08E-01
8.89E-01
4.99E-02
2.25E-01
6.40E-02
3.36E-02
6.30E-02
2.09E-02
1. 56E-01
8.67E-02
3.57E-02
5.42E-01
1.20E-01
2.21E-01
4.58E-02
3.13E-02
1.89E-02
1.22E-01
2.23E-02
2.18E-02
1.11E-02
1. OOE-02
2.4
5.7
35.2
8.9
18.1
4.6
44.1
9.1
23.7
48.8
24.2
49.0
9.9
13.6
27.9
4.8
15.4
9.0
18.5
27.7
41.9
10.9
46.3
26.6
31.6
33.3
Fit
5.93E+00
7.57E+00
3.59E+00
1. 01E+01
1.49E+00
9.17E+00
1.27E+00
29

Sample ID : 1307147-12
Acquisition date

26
22
4
Page :
2
6-AUG-2013 12:24:59
15.38%

Nuclide
BA-133
Hlife
10.50Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 3.834E+02
Total Activity
---------
3.834E+02
Wtd Mean
Decay Corr
pCi/filter
3.834E+02
Decay Corr
2-Sigma
18.24
0.699E+02
---------
3.834E+02

Nuclide
Hlife
TH-234 4.47E+09Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 7.029E+02
Total Activity
Flags: "K"
"E"
=
=
---------
Wtd Mean
Decay Corr
pCi/filter
7.029E+02
---------
7.029E+02
7.029E+02
1.086E+03
1.086E+03
Keyline not found

Manually edited
2-Sigma
Decay Corr
1.340E+02
19.07
"M"
"A"
=
=
Manually accepted

Sample ID : 1307147-12
Acquisition date
Page :
3
6-AUG-2013 12:24:59

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
1.899E+01 3.834E+02
3.834E+02 18.24
6.222E+00 3.809E+02
3.809E+02 28.55
5.860E+OO 4.164E+02
4.164E+02 16.69
3 Valid Peaks
Status
OK
OK
OK
3.834E+02+/- 6.994E+01 ( 18.24%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag: "*"

%Eff
2.648E+01 7.029E+02
7.029E+02 19.07
1 Valid Peaks
Status
OK
7.029E+02+/- 1.340E+02 ( 19.07%)
= Keyline
til531

Sample ID : 1307147-12
Acquisition date
Page :
4
6-AUG-2013 12:24:59
Identified Nuclides
Nuclide
BA-133
TH-234
Activity
(pCi/ filter)
3.834E+02
7.029E+02
Act error
6.994E+01
1.340E+02
MDA
(pCi/filter)
1.958E+01
1.412E+02
MDA error
Act/MDA
2.995E+00
7.583E+00
19.577
4.978
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
1.900E-02
-6.671E+01
1.725E+00
2.234E+00
7.427E+00
2.017E+01
Act error
MDA
(pCi/filter)
MDA error
Act/MDA
6.133E+00
1.414E+02
1.716E+00
1.351E+00
3.887E+01
9.872E+00
9.893E+00
1.858E+02
3.280E+00
2.596E+00
5.630E+01
1.786E+01
1.130E+00
1.532E+01
4.665E-02
3.692E-02
4.551E+00
8.781E-01
0.002
-0.359
0.526
0.861
0.132
1.129

Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
DKA100: [GAMMA.SCUSR.ARCHIVE]SMP_130714713 GE3

PZ-304-AS DIS
6-AUG-2013 00:00:00.
1307147-13
FILTER
GE3
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30.85
35.17
52.10
61.77
65.81
81.20
92.30
111.82
116.38
213.95
276.98
302.99
307.04
334.00
338.17
351.70
356.32
376.86
384.04
387.05
391.75
415.38
421.53
437.48
464.52
467.88
471.70
511.47
609.50
2046
504
44
249
135
746
38
213
33
40
67
172
31
70
25
18
494
18
98
209
35
33
14
107
5
25
7
15
12
112
91
102
77
99
206
60
43
55
85
24
17
16
15
18
3
15
10
37
48
18
8
8
5
3
2
0
3
2
4
4
0
4
4
0
0
2
2
0
0
2
2
3
3
3
3
0
2
2
0
3
3
0
1
1
1
0
0
6-AUG-2013 12:56:00.49
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1. 53
1. 71
1. 81
1.69
2.02
1. 91
1.15
1. 75
1. 76
7.83
1.29
1. 98
1. 99
1. 98
2.22
1. 68
1. 71
2.60
1.75
1. 78
1. 38
2.29
1.90
1.65
1. 93
1.93
1. 76
3.79
3.25
31.17
35.49
52.41
62.09
66.13
81.52
92.61
112.13
116.69
214.26
277.28
303.30
307.34
334.31
338.48
352.00
356.63
377.16
384.34
387.36
392.06
415.68
421. 83
437.78
464.82
468.18
472.00
511.77
609.79
Left
Pw
27
27
50
58
58
76
90
107
107
207
273
298
298
330
330
351
351
375
382
382
391
410
410
433
462
462
462
508
606
14
14
7
12
12
12
6
14
14
12
8
16
16
12
12
10
10
5
9
9
5
22
22
10
14
14
14
8
7
C-
It
BAFI~19~?
CN
6-AUG-2013 12:40:38.
1.00000E+00 filter
0
BAFIL
0 00:15:05.09 0.6%
4096
10.00000
Cts/Sec %Err
2.27E+OO
5.60E-01
4.87E-02
2.77E-01
1.51E-01
8.28E-01
4.28E-02
2.37E-01
3.62E-02
4.44E-02
7.46E-02
1.91E-01
3.49E-02
7.83E-02
2.75E-02
1.97E-02
5.49E-01
1.95E-02
1.09E-01
2.33E-01
3.90E-02
3.70E-02
1.53E-02
1.19E-01
5.25E-03
2.82E-02
8.16E-03
1.63E-02
1.36E-02
2.3
5.4
40.8
8.3
15.3
5.3
35.6
8.4
38.9
49.8
17.6
8.2
38.3
15.1
40.7
9.3
4.6
36.2
14.4
8.8
27.3
27.3
48.3
10.4
74.0
23.8
67.5
34.8
33.7
Fit
6.09E+00
2.37E+00
2.39E+00
8.76E+OO
2.59E+00
9.97E+00
1.49E+01
2.20E+00
1.68E+00
i533

Sample ID : 1307147-13
Acquisition date

29
25
4
Page :
2
6-AUG-2013 12:40:38
13.79%

Nuclide
BA-133
Hlife
10.50Y
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
3.573E+02
Total Activity
Nuclide Type
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 7.446E+02
Total Activity
=
=
2-Sigma
Decay Corr
19.07
0.682E+02
---------
3.573E+02
NATURAL
Nuclide
Hlife
TH-234 4.47E+09Y
Flags: "K"
"E"
--------3.573E+02
Wtd Mean
Decay Corr
pCi/filter
3.573E+02
---------
Wtd Mean
Decay Corr
pCi/filter
7.446E+02
---------
7.446E+02
7.446E+02
1.102E+03
1.102E+03
Keyline not found

Manually edited
"M"
"A"
=
=
Decay Corr
2-Sigma
1.330E+02
17.86
Manually accepted
8534

Sample ID : 1307147-13
Acquisition date
Page :
3
6-AUG-2013 12:40:38

Nuclide
BA-133
Energy
81.00
302.84
356.01
%;Abn
33.00*
17.80
60.00
Final Mean for
Uncorrected Decay Carr 2-Sigma

%Eff
1.899E+01 3.573E+02
3.573E+02 19.07
6.222E+00 4.662E+02
4.662E+02 26.30
5.860E+00 4.220E+02
4.220E+02 16.44
3 Valid Peaks
Status
OK
OK
OK
3.573E+02+/- 6.815E+01 ( 19.07%)
Nuclide Type: NATURAl,

Nuclide
TH-234
Energy
63.29
%:Abn
3.80*
Final Mean for

Flag: "*"

%Eff
2.648E+01 7.446E+02
7.446E+02 17.86
1 Valid Peaks
Status
OK
7.446E+02+/- 1.330E+02 ( 17.86%)
Keyline
B535

Sample ID : 1307147-13.
Acquisition date
4
Page :
6-AUG-2013 12:40:38
Identified Nuclides
Nuclide
BA-133
TH-234
Activity
(pCi/filter)
Act error
MDA
(pCi/ filter)
MDA error
Act/MDA
3.573E+02
7.446E+02
6.815E+01
1.330E+02
1.987E+01
1.340E+02
3.038E+00
7.200E+00
17.987
5.555
Act error
MDA
(pCi/filter)
MDA error
Act/MDA
7.013E+00
1.233E+02
1.678E+00
1.437E+00
3.626E+01
9.766E+00
1.083E+01
1.736E+02
3.345E+00
2.847E+00
5.466E+01
1.811E+01
1.238E+00
1.432E+01
4.757E-02
4.049E-02
4.419E+00
8.902E-01
-0.176
-0.037
0.831
1. 274
0.295
1. 341
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
-1.904E+00
-6.396E+OO
2.780E+00
3.627E+00
1.611E+01
2.429E+01
1536
CL-

Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
'6!vtQ
DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP_130714714 GE3 BAFIL 194366.CN

MW-104 TOT
6-AUG-2013 00:00:00.
1307147-14
FILTER
GE3
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
30.81
34.81
53.06
61.74
66.19
81.12
84.84
111.89
115.77
143.28
153.22
205.04
276.89
294.92
303.36
312.29
334.04
338.34
352.70
356.25
386.11
391.51
415.02
418.47
422.06
437.08
463.91
469.00
505.61
511.27
542.70
610.51
696.04
1804
396
81
278
119
743
31
215
59
28
19
13
45
20
119
12
75
27
16
431
305
34
45
38
13
112
7
9
6
15
10
15
6
72
61
117
79
84
64
47
58
53
75
103
61
46
19
47
20
6
1
5
22
54
14
5
4
3
15
3
10
3
4
0
0
3
1
1
0
4
4
3
3
2
2
0
0
0
0
0
0
0
2
2
4
4
0
0
2
2
2
0
0
0
0
0
0
0
0
6-AUG-2013 13:11:53.36
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1.44
1. 45
2.93
2.01
2.02
1. 54
1. 87
1. 75
1. 76
1. 69
2.66
2.78
1. 60
1. 80
1. 91
1. 08
2.01
2.02
1. 68
1. 64
4.05
1. 24
2.08
2.09
2.09
2.01
2.02
1. 75
1. 73
2.81
1. 77
1.28
1.10
31.13
35.13
53.38
62.06
66.51
81.44
85.16
112.21
116.08
143.59
153.54
205.35
277.20
295.23
303.67
312.59
334.35
338.65
353.00
356.55
386.42
391.81
415.32
418.78
422.36
437.38
464.21
469.30
505.91
511.57
543.00
610.80
696.33
6-AUG-2013 12:56:31.
l.OOOOOE+OO filter
0
BAFIL
0 00:15:05.13 0.6%
4096
10.00000
Left
Pw
Cts/Sec %Err
26
26
49
58
58
76
76
108
108
139
150
204
273
292
299
311
328
328
352
352
381
391
412
412
412
432
460
466
503
508
540
607
693
15
15
9
15
15
14
14
17
17
9
10
7
9
7
8
6
14
14
11
11
10
5
17
17
17
9
7
6
5
8
6
8
6
2.00E+00 2.5
4.40E-01 6.1
9.04E-02 26.4
3.09E-01 7.8
1. 32E-01 16.7
8.26E-01 4.0
3.42E-02 75.3
2.39E-01 8.6
6.59E-02 27.3
3.06E-02 59.6
2.13E-02101.3
1.42E-02103.3
5.05E-02 30.5
2.17E-02 43.7
1.33E-01 13.6
1.37E-02 62.4
8.30E-02 13.4
2.99E-02 25.4
1.79E-02 17.7
4.79E-01 5.1
3.39E-01 7.4
3.79E-02 26.8
5.00E-02 18.2
4.28E-02 22.3
1.48E-02 54.4
1.24E-01 11.4
7.56E-03 59.1
1.04E-02 60.9
6.11E-03 60.6
1.67E-02 34.6
l.llE-02 31.6
1. 67E-02 25.8
6.67E-03 61.2
Fit
1.52E+01
2.13E+00
4.13E+00
1.66E+00
1.68E+00
3.32E+00
8.92E-01

Sample ID : 1307147-14
Acquisition date

33
28
5
Page :
2
6-AUG-2013 12:56:31
15.15%

Nuclide
Hlife
BA-133
10.50Y
NP-237 2.14E+06Y
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
3.562E+02
1. 00
4.189E+01
Total Activity
---------
3.981E+02
Wtd Mean
Decay Corr
pCi/filter
3.562E+02
4.189E+01
Decay Corr
2-Sigma
0.631E+02
17.70
6.319E+01
150.85
---------
3.981E+02

Nuclide
Hlife
TH-234 4.47E+09Y
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
8.309E+02
Total Activity
---------
Wtd Mean
Decay Corr
pCi/filter
8.309E+02
---------
8.309E+02
8.309E+02
1.229E+03
1.229E+03

Decay Corr
2-Sigma
1.412E+02
16.99


Sample ID : 1307147-14
Acquisition date
Page :
3
6-AUG-2013 12:56:31

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

NP-237
86.50
3 Valid Peaks
12.60*
Final Mean for

%Eff
1.899E+01 3.562E+02
3.562E+02 17.70
6.222E+00 3.238E+02
3.238E+02 34.05
5.860E+00 3.679E+02
3.679E+02 17.02
1.749E+01
1 Valid Peaks
3.562E+02+/- 6.306E+01 ( 17.70%)
4.189E+01
=
Status
OK
OK
OK
4.189E+01 150.85
OK
4.189E+01+/- 6.319E+01 (150.85%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag: "*"

%Eff
2.648E+01 8.309E+02
8.309E+02 16.99
1 Valid Peaks
Status
OK
8.309E+02+/- 1.412E+02 ( 16.99%)
Keyline
535

Sample ID : 1307147-14
Acquisition date
4
Page :
6-AUG-2013 12:56:31
Identified Nuclides
Nuclide
BA-133
TH-234
NP-237
Activity
(pCi/filter)
Act error
3.562E+02
8.309E+02
4.189E+01
6.306E+01
1.412E+02
6.319E+01
MDA
(pCi/filter)
1.809E+01
1.147E+02
5.158E+01
MDA error
Act/MDA
2.767E+00
6.161E+00
4.170E+00
19.686
7.243
0.812
MDA error
Act/MDA
1.183E+00
1.387E+01
4.301E-02
3.972E-02
8.971E-01
0.050
-0.098
0.618
1. 507
1. 742
Nuclide
C0-57
CD-109
PA-231
PA-234
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
5.151E-01
-1.644E+01
1.870E+OO
4.208E+00
3.178E+01
Act error
6.381E+00
1.060E+02
1.538E+00
1.427E+00
9.346E+00
MDA
(pCi/filter)
1.036E+01
1.683E+02
3.024E+00
2.793E+00
1.825E+01

Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
~(~II)

MW-104 DIS
6-AUG-2013 00:00:00.
1307147-15
FILTER
GE3
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
30.81
35.15
51.46
61.78
65.82
81.08
111.87
116.24
199.03
239.43
243.95
276.79
294.62
302.86
307.53
334.11
356.46
364.94
383.82
386.87
391.53
407.84
414.87
417.87
437.22
467.93
508.62
511.68
609.76
927.56
1928
531
133
199
87
823
208
52
19
18
12
48
17
126
29
75
460
18
79
195
30
9
36
17
92
29
6
15
17
6
85
89
199
68
75
181
80
80
55
34
27
47
15
15
15
34
55
11
7
13
20
12
12
12
9
2
0
0
5
0
4
4
0
1
1
0
0
0
0
4
4
0
1
1
1
0
0
0
1
1
1
1
1
1
0
0
2
2
0
0
6-AUG-2013 13:27:43.64
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1.48
1. 72
7.68
1. 51
1.52
1. 80
1.62
2.49
2.95
2.32
2.33
1. 23
1.80
1. 80
1. 81
1.84
1. 80
2.75
1.60
1. 87
1. 88
1. 89
1. 89
1. 90
1.98
1. 83
2.16
2.16
1.18
2.74
31.13
35.47
51.77
62.09
66.14
81.40
112.19
116.55
199.34
239.74
244.26
277.10
294.93
303.16
307.84
334.41
356.77
365.24
384.13
387.17
391.83
408.14
415.17
418.17
437.52
468.23
508.92
511.98
610.06
927.83
Left
Pw
26
26
43
58
58
76
108
116
196
236
236
273
290
290
290
331
353
362
382
382
382
403
403
403
433
465
508
508
606
924
14
14
15
12
12
11
7
6
7
12
12
8
22
22
22
7
9
6
16
16
16
25
25
25
9
6
9
9
7
7
6-AUG-2013 13:12:19.
l.OOOOOE+OO filter
0
BAFIL
0 00:15:05.16 0.6%
4096
10.00000
Cts/Sec %Err
2.14E+00
5.90E-01
1.48E-01
2.21E-01
9.70E-02
9.15E-01
2.31E-01
5.73E-02
2.08E-02
2.00E-02
1. 33E-02
5.32E-02
1. 90E-02
1.40E-01
3.26E-02
8.33E-02
5.11E-01
2.04E-02
8.82E-02
2.17E-01
3.30E-02
l.OOE-02
4.01E-02
1.94E-02
1.02E-01
3.27E-02
6.17E-03
1.65E-02
1.86E-02
6.67E-03
2.3
5.1
24.7
10.0
20.1
4.7
9.9
32.6
70.2
59.7
85.5
28.9
43.6
10.1
27.2
17.2
5.6
36.5
14.3
9.2
30.3
66.6
22.1
52.8
12.0
19.6
31.2
31.6
33.4
40.8
Fit
1.30E+Ol
6.17E+00
1.14E+00
2.32E+00
6.64E+00
1.36E+00
1.36E+00

Sample ID : 1307147-15
Acquisition date

30
26
4
Page :
2
6-AUG-2013 13:12:19
13.33%

Nuclide
BA-133
Hlife
10.50Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 3.945E+02
Total Activity
3.945E+02
Wtd Mean
Decay Corr
pCi/filter
3.945E+02
2-Sigma
Decay Corr
18.40
0.726E+02
3.945E+02

Nuclide
Hlife
TH-234 4.47E+09Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 5.932E+02
Total Activity
Flags: "K"
"E"
Wtd Mean
Decay Corr
pCi/filter
5.932E+02
5.932E+02
5.932E+02
9.877E+02
9.877E+02
= Keyline not found

= Manually edited
"M''
"A"
=
=
Decay Corr
2-Sigma
21.05
1.249E+02
Manually accepted
4!:542

Sample ID : 1307147-15
Acquisition date
Page :
3
6-AUG-2013 13:12:19

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
1.899E+01 3.945E+02
3.945E+02 18.40
6.222E+00 3.419E+02
3.419E+02 28.92
5.860E+00 3.932E+02
3.932E+02 17.64
3 Valid Peaks
Status
OK
OK
OK
3.945E+02+/- 7.260E+01 ( 18.40%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag: "*"
Keyline

%Eff
2.648E+01 5.932E+02
5.932E+02 21.05
1 Valid Peaks
Status
OK
5.932E+02+/- 1.249E+02 ( 21.05%)

Sample ID : 1307147-15
Acquisition date
Page :
4
6-AUG-2013 13:12:19
Identified Nuclides
Nuclide
BA-133
TH-234
Activity
(pCi/filter)
Act error
MDA
(pCi/filter)
MDA error
Act/MDA
3.945E+02
5.932E+02
7.260E+01
1.249E+02
2.225E+01
1.309E+02
3.402E+00
7.028E+00
17.734
4.533
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
1.569E+00
1.362E+02
1.375E+00
4.828E+00
4.322E+01
1.760E+01
Act error
MDA
(pCi/filter)
MDA error
Act/MDA
5.654E+00
1.143E+02
1.503E+00
1.537E+00
3.480E+01
9.125E+00
9.522E+00
2.052E+02
2.904E+00
2.990E+00
6.222E+01
1.662E+01
1.088E+00
1.692E+01
4.131E-02
4.253E-02
5.029E+00
8.173E-01
0.165
0.664
0.473
1. 614
0.695
1.059
~~\0

Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP_130714716 GE3 BAFIL 194369.CN

PZ-204A-SS TOT
6-AUG-2013 00:00:00.
1307147-16
FILTER
GE3
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
28.26
30.89
34.88
52.37
61.81
65.77
81.04
84.12
103.06
111.74
116.57
146.47
184.41
192.00
276.53
279.85
302.98
308.45
333.82
338.44
356.41
383.86
387.20
3 91. 62
414.86
418.53
421.87
437.17
447.03
468.42
473.07
511.18
582.82
609.11
72
2029
479
46
273
129
787
25
22
223
88
18
22
39
66
10
122
26
75
37
470
115
200
49
41
28
12
109
6
25
11
22
9
15
4
4
4
0
3
3
7
7
0
3
3
0
0
0
1
1
0
0
4
4
0
5
5
0
1
1
1
0
0
2
2
0
0
0
6-AUG-2013 13:43:11.85
Bkgnd
135
78
84
109
76
89
68
62
122
51
36
52
50
80
20
13
18
25
22
15
60
38
57
14
7
5
4
4
8
2
4
4
0
0
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1. 90
1.39
1. 93
1. 90
1. 82
1. 83
1.49
1. 50
2.71
1. 93
1. 93
2.76
1. 30
2.02
1. 78
1. 78
1. 85
1.34
1. 97
1. 96
1. 87
1. 61
1. 74
2.69
1.89
1. 90
1. 90
2.01
1.24
2.13
2.13
1. 90
2.32
2.95
28.58
31.21
35.20
52.69
62.13
66.09
81.36
84.44
103.38
112.05
116.89
146.79
184.72
192.31
276.84
280.16
303.29
308.76
334.12
338.75
356.71
384.16
387.51
391.92
415.16
418.83
422.17
437.47
447.33
468.72
473.37
511.48
583.11
609.40
Left
Pw
26
26
26
50
57
57
78
78
98
107
107
145
182
188
273
273
300
307
330
330
353
382
382
391
411
411
411
433
443
466
466
507
581
605
15
15
15
7
16
16
9
9
9
17
17
6
7
10
11
11
6
6
15
15
10
9
9
5
20
20
20
8
8
12
12
9
5
9
6-AUG-2013 13:27:51.
l.OOOOOE+OO filter
0
BAFIL
0 00:15:05.39 0.6%
4096
10.00000
Cts/Sec %Err
7.95E-02
2.25E+00
5.32E-01
5.06E-02
3.04E-01
1.44E-01
8.74E-01
2.79E-02
2.49E-02
2.47E-01
9.73E-02
1.98E-02
2.45E-02
4.33E-02
7.38E-02
1. 08E-02
1.36E-01
2.87E-02
8.34E-02
4.16E-02
5.22E-01
1.27E-01
2.22E-01
5.48E-02
4.59E-02
3.07E-02
1.28E-02
1.21E-01
6.67E-03
2.74E-02
1.26E-02
2.44E-02
l.OOE-02
1.67E-02
Fit
59.9 1.74E+Ol
2.3
7.5
40.8
7.5 2.67E+00
15.8
3.8 5.27E+00
88.2
92.2
8.7 4.69E+00
16.8
67.2
56.9
45.8
14.7 4.43E+00
95.3
10.6
38.3
15.1 1. 94E+00
24.8
5.7
12.7 2.49E+Ol
9.2
21.1
19.8 1.40E+00
28.5
56.1
10.1
91.3
24.5 8.40E-01
45.4
27.4
33.3
25.8
1545

Sample ID : 1307147-16
Acquisition date

34
30
4
Page :
2
6-AUG-2013 13:27:51
11. 76%

Nuclide
BA-133
Hlife
10.50Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 3.772E+02
--------
Total Activity
Nuclide Type
3.772E+02
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00 8.155E+02
--------
Total Activity
Grand Total Activity
=
=
Decay Corr
2-Sigma
17.56
0.662E+02
--------
3.772E+02
NATURAL
Nuclide
Hlife
TH-234 4.47E+09Y
Flags: "K"
"E"
Wtd Mean
Decay Corr
pCi/filter
3.772E+02
Wtd Mean
Decay Corr
pCi/filter
8.155E+02
--------
8.155E+02
8.155E+02
1.193E+03
1.193E+03
Keyline not found

Manually edited
"M"
"A"
=
=
Decay Corr
2-Sigma
1.341E+02
16.44
Manually accepted

Sample ID : 1307147-16
Acquisition date
Page :
3
6-AUG-2013 13:27:51

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
1.899E+01 3.772E+02
3.772E+02 17.56
6.222E+00 3.319E+02
3.320E+02 29.49
5.860E+00 4.011E+02
4.011E+02 17.72
3 Valid Peaks
Status
OK
OK
OK
3.772E+02+/- 6.624E+01 ( 17.56%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag: "*"
Keyline

%Eff
2.648E+01 8.155E+02
8.155E+02 16.44
1 Valid Peaks
Status
OK
8.155E+02+/- 1.341E+02 ( 16.44%)

Sample ID : 1307147-16
----
Acquisition date
Page :
4
6-AUG-2013 13:27:51
Identified Nuclides
Nuclide
BA-133
TH-234
Activity
(pCi/filter)
Act error
3.772E+02
8.155E+02
6.624E+01
1.341E+02
MDA
(pCi/filter)
2.109E+01
1.172E+02
MDA error
Act/MDA
3.226E+OO
6.293E+00
17.883
6.960
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
-6.618E+00
-3.710E+01
1.416E+00
2.695E+00
1.749E+01
3.082E+01
Act error
MDA
(pCi/filter)
MDA error
Act/MDA
6.160E+00
1.071E+02
1.657E+00
1.521E+00
3.094E+01
9.389E+OO
8.340E+00
1.658E+02
3.151E+00
2.764E+OO
5.310E+01
1.821E+01
9.528E-01
1.367E+01
4.481E-02
3.932E-02
4.292E+00
8.955E-01
-0.794
-0.224
0.450
0.975
0.329
1. 692
~\Q,\\:J

Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
D~lOO:
[GAMMA.SCQSR.ARCHIVE]SMP_130714717 GE3_BAFIL_l9437l.CN
PZ-204A-SS DIS
6-AUG-2013 00:00:00.
1307147-17
FILTER
GE3
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
30.83
35.04
53.94
61.71
65.63
81.06
92.83
96.68
111.79
116.54
160.80
186.53
190.62
276.76
293.97
299.44
303.04
307.78
333.74
338.53
356.35
384.01
387.09
415.89
437.23
468.39
510.98
610.07
2043
518
53
286
104
848
32
16
236
61
29
26
21
57
22
13
154
24
81
21
508
103
157
78
114
16
19
5
101
94
117
63
68
118
37
29
35
35
111
51
47
17
14
10
10
5
13
18
32
41
54
9
12
7
2
2
4
4
0
1
1
0
1
1
1
1
0
1
1
0
0
2
2
2
1
1
0
4
4
0
0
0
0
0
6-AUG-2013 13:59:27.76
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1.52
1. 59
1. 94
1. 51
1. 52
1.90
1. 56
1.43
1. 59
1. 60
1. 54
1. 69
1. 69
1. 42
3.19
1.98
1. 92
1. 99
1. 72
1.83
1. 90
2.32
1.71
4.52
1.95
1. 29
2.12
0.90
31.15
35.36
54.25
62.02
65.95
81.37
93.14
97.00
112.11
116.85
161.11
186.85
190.94
277.07
294.28
299.75
303.34
308.09
334.05
338.83
356.66
384.32
387.39
416.20
437.53
468.69
511.27
610.36
Left
Pw
26
26
49
58
58
77
90
90
107
107
157
183
183
274
291
298
298
298
330
330
353
381
381
410
432
465
507
607
15
15
8
12
12
10
17
17
17
17
9
11
11
7
7
17
17
17
12
12
8
10
10
12
12
7
10
5
6-AUG-2013 13:44:07.
l.OOOOOE+OO filter
0
BAFIL
0 00:15:05.41 0.6%
4096
10.00000
Cts/Sec %Err
2.27E+00
5.75E-01
5.84E-02
3.18E-01
1.16E-01
9.42E-01
3.58E-02
1.80E-02
2.62E-01
6.78E-02
3.18E-02
2.87E-02
2.28E-02
6.34E-02
2.41E-02
1.44E-02
1. 72E-01
2.70E-02
9.02E-02
2.34E-02
5.65E-01
1.14E-01
1.75E-01
8.70E-02
1.27E-01
1. 78E-02
2.11E-02
5.24E-03
2.3
5.3
38.3
7.4
16.4
4.2
34.2
54.7
7.8
20.8
69.2
46.2
54.3
17.9
35.8
40.0
8.8
31.7
12.9
39.1
4.8
17.6
10.9
13.6
11.2
37.1
27.5
67.5
Fit
9.13E+00
7.01E+OO
2.74E+00
2.79E+00
1.27E+00
3.21E+00
7.17E-01
1.04E+Ol
1549

Sample ID : 1307147-17
Acquisition date

28
24
4
Page :
2
6-AUG-2013 13:44:07
14.29%

Nuclide
BA-133
Hlife
10.50Y
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
4.064E+02
Total Activity
---------
4.064E+02
Wtd Mean
Decay Carr
pCi/filter
4.064E+02
2-Sigma
Decay Carr
17.90
0.727E+02
---------
4.064E+02

Nuclide
Hlife
TH-234 4.47E+09Y
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
8.548E+02
Total Activity
---------
Wtd Mean
Decay Carr
pCi/filter
8.548E+02
---------
8.548E+02
8.548E+02
1.261E+03
1.261E+03

Decay Carr
2-Sigma
1.390E+02
16.27


Sample ID : 1307147-17
Acquisition date
Page :
3
6-AUG-2013 13:44:07

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
1.899E+01 4.064E+02
4.064E+02 17.90
6.222E+00 4.185E+02
4.186E+02 27.03
5.860E+00 4.342E+02
4.343E+02 16.74
3 Valid Peaks
Status
OK
OK
OK
4.064E+02+/- 7.274E+01 ( 17.90%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag: "*"

%Eff
2.648E+01 8.548E+02
8.548E+02 16.27
1 Valid Peaks
Status
OK
= 8.548E+02+/- 1.390E+02 ( 16.27%)
= Keyline
B551

Sample ID : 1307147-17
Acquisition date
Page :
4
6-AUG-2013 13:44:07

Nuclide
BA-133
TH-234
Activity
(pCi/filter)
Act error
MDA
(pCi/filter)
MDA error
Act/MDA
4.064E+02
8.548E+02
7.274E+01
1.390E+02
1.809E+01
1.253E+02
2.767E+00
6.732E+00
22.461
6.820
Act error
MDA
(pCi/ filter)
MDA error
Act/MDA
5.920E+OO
1.070E+02
1.487E+00
1.484E+00
2.985E+01
1.014E+01
9.068E+00
1.490E+02
2.823E+00
2.883E+00
4.557E+01
1.955E+01
1.036E+00
1.228E+01
4.016E-02
4.101E-02
3.683E+00
9.614E-01
-0.246
-0.123
0.341
1.527
0.231
1.831
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
-2.230E+00
-1.S26E+01
9.626E-01
4.403E+00
1.051E+01
3.581E+01
!!!552
"-S\t)u)

Configuration
Analyses by
Client ID
Deposition Date
Sample :Oate
Sample I:O
Sample type
:Oetector name
Elapsed live time:
Start channel
Sensitivity
Critical level
:0~100:
[GAMMA.SCUSR.ARCHIVE]SMP_l30714718 GE3 BAFIL 194373.CN

PZ-302-AI TOT
6-AUG-2013 00:00:00.
1307147-18
FILTER
GE3
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
30.85
35.09
46.46
52.96
61.74
65.91
70.52
81.17
92.68
111.87
115.87
241.22
255.60
277.07
303.04
307.15
310.43
333.89
338.34
356.26
376.91
383.90
387.05
391.06
414.76
417.87
437.40
468.11
510.49
609.58
804.86
2106
503
33
54
295
137
16
910
37
227
56
12
19
67
172
28
14
84
24
511
12
133
205
38
37
28
98
21
23
8
7
91
97
90
115
67
72
74
99
76
57
46
39
32
20
13
10
11
22
19
33
29
16
10
7
17
10
7
13
0
4
0
4
4
0
0
2
2
2
0
0
2
2
0
0
0
6
6
6
2
2
0
0
2
2
2
1
1
0
0
0
0
0
6-AUG-2013 14:14:59.81
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1. 47
1.62
1. 20
2.03
1.66
1. 67
1. 68
1. 89
1. 90
1. 74
1. 76
1. 50
4.46
1.60
1. 67
2.19
2.91
2.01
2.02
1.95
1.15
2.06
1.84
2.06
1. 89
1. 90
1. 89
1. 77
1. 66
3.81
2.70
31.17
35.41
46.78
53.28
62.06
66.23
70.84
81.48
92.99
112.18
116.18
241.53
255.91
277.37
303.35
307.46
310.74
334.20
338.65
356.56
377.22
384.20
387.35
391.36
415.06
418.17
437.70
468.41
510.78
609.87
805.14
Left
Pw
26
26
44
50
58
58
58
77
90
108
108
238
252
274
300
300
300
329
329
351
373
380
380
380
412
412
434
463
506
606
802
15
15
7
7
16
16
16
10
6
19
19
6
9
8
15
15
15
13
13
10
8
16
16
16
13
13
7
9
9
8
6
6-AUG-2013 13:59:38.
1.00000E+OO filter
0
BAFIL
0 00:15:04.89 0.5%
4096
10.00000
Cts/Sec %Err
2.34E+00
5.59E-01
3.72E-02
5.98E-02
3.28E-01
1.52E-01
1. 78E-02
1.01E+00
4.12E-02
2.52E-01
6.20E-02
1.34E-02
2.08E-02
7.48E-02
1.91E-01
3.14E-02
1.59E-02
9.31E-02
2.69E-02
5.68E-01
1.34E-02
1.48E-01
2.27E-01
4.27E-02
4.08E-02
3.12E-02
1.09E-01
2.32E-02
2.56E-02
8.61E-03
7.78E-03
Fit
2.3 5.29E+00
5.4
49.9
35.6
7.2 3.07E+00
12.9
82.0
3.9
40.7
8.3 8.96E-01
24.1
85.9
59.0
17.0
8.1 3.78E+00
42.2
71.1
14.1 3.21E+00
36.4
4.9
81.6
10.0 8.40E+00
8.3
32.7
23.2 1.04E+01
36.1
11.1
38.4
20.9
57.7
37.8
&553

Sample ID : 1307147-18
Acquisition date

31
27
4
Page :
2
6-AUG-2013 13:59:38
12.90%

Nuclide
BA-133
Hlife
10.50Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 4.363E+02
Total Activity
---------
4.363E+02
Wtd Mean
Decay Corr
pCi/filter
4.364E+02
l)ecay Corr
2-Sigma
17.63
0.770E+02
---------
4.364E+02

Nuclide
Hlife
TH-234 4.47E+09Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 8.800E+02
Total Activity
Flags: "K"
"E"
=
=
---------
Wtd Mean
Decay Corr
pCi/filter
8.800E+02
---------
8.800E+02
8.800E+02
1.316E+03
1.316E+03
Keyline not found

Manually edited
"M"
"A"
=
=
2-Sigma
Decay Corr
1.393E+02
15.83
Manually accepted
1554

Sample ID : 1307147-18
Acquisition date
Page :
3
6-AUG-2013 13:59:38

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
1.899E+01 4.363E+02
4.364E+02 17.63
6.222E+OO 4.650E+02
4.650E+02 26.16
5.860E+00 4.367E+02
4.367E+02 16.79
3 Valid Peaks
Status
OK
OK
OK
4.364E+02+/- 7.695E+01 ( 17.63%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag:
11
* 11

%Eff
2.648E+01 8.800E+02
8.800E+02 15.83
1 Valid Peaks
Status
OK
8.800E+02+/- 1.393E+02 ( 15.83%)
Keyline
msss

Sample ID : 1307147-18
Acquisition date
4
Page :
13:59:38
6-AUG-2013
Nuclide
BA-133
TH-234
Activity
(pCi/filter)
Act error
4.364E+02
8.800E+02
7.695E+01
1.393E+02
MDA
(pCi/filter)
1.840E+01
1.196E+02
MDA error
Act/MDA
2.814E+00
6.422E+00
23.713
7.360
MDA error
Act/MDA
1.108E+00
1.408E+01
4.398E-02
4.059E-02
3.926E+00
9.298E-01
-0.489
0.203
0.837
1. 278
-0.018
1. 797
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
-4.744E+00
3.469E+01
2.587E+00
3.648E+00
-8.539E-01
3.399E+01
Act error
6.096E+00
1.142E+02
1.524E+00
1.517E+00
3.422E+01
9.737E+00
MDA
(pCi/filter)
9.697E+00
1.708E+02
3.092E+00
2.854E+00
4.856E+01
1.891E+01
\ell
~'\ \t \0
Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level

PZ-302-AI DIS
6-AUG-2013 00:00:00.
1307147-19
FILTER
GE3
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
30.81
35.06
51.90
61.85
66.02
80.98
83.68
111. 86
116.51
142.30
163.18
276.70
303.01
333.68
338.56
356.28
383.84
387.09
391.68
414.72
417.90
421.89
437.76
468.16
512.63
830.05
1958
473
58
264
118
734
17
200
47
31
43
54
129
76
18
510
115
217
39
42
35
8
104
17
15
6
70
81
113
71
80
76
52
47
50
42
75
27
58
18
28
19
13
8
4
9
9
9
25
9
6
0
4
4
0
4
4
2
2
4
4
0
0
0
0
1
1
0
5
5
5
2
2
2
0
0
0
0
6-AUG-2013 14:30:49.52
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1.45
1.68
3.81
1. 66
2.02
1. 70
1.41
1. 60
2.13
2.86
2.05
1.44
1. 74
1. 83
1. 83
1.94
1. 98
2.05
1. 99
2.08
1. 91
2.09
1. 86
2.02
1. 51
1.92
31.13
35.38
52.22
62.17
66.34
81.29
84.00
112.18
116.83
142.61
163.50
277.01
303.32
333.98
338.87
356.59
384.14
387.39
391.98
415.02
418.20
422.19
438.06
468.46
512.92
830.33
6-AUG-2013 14:15:25.
l.OOOOOE+OO filter
0
BAFIL
0 00:15:05.38 0.6%
4096
10.00000
Left
Pw
Cts/Sec %Err
27
27
49
57
57
77
77
108
108
140
159
274
299
329
329
354
380
380
380
411
411
411
432
465
509
827
14
14
8
13
13
13
13
13
13
6
10
8
8
14
14
9
16
16
16
15
15
15
11
7
8
6
2.18E+00 2.3
5.25E-01 5.5
6.44E-02 34.3
2.94E-01 7.7
1. 32E-01 17.1
8.16E-01 4.0
1.84E-02122.5
2.22E-01 8.7
5.18E-02 29.9
3.47E-02 37.6
4.77E-02 41.2
6.01E-02 21.7
1.44E-01 13.5
8.48E-02 15.0
1.97E-02 49.8
5.67E-01 4.7
1.28E-01 11.0
2.41E-01 8.4
4.36E-02 22.4
4.67E-02 20.4
3.92E-02 28.0
8.97E-03 80.8
1.16E-01 13.5
1. 89E-02 37.9
1.70E-02 37.6
6.67E-03 40.8
Fit
3.54E+00
1.97E+00
1.02E+Ol
1.39E+00
4.88E+00
7.49E+00
3.19E+00

Sample ID : 1307147-19
Acquisition date

26
22
4
Page :
2
6-AUG-2013 14:15:25
15.38%

Nuclide
BA-133
Hlife
10.50Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 3.518E+02
Total Activity
3.518E+02
Wtd Mean
Decay Corr
pCi/filter
3.518E+02
Decay Corr
2-Sigma
17.76
0.625E+02
3.518E+02

Nuclide
Hlife
TH-234 4.47E+09Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 7.890E+02
Total Activity
Flags: "K"
"E"
Wtd Mean
Decay Corr
pCi/filter
7.890E+02
7.890E+02
7.890E+02
1.141E+03
1.141E+03
Keyline not found

Manually edited
"M"
"A"
Decay Corr
2-Sigma
1.332E+02
16.88
= Manually accepted
8558

Sample ID : 1307147-19
Acquisition date
Page :
3
6-AUG-2013 14:15:25

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for
l}ncorrected Decay Corr 2-Sigma

%Eff
1.899E+01 3.518E+02
3.518E+02 17.76
6.222E+00 3.505E+02
3.506E+02 33.90
5.860E+00 4.360E+02
4.360E+02 16.52
3 Valid Peaks
Status
OK
OK
OK
3.518E+02+/- 6.246E+01 ( 17.76%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag: "*"
Keyline

%Eff
2.648E+01 7.890E+02
7.890E+02 16.88
1 Valid Peaks
Status
OK
7.890E+02+/- 1.332E+02 ( 16.88%)

Sample ID : 1307147-19
----
Acq'l)isition date
Page :
4
6-AUG-2013 14:15:25
Identified Nuclides
Nuclide
BA-133
TH-234
Activity
(pCi/filter)
Act error
MDA
(pCi/ filter)
MDA error
Act/MDA
3.518E+02
7.890E+02
6.246E+01
1.332E+02
1.900E+01
1.207E+02
2.906E+00
6.485E+00
18.513
6.535
Act error
MDA
(pCi/ filter)
MDA error
Act/MDA
5.850E+00
1.098E+02
1.658E+00
1.364E+00
3.047E+01
9.361E+00
9.963E+00
1.763E+02
3.260E+00
2.692E+00
5.182E+01
1.794E+01
1.138E+00
1.453E+01
4.636E-02
3.829E-02
4.189E+00
8.821E-01
0.238
-0.027
0.707
1.142
-0.152
1.567
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
2.369E+00
-4.838E+00
2.306E+00
3.074E+00
-7.896E+00
2.812E+01

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ENGINEERING MANAGEMENT SUPPORT, INC.

West Lake OU-1

WORK ORDER #13-07147-0R

August 29, 2013

EBERLINE ANALYTICAL/OAK RIDGE LABORATORY

Chain of Custody & pH Check Sheet

Analytical Results Summary

Quality Control Sample Results Summary

Laboratory Technician's Notes

Analytical Data (Isotopic Uranium)

Analytical Data (Isotopic Thorium)

Analytical Data (Radium-226)

Analytical Data (Radium-228)

Barium-133 Analytical Tracer Data

Last Page Number

STANDARD OPERATING PROCEDURE

Eberline Services -Oak Ridge Laboratory

LABORATORY DATA SUPPORT CHECKLIST

Electronic Deliverable Proof

Client in Possession of Data

Technical/Clerical Corrections, Signatures Needed, Problems, Etc

Chain of Custody Record

Sampler (Print Name):

A\a.J - ' 0'-l

Received by: (Signature)

Receivecl by: (Slgnature)

'I 3r~ ......... .L..:

Relinquished by: (Signature)

-"llnqu~ :;;,, 1gn""""?'T

t:? ... '$:!3~ ')

t'\c,J ... ,03

Sample Custodian R8lnlllb (Completed By Laboratory):

Total # Containers Received?

COC Seals Present?

COC Seals Intact?

Received Containers Intact?

Oak Ridge Laboratory

MUST USE FXN 04 FOR DUP

Printed: 7/23/2013 3:48PM

Oak Ridge Laboratory

Re-Analysis: 2Fxns 94, 9&, 98, 1&,

12, 1-4, I 8 & 1B-are TOTAL

Original Lab Deadline: 08/20/13

'OlfJ~;q-!r J:1 /2--0'd

t(i) rt} 1'3""

Location (circle one)

Oak Ridge Laboratory

Printed: 7/23/2013 3:48PM

Oak Ridge Laboratory

MUST USE FXN 04 FOR DUP

Printed: 7/23/2013 3:48PM

Oak Ridge Laboratory

Printed: 7/23/2013 3:48PM

Printed: 7/23/2013 3:18 PM

e . . E:: R.'-1.. . ~ . .1::

Sample Receiving Report

(Volumes, pH,&. CPM)

Rec Vol Ttl CPM Max

PZ-208-SS DIS '

MW-104 DIS "'

Container Number :. PHOri!l

,; Volunie'ICI :: .. ;.1 Cf'M>

Printed: 7/23/2013 3:18PM