Sie sind auf Seite 1von 439

ENGINEERING MANAGEMENT SUPPORT, INC.

West Lake OU-1

STANDARD LEVEL IV

REPORT OF ANALYSIS

WORK ORDER #13-07149-0R

August 29, 2013

EBERLINE ANALYTICAL/OAK RIDGE LABORATORY

OAK RIDGE, TN

TABLE OF CONTENTS

SECTION

DESCRIPTION

PAGE

Chain of Custody & pH Check Sheet

0004

II

Sample Acknowledgement

0011

III

Case Narrative

0014

IV

Analytical Results Summary

0018

Analytical Standards

0023

VI

Quality Control Sample Results Summary

0048

VII

Laboratory Technician's Notes

0057

VIII

Analytical Data (Isotopic Uranium)

0085

IX

Analytical Data (Isotopic Thorium)

0179

Analytical Data (Radium-226)

0273

XI

Analytical Data (Radium-228)

0362

XII

Barium-133 Analytical Tracer Data

0377

Last Page Number

0437

STANDARD OPERATING PROCEDURE

MP-001, Rev.12

Sample Receiving

Effective: 10131112
Page 14 of14

Eberline Services - Oak Ridge Laboratory

LABORATORY DATA SUPPORT CHECKLIST

MP-001-3

Eberline Services Work Order#_ _ _ _ _ _ _ _ _ _ _ _ _ _ __

The checklist items listed below are to be initialed by appropriate staff upon completion/verification.

Date for Partial

Initials

Date

Checklist Items

Initials

1/z!>/1>
'i)-14-13

\((.

Sample Log-In

J&

Data Compilation

f'-.M-"

/Vd

First Technical Data Review

,r; ,,.,_

.~' 1)11\

Second Technical Data Review

~ ir,

;:

Data Entry/Electronic Deliverable

~!)'!. L3

~,.../
ftf!,,

~r,- 13

!A<.Ft.

e ii'

L.

'I

-l(l'.l..-i 'I)

'

Case Narrative
Electronic Deliverable Proof
Samples ,<\nijfyzed within Holding Time
Voo? J

VI.

f\I,..? I

'

QNQC R<(v;ew

r . ,
l/l'7\\

Client in il'ossession of Data


-

. ...... u,,....-1

r"'nnu

Invoiced by Laboratory

Technical/Clerical Corrections, Sign~tures Needed, Problems, Etc

Date/Initials

~
Date package approved by:

~~

Laboratory Manager

Copy No. _ _ __

)'

J7h-4f v0
Date

Radiochemistry Services

SECTION I

CHAIN OF CUSTODY

&

pH CHECK SHEET

REC'D JUL 2 2 2013

13~07149
Project Name:fJ.. b~
Send Report

To:~

tA. ~(JY/

Project Number:

IM..--d

Sampler (Print Name):

Address:~0 <.J.J. ~k

Sampler (Print Name):

5.it' k tcfJ

Shipment Method:~

~ka~.(io ~55

Airbill Number;

N~

601 SCluboto Road

1604

Oak Rldgo, TN 37830


!865) 481.Q683 Phone (865) 483-4621 Fax

If;

.:H-.S

SCAYICCS

Pag~orS

(D

~~~of
ff~

~
J

Purchase
Ofder
......__ _ _ _ _ _ __

Laboratory Receiving:

Phone:

,EBERLl~E
~

abertlne Servtca

Chain of Custody Record

Fax:
Sample
Date

Field Sample 10

1~1

P? _.Jo?. ... AS
Lll-catJ

4.~

1:1f,&f1

r'.'.r3o

c.,, ..,

,~,.~/13

IOU I

,f).,,8,

R.

p:, ., Zo{ - SS

\u, \ \

t.i_ ... ,03

\'2, 13

/> .:z..-1 ll .. '<S


_,.Pi .. to3 -53
..0-8~
J)Jp )<~

s-~J

0 . . 1'(
p ~.... 'ltoS' .. AJ

ct

I '-\I

IS-

!3s1.

.o.. 3

P~- 11)-{-~

I'1 ... 'Zf1'.1, -

lr5

Rellnquisheifl)y; (Signature)

z..

l~ltJ

v ,,, , I ......-1 "",/I.-'

0~30

Z.. I...-rl . . .-1 ~ ....., .,.,,, ..,.....


i..
I.,....,,,.... ,.., I_....r.,.

D1c/r-

2..

'l

I,,;I,; I~ 1,...,.. v

t2.c1

2.
2..

l./f A" A.,.....-1..,....1.,.....

13Jr-

3cJ

I ~u-

/'(,&LA

Recelve<f6Y:cs1gnature)

~f ~-~( f.iiunv

3
'Z
Date:

Vl........t.....-1..-.1....,.,......
1.........-1

1.,.,. 19"1 v"'l,/l ,, .......


l.;I ~ ...-t.......i..,i,...-,,...,.., ""'" ""'" ,...,. .......-i.......
nme:

lJ)

(/)

Sample Custodian Remarks (Completed By Laboratory):


QA/QC Level

Turnaround

Received oy:"(SlijnatlJre)

I
II
Ill

...

Other

~\c..\~

\5~~~
01~\e,

1::13~~l51::
VI "1 ""''A.,,,,,,,,

~\
~A
Yedbi:(igiliture)
i:

{\

1..-11......-1,..-1,,-1 -'f ........


2. I Y".'I ~ -'"! ....-1 A.......-

~
t).1-lo

,3~,

(to be completed by lab)

(7'>)

l_,IV"'l ....-1.....-1/1......I 3 .tt 1.,-1/I .,i _,.,, .,...,..,,........

.J

tlli

=1l1':fI13
t.7116\IJ

I~./ ltl'. lfl"f,..;1,,

Z..

t...
'Z.

1('(0

titr

:z: . . &~

pl' . . 'ZOt1 -SS

'f' I

10"3 I I

Cab-sample 10

Comments, Special
Instructions, etc.

SamPIGTSample
Tinie
I Matrix

Routine

24Hour [J

0
0

1 Week 0
Other _ _

Sample Receipt
Total # Containers Received?
COC Seals Present?
COC Seals Intact?
Received Containers Intact?
Temperature?

.
EBERLINE
SERVICES

Oak Ridge Laboratory

Internal

Work Order#

13-07149

Chain of

Custody

Lab Deadline

8/13/2013

Comments

Analysis

UUISO - Level 4
Water

Sample Matrix

Sample
Fraction

HP 210 I 270
Detector Activity

04

46

Storage
Location

05
06

Fxns 04, 06, 08, 10, 12 & 14 are TOTAL

47
45
45
43
43
45
45
41
41

Fxns 05, 07, 09, 11, 13 & 15 are DISSOLVED

Wl.1
Wl.1
Wl.1
Wl.1
Wl.1
Wl.1
Wl.1
Wl.1
Wl.1

MUST USE FXN 08 FOR DUP

Date

Location circle one


Rough Prep

Relinquished by

Sample Storage

Received by

Sample Storage

Relinquished by

Sample Storage

Received by

Sample Storage

Relinquished by

Separations

Count Room

Count Room

Rough Prep

Count Room

Rough Prep

Rough Prep

Received by

Prep

Prep

Separations

Count Room

Relinquished by

Sample Storage

Rough Prep

Prep

Separations

Count Room

Received by

Sample Storage

Rough Prep

Prep

Separations

Count Room

Relinquished by

Sample Storage

Rough Prep

Prep

Separations

Count Room

Received by

Sample Storage

Rough Prep

Prep

Separations

Count Room

Relinquished by

Sample Storage

Rough Prep

Prep

Separations

Count Room

Received by

Sample Storage

Rough Prep

Prep

Separations

Count Room

Relinquished by

Sample Storage

Rough Prep

Prep

Separations

Count Room

Printed: 7/23/2013 4:30 PM

fi fj f!ib

.
EBERLINE
SERVICES

Oak Ridge Laboratory

Internal

Work Order#

13-07149

Chain of
Custody

Lab Deadline

8/13/2013

Analysis

ThlSO - Level 4
Water

Sample Matrix

Sample
Fraction

Comments

04......................................... ,
05

06

Fxns 04, 06, 08, 10, 12 & 14 are TOTAL

HP 210 I 270 j
Detector Activity !

Storage
Location

46
46
Wl.1
Wl.1
Wl.1
Wl.1

Fxns 05, 07, 09, 11, 13 & 15 are DISSOLVED

Wl.1

Wl.1
'""""'""""''"'''"''1

Wl.1

MUSTUSEFXNOBFORDUP

Date

Location circle one


Received by

Separations

Relinquished by

Sample Storage

Rough Prep

Received by

Sample Storage

Rough Prep

Relinquished by

Sample Storage

Rough Prep

Count Room

Separations

'''~'"'"
Prep

Received by

Separations
Separations

Relinquished by

~~a~.

Rough Prep

Prep

Separations

Relinquished by

Sample Storage

Rough Prep

Prep

Separations

Count Room

Received by

Sample Storage

Rough Prep

Prep

Separations

Count Room

Relinquished by

Sample Storage

Rough Prep

Prep

Separations

Count Room

Received by

Sample Storage

Rough Prep

Prep

Separations

Count Room

Relinquished by

Sample Storage

Rough Prep

Prep

Separations

Count Room

Received by

Sample Storage

Rough Prep

Prep

Separations

Count Room

Relinquished by

Sample Storage

Rough Prep

Prep

Separations

Count Room

Received by

Printed: 7/23/2013 4:30 PM

:fj fH!i 7

.
EBERLINE
SERVICES

Oak Ridge Laboratory

Internal

Work Order#

13-07149

Chain of
Custody

Lab Deadline

8/13/2013

Analysis

Ra226 - Level 4
Water

Sample Matrix

Sample
Fraction

Comments

HP 210 I 270
Detector Activity

46
46
47
47
45
45
43
43

Fxns 04, 06, 08, 10, 12 & 14 are TOTAL


Fxns 05, 07, 09, 11, 13 & 15 are DISSOLVED

41
41

Storage
Location

Wl.1
Wl.1
Wl.1
Wl.1
Wl.1
Wl.1
Wl.1
Wl.l
Wl.l
Wl.1

MUST USE FXN 08 FOR DUP

Received by

Count Room

Relinquished by

Count Room

Received by

Count Room

Relinquished by

Count Room

Received by

Sample Storage

Rough Prep

Prep

Separations

Relinquished by

Sample Storage

Rough Prep

Prep

Separation

Received by

Sample Storage

Rough Prep

Prep
~>OOe-~~~H'~

-~~

Count Room

"""-'""~---"'"~'"

Relinquished by

Sample Storage

Rough Prep

Prep

Separations

Count Room

Received by

Sample Storage

Rough Prep

Prep

Separations

Count Room

Relinquished by

Sample Storage

Rough Prep

Prep

Separations

Count Room

Received by

Sample Storage

Rough Prep

Prep

Separations

Count Room

Relinquished by

Sample Storage

Rough Prep

Prep

Separations

Count Room

Received by

Sample Storage

Rough Prep

Prep

Separations

Count Room

Relinquished by

Sample Storage

Rough Prep

Prep

Separations

Count Room

Printed: 7/23/2013 4:30 PM

iUJ fj 8

Internal

EBERLINE

Lab Deadline

Chain of
Custody

SERVICES

Oak Ridge Laboratory

13-07149

Work Order#
1

Ra228 - Level 4

Analysis
Sample Matrix

Sample
Fraction

Comments

8/13/2013
Water

HP 210 I 270
Detector Activity

Storage
Location

Initials

Date

Fxns 04, 06, 08, 10, 12 & 14 are TOTAL


Fxns 05, 07, 09, 11, 13 & 15 are DISSOLVED

MUST USE FXN 08 FOR DUP

Location circle one


Received by

Count Room

Separations

Relinquished by

Sample Storage

Rough Prep

Received by

Sample Storage

Rough Prep

Relinquished by

Sample Storage

Rough Prep

Received by

Sample Storage

Rough Prep

{l,,,,,q
Prep
""-'~-'"~'"--"

Separations
"""-~-'"-0''""'"'-

-"-""'""~"""'-" ~~

Relinquished by

Sample Storage

Rough Prep

Prep

Separations

Received by

Sample Storage

Rough Prep

Prep

~~6?__

"""-~"""W'"'-~--""-"'"""W'" '~""

Relinquished by

Sample Storage

Received by

Sample Storage

Relinquished by

Sample Storage

Rough Prep

Prep

~m
Count Room

~ons"'
Separations

Prep

Received by

Rough Prep

Prep

Relinquished by

Rough Prep

Prep

Separations

Count Room

Received by

Sample Storage

Rough Prep

Prep

Separations

Count Room

Relinquished by

Sample Storage

Rough Prep

Prep

Separations

Count Room

Printed: 7/23/2013 4:30 PM

fi Im 9

Page 1of1

Printed: 7/23/2013 4:13 PM

KCOULSTON

~~

PZ-302-AS DIS'

..

2
..

'.

LR-100 TOT I

LR-100 DIS I

08

D-81 TOT

2
<

. ..

09

10

D-81 DIS

PZ-204-SS TOT .

WA

Wl.1

WA

Wl.1

nHOria

PH Flrial

~~

<2

h..

...

47
CPM
37

'...

.Volilm&;tlr
4.0000

4:ocfoo

;~

;;r~

47

0.00

oHFinal

.Volumelkl"

:_.:CPM::.::: ...

f,'',;

Container Number
1

2
container N:::rr

45
: .: CPM
38

-45-
__

.. ....

WA

Wl.1

8.00

oHOria

oHFinal

<2
<2

<2
<2

Volume!U
4.0000
~ .. 4.oooo

Wl.1

0.00

o.H.Orla

..

43
C.PM
43 .......
35

container Number
1

13

LR-103 DIS/

WA

Wl.1

8.00

DHOria

DH.Final

Volume:tb.
4.0000
4.0000

<2 .........
<2
...........<2
--:;:2..

WA

..

Container Number

Wl.1

oHOria .

45

~-~~"~""~;-.-,.-.--

PZ-111-KS TOT

,,

oH Final

45

...

Container Number
1

15

PZ-111-KS DIS /

2
.

..

Container Number
1

Received

"""3"r
WA

by:~~

Date:

7/2..?,/(3

CPMF
45

Volume.Ill :

2
2

34~

0.00

14

"CFIM
45

i.

llHOrla

<2
<2

Wl.1
..

~-- '""~"-~~-m~Frn

8.00

oHFinal:

<2
<2

,,~~,,~~

41

Volume'tLu. .;;:;cPM"" :
4.0000
40
~--"" 4.0000 ....
41
,_rn

WA

Wl.1

0.00

DHOria

oHFirial

VolumelU
- . ...............

...

,_,

.........35

LR-103 TOT,,

'"

... CPM.
43

12

..

43

DH Final -r-::==ell;I.,

'.

"'~~~

0.00
Votlime"1L1 .

ol-tFinal

WA

45

~"~-

Wl.1

3 .....

12.00

> ":CPM,,; ...::


Volume.1u.:
4.0000
38
~~45
"""4:0000""
..
4.0000
39

<2
<2
<2

oHOriii

Container Number".
1

1~

PZ-204-SS DIS/

<2
<2

Container Number

,...

CPM. ...
41

8.00

pHFinal

~~

WA

........ ...

...

-3~7-~.
47

11

oHOria

-
- ......

46

45

Ccmtainer Number
1
2

"

vorumeitt:;l

Wl.1

bHOrig

Container Number
1

07

oHFlnal ...

'.

WA

46

0.00

......

Wl.1

. DH.Orio

Container Number
1

..

CPM~

<2
<2

WA

~-

06

-~~<2

46

8.00

..

DH Final

oH Oria

Container. Number
1

___

41
.
...

CPM
40

.. . . _41""-""

MP-001, Rev 5
Effective: 11/22/02

DUP

'

BLANK

Rec Vol Ttl CPM Max

Storaae
Wl.1
Wl.1
Wl.1
Wl.1

PZ-302-AS TOT

0
0
0

04

Matrix
WA
WA
WA
WA

Comments

# Btls

LCS

ClientID

01
02
03

05

Received By

(Volumes, pH, & CPM)

SERVICES

FR

13-07149

Sample Receiving Report

E:: BE BJ,.... 1 NJ;:

Internal Work Order

SECTION II

SAMPLE ACKNOWLEDGEMENT

Client Name

Contract/PO

~Engineerin~ Management Support, I~~~est Lake ou-~r


r

..

We::o:~:~U-1

Internal ID

Client ID

Wes:;::::U-1j

Project Type

Date Received

environmental

07 /22/2013

-..

28

Sam:Disp

oa11b3i2no13

....

o8/t1"9/2oe13

Sample Date

Matrix

Storage

Required Turnaround Days

13-07149
oa12oi2013

.11: I .J

!='.

01

LCS

07/23/13

WA

Wl.1

02

BLANK

07/23/13

WA

Wl.1

03

DUP

07/23/13

WA

Wl.1

04

PZ-302-ASTOT

07/16/1315:30

WA

Wl.1

05

PZ-302-AS DIS

07/16/1315:30

WA

Wl.1

06

LR-100 TOT

0111111310:23

WA

Wl.1

07

LR-100 DIS

0111111310:23

WA

Wl.1

08

D-81 TOT

07/17/1310:43

WA

Wl.1

09

D-81 DIS

07/17/1310:43

WA

Wl.1

10

PZ-204-SS TOT

01111/1311:40

WA

Wl.1

11

PZ-204-SS DIS

07/17/1311:40

WA

Wl.1

12

LR-103TOT

07/17/1312:15

WA

Wl.1

13

LR-103 DIS

0111111312:15

WA

Wl.1

14

PZ-111-KS TOT

07/17/1313:09

WA

Wl.1

15

PZ-111-KS DIS

01111/1313:09

WA

Wl.1

0
0
0
0
0

Totals Per Analysis (non QA samples)

12

12

12

Invoice

~
,,..

E...... B
E R
...... . . . .

L. I N
E
. . . .
s

E Rv, c Es

Oak Ridge laboratory

601 S~arboro Rd

Oak Ridge, TN 37830

V~ce: ~6~481~683
Fax:
(865) 483-4621

Paul

v.

Rosasco. P.E.

I
f

Report Data

Engineering Management Support, Inc

1220 west Jefferson Aven" s,rte406

7220 West Jefferson Ave. Surte 406

co 80235

303-640-3426

Lakewood,

Voice

'
j

I
I

co 80235

303-940-3426

~~~~~~~~~~~~~~~~F=~~~~~~~~~~~~~~~~~~
Contact

Lyn Fitzgerald

Voice

303-601-4255

Fax

~
~

....

!'-Ji

Paul V. Rosasco. P.E.

Engineering Management Support, Inc

Lakewood,

Voice

Samp~LoglnReport

12

'

Printed:

7/24/2013 1O:13 AM

STANDARD OPERATING PROCEDURE

MP-001, Rev. 12
Effective: 10131112
Page 13of14

Sample Receiving

Eberline Services - Oak Ridge Laboratory


SAMPLE RECEIPT CHECKLIST

13 - Q 7 1 ,4 gMP-001-2
WORK ORDER# _ _ _ _ _ _ _ __
SAMPLE MATRIX/MATRICES:

(CIRCLE ONE OR BOTH)

NON-AQUEOUS

(CIRCLE EITHER YES, NO, OR N/A)


WERE SAMPLES

Present on outside of package?

Unbroken on outside of package?

Present on samples?

C0

Unbroken on samples?

(J

Was chain of custody present upon sample receipt?

Received in good condition?


If aqueous, properly preserved

N/A

WERE CHAIN OF CUSTODY SEALS

IF THE RESPONSE TO ANY OF THE ABOVE IS NO, A DISCREPANT SAMPLE RECEIPT REPORT
(DSR) HAS BEEN ISSUED.
REMARKS:~~~~~~~~~~~~~~~~~~~~~~~~~~~~

DATE:

Copy No. _ _ __

I?..3 /13

Radiochemistry Services

flH\113

SECTION III

CASE NARRATIVE

EBERLINE ANALYTICAL CORPORATION


601 SCARBORO ROAD

EBERLINE

OA~ RIDGE, TENNESSEE 37830

SERVICES

PHONE (865) 481-0683


FAX (865) 483-4621

EBS-OR-36005
August 29, 2013
Paul V. Rosasco, P.E.
Engineering Management Support, Inc.
7220 West Jefferson Ave, Suite 406
Lakewood, CO 80235
CASE NARRATIVE
Work Order# 13-07149-0R
SAMPLE RECEIPT
This work order contains six water samples received 07/22/2013. All samples were analyzed as total and
dissolved for Isotopic Uranium, Isotopic Thorium and Radium-226/228.
CLIENT ID

LAB ID

CLIENT ID

LAB ID

PZ-302-AS TOT
PZ-302-AS DIS
LR-lOOTOT
LR-100 DIS
D-81 TOT
D-81 DIS

13-07149-04
13-07149-05
13-07149-06
13-07149-07
13-07149-08
13-07149-09

PZ-204-SS TOT
PZ-204-SS DIS
LR-103 TOT
LR-103 DIS
PZ-111-KS TOT
PZ-111-KS DIS

13-07149-10
13-07149-11
13-07149-12
13-07149-13
13-07149-14

13-07149-15

ANALYTICAL METHODS

Isotopic Uranium and Isotopic Thorium were analyzed using Method HASL 300, 4.5.2. Radium-226 was

analyzed using Method EPA 903.0. Radium-228 was analyzed using Method EPA 904.0.

Laboratory qualifiers are as follows:

J-

Indicates a situation where the result minus the error is less than the detection limit but greater

than zero.

U-

Indicates a situation where the result minus the error is less than or equal to zero.

ANALYTICAL RESULTS
Combined Standard Uncertainty is reported at 2-sigma value.

Page I of3

8815

ANALYTICAL RESULTS CONTINUED


ISOTOPIC URANIUM
Samples were prepared by removing representative aliquots followed by mixed acid digestions as
appropriate. Uranium was selectively extracted by ion exchange. Uranium was eluted, micro
precipitated and mounted on micro-porous filter media. Sample activities were then determined by alpha
spectroscopy using energy specific regions of interest for Uranium-234, Uranium-235 and Uranium-238.
Chemical recovery was determined by the use of a Uranium-232 tracer. Activity of the Uranium-232
tracer was determined by alpha spectroscopy using an energy specific region of interest.
Samples demonstrated acceptable results for all Uranium analyses. Chemical recovery was slightly low
for sample numbers LR-I 00 TOT and LR-I 00 DIS. Chemical recovery was acceptable for all other
samples. The Uranium-234 method blank demonstrated results slightly greater than the detection limit.
The Uranium-235 and Uranium-238 method blank demonstrated acceptable results. Results for the
Uranium-234 and Uranium-238 duplicate demonstrated an acceptable relative percent difference and
normalized difference. Results for the Uranium-235 duplicate demonstrated a high relative percent
difference; however, normalized difference is within acceptable limits for the analytical technique.
Results for the Uranium-234 and Uranium-238 laboratory control sample demonstrated an acceptable
percent recovery.
ISOTOPIC THORIUM
Samples were prepared by removing representative aliquots followed by mixed acid digestions as
appropriate. Thorium was selectively extracted by ion exchange. Thorium was eluted, micro-precipitated
and mounted on micro-porous filter media. Sample activities were then determined by alpha
spectroscopy using energy specific regions of interest for Thorium-228, Thorium-230 and Thorium-232.
Chemical recovery was determined by the use of a Thorium-229 tracer. Activity of the Thorium-229
tracer was determined by alpha spectroscopy using an energy specific region of interest.
Samples demonstrated acceptable results for all Thorium analyses. Chemical recovery was acceptable for
all samples. The Thorium-228, Thourium-230 and Thorium-232 method blank demonstrated acceptable
results. Results for the Thorium-228 and Thorium-230 duplicate demonstrated a high relative percent
difference; however, normalized difference is within acceptable limits for the analytical technique.
Results for the Thorium-232 duplicate demonstrated an acceptable relative percent difference and
normalized difference. Results for the Thorium-228, Thorium-230 and Thorium-232 laboratory control
sample demonstrated an acceptable percent recovery.
RADIUM-226
Samples were prepared by removing representative aliquots as appropriate. This was followed by
selective sulfate precipitations of the Radium. Samples were then mounted by semi-micro-precipitations
onto micro-porous filters. Samples were counted by alpha spectroscopy using an energy specific region
of interest for Radium-226. Chemical recovery was calculated by the use of a Barium-133 tracer, which
was determined by HPGe gamma spectroscopy.
Samples demonstrated acceptable results for all Radium-226 analyses. Chemical recovery was acceptable
for all samples. The Radium-226 method blank demonstrated acceptable results. Results for the Radium
226 duplicate demonstrated a high relative percent difference; however, normalized difference is within
acceptable limits for the analytical technique. Results for the Radium-226 laboratory control sample
demonstrated an acceptable percent recovery.

Page 2 of3

ANALYTICAL RESULTS CONTINUED


RADIUM-228
Following alpha spectroscopy analysis of Radium-226, Barium/Radium Sulfate precipitates were
redissolved and allowed for sufficient ingrowth of the Actinium-228 daughter. After ingrowth, Actinium
228 was selectively precipitated. Precipitates were filtered and beta emissions for Actinium-228 were
then counted on a gas proportional counter. Chemical recovery was determined by the use of a Barium
133 tracer, the activity of which was determined by HPGe gamma spectroscopy and an elemental Yttrium
carrier by gravimetric measurements. The product of these two recoveries was used to calculate chemical
yield.
Samples demonstrated acceptable results for all Radium-228 analyses. Chemical recovery was acceptable
for all samples. The Radium-228 method blank demonstrated acceptable results. Results for the Radium
228 duplicate demonstrated an acceptable relative percent difference and normalized difference. Results
for the Radium-228 laboratory control sample demonstrated an acceptable percent recovery.
CERTIFICATION OF ACCURACY
I certify that this data report is in compliance with the terms and conditions of the Purchase Order, both
technically and for completeness, for other than the conditions detailed above. Release of the data
contained in this hard copy data package has been authorized by the cognizant project manager or his/her
designee to be accurate as verified by the following signature.

M.R. McDougall
Laboratory Manager
Date: 8/29/2013
Eberline Analytical wants and encourages your feedback regarding our performance providing radioanalytical services. Please
visit http://www.eberlineservices.com/client.htm to provide us with feedback on our services.

Page 3 of3

SECTION IV

ANALYTICAL RESULTS SUMMARY

Paul V. Rosasco, P.E.


Engineering Management Support, lnc.
7220 West Jefferson Ave, Suite 406
Lakewood, CO 80235

Client Sample ID

Lab Sample ID

Analysis Date/Time

LCS13-07149-01
LCS13-07149-01
LCS13-07149-01
LCS13-07149-01
LCS13-07149-01
LCS13-07149-01
LCS13-07149-01
LCS13-07149-01

13-07149-01
13-07149-01
13-07149-01
13-07149-01
13-07149-01
13-07149-01
13-07149-01
13-07149-01

08/07/2013 16:06:13
08/14/2013 07:52:49
08/12/201312:55:09
08/12/201312:55:09
08/12/2013 12:55:09
08/12/2013 05:37:29
08/12/2013 05:37:29
08/12/2013 05:37:29

Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238

E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,

BLANK13-07149-02
BLANK13-07149-02
BLANK13-07149-02
BLANK13-07149-02
BLANK13-07149-02
BLANK13-07149-02
BLANK13-07149-02
BLANK13-07149-02

13-07149-02
13-07149-02
13-07149-02
13-07149-02
13-07149-02
13-07149-02
13-07149-02
13-07149-02

08/07/2013 16:06:14
08/14/2013 07:52:49
08/12/201312:55:04
08/12/201312:55:04
08/12/201312:55:04
08/12/2013 05:37:30
08/12/2013 05:37:30
08/12/2013 05:37:30

Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238

E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,

13-07149-03
13-07149-03
13-07149-03
13-07149-03
13-07149-03
13-07149-03
13-07149-03
13-07149-03

08/07/201316:06:15
08/14/2013 07:52:49
08/12/201312:55:05
08/12/201312:55:05
08/12/201312:55:05
08/12/2013 05:37:32
08/12/2013 05:37:32
08/12/2013 05:37:32

Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238

E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,

13-07149-04
13-07149-04
13-07149-04
13-07149-04
13-07149-04
13-07149-04
13-07149-04
13-07149-04

08/07/201316:06:16
08/14/2013 07:52:50
08/1212013 12:55:06
08/12/201312:55:06
08/12/201312:55:06
08112/2013 09:40:25
08/12/2013 09:40:25
08/1212013 09:40:25

Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238

E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,

D-81 TOT_07_17_2013
D-81TOT_07_17_2013
D-81 TOT_07_17_2013
D-81 TOT_07_17_2013
D-81 TOT_07_17_2013
D-81 TOT_07_17_2013
D-81 TOT_07_17_2013
D-81 TOT_07_17_2013

DUP
DUP
DUP
DUP
DUP
DUP
DUP
DUP

PZ-302-AS TOT_07_16_2013
PZ-302-AS TOT_07_16_2013
PZ-302-AS TOT_07_16_2013
PZ-302-AS TOT_07_16_2013
PZ-302-AS TOT_07_16_2013
PZ-302-AS TOT_07_ 16_2013
PZ-302-AS TOT_07_16_2013
PZ-302-AS TOT_07_16_2013

ta

l<il

!,.,.t,
~~o

Project: West Lake OU-1


SDG: 1307149
Received: 07/22/2013
Matrix: Water

EBERLINE
SERVICES

AnaMe

Final Report of Analysis


Date: 8/29/2013
Page 1 of4

Result

Error

CSU

MDA

4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2

11.53
7.81
4.65
4.95
4.44
7.76
1.19
9.35

1.37
0.86
0.70
0.73
0.67
1.11
0.32
1.30

2.80
1.97
0.82
0.95
0.78
1.24
0.33
1.46

0.16
1.09
0.11
0.09
0.07
0.06
0.09
0.07

4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2

-0.02
0.95
0.06
0.40
0.10
0.23
0.14
0.13

0.09
0.52
0.13
0.24
0.13
0.11
0.10
0.08

0.09
0.56
0.13
0.24
0.13
0.12
0.10
0.08

0.29
0.98
0.24
0.20
0.19
0.08
0.10
0.06

4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2

0.84
0.97
0.04
0.26
0.04
1.88
0.29
1.30

0.39
0.58
0.06
0.12
0.05
0.40
0.15
0.32

0.43
0.62
0.06
0.13
0.05
0.42
0.16
0.33

0.32
1.12
0.08
0.06
0.06
0.06
0.11
0.06

4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2

0.85
1.26
0.17
0.43
0.22
2.35
0.62
1.44

0.40
0.64
0.12
0.19
0.13
0.59
0.29
0.43

0.44
0.70
0.12
0.20
0.14
0.61
0.29
0.44

0.34
1.23
0.11
0.08
0.11
0.12
0.13
0.15

Method

EBERLINE ANALYTICAL CORPORATION


601 SCARBORO ROAD OAK RIDGE, TN 37830

865/481-0683

FAX 865/483-4621

Qualifier

Units
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I

u
J

u
J

u
J
J

u
u

J
J
J

pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCill
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I

Paul V. Rosasco, P.E.


Engineering Management Support, Inc.
7220 West Jefferson Ave, Suite 406
Lakewood, CO 80235

Client Sample ID

PZ-302-AS
PZ-302-AS
PZ-302-AS
PZ-302-AS
PZ-302-AS
PZ-302-AS
PZ-302-AS
PZ-302-AS

~~,

!l'-1iji
t;!ljl

DIS_07_16__2013
DIS_07_16_2013
DIS_07_16_2013
DIS_07_16_2013
DIS_07_16_2013
DIS_07_16_2013
DIS_07_ 16_2013
DIS_07_16_2013

Analvsis Date/Time

AnaMe

Method

13-07149-05
13-07149-05
13-07149-05
13-07149-05
13-07149-05
13-07149-05
13-07149-05
13-07149-05

08/07/2013 16:06:17
08/14/2013 07:52:54
08/12/201312:55:07
08/12/2013 12:55:07
08/12/2013 12:55:07
08/12/2013 05:37:35
08/12/2013 05:37:35
08/12/2013 05:37:35

Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238

E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,

LR-100 TOT_07_17 _2013


LR-100 TOT_07_17_2013
LR-100TOT_07_17_2013
LR-100TOT_07_17_2013
LR-100TOT_07_17 _2013
LR-100TOT_07_17 _2013
LR-100 TOT_07_17_2013
LR-100 TOT_07_17_2013

13-07149-06
13-07149-06
13-07149-06
13-07149-06
13-07149-06
13-07149-06
13-07149-06
13-07149-06

08/07/201316:06:18
08/14/2013 07:52:55
08/12/2013 12:55:08
08/12/201312:55:08
08/12/201312:55:08
08/12/2013 05:37:37
08/12/2013 05:37:37
08/12/2013 05:37:37

Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238

E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,

LR-100
LR-100
LR-100
LR-100
LR-100
LR-100
LR-100
LR-100

13-07149-07
13-07149-07
13-07149-07
13-07149-07
13-07149-07
13-07149-07
13-07149-07
13-07149-07

08/07/201316:06:19
08/14/2013 07:52:55
08/12/2013 12:55:09
08/12/201312:55:09
08/12/2013 12:55:09
08/12/2013 05:37:38
08/12/2013 05:37:38
08/12/2013 05:37:38

Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238

E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,

13-07149-08
13-07149-08
13-07149-08
13-07149-08
13-07149-08
13-07149-08
13-07149-08
13-07149-08

08/07/201316:06:19
08/14/2013 07:52:56
08/12/2013 12:55:35
08/12/2013 12:55:35
08/12/2013 12:55:35
08/12/2013 05:37:40
08/12/2013 05:37:40
08/12/2013 05:37:40

Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238

E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,

D-81
D-81
D-81
D-81
D-81
D-81
D-81
D-81

!iii~

Lab Sample ID

Project: West Lake OU-1


SDG: 1307149
Received: 07/22/2013
Matrix: Water

DIS_07_17_2013
DIS_07_17_2013
DIS_07_17_2013
DIS_07_17_2013
DIS_07_17_2013
DIS_07_17_2013
DIS_07_17_2013
DIS_07_17_2013

TOT_07_17_2013
TOT_07_17_2013
TOT_07_17_2013
TOT_07_17_2013
TOT_07_17_2013
TOT_07_17_2013
TOT_07_17_2013
TOT_07_17_2013

r-J,EBERLINE
Je)

SERVICES

Final Report of Analysis


Date: 8/29/2013
Page 2 of4

Result

Error

CSU

MDA

Qualifier

Units

0.26
0.81
0.04
0.13
0.06
0.54
0.22
0.37

0.27
0.87
0.04
0.13
0.06
0.56
0.22
0.39

0.26
1.57
0.10
0.07
0.06
0.09
0.15
0.12

J
J

4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2

0.34
1.43
0.01
0.26
0.05
2.45
0.46
1.39

pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I

4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2

0.58
-0.17
0.00
0.55
-0.01
0.35
0.00
0.12

0.33
0.60
0.08
0.23
0.04
0.33
0.24
0.20

0.35
0.60
0.08
0.24
0.04
0.33
0.24
0.20

0.31
1.30
0.20
0.11
0.11
0.30
0.53
0.34

4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2

0.36
0.51
0.05
0.41
0.04
0.38
0.31
0.08

0.23
0.65
0.07
0.19
0.05
0.30
0.29
0.15

0.25
0.66
0.07
0.20
0.05
0.30
0.29
0.15

0.18
1.34
0.11
0.11
0.08
0.29
0.27
0.27

4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2

0.30
1.22
0.06
0.37
0.04
1.66
0.73
1.39

0.28
0.63
0.07
0.17
0.06
0.46
0.31
0.42

0.29
0.68
0.07
0.18
0.06
0.48
0.32
0.43

0.39
1.21
0.08
0.10
0.08
0.12
0.13
0.15

EBERLINE ANALYTICAL CORPORATION


601 SCARBORO ROAD OAK RIDGE, TN 37830
865/481-0683

FAX 865/483-4621

u
u
u
J

u
u
J

u
u
J
J

u
J
J

u
u

pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCiil
pCi/I
pCi/I

Paul V. Rosasco, P.E.


Engineering Management Support, Inc.
7220 West Jefferson Ave, Suite 406
Lakewood, CO 80235

Client Sample ID

~ib

Analyte
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238

E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,

PZ-204-SS TOT_07_17_2013
PZ-204-SS TOT_07_17_2013
PZ-204-SS TOT_07_17_2013
PZ-204-SS TOT_07_17_2013
PZ-204-SS TOT_07_17_2013
PZ-204-SS TOT_07_17_2013
PZ-204-SS TOT_07_17_2013
PZ-204-SS TOT_07_17_2013

13-07149-10
13-07149-10
13-07149-10
13-07149-10
13-07149-10
13-07149-10
13-07149-10
13-07149-10

08/07/2013 16:06:45
08/14/2013 07:52:48
08/12/201312:55:37
08/12/201312:55:37
08/12/201312:55:37
08/12/2013 05:37:43
08/12/2013 05:37:43
08/12/2013 05:37:43

Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238

E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,

PZ-204-SS
PZ-204-SS
PZ-204-SS
PZ-204-SS
PZ-204-SS
PZ-204-SS
PZ-204-SS
PZ-204-SS

13-07149-11
13-07149-11
13-07149-11
13-07149-11
13-07149-11
13-07149-11
13-07149-11
13-07149-11

08/07/201316:06:39
08/14/2013 07:52:48
08/12/2013 12:55:38
08/12/201312:55:38
08/12/201312:55:38
08/12/2013 05:37:45
08/12/2013 05:37:45
08/12/2013 05:37:45

Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238

E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,

13-07149-12
13-07149-12
13-07149-12
13-07149-12
13-07149-12
13-07149-12
13-07149-12
13-07149-12

08/07/201316:06:41
08/14/2013 07:52:48
08/12/201312:55:39
08/12/2013 12:55:39
08/12/2013 12:55:39
08/12/2013 05:37:47
08/12/2013 05:37:47
08/12/2013 05:37:47

Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238

E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,

DIS_07_17_2013
DIS_07_17_2013
DIS_07_17_2013
DIS_07_17_2013
DIS_07_17_2013
DIS_07_17_2013
DIS_07_17_2013
DIS_07_17_2013

~,EBERLINE
Jt!J
SERVICES

Final Report of Analysis


Date: 8/29/2013
Page 3 of4

Result

Error

CSU

MDA

4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2

0.84
1.15
0.07
0.30
0.04
2.10
1.28
1.80

0.35
0.59
0.08
0.15
0.05
0.52
0.41
0.47

0.40
0.65
0.08
0.15
0.05
0.54
0.42
0.49

0.21
1.14
0.13
0.12
0.08
0.15
0.16
0.16

4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2

0.88
0.20
0.09
0.29
0.03
2.85
0.44
1.73

0.40
0.80
0.07
0.13
0.05
0.54
0.20
0.39

0.44
0.81
0.07
0.14
0.05
0.58
0.20
0.41

0.26
1.69
0.06
0.08
0.07
0.08
0.12
0.10

4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2

0.58
1.34
0.01
0.55
0.06
2.42
0.28
1.50

0.29
0.76
0.07
0.23
0.08
0.47
0.15
0.35

0.31
0.82
0.07
0.24
0.08
0.50
0.15
0.36

0.15
1.48
0.16
0.13
0.11
0.09
0.11
0.09

4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2

0.71
0.72
0.06
0.52
0.06
0.83
0.53
0.64

0.36
0.76
0.09
0.22
0.07
0.37
0.32
0.32

0.39
0.78
0.09
0.23
0.07
0.37
0.32
0.32

0.29
1.55
0.14
0.10
0.11
0.15
0.19
0.15

Method

08/07/201316:06:44
08/14/2013 07:52:47
08/12/2013 12:55:36
08/12/2013 12:55:36
08/12/2013 12:55:36
08/12/2013 05:37:42
08/12/2013 05:37:42
08/12/2013 05:37:42

DIS_07_17_2013
DIS_07_17_2013
DIS_07_17_2013
DIS_07_17_2013
DIS_07_17_2013
DIS_07_17_2013
DIS_07_17_2013
DIS_07_17_2013

LR-103 TOT_07_17_2013
LR-103 TOT_07_17_2013
LR-103TOT_07_17_2013
LR-103 TOT_07_17_2013
LR-103 TOT_07_17_2013
LR-103 TOT_07_17_2013
LR-103 TOT_07_17_2013
LR-103 TOT_07_17_2013

~~

Analvsis Date/Time

13-07149-09
13-07149-09
13-07149-09
13-07149-09
13-07149-09
13-07149-09
13-07149-09
13-07149-09

D-81
D-81
D-81
D-81
D-81
D-81
D-81
D-81

!ll)I
I\)

Lab Sample ID

Project: West Lake OU-1


SDG: 1307149
Received: 07/22/2013
Matrix: Water

EBERLINE ANALYTICAL CORPORATION


601 SCARBORO ROAD OAK RIDGE, TN 37830
865/481-0683

FAX 865/483-4621

Qualifier

u
u

u
J

u
u

u
u
u

Units
pCill
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I

Project: West Lake OU-1


SDG: 1307149
Received: 07/22/2013
Matrix: Water

Paul V. Rosasco, P.E.


Engineering Management Support, Inc.
7220 West Jefferson Ave, Suite 406
Lakewood, CO 80235

Client Sample ID

~~I

l<i'~
~
r1~1

Lab Sample ID

Analvsis Date/Time

LR-103 DIS_07_17_2013
LR-103 DIS_07_17_2013
LR-103 DIS_07_17_2013
LR-103 DIS_07_17_2013
LR-103 DIS_07_17_2013
LR-103 DIS_07_17_2013
LR-103 DIS_07_17_2013
LR-103DIS_07_17 _2013

13-07149-13
13-07149-13
13-07149-13
13-07149-13
13-07149-13
13-07149-13
13-07149-13
13-07149-13

08/07/2013 16:06:43
08/14/2013 07:53:36
08/12/2013 12:55:40
08/12/201312:55:40
08/12/201312:55:40
08/12/2013 05:37:49
08/12/2013 05:37:49
08/12/2013 05:37:49

Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238

E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,

PZ-111-KS TOT_07_17_2013
PZ-111-KS TOT_07_ 17_2013
PZ-111-KS TOT_07 _17_2013
PZ-111-KS TOT_07_17 _2013
PZ-111-KS TOT_07_17 _2013
PZ-111-KS TOT_07_17_2013
PZ-111-KS TOT_07 _17_2013
PZ-111-KS TOT_07_17_2013

13-07149-14
13-07149-14
13-07149-14
13-07149-14
13-07149-14
13-07149-14
13-07149-14
13-07149-14

08/07/2013 16:06:47
08/14/2013 07:53:43
08/12/201312:55:40
08/12/201312:55:40
08/12/201312:55:40
08/12/2013 05:37:51
08/12/2013 05:37:51
08/12/2013 05:37:51

Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238

E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,

PZ-111-KS
PZ-111-KS
PZ-111-KS
PZ-111-KS
PZ-111-KS
PZ-111-KS
PZ-111-KS
PZ-111-KS

13-07149-15
13-07149-15
13-07149-15
13-07149-15
13-07149-15
13-07149-15
13-07149-15
13-07149-15

08/07/2013 16:06:49
08/14/2013 07:53:43
08/12/201312:55:41
08/12/2013 12:55:41
08/1212013 12:55:41
08/12/2013 05:37:53
08/12/2013 05:37:53
08/12/2013 05:37:53

Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238

E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,

DIS_07_17_2013
DIS_07_ 17_2013
DIS_07_17_2013
DIS_07_17_2013
DIS_07_17_2013
DIS_07_17_2013
DIS_07_17_2013
DIS_07_17_2013

EBERLINE
SERVICES

Analvte

Final Report of Analysis

Date: 8/29/2013
Page 4 of4

Result

Error

CSU

MDA

4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2

1.05
1.99
0.02
0.55
0.09
0.18
0.12
0.14

0.47
0.74
0.06
0.20
0.08
0.14
0.13
0.12

0.52
0.87
0.06
0.22
0.08
0.14
0.13
0.12

0.35
1.37
0.13
0.11
0.10
0.12
0.18
0.11

4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2

0.21
0.52
0.02
0.42
-0.02
7.02
0.82
2.41

0.19
0.63
0.06
0.17
0.03
1.15
0.29
0.52

0.20
0.64
0.06
0.18
0.03
1.25
0.30
0.55

0.25
1.28
0.13
0.07
0.10
0.08
0.10
0.11

4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2

0.37
0.57
0.00
0.49
0.00
8.15
0.99
3.47

0.23
0.57
0.04
0.20
0.03
1.50
0.38
0.78

0.24
0.58
0.04
0.21
0.03
1.60
0.39
0.82

0.19
1.15
0.11
0.09
0.10
0.11
0.19
0.12

Method

EBERLINE ANALYTICAL CORPORATION


601 SCARBORO ROAD OAK RIDGE, TN 37830

865/481-0683

FAX 865/483-4621

Qualifier

u
J
J

u
J
J

u
u
u

u
u
u

Units

pCi/l
pCi/l
pCi/l
pCi/l
pCi/l
pCi/I
pCi/l
pCi/l
pCi/l
pCi/l
pCi/l
pCi/l
pCi/l
pCi/l
pCi/l
pCi/l
pCi/l
pCi/l
pCi/l
pCi/l
pCi/l
pCi/I
pCi/l
pCi/I

SECTIONV

ANALYTICAL STANDARDS

QA/QC REVIEWED CERTIFICATE OF CALIBRATION

'1q(l11itialsA ALPHA STANDARD SOLUTION



Date
Radionuclide:
Half Life:
(4.468
Catalog No.:
Source No.:

TMA EBERLINE
Customer:
OR2778
P.O.No.:
Reference Date:
January 11995
12:00 PST.
Contained Radioactivity: (Total U) 8.016 .Ci
Contained Radioactivity: (Total U) 297 k.Bq

U-238NAT
0.005) x 10"9 years
7338
479-50

Description of Solution
a. Mass of solution:
b. Chemical form:
c. Carrier content:
d. Density:

65. 2896 g in a 50 ml flame sealed ampoule


Uranyl Nitrate in H20
None
Approximately 1.3202

Radioimpurities

...

,,

'

g/ml@20C.

,::;.'

Refer to attached technical data sheet

:~

Radioactive Daughters
-:~

Refer to attached technical data sheet

..

Radionuclide Concentration
(Total U) 0.1228

p.Ci/g.

Method of Calibration

: :,
'

Activity calculations are based upon known specific activity and mass.
......... ,:;

. ~..

Uncertainty of Measurement
a. Systematic uncertainty in instrument calibration:
b. Random uncertainty in assay:
c. Random uncertainty in weighing(s):
d. Total uncertainty at the 99 % confidence level:

3.0%
0.0%
2.0%
3.6%

NIST Traceability
This calibration is implicitly traceable to the National Institute of Standards and Technology.
Leak Test(s)
See reverse side for Leak Test(s) applied to this source.
Notes

..

..

.~

'

. '.

.' .....

1. Nuclear data were taken from "Table of Radioactive Isotopes", edited by Virginia S. Shirley, 1986.
2. IPL participates in an NIST measurement assurance program to .:~tablish and maintain implicit traceability for a riumber of maclides,
based on the blind assay (and later NIST certification) of Standard Reference Materials (As in NRC Regulatory Guide 4.15).

EEftfvAu.AS.

,,.

YCONTROL

I F

~~M~f~
Date Signed

~..\

ISOTOPE
PRODUCTS
LABORATORIES

ISOTOPE PRODUCTS LABORATORIES

\.:

3017 N. SAN FERNANDO BLVD.


BURBANK, CALIFORNIA 91504
8188437000

FAX

1.:-:

... , , '

8188436168
:.
:;,

.::

.'

..

"'"

-:~

.,. ~

:. ' ..

- ... ,,

, ... ..

,. ,.,-., .

.... ,,,,;

: .:..;. ,;

....

:,."'

... "~'

..

~:

"{'.!~

":

. l,1<

;9~12i

QUALITY CONTROL PROGRAM


MP-009

Rev.a: 11101103
Title: Radioactive Reference Standards Solutions & Records

EBERLINE SERVICES OAK RIDGE LABORATORY

RADIOACTIVE REFERENCE SOLUTIONS

PRIMARY DILUTION RECERTIFICATION


MP009

Half Life, Days

Half Life, Years

I ..

I :4.4s8e+ogl

Reference Date!

1.632E+12I

?;1)1/199.5 O:ooj

Ampoule /Solution Gross ' . 97i6400 Weight, Grams


. 32:5020 Weight, Grams
Empty Ampoule
65.1380 Weight, Grams
Solutlon Net
8.0160 Cl
Total Activity In Ampoule

Dilution Instructions:

Dilution Solvent Used

Dilute to a volume ofl . 1000:00 .

Certified Total Activity ofl

. 8;0160lCI

Imilliliters

Which Eauals

1.780E+07jdpm at the date listed above

This activity concentration Is based on the original


And after dilution the activity of this solution is 1.77955E+04Idpm/ml-eterence date listed above. All actl'vlties are corrected
to the date and time of analysis by the laboratory data

processing software.

Expiration Date:! September6, 2013

Date:

------9/26/2012 0:00

Date: _ _1-+/_u__,./_1"2__

~ E: B EF<l!;.t~o~ I QUALITY C~:!!,RQL PROGRAM


Rev.8; 11101/03
Title: Radioactive Reference Standards Solutions & Records

EBERLINE SERVICES - OAK RIDGE LABORATORY


RADIOACTIVE REFERENCE STANDARD SOLUTIONS
SECONDARY DILUTION RECERTIFICATION
MP-009
Solution Reference# IPL47g.,.50 .
Half Life, Years

I '"f4sae+o9 I

Radionuclide of lnteresj: 2~?ii!l:2#u<j


Parent Solution Cone. 1:TZ96E+04 dpm/ml

Dilution Instructions:

Reference Date I... '1/1/19950:00l

l1MHNOJ> ..

Dilution Solvent Used


SECONDARY VOLUMETRIC DILUTION

Vol. Parent Solution:


Total Activity:
Final Volume:

< : 4:0000 ml
7 .1182E+04 dpm
. . 1OOO;OO ml

7.1182E+01ldpm/ml

Final Activity Concentration:!

This activity concentration is based on the original


reference date listed above. All activities are
NOTES:
corrected to the date and time of analysis by the
..,_..,......,-=...,...,,.-.,,...----------------UIU.L<EUJtory data processing software.
Isotopic Distribution as:

U-238 Atom % = 48.239 U-238 = 71.182 dpmlml X 0.48249 34.345 dpm/ml

U-235 Atom % 2.25


U-235 = 71.182 dpm/ml X 0.0225'" 1.602 dpm/ml

U-234 Atom % = 49.501 lJ..238 =71.182 dpm/ml X 0.49501 = 35.236 dpm/ml

All values +/- 3.6%

Expiration Date:I September 6, 2013

Isotopic ratios from manufacturer's data sheet

Date:

9126/2012 0:00
-------

q....{"'"z.f#....,/....,r-=-z-_

Date: _ _

.RECORD COPY

Tracer Solution for EnvirQnmental Analysis & Disequililirium Studies

(!

Product Description & Measurement Certificate


Description

Principal radionuclide:
Daughter Nuclide:

Measurement

Reference date:
Radioactive concentration U-232
which is equivalent to

uranium 232 (U-232)


Th-228

Volume ofsolution
Total activity ofU-232
which is equivalent to

01 March 2000
6.739E+03 becquerels per gram ofsolution
1.821E-01 microcuries per gram ofsolution
5.35 gru.-;~
5.035 millilitres
3.61E+04 becquerels
9.76E-01 microcuries

Method ofmeasurement (see reverse ofthis certificate)

Random uncertainty is: 0.7%


Systematic uncertainty: 0.5%

Overall uncertainty in the radioactive c0ncentration quoted above: 1.7%

Overall uncertainty is defmed on the reverse of this certificate.

Accuracy

Radionuclidic
Purity

Product code: UDP10050


Batch Number: 921232/67

Any radioactive impurities measured are listed below, expressed as percentages

of the activity ofthe principle radionuclide at the reference date .

Th-228 and daughter activity removed 2 Feb 2000

U-232 daughters activity will increase with time. By alpha 88% U-232, 12% daughters on 1/3/00

Isotopic
Purity

...-ne isotopic composition, exprP.ssed as atom per cent at the reference date .

i'-fot measured

Chemical
Composition

Calculated weight ofU-232, 4.42E-08 grams, as 2M HN03 solution in a flame sealed glass vial.

This Tracer solution has been produced 'carrier free'.

Physical
Data

Recommended halflife of uranium 232: 6.980E+Ol years

Principle energies of alpha emissions (MeV): 5.263 31.7%, 5.320 68.00/o

Branching ratio for alpha emission: I 00%

Calculated specific activity of uranium 232: 8.167E+05 Bq per microgram U-232.

Remarks

For safety information and notes to ensure correct usage by all persons handling this radio~ive Tracer

solution please read the instructions accompanying the package.

AEA Technology operates a quality management system which has been independently audited and

approved to ISO 9001.

Approved
Signatory

Project Ref. AE231S

Roger Wiltshire
Prepared and characterised .in the UK, for world wide distnbution by lsotrak, AEA Technology, QSA.

Trkcert.wps 10/03/00

AEA Technr>logy is the trading name of AEA Technology pie tJ !

27

QUALITY CONTROL PROGRAM


MP..009

Rev.8; 11/01/03
Title: Radioactive Reference Standards Solutions & Records

EBERLINE SERVICES OAK RIDGE LABORATORY


RADIOACTIVE REFERENCE SOLUTIONS
PRIMARYD~UTIONRECERTIRCATION

MP009

Half Life, Years

I. . .

I < 1.2o()l:+otl
0

ee!"~ :~~1 <~.:E~11CI


. . . . . . . .

Certified Concentration

Reference Date!

2.630E+04I
>31112000 O:OOI

Cl per gram

Ampoule /Solution Gross~


. . . ... Weight, Grams
Empty Ampoule . .. .. . Weight, Grams
Solution Net . . . . Weight, Grams
Total Activity in Ampoule
0.9760 Cl
Chemical Composition of Standard Solution

2
in .2M
HNO .<

. 3\i(NO)
... ...3 6 ...
.. .......3.
1

: .

.,

Dilution Instructions:

Dilution Solvent Used

Dilute to a volume ofl 1000.00


Certified Total Activity of

0.9760JCI

Imilliliters

Which Eauals

I . 2.167E+06ldpm at the date listed above

And after dilution the activity of this solution Is 1 2.167E+03ldpm/ml

This activity concentration is based on the original


reference date listed above. All activities are corrected
to the date and time of analysis by the laboratory data
processing software.

Expiration Date:

Date:
Date:

I December 7, 2013 I

1211312012 0:00

1f'3/r.J
/

Rev.6; 11/01/03

Title:

Radioactive Reference Standards Solutions & Records

EBERLINE SERVICES - OAK RIDGE LABORATORY


RADIOACTIVE REFERENCE STANDARD SOLUTIONS
SECONDARY DILUTION RECERTIFICATION

MP-009

Solution Reference # AEA/Amersham 92/232167

Half Life, Years

1.200E+o1

Radionuclide of lnteresj *32u . 1


Parent Solution Cone._ 2.167E+o3 .. dprnlml

Reference Datel' .

311120000:00l

Chemical Composition of Standard Solution

l232:.U(NQ)e..
o:
.... ..
. ..
m2MHN.
. 3. ..
. . .
~

>

.: .

:< ..

.........
.
. .

Dilution Instructions:

Dilution Solvent Used

SECONDARY VOLUMETRIC DILUTION


Vol. Parent Solution: .. .. 10.0000 ml
Total Activity: 2.1670E+04 dpm
Final Volume:
1000.00 ml

NOTES:

Final Activity Concentration:!

. 2.1670E+01 ldprnlml

This activity concentration is based on the original


reference date listed above. All activities are
corrected to the date and time of analysis by the
laboratory data processing software.

Expiration Date:I December 7, 2013

Date: _ _.....1...,2/_13_12_0._1....
2_0_:00_
Date: __1
...1.,.._~..,..b.,..;2.........__ _

29

RID1CATE OF ALIBRATI .I~ fl1,


LPHA STANDARD SOLUTIO
uci \~tt\\~0
Radionuclide
Th-230
Half Life:
(7.54 0.03) x 104 years
Catalog No.:
7230
Source No.:
388-116
Description of Solution
a. Mass of solution:
b. Chemical form:
c. Carrier content:
d. Density:

~
~\\\'' \.~
\)\\l

Customer:
TMA
P.O.No.:
TT4944
Reference Date:
November 1 1991
Contained Radioactivity:
1.036
5.0042
Th(N03)4 in O.IN HN03
None added
1.0016

..

12:00 PST.

"Ci.
grams.

gram/ml @ 20C.

Radioimpurities

See attached technical data sheet


Radioactive Daughters
See attached technical data sheet

Radionuclide Concentration
0.'1D1

Method of Calibration

Weighed aliquots of the solution were assayed using a liquid scintillation counter.

Uncertainty of Measurement
a. Systematic uncertainty in instrument calibration:
b. Random uncertainty in iway:
c. Random uncertainty in weighing(s):
d. Total uncertainty at the 99% confidence level:

2.0%
0.5%
0.2%
2.7%

NIST Traceability
This calibration is implicitly traceable to the National Institute of Standards and Technology.
Notes
1. Nuclear data were taken from "Table of Isotopes", Seventh Edition, edited by Virginia S. Shirley.
2. IPL participates in an NIST measurement assurance program to establish and maintain implicit
traceability for a number of nuclides, based on the blind assay(and later NIST certification) of
Standard Reference Materials. (As in NRC Regulatory- Guide 4.15)

ISOTOPE PRODUCTS LABORATORIES


1800 No. Keyst.one Street.,
Burbank, California 91504
818 843 - 7000

Ell E RLI

hl~ I QUALITY CONTROL


PROGRAM
MP-009

S&AVICl!S

Rev.8; 11/01/03
Title: Radioactive Reference Standards Solutions & Records

EBERLINE SERVICES - OAK RIDGE LABORATORY

RADIOACTIVE REFERENCE STANDARD SOLUTIONS

SECONDARYD~UTIONRECERTIFICATION

Date
3/4/2013 0:00
Solution#, . 'Th~1b>>
Half Life, Days

MP-009
Solution Reference# IPL 388"116 >:
Half Life, Years

l:v;54oe+041

Radionuclide of lnteres ~,fl1ofium


Parent Solution Cone. >' 2,30E+03

> dpm/ml

Dilution Instructions:

Reference Date

I<> 11/1/19Qf;b':OOI

Dilution Solvent Used

SECONDARY VOLUMETRIC DILUTION


Vol. Parent Solution: \ ' r 10.0000 ml
Total Activity: 2.2999E+04 dpm
Final Volume: .fOOO~OO ml

Final Activity Concentration:!

2.2999E+01 ldpm/ml

This activity concentration is based on the original


reference date listed above. All activities are
corrected to the date and time of analysis by the
laboratory data processing software.

NOTES:

Expiration Date:I

Recertified

Date:

Verified & Approved By

Date:

QC Approval

Date:

March 4, 2014

3121/2013 0:00

j~l'~
~1\{1'

31

QUALITY CONTROL PROGRAM


MP-009

Rev.8; 11/01/03

Radioactive Reference Standards Solutions & Records

Title:

EBERLINE SERVICES - OAK RIDGE LABORATORY


RADIOACTIVE REFERENCE SOLUTIONS
PRIMARY DILUTION RECERTIFICATION
MP009
SOLUTION REFERENCE #""'IP""'t..,..,:3.....8""'"'&;..,..11""'6.,_:......: .. ..Princi al Radionuclide
Half Life, Years

j.: 7l546E+o41

h<<

CURRENT DATE
3/4/2013 0:00
.........._,..,.,
SOLUTION# .. ' _,;.>Th.::t,::.: ;
Half Life, Days.
2.754E+07l

Radionuclide
.. tiorium<
Certified Activity \:f:.036Et0:0 Ci
Certified Concentration
Ci per gram

Reference Date, ..

"::111111991 o:od I

Ampoule /Solution Gross .. <9;2660 Weight, Grams


Empty Ampoule 1 . / 4'.6218 Weight, Grams
4.6442 Weight, Grams
Solution Net
1.0360 Cl
Total Activity in Ampoule
Chemical Composition of Standard Solution

Dilution Instructions:

Dilution Solvent Used

Dilute to a volume ofl

Certified Total Activity ofl

1.0360lCi

toomoo>

!milliliters

Which Eauals

2.300E+06ldpm atthe date listed above

And after dilution the activity of this solution Is 2.300E+03ldpm/ml

This actlvity concentration is based on the original


reference date listed above. All activities are corrected
to the date and time of analysis by the laboratory data
processing software.

Expiration Date:

Date:
Date:

March 4, 2014

3/21/2013 0:00

sj'M/r :::s

1h-B

CERTIFICATE OF CALIBRATION

ALPHA STANDARD SOLUTION

TMA EBERLINE
Customer:
VH1632
P.O.No.:
Reference Date:
November 11993
12:00 PST.
Ci.
Contained Radioactivity:
(Th-232) 0.0933
Contained Radioactivity:
(Th-232)
3.45
kBq.

Radionuclide:
Th-232
Half Life:
(1.405 0.006) x lOA 10 years
Catalog No.:
7232
Source No.:

435-104-2

Description of Solution
a. Mass of solution:

b. Chemical form:
c. Carrier content:
d. Density:

11.9712 g (iri a 10 ml flame sealed amP,oule)


Th(N03)4 iri water
None added
Approx. 1.21

g/ml@20C.

None detected (other than daughters).

Raciioimpurities

Radioactive Daughters
.
Ra-228, Ac-228, Th-228, Ra-224, Rn-220, Po-216, Pb-212, Bi-212,_Po-212, TI-208
Radionuclide Concentration
(Th-232) 0.00779

l'Cilg.

Method of Calibration
Activity calculations are based upon known specific activity and mass.

Uncertainty of Measurement
a. Systematic uncertairity in instrument calibration:
b. Random uncertainty in assay:

c. Random uncertainty iri weighing(s):.


d. Total uncertainty at the 99% confidence level:

3.0%
0.0%
2.0%
3.6%

NIST Traceability
This calibration is implicitly traceable to the National Institute of Standards and Technology.
Leak Test(s)
See reverse side for Leak Test(s) applied to this source.
Notes
1. Nuclear data.\\'ere taken from "'I'.able of Radioactive Isotopes", edited by Virginia S. Shirley,.l986.
2. IPL partici~tes in an NIST measurement assurance program to establish and maintain implicit traceability for a number of nuclid~s.
ba5Cd on the blind assay (and later NIST certification) of Standard Reference Materials (As in NRC Regulatory Guide 4.15).

QUALITY CONTROL

Date Signed
ISOTOPE PRODUCTS LABORATORIES
1800 North Keystone Street
Burbank, California 91504
818 843 - 7000

1'1-B

CERTIFICATE OF CALIBRATION

ALPHA STANDARD SOLUTION

Customer:

Radionuclide:
Th-232
Half Life:
. (1.~0S 0.006) x lOA 10 years
Catalog No.:

7232

Source No.:

435-104-2

Description of Solution
a. Mass of solution:
b. Chemical form:
c. Carrier content:
d. Density:

TMA EBERLINE

VH1632

P.O.No.:
Reference Date:
November 11993.
12:00PST.

Contained Radioactivity:
(Th-232) 0.0933
Ci.

Contained Radioactivity:
(Th-232)
3.45
kBq.
11.9712 g (in a 10 ml flame sealed ampoule)
Th(N03)4 in water
None added
Approx. 1.21

81m1@20c.

None detected (other than daughters).

Radioimpurities

Radioactive Daughters
Ra-228, Ac-228, Th-228, Ra-224, Rn-220, Po-216, Pb-212, Bi-212,Pp-212, Tl-208
Radionuclide Concentration
(Th-232) 0.00779

.CUg.

Method of Calibration
Activity calculations are based upon known specific activity and mass.

Uncertainty of Measurement
a. Systematic uncertainty in instrument calibration:

3.0%

b. Random uncertainty in assay:


c. Random uncertainty in weighing(s):

0.0%

d. Total uncertainty at the 99 % confidence level:

3.6%

2.0%

NIST Traceability
This calibration is implicitly traceable to the National Institute of Standards and Technology.
Leak Test(s)
See reverse side for Leak Test(s) applied to this source.
Notes
1. Nuclear data \Vere taken from ralile of Radioactive Isotopes"; edited by Virgiiiia S. Shirley, l986.
2. IPL particip~tes an NIST measurement assurance program to establish and maintain implicit traceability for a number of nucli~,
based on the blind assay (and later NIST certification) of Standard Reference Materials (As in NRC Regulatory Guide 4.15).

in

QUALITY CONTROL

Date Signed
ISOTOPE PRODUCTS LABORATORIES
1800 North Keystone Street
Burbank, California 91504
818 843 - 7000

QUALITY CONTROL PROGRAM


MP.009

Rev.8; 1/10103
Radioactive Reference Standards Solutions & Records

Title:

EBERLINE SERVICES - OAK RIDGE LABORATORY

RADIOACTIVE REFERENCE SOLUTIONS

PRIMARYD~UTIONRECERTIRCATION

MP009

Half Life, Years

F;'d/d'i4o5E:t101

Ampoule /Solution Gross :('~:;1;8i64.'.h5. Weight, Grams


Empty Ampoule :;':}':S:92$6 Weight, Grams
Solution Net }1,9t19 Weight, Grams
Total Activity in Ampoule
<0.0933 Ci
Chemical Composition of Standard Solution

Dilution Instructions:

Diiution Solvent Used

Diiute to a volume ofj,y:'.'1000:00:/ Jmllllllters

Certified Total Activity ofl

< '. ' o,0933lCi

Which Eauals

I>

<>2,071E+osldpm at the date listed above

And after dilution the activity of thi$ solution isl 2;071E+Q2ld.pm/ml

::~:;,,_:::==e~s:.~===~~ri!~
to the date and time of analysis by the laboratory data
processing software.

Expiration Date:I :

Date:

OCtOber 9,:201:r

__

10/9/2012 0:00

..;...;..;..;;.;..;;;.;;~~-

Rev.8; 1/10/03
Title: Radioactive Reference Standards Solutions & Records

EBERLINE SERVICES - OAK RIDGE LABORATORY

RADIOACTIVE REFERENCE STANDARD SOLUTIONS

SECONDARY DILUTION RECERTIFICATION


MP-009

Solution Reference# IPL 436~104.-2


Half Life, Years

I +.4o5E;.;1ol

Reference Dater'

Chemical Composition of Standard Solution

ITh(N03)4 in .1 % HN03 ....

Dilution Instructions:

. .

1111/1993 '0:00 I

I
I1% NitricAcid<

Dilution Solvent Used

SECONDARY VOLUMETRIC DILUTION


Vol. Parent Solution:
Total Activity:
Final Volume:

NOTES:

. 500;0000. ml
1.0356E+06 dpm
1000.00 ml

Final Activity Concentration:!

1.0356E+02 ldpm/ml

This activity concentration is based on the original


reference date listed above. All activities are
corrected to the date and time of analysis by the
laboratory data processing software.

Expiration

Date:I. October9, 2013

Date:

11/9/2012 0:00
------

Isotope Products

Laboratories

lli-18

24937 Avenue Tibbitts


Valencia, California 91355
Tel 6613091010

An Eckert &Ziegler Company

Fax 6612578303

CERTIFICATE OF CALIBRATION

ALPHA STANDARD SOLUTION

Th-229
7340 160 years
7229
867-54

Radionuclide:
Half-life:
Catalog No.:
Source No.:

Physical Description:
A. Mass of solution:
B. Chemical form:
C. Carrier content:
D. Density:

EBERLINE SERVICES
00009633
15-Jan-02 12:00 PST
1.013
Ci
37.48

Customer:
P.O. No.:
Reference Date:
Contained Radioactivity:
(Th-229 only)

kBq

5.0147 gin 5 ml flame-sealed ampoule


Th(N0 3) 4 in 0.1 M HN03
10g Th/ml
1.0016 g/ml@ 20c.

Radioimpurities:
None detected (daughters in equilibrium)

Radionuclide Concentration:

0.2020 Ci/g,

kBq/g

7.474

Method of Calibration:
This source was prepared from a weighed aliquot of solution whose activity in Ci/g was determined
using gamma ray spectrometry.

Peak energy used for integration:


193.5 keV
Branching ratio used:
0.0441 gammas per decay

Uncertainty of Measurement:
A. Type A (random) uncertainty:
B. Type B (systematic) uncertainty:
C. Uncertainty in aliquot weighing:
D. Total uncertainty at the 99% confidence level:

0.7
3.0
0.0
3.1

%
%
%
%

Notes:
- See reverse side for leak test(s) performed on this source.
- IPL participates in a NIST measurement assurance program to establish and maintain implicit traceability
for a number of nuclides, based on the blind assay (and later NIST certification} of Standard Reference
Materials (As in NRC Regulatory Guide 4.15}.
- Nuclear data was taken from IAEA Technical Report Series No. 261.
~ This solution has a working life of 5 years.

1- J(J,ri-02
Quality'Control

Date Signed

IPL Ref. No.:

867-54

- - - - - - - - - - - - - - - - - 1509001 CERTIFIED - - - - - - - - - - - - - - - -

Medical Imaging Laboratory


24937 Avenue Tibbitts

Valencia, California 91355

Industrial Gauging Laboratory


1800 North Keystone Street

Burbank, California 91504

QUALITY CONTROL PROGRAM


MP-009
Rev.8; 1/10103
Title: Radioactive Reference Standards Solutions & Records

EBERLINE SERVICES - OAK RIDGE LABORATORY


RADIOACTIVE REFERENCE SOLUTIONS
PRIMARY DILUTION RECERTIFICATION
MP009
CURRENTOATE......,._,....,.,-1~1=/9~~=01_2_0~:0-"10

SOLUTION REFERENCE #,...IP_L_8_67_:;.s4-----......-.


__

SOLUTION#

Half Life, Days

Half Life, Years

Th.;;18 , .

1.340!:+031

c..:=. ::1>1.=~1CI
0

2.ss1 E+osl

Reference Date! : 1f15/200.2'0:00!

Certified Concentration . . >>.. . . . . .Ci per gram


Ampoule /Solution Gross
Empty Ampoule
Solution Net
Total Activity In Ampoule

..

s.ns2 Weight, Grams


.'.'3.7591 Weight, Grams

5.0161 Weight, Grams


1.0130 Cl

Chemical Composition of Standard Solution

. - 1
..

Dilution Instructions:

Dilution Solvent Used

Dilute to a volume oft . 1000.00 . lmillillters

Certified Total Activity of

I -.1.0130lCi

Which Eauals 1

2;249E+06ldpm at the date listed above

And after dilution the activity of this solution is 12.249E+03ldpm/ml

This activity concentration Is based on the original


reference date listed above. All activities are corrected
to the date and time of analysis by the laboratory data
processing software.

Expiration Date:I

Date:
Date:

October 9, 2013 ]

11/9/2012 0:00
-------

,,/rz/,z_
_...,,,..,
_,,..,...,---

Rev.7; 9129199

Tiiie: Radioactive Reference Standards Solutions & RecOrds

EBERLINE SERVICES OAK RIDGE LABORATORY

RADIOACTIVE REFERENCE STANDARD SOLUTIONS

SECONDARY DILUTION RECERTIFICATION


Date
Solution#

MP-009
Solution Reference# IPL867~4
I Radionuclide
Half Life, Years

Princi
2.? 9Th .

I. . 7.34oE+o3 I

I
Reference Date

Chemical Composition of Standard Solution


jTH{N03)4in0.1MHN0:f
.. .. ... ..> . . > .

Dilution Instructions:

11/912012 0:00
Th.. 1aa

2~ss1e+osl
1/fS/2002 o:oo

I
... .... 'I
... . . 3.

l-o..1.MHNo.......

Dilution Solvent Used


SECONDARY VOLUMETRIC DILUTION

Vol. Parent Solution:


Total Activity:
Final Volume:

NOTES:

10.0000 ml
2.2490E+04 dpm
1000.00 ml

Flnal Activity Concentration:!

2.2490E+01 Jdpm/ml

This activity concentration Is based on the original


reference date listed above. All activities are
corrected to the date and time of analysis by the
laboratory data processing software.

Expiration Date:I

Date:

October 9, 2013

-----------

0 ate: _

11/9/2012 0:00

1z....J&..c......
z... __

__..11/
........

Jllattonal 3lnstitute of

~tanbarbs

& ~ecbno logp

<terttftcate''
Standard Reference Material 4251,C .,
.:Barium-13~ Radioactivity .Standard . ,
This Standard Reference Material (SRM) copsists of radioactive barium-133. chloride, non-radioactive barium
chloride, and hydrochloric acid diSsolved in 5 rnL of distilled water. The solution is.contained in a flame
sealed NIST borosilicate-glass ampoule. The SRM is intended for the calibration of ionization chambers and
solid-state gamma-ray.:spectrometry .sy~tems.
Radiological Hazard
The SRM ~mpoule contains bariuni-133 with 3 total activity of approximately 2.5 MBq. Barium-133 decays
by electron capture and during ttie decay process X-rays, and g~a:rays with energies from 4 ~o 400 keV are
emitted. Most of these photons escape from the SRM ampoule and can represent a radiation hazard.
Approximate unshielded dose rates at several distances (as of the reference time) are given in note [a]*.
Appropriate shielding and/or distance should be used to minimize personnel exposure. '-The SRM should be
used only by persons qualified to handle
,
.
'.
.. radioactive. material.
.
Chemical Hazard
The SRM ampoule contains hydrochloric acid (HCI) with l'!- concentration of l mole per liter of .water. The
solution is corrosive and represents a health hazard if it comes in contact With.eyes or skin~. If the ampoule
is to be opened to transfer the solution, the recommended procedure is given on page 2. The ampoule should
be opened cmly by persons qualified to handle both radioactive material and strong acid solution.
Storage and Handling

.7

;.

The SRM should be stored and used at a temperature between 5 and 65 C. The solution in an unopened
ampoule should remain stable and homogeneous until at least June 2004.
The ampoule (or any subsequent container) should always be clearly marked as containing radioactive

material. If the ampoule is transported it should be packed, marked, labeled, and shipped in accordance with
the applicable national, international, and carrier regulations. The solution in the ampoule is a dangerous
good (hazardous material) both because of the radioactivity and because of the strong acid.

,i ..
!.

Preparation
This Standard Reference Material was prepared in the Physics Laboratory, Ionizing Radiation Division,
Radioactivity Group, J.M.R. Hutchinson, Group Leader. The overall technical direction and physical
measurements leading to certification were provided by L.L. Lucas of the Radioactivity Group and D.B. Golas,
Nuclear Energy Institute Research Associate.

i.

The support aspects involved in the preparation, certification, and issuance of this SRM were coordinated
through the Standar~ Reference Materials Program by N.M. Trahey.

II

f.

i .
Gaithersburg, Maryland 20899
October 1994

Thomas E. Gills, Chief


Standard Reference Materials Program

I
;

SRM 42SlC,,p~geJ

of 6

*Notes and references. are. on pages~ and 6.

.\
I

QUALITY CONTROL PROGRAM


QCP-009

Rev.8; 11/10/03

Title: Radioactive Reference Standards Solutions & Records

EBERLINE SERVICES - OAK RIDGE LABORATORY


RADIOACTIVE REFERENCE SOLUTIONS
PRIMARY DILUTION RECERTIFICATION
QCP 009-1

CURRENT DATE >


6116/2013 0:00
SOLUTION REFERENCE# NISTSSRM4.251C;?'; ;Ji/:<?.
SOLUTION# C//;,:"\':;;ea;e/_:\'Y<:
Princl al Radionuclide
Half Life, Days
Half Life, Years
< 1 ~aaHu.m:_
1:vr:::1:.045i::+o1I
1- >\.C:3;a28E:+03I
..,.,.,.,,~,.,,,..,....-.~,.,.,,,.......,...,...,.,.,.,...,...

Radionuclide
Certified ActivityH7~~~CI
Certified Concentration }1:'318Et0} Ci per gram

Reference Datef<'./j

}~91.111$aao:otl'!

Ampoule /Solution Gross \: ><$:30$1 Weight, Grams


Empty Ampoule ./?')}4f2582 Weight, Grams
Solution Net - <:5;0499 Weight, Grams
Total Activity in Ampoule
66~5577 Cl
Chemical Composition of Standard Solution

Dilution Instructions:

Diiution Solvent Used

Dilute to a volume otl':,:/tooo;oo:: 'lmllliliters

Certified Total Activity ofl

>

66:5577lCi

Which Eauals

I->

:1A78E+08ldpm at the date listed above

And after dilution the activity of this solution is I1478E+05 Idpm/ml

This activity concentration is based on the original


reference date listed above. All activities are corrected

to the date and time of analysis by the laboratory data


processing software.

Expiration Date:!.- <June 16, 2014 _ -

Il

lj:..

!
I

Date:

------7/1/13

Date: ___1....,./~-1.:3_ _

,
\

!
l

~EBER~ I QUALITYC~1!,0LPROGRAM
Rev.8; 11/10/03
Trtle: Radioactive Reference Standards SoJutlons & Records

EBERLINE SERVICES - OAK RIDGE LABORATORY


RADIOACTIVE REFERENCE STANDARD SOLUTIONS
SECONDARYD~UTIONRECERnRcAnoN

Solution Reference# NIS17$RIVl4251.C''''.: '' .


Half Life, Years

Half Life, Days


<. ...'3.828E+b3)

l.'f :1'io48E;j;()'1:I

':~ .,:.:::~

... :,.;

).>

Radionuclide of lnterest,WF/)J~&ld.:''fol

Parent Solution Conc.;>:ofJ48Ef.05:\\f dpm/ml

Dilution Instructions:

Dilution Solvent Used


SECONDARYVOLUMETRJCD~UTION

Vol. Parent Solution: ~: +0::.25.'.00oo: ml


Total Activity:
3~6950E+06 dpm
Final Volume: '?6''.1000;'00 ml

NOTES:

Final Activity Concentration:)

3~6950E+03ldpm/ml

This activity concentration is based on the original


reference date listed above. All activities are
corrected to the date and time of analysis by the
laboratory data processing software.

Expiration Date:I

June 18, 2014

7/1/13
------Date:
'7/:L-/ ---
I_,
--,Date:

.....

fHl4~

CERTIFICATE OF CALIBRATI :rfA/QG REVIEWED


ALPHA STANDARD SOLUTIO ote d- g
Radionuclide:
Half Life:
Catalog No.:

1600

Source No.:

TMA EBERLINE

Ra-226

Customer:

7 years

VH1888

P.O.No.:
Reference Date:
February 1 1994
12:00PST.

.Ci.

Contained Radioactivity: (Ra-226) 1.001


Contained Radioactivity: (Ra-226)
37.0 kBq.

7226
453-26

Description of. Solution

a. Mass of solution:

5.1864 g (in a 5 ml Flame Sealed Ampoule)

b. Chemical form:
c. Carrier content:

Ra(N03)2 in 1 N HN03

d. Density:

1..0318

None added
g/m1@20C.

None detected(other than daughters)

Radioimpurities

Radioactive Daughters

Rn-222, Po-218, At-218, Pb-214, Bi-214, Po-214, Tl-210, Pb-210, Bi-210, Po-210 and Tl-206.

Radionuelide Concentration

(Ra-226) .. 0.1929

Ci/g.

Method of Calibration
Weighed aliquots of the solution were assayed using gamma spectrometry:

Energy peak(s) integrated under: 186 keV.

Branching ratio(s) used:


0.0351
gamma rays per decay.

Uncertainty of Measurement
a. Systematic uncertainty in instrument calibration:

b. Random uncertainty in assay:

3.4%
3.1%

c. Random uncertainty in weighing(s):

0.2%

d. Total uncertainty at the 99 % confidence level:

4.6%

NIST Traceability

This calibration is implicitly traceable to the National Institute of Standards and Technology.

Leak Test(s)

See reverse side for Leak Test(s) applied to this source.

Notes

1. Nuclear data were taken from "Table ofRadioactive Isotopes", edited by Virginia S. Shirley, 1986.
2. IPL participates in an NIST measurement assurance program to e&tablish and maintain implicit traceability for a number of nuclides,
based on the blind way(aiid later NIST ceitificationfofStiiidliro Reference Materiiils{AS in NRC Reguliitory Giiide 4. rs); -

QUALITY CONTROL

/iA,. ;

199 If

Date Signed
ISOTOPE PRODUCTS LABORATORIES
1800 North Keystone Street
Burbank, California 91504

818 843 - 7000

43

QUALITY CONTROL PROGRAM


MP009

Rev.8; 11/01/03
Title: Radioactive Reference Standards Solutions & Records

EBERLINE SERVICES OAK RIDGE LABORATORY


RADIOACTIVE REFERENCE SOLUTIONS
PRIMARY DILUTION RECERTIFICATION
MP009
CURRENT DATE!
11/9/2012 0:001
SOLUTION REFERENCE #,...IP_L_4_5_3_,._,26-.--.:. :- -.- - -..........J
SOLUTION #I Ra~
: I
Principal Radionuclide
Half Life, Days
Half Life, Years
~;ti:;
. .
I
j .. 1.600E+o31
s.a44E+osl
. Radium

Reference Date I < .. 2/1/1994 O:Ool

Radionuclide ""llRadiull1.
Certified Activity >1.001E"fo00 Cl
Certified Concentration : . . :. : Cl per gram

.... :..... . . :. We~ght, Grams


Ampoule /Solution Gross~
Empty Ampoule .. . . : :: . Weight, Grams
Weight, Grams
Solution Net
. .
1.0010 Cl
Total Activity in Ampoule
Chemical Composition of Standard Solution

Dilution Instructions:

Dilution Solvent Used

Dilute to a volume ofl

Certified Total Activity of!

1;0010jCI

1000.00 !milliliters
Which Eauals

. 2.222E+06ldpm at the date listed above

And after dilution the activity of this solution isl 2.222E+03ldpm/ml

This activity concentration is based on the original


reference date llsted above. All activities are corrected
to the date and time of analysis by the laboratory data
processing software.

Expiration Date:! November 9, 2013

Verified & Approved

QC

By_~-~----...1---+- ~-'""'"-......

Approval_-\~......,,,,..<IA~-w.~::..;l
......._ _ _
~..;;.-

Date;
Date:

11/9/2012
-------

If/1 n,/r?
----f-i-;;.+-:.---
,

Rev.8; 11/01/03
TrUe: Radioactive Reference Standards Solutions & Records

EBERLINE SERVICES - OAK RIDGE LABORATORY


RADIOACTIVE REFERENCE STANDARD SOLUTIONS
SECONDARYDILUTION RECERTIFICATION
111912012 0:00
Date
Solution # ii:)\'.:.:;\vRa~5b'\!fi:;>.1 /.
Half Ufe, Days

MP009
Prine! al Radionuclide
:;:ll!~RaetiUm'!

Half Life, Years

I >' . '. /5:a44e+osl

1;,;,;:;eooo6to31

Radionuclide of Interest ':,~R~dilim!'/i


Parent Solution Cone. :C/:2:22Et03{/ dpm/ml

Reference

Datel:'r; :,21.1t1'9'9.4'6:0ol

Chemical Composition of Standard Solution

Dilution Instructions:

Dilution Solvent Used

SECONDARY VOLUMETRIC DILUTION


Vol. Parent Solution: ::: .:;:2010000 ml
Total Activity: . :4'4440E+.04 dpm
Final Volume: ::: >::Jo.00'.00. ml

NOTES:

Final Activity Concentration: I.... . . , A.4440E+01ldpm/ml


This activity concentration is based on the original
reference date listed above. All activities are
corrected to the date and time of analysis by the
laboratory data processing software.

Expiration Date:I November 9, 2013

Date:

11/9/2012 0:00

Date:

''

/t-z. Il 1l

RA-\\
ANALYTICS

1380 Seaboard Industrial Blvd.


Atlanta, Georgia 30318 U.S.A.
Phone (404)352-8677
Fax (404) 352-2837

CERTIFICATE OF CALIBRATION
Standard Radionuclide Source
62680-416

Ra-228 5 mL Liquid in Flame Sealed Vial

This
standard
radionuclide
source
was
prepared
gravimetrically from a calibrated master solution.
The
master solution was calibrated using a germanium gamma
spectrometer system.
Radionuclide purity and calibration were checked using a
germanium gamma spectrometer system. The nuclear decay rate
and assay date for this source are given below.
ANALYTICS maintains traceability to the National Institute
of Standards and Technology through Measurements Assurance
Programs as described in USNRC Reg. Guide 4.15, Revision 1.
ISOTOPE:

Ra-228

ACTIVITY (dps) :

2.585 E3

HALF-LIFE:

5.75 years

CALIBRATION DATE:

November 7, 2001 12:00 EST

TOTAL UNCERTAINTY*:

4.0%

SYSTEMATIC:

3.0%

RANDOM:

1. 0%

*99% Confidence Level

Impurities: y-impurities (other than decay products) <0.1%

5.07198 grams O.lM HCl solution with 50 g/g Ba carrier.

P 0 NUMBER

9508, Item 1 (Part #4339A)

SOURCE PREPARED BY:

Q A APPROVED:

M~l<J.d~mist

,EBERLIN_!;;

se:1w1c1<e

QUALITY CONTROL PROGRAM

MP-009

Rev.8; 1/10/03
Trtle: Radioactive Reference Standards Solutions & Records

EBERLINE SERVICES OAK RIDGE LABORATORY


RADIOACTIVE REFERENCE SOLUTIONS
RECERTIFICATION
MP009

Princi al Radionuclide

.') ~~8~::<?:

Half Life, Years

Half Life,

1.,:;"s'?'tooeb:ol

Radionuclide :,:)':(,~R,~%\/,i
certified Activity ;':.:a~98ee;oz Ci
Certified Concentration
Ci per gram

Reference

Days

Datel'.6;3 ';'.fifl:i2o0.1~'0t.Obl

Ampoule /Solution Gross :.\'\/i.;~;~982 Weight, Grams


Empty Ampoule,,.,.:=-;. :.~?4~48-9.$.. Weight, Grams
Solution Net ' 5;008.7 Weight, Grams
Total Activity in Ampoule!> < o:0699 Ci
Chemical Composition of Standard Solution

Dilution Instructions:
Dilute to a volume off;

Dilution Solvent Used

:,1()00;-0Cf\

Certified Total Activity ofL;' ' o.oe99lCi

/I milliliters

Which Eauals

I / ).

:1;55tEt05Jdpm at the date listed above

And after dilution the activity of this solution isl1:551E+.02ldpm/ml

~:~:r!n':~:;:ete'::'!:.!!s~:=:~~:!:!;!~~~
to the date and time of analysis by the laboratory data
processing software.

Expiration Date:

Date:

I . March 26; 2014 I


5/30/13

----~--

SECTION VI

QUALITY CONTROL SAMPLE RESULTS SUMMARY

Eberline Services
Analysis Control Chart

Printed: 8/12/2013 2:25 PM

Page 1of2

WO

- - -Analysis

------1!

UUISO

13-07149

Run

Activity Units

pCi

Aliquot Units

Client Name

Engineering Management Support, Inc.

Laboratory Control Sample


Analyte

~-

U-234

CSU
Measured

LCS
Expected

Uncert.
Expected

Known

Known
Error

0.63

~-95.~4%

16.03%

100.00%

3.60%

8.17E+OO

2.94E-01

1.85

I 111.46%

15.62%

100.00%

3.60%

7.96E+OO

2.87E-01

U-238

LCS
Measured

Nonnalized
Difference

I
I

______ji

Result

CSU

Standard
ID

Standard
ACT(dpm)

Standard
Error

Standard
Added(g)

7.76E+OO

1.24E+OO

U-8a

3.52E+01

3.60E+OO

5.14E-01

9.35E+OO

1.46E+OO

U-8a

3.44E+01

3.60E+OO

5.14E-01

Sample
Aliquot

Standard
ID

Standard
Error%

Standard
Added(g)

~--

Matrix Spike
Normalized
Difference

Analyte

MS Actual

Expected
MS Result

%Rec

Expected
MSUncert

Actual
MS Result

Actual
MS CSU

I
I
I

Normalized
Difference

I
I

RPD

I
I

Original
Result

Original
CSU

Replicate
Result

!
I

---"' I

0.67

U-238

~~I

~
t.~.

il/QI

Version

-------i
I

Replicate
CSU

12.41

1.66E+OO

4.80E-01

I 1.88E+OO
I-----

~i

U-235

Sample
CSU

Replicate Sample

U-234

Sample
Result

I
I

Standard
ACT(dpm)

'

Analyte

0.33

6.71

2.46

87.11

1.39E+OO I 4.29E-01

I 7.31E-01 I

3.17E-~~

1.30E+OO

LCS Relative
Bias

QC Summary
I

LCS%R

LCSND

MS%R

MSND

RepRPD

Rep ND

4.22E-01
-

3.30E-01

2.;;E-01 I 1.55E-01

~:: -!-::
J:;
~=-I +~;-1- ::
t~; I-~;- ----t--
I

INV

OK

Printed: 8/12/2013 2:25 PM

Page 2 of 2

Eberline Services
Analysis Control Chart

13-07149

Analysis

Run

Acti\(ity Units

UUISO

pCi

Aliquot Units

Client Name

Engineering Management Support, Inc.

Replicate Sample RPO

LCS % Recovery
130.00
40.00
120.00

35.00
110.00

3000

100.00

25.00
20.00

90.00

15.00
80.00
10.00
7000-t--------------------~-----------------~

Lower Error

---Mean
-

-UCL

U-234
75.41
114.67
95.04
80
100
120

U-238
98.24
136.68
117.46
80
100
---------1
120

!
i

5.00
0.00

+-------------~------

U-234
13.99
Lower
- -Error
--+-----------
Upper Error
I U.ti,j
- -

RPO
-CL

12.41
35

U-238
7.65
5.76
- - - - 6.71
35

Normalized Difference
No Matrix Spike

REP ND

0.00
3

~~

t;l~

u~

r.;~

Version

MSND

0.00
0.00
0.00
--------
3

U-235
107.31
66.90
87.11
35

Printed: S/13/2013 S:54 AM

Page 1of2

Eberline Services
Analysis Control Chart

lllDlim_~ . .i . ";

'';~~"'"

.--"""~""'" .

Engineering

Ma::~::ent Support, Inc.

Laboratory Control Sample


A nayte
I

I:
1

Normalized
.
Difference

LCS
Measured

TH-22S

0.50

TH-230

1.03

TH-232

1.06

I.
i

95.61%

1
CSU
Measured

LCS
Expected

Uncert.
Expected

R
It
esu

CSU

If

II

17.73%

100.00%

3.60%

I 90.74% ! 19.29%

100.00%

2.70%

' 5.45E+OO

I 1.47E-01

100.00%

3.60%

4.S7E+OO

1.75E-01

Standard
ID

I
t-----------------t------j-,----1---

91.26%

Known
Error

Known

17.52%

4.S7E+OO I 1.75E-01 I 4.65E+OO

+- -------

'

S.25E-01

I
I

Th-Sb

Standard
ACT (dpm)

!I

Standard
Error

I'

Standard
Added (g)

1.04E+02

'

3.60E+OO

'

I 1.04E-01

---+---------+'- - - - + - - - - - - - + - - - - - + - - - - - - - !

4.95E+OO
4.44E+OO

9.55E-01

Th-1b

7.7SE-01

Th-Sb

Sample
Aliquot

Standard
ID

2.35E+01

2.70E+OO

5.15E-01

1.04E+02

3.60E+OO

[ 1.04E-01

Matrix Spike
A

lyt
na

:I

Normalized
Difference

i'

MS Actual
% Rec

I:

Expected
MS Result

Expected
MS Uncert

Actual
MS Result

Actual
MS CSU

II
I

Sample
Result

'

Sample
CSU

II

Standard
ACT (dpm)

----I

I
I

Standard
Error%

Ii

Standard
Added (g)

--

----~---

Replicate Sample
Analyte

Normalized
Difference

RPD

Original
Result

------------t--------t--------j---------+--------1

QC Summary
!

Original
CSU

Replicate
Result

Replicate
CSU

LCS R_elative
Bias

4.31E-02

5.52E-02

0.96

1.77E-01 I 2.65E-01

1.29E-01

0.91

LCS % R

LCS ND

MS % R

MS ND

Re RPO
p

I
l

Re

ND
p

TH-22S

0.44

- TH-230
~------

TH-232

Version

U1
Qolll"ll!'

0.94

37.64

! 6.31E-02

33.16

3.70E-01

6.92E-02

.. -------------

0.1S

16.S5

4.47E-02

I
!

5.S2E-02

i
I

4.60E-02

0.91

OK

l~~---r~~---~i

-~-!

3.77E-02

OK

--- ---------;--
I

OK

OK

OK

NA

OK

INV
1

NA

'

OK

Eberline Services
Analysis Control Chart

Printed: 8/13/2013 8:54 AM

Page 2 of 2

WO

Analysis

13-07149

Th ISO

----'--~llr1_ __ j

Aliquot Units

Activityl)nits

Engineering Management Support, Inc.

pCi

Replicate Sample RPO

LCS % Recovery

------t--

130.00
40.00
120 00

Client Name
-------------

- UCL
35.00

110 00
30.00
100.00

25.00
20 00

90 00

15.00
80.00

.. LCL
10.00

70001-------------,--------=~~;:;-----,-------,:;~;;:;;----~
TH-228
TH-230
TH-232
74.28

68.75
112.73

116.94
95.61

90.74

112.38
91.26

80

80

---Mean

80
100

120

120

120

-UCL

5 00

70.14

0.00+--------------~------------~------------~

TH-228

TH-230

TH-232

Lower Error

59.68

41.15

=-~rror

15.59

25.18

27.51
6.19

~b

16.85
35

RPO
CL

----~-37:64

35

33::,5-

Normalized Difference
No Matrix Spike

3.50
3.00

-------------

2.50
2.00
1.50
1.00
0.50
000

~~~I
~

tt.111
V'oJI

Version

LCS ND

REP ND

MSND

0.50

044

0.00

1 03

0.94

0.00

Eberline Services
Analysis Control Chart

Printed: 8/8/2013 8:43 AM

Page 1of2

WO

.. _,______f<_tJ_ri__--+-

Analysis

za_caaa_

Ra 226

___ . Activity Units

Aliquot Units

pc1

I __________

------~- Clie_nt N<lme

1Engmeermg

M anagemen t s uppo rt , 1nc.


I

Laboratory Control Sample


I

I
Analyte

....,,.

Normalized
Difference

LCS

Uncert.
Expected

Known

I
j

Known
Error

., ,

-I -I

"'-"% ,..,.%__r-;;;~""
1

1-----

LCS
Expected

CSU
red

-i -1

II

Result

CSU

I'

Standard
ID

Standard
Error

Standard
ACT (dpm)

Standard
Added (g)

U%-+ .,.+., I .70~:".' _I '": '+ -~, .._., + .,....,


1

-~---l----~!--------+-

Matrix Spike
Normalized
Difference

- - - - -_t

Analyte

t---

----

MS Actual
%Rec

Expected
MS Uncert

Expected
MS Result

Actual
MS Result

Actual
MS CSU

II

Sample
Result

Sample
CSU

Sample
Aliquot

Standard
Error%

Standard
Added(g)

RepRPD

Rep ND

NA

OK

Standard
ACT(dpm)

I
--------~-----+---

------+--------+-------+-------+

Replicate Sample
Analyte

Standard
ID

Normalized
Difference

I
I

!
RPO

II

QC Summary
I

Original
Result

Original
CSU

Replicate
Result

Replicate
CSU

LCS Relative
Bias

LCS%R

II

LCSND

MS%R

MSND

RA-226

2.07

95.65

I 2.96E-01

2.89E-01

8.39E-01

4.26E-01

1.13

OK

OK

!
i

..

II

~~

t..:ii

Version

I
I

-+
I

-----+ -----
I

----+-------
I

Eberline Services
Analysis Control Chart

Printed: 8/8/2013 8:43 AM

Page 2 of 2

-~alysis

WO

Run

Ra226

13-07149

Aliquot
- - - -Units
- - - - - - -i,-------

___A_ctivity Uriit_s_____

pCi

Client ----Name
--------------------------1

Engineering Management Support, Inc.

Replicate Sample RPO

LCS % Recovery
130.00

40.00

'

/U.UU

~-

UeeerError
%R

=--.=-LCL
---Mean
-

RA-226
84.03
141.74
----------:i12 8-9
--80___ -

Lower Error

-~

- -
--

------100- - - - - - -

----

-------

120

-UCL

---

-~
-

Lower Error
U per Error

RPO
-CL

RA-226
125.74
65.55
95.65
35

Normalized Difference
3.50

No Matrix Spike

-----

~---

3.00
2.50 +---------
2.00

+-

---------

1.50 +-------

---

1.00 -j
0.50
0.00
-RA-226
1
-

!<"!!:~

ta

tn
t~.

UCL

Version

LCS ND

REP ND

MSND

0.92

2.07

0_00

----~

--

Eberline Services
Analysis Control Chart

Printed: 8/14/2013 10:47 AM

Page 1of2

Analysis

WO

Ra228

13-07149

Run

Activity Units_____ ~-+---__)\li_qlJCl!LJll_its

pCi

Client Name

Engineering Management Support, Inc.

Laboratory Control Sample


Normalized
Difference

Analyte

RA-228
--mm

I__.:"

LCS
Measured

CSU
Measured

89.51%

I 25.17%

LCS
Expected

100.00%

Uncert.
Expected

5.10%

1----_j___ _j__

Known
Error

Known

8.73E+OO ! _4.45E-01

- ---
I

Standard
ACT(dpm)

Standard
Error

Standard
Added (g)

Result

CSU

Standard
ID

7.81E+OO

1.97E+OO

Ra-11

3.77E+01

5.10E+OO

5.14E-01

Sample
CSU

Sample
Aliquot

Standard
ID

Standard
ACT(dpm)

Standard
Error%

Standard
Added(g)

RepRPD

Rep ND

NA

OK

----t
I

Matrix Spike
Analyte

MS Actual
%Rec

Normalized
Difference

Expected
MS Result

Expected
MS Uncert

Actual
MS Result

Actual

MS CSU

Sample
Result

Replicate Sample
Analyte

RA-228
!-----

~!'ll
~i

U1!
u~

Version

Normalized
Difference

0.54

QC Summary

RPD

Original
Result

Original
CSU

Replicate
Result

23.04

1.22E+OO

6.84E-01

9.69E-01

---r~~~~-j----~~---t-~~~~+---~~

Replicate
CSU

6.16E-01

LCS Relative'
Bias

LCS%R

0.90

OK

-+-~~~---+

LCSND

OK
--+-

MS%R

MSND

Eberline Services
Analysis Control Chart

Printed: 8/14/2013 10:47 AM

Page 2 of 2

_____
A_nalysis

Ra228

13-07149

_RLJ_n_T.
1

Activity Units

Aliquot Units

Client Name

Engineering Management Support, Inc.

pCi

Replicate Sample RPO

LCS % Recovery
130.00
40.00

1
80 00

70.00

Lower Error
Uooer Error
%R

;:-:::-. -LCL
~.~ean

-UCL

RA-228
59.25
119.78
89.51
80
100
120

Lower Error

Uooer Error
RPD
-CL

..

RA-228
29.88
16.21
23.04
35

Normalized Difference
No Matrix Spike

3.50 , - - - - - - -
3.00 +-----~2.50 + - - - - - - - - - - -
2.00

+-------

1.50 + - - - - - - - - - - -
1.00

t-------

0.50
0.00
-RA-~~
1

(ll:!ll
l:!l\~

ucL

Version

LCS ND

REP ND

0.90

0.54

MSND

000 ___ _,
_::.:::_

----

SECTION VII

LABO RA TORY TECHNICIAN'S NOTES

ISOUNOTES

Page 1 of 1

Printed: 8/5/2013 9:26 AM

~EB!::R~~~c~
Work Order Analysis Notes

#
1

Date

Dept

08/05/13 09:26

PREP

User
JWOLFE

Oak Ridge Laboratory

601 Scarboro Rd.


Oak Ridge, TN 37830
Voice: 865.481.0683
www.eberlineservices.com

Internal Work Order

Analysis Code
Run Number

13-07149
UUISO
1

Notes
ALIQUOTED AND ADDED SPIKES AND TRACERS- PRESERVED FRACTIONS 4-7, 12, 13 AND 15 WITH
HN03- DRIED SAMPLES DOWN

Printed: 8/8/2013 6:36 PM

Page 1of1

~EBER~~~c~
Work Order Analysis Notes

Oak Ridge Laboratory

I
I

601 Scarboro Rd.


Oak Ridge, TN 37830
Voice: 865.481.0683
www.eberlineservices.com

Internal Work Order

Analysis Code
Run Number

13-07149
UUISO
1

Date

Dept

08/05/13 09:26

PREP

JWOLFE

ALIQUOTED AND ADDED SPIKES AND TRACERS- PRESERVED FRACTIONS 4-7, 12, 13 AND 15 WITH
HN03- DRIED SAMPLES DOWN

,2

08/08/13 18:36

CHEM

JDEMELAS

Added concentrated HCI to sample beakers and heated to dryness; Added 20 ml 8N HCL to samples and
transferred to new, labeled C-Tubes, rinsing with 8N HCI to bring volume to -35 ml; Preconditioned resin
columns with 35 ml 8N HCI; Centrifuged samples and loaded onto columns; Rinsed C-Tubes with 20 ml 8N
HCI, centrifuged as needed and loaded onto columns; Rinsed columns with 35 ml 8N HCI 0.1 N NH41, 35 ml
of 6.5N HCI 0.04N HF, and 1O ml of 6.5N HCI; Eluted Uranium with 50 ml of 0.5N HCI into clean, labeled 100
ml beakers; Dried-down samples on hotplate; Dissolved samples in -1 O ml of concentrated HCI; Transferred to
new, labeled C-Tubes with DI H20. Set samples aside for later precipitation and filtering.

User

Notes

Printed: 8/9/2013 6:53 AM

Page 1 of 1

Oak Ridge Laboratory

JfJ
E:e E: R 1,,..J N E:
~

601 Scarboro Rd.


Oak Ridge, TN 37830
Voice: 865.481.0683
www.eberlineservices.com

SERVICES

Work Order Analysis Notes

Date

OS/05/13 09:26

OS/OS/13 1S:36

Dept

User

Notes
5

:::~ -f-I ~;:~:~As ~~d~r~~::~!:f~~~:D~:ie~b:;::;:::t~:~:::~::~~:;:;~1ss~~~c~:1~:;;:e: a:TH

transferred to new, labeled C-Tubes, rinsing with SN HCI to bring volume to -35 ml; Preconditioned resin
columns with 35 ml SN HCI; Centrifuged samples and loaded onto columns; Rinsed C-Tubes with 20 ml SN
HCI, centrifuged as needed and loaded onto columns; Rinsed columns with 35 ml SN HCI - 0.1 N NH41, 35 ml
of 6.5N HCI - 0.04N HF, and 10 ml of 6.5N HCI; Eluted Uranium with 50 ml of 0.5N HCI into clean, labeled 100
ml beakers; Dried-down samples on hotplate; Dissolved samples in -1 Oml of concentrated HCI; Transferred to
new, labeled C-Tubes with DI H20. Set samples aside for later precipitation and filtering.

OS/09/13 06:53

CHEM

RMARTZ

ADDED 0.1 ML NEODYMIUM CARRIER, 0.3 ML TITANOUS CHLORIDE, & 1 ML HF TO C-TUBES; LET SET
SIT IN ICE BATH FOR ONE HOUR SET UP FILTERS BY ADDING ALCOHOL & CARBON SUBSTRATE
THEN ADDED SAMPLES; WHEN SAMPLES WERE THROUGH FILTERS, ADDED 10 ML DI H20 RINSES
FROM C-TUBES, REMOVED FILTERS, LET DRY IN DESSICATOR, THEN SENT SET TO COUNT ROOM.

Eberline Analytical
Oak Ridge Laboratory

Printed: 8/9/2013 6:54 AM

Page 1of1

Internal Work Order

EeE:R~NE:

SERVICES

Analysis Code

UUISO

Reagents Used in an Analysis


Reagent
ID

Reagent
Name

__

''-"'""-'"'''

Run

Reagent
Concentration

agent Grade
,,,,,~-~~'~'"'-"'''''""'""~-""""'""''''"'"''''""""""""'""""''""'"'"-~-~

Reagent Grade
6.SN - 0.04N

__

,,,,,,,

0142255

,,,,,,,,,,,,,,,,,,,

O.SN

8/8/2013

6.SN

8/8/2013

Hydrochloric Acid

8/8/2013

Hydrochloric Acid

8/8/2013

,,,_ _,,,,,,,,,,j,, , , , , , , , , ,,,,,,,

Hydrochloric Acid

JDEMELA5

,,,,,,,~~-~,,,,J,,,,,~~---,,-,~--,,,,-,,~-,,

HCI - NH41

JDEMELA5
'~"'"'"""'"'''~"'*"'

rbon substrate

RMARTZ

Hydrofluoric Acid
0131915

Neodymium Carrier
,,,,,,,,,,,,,~-

Reagent Alcohol
,,,,,,,,,~,,,,,,,,,,,,,,,,,

Titanous Chloride

Reagent Grade

RMARTZ

10
---------

L-~~~~~~~~---.-~~::::::~~~.2!:!:~::f:L..~~~~~,h:,~~

------------------_U

_____

~-

------~

____
-

__

f6jJt1?_

-~-ct

l,._(

5 - _(.,,-~(.,_

___ ----~--------D_C_o&:___-L_~

---

---~-

___

--- __tP[1;__ ---- 'V-i-7

,..;-~-

-:

---

- - --. "'~~~
l~~7;?~r'.1) '' ~~~;cf ~_:,.,~-'~~ ~
<2\0i \I'~ \ ')oioo_)~ LJ~'\) f+cc..t-~~ __ L~()-~-- _1-,j\~
--~---Jlt
)

___________ 1

____q\q_\ l"> _ ~~~~~ ~ \C-Jcl

__

__

__ l\.t'l.-l/___ L(e~\)_t\l--~

__~-----\ff:

. . --- .... _ ~!~i(~- '~~)~1~~} ~~~~=-r'~~i ~i~~~~- '~~ii-: ~


-------- - '6/t-vl/J -

---- ___

1C11-un

. ----t--

u- _

Qe.-,;cyQ~~
Ja~'tJ.Ar1-1r)

----~- ----

~./12~--

_fJCL)_______L~------~-------

_ __fL0r

____ 1~ _ ----~ltfa-;o_:___~

----

- ..

----

--

----------

---- ---.----

----

------------- - - - - - - - - - - - - - - - - -

- - - - -----

--

.- ----t---

--------

------

. --~-

- --

----------------

--------~---- ------" --~----

--------------

-----

ISO TH NOTES

Printed: 8/5/2013 9:26 AM

Page 1 of 1

j!J E_EI I;; R Lt.~ I;;


~

SERVICES

Work Order Analysis Notes

#
1

Date

Dept

08/05/13 09:26

PREP

User
JWOLFE

Oak Ridge Laboratory


601 Scarboro Rd.
Oak Ridge, TN 37830
Voice: 865.481.0683
www.eberlineservices.com

Internal Work Order

Analysis Code
Run Number

13-07149
Th ISO
1

Notes
ALIQUOTED AND ADDED SPIKES AND TRACERS- PRESERVED FRACTIONS 4-7, 12, 13 AND 15 WITH
HN03- DRIED SAMPLES DOWN

Printed: 8/9/2013 5:24 PM

Page 1of1

Oak Ridge Laboratory

,EBERLINE;:

SERVICES

Work Order Analysis Notes j

Date

Dept

User

601 Scarboro Rd.


Oak Ridge, TN 37830
Voice: 865.481.0683
www.eberlineservices.com

Internal Work Order

Analysis Code
Run Number

13-07149

Thi SO
1

Notes

1
08/05/13 09:26

PREP

JWOLFE

ALIQUOTED AND ADDED SPIKES AND TRACERS- PRESERVED FRACTIONS 4-7, 12, 13 AND 15 WITH
HN03- DRIED SAMPLES DOWN

CHEM

JOEMELAS

Added concentrated HN03 to sample beakers and heated to dryness; Added 20 ml 8N HN03 to samples and
transferred to new, labeled C-Tubes, adding 8N HN03 to bring volume to -35 ml; Preconditioned resin
columns with 50 ml 8N HN03; Centrifuged samples as needed, and passed through columns; Rinsed C-Tubes
with 20 ml 8N HN03; Centrifuged rinsates and loaded onto columns; Rinsed columns with 40 ml 8N HN03;
Eluted Thorium with 50 ml of 8N HCI into clean, labeled 100-ml beakers; Dried-down samples on hotplate;
Dissolved samples in -1 Oml of concentrated HCI; Transferred to new, labeled C-Tubes with deiononized
water brinaina volume to -15ml. Set samoles aside for later orecioitation and filterinn.

08/09/13 17:24

Printed: 8/12/2013 5:48 AM

~
f;;:.f:::I
~

Page 1 of 1

Oak Ridge Laboratory

E;:.R.LI NE;:

601 Scarboro Rd.


Oak Ridge, TN 37830
Voice: 865.481.0683
www.eberlineservices.com

SECF<VICECS

Work Order Analysis Notes

I
I

Date
08/05/13 09:26

I
I
I

3t

Dept

!I

PREP

nwm.--.~-._,,.,,,,,

User
JWOLFE

~--~-"'"

Run Number

13-07149
Thi SO
1

Notes

ALIQUOTED AND ADDED SPIKES AND TRACERS- PRESERVED FRACTIONS 4-7, 12, 13 AND 15 WITH
HN03- DRIED SAMPLES DOWN

Added concentrated HN03 to ;;ample beakersand.heaied io drYne5s;Added2omT8N Hiii63fosampfes and


transferred to new, labeled C-Tubes, adding 8N HN03 to bring volume to -35 ml; Preconditioned resin
columns with 50 ml BN HN03; Centrifuged samples as needed, and passed through columns; Rinsed C-Tubes
with 20 ml 8N HN03; Centrifuged rinsates and loaded onto columns; Rinsed columns with 40 ml 8N HN03;
Eluted Thorium with 50 ml of 8N HCI into clean, labeled 100-ml beakers; Dried-down samples on hotplate;
I
Dissolved samples in -1 Oml of concentrated HCI; Transferred to new, labeled C-Tubes with deiononized
:::--t-~.:~c:::::":--+-~~=~--~-+--"'w0 ~a:::te::.r,c,:b:.:.r::.:in~<:1ic:.:n<l,.__,v__o::::l::u:m:.:.!!. to -15ml. Set samJ?les aside for later J?reciJ?itation and filterino.

08/12/13 05:47
CHEM

RMARTZ
ADDED 0.75 ML 0.1MG/ML CERIUM CARRIER & 1 ML HF TO C-TUBES & LET SET SIT IN ICE BATH FOR
ONE HOUR; SET UP FILTERS BY ADDING ALCOHOL & CARBON SUBSTRATE THEN ADDED SAMPLES;
WHEN SAMPLES WERE THROUGH FILTERS, ADDED 10 ML DI H20 RINSES FROM C-TUBES,
REMOVED FILTERS LET DRY IN DESSICATOR THEN SENT SET TO COUNT ROOM.
08/09/13 17:24

Internal Work Order

~~---~~,~~

I
I

CHEM

JDEMELAS

I
I

Eberline Analytical
Oak Ridge Laboratory

Printed: 8/12/2013 5:48 AM

Page 1 of 1

Internal Work Order

13-07149
Reagents Used in an Analysis
Reagent
ID

014109P

Reagent
Name

Analysis Code

Run

Th ISO

Reagent
Concentration

Nitric Acid

Grade

mm-,~~~~'"'+

Analyst
ID

Date
Recorded

JWOLFE

S/5/2013

014164P

Anion Exchange Resin

Reagent Grade

JDEMELAS

S/9/2013

0142375

Hydrochloric Acid

SN

JDEMELAS

S/9/2013

Reagent Grade

JDEMELAS

SN

JDEMELAS

Reagent Grade

JDEMELAS

014142P

RMARTZ
MARTZ
Hydrofluoric Acid
Reagent Alcohol

- - - - - - - - - - - - - --------------

--------~

-t----------
-+---------------'---------
~------

- --

-------------

- - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - ---------------

---~-----+-----!------\'.

---------------------- ------------------- ------------ - - - - - - - - - - - -

- - - - t - - - - - - - - - - - - - - - - - - - - -----------------

-------- - - - - - - -

--------+---------!

----------

,I__

,.

---r i

GE7:1

RA-226 NOTES

Printed: 8/2/2013 8:37 AM

Page 1of1

~
#

Oak Ridge Laboratory

EelE~J-1

....... E

SERVICES

Work Order Analysis Notes

Date

Dept

08/02/13 08:37

PREP

User
JWOLFE

601 Scarboro Rd.


Oak Ridge, TN 37830
Voice: 865.481.0683
www.eberlineservices.com

Internal Work Order

Analysis Code
Run Number

13-07149
Ra226
1

Notes
ALIQUOTED AND ADDED SPIKES AND TRACERS- DRIED FRACTIONS 4 AND 5 DOWN AND DIGESTED
DUE TO HIGH AMOUNT OF SOLIDS PRESENT- PH'D ALL SAMPLES- PRECIPITATED WITH BA AND PB
CARRIERS AND AMMONIUM SULFATE- DECANTED SAMPLES AND CENTRIFUGED- SUBMITTED
RADIUM PRECIP TO SEPARATIONS

..:J\A))\~l

GG73

Printed: 8/27/2013 12:13 PM

Page 1of1

~EBER~~~~
Work Order Analysis Notes

Date

Dept

08/02/13 08:37

PREP

JWOLFE

08/27/13 12:13

PREP

LWALKER

User

!
I

Oak Ridge Laboratory


601 Scarboro Rd.
Oak Ridge, TN 37830
Voice: 865.481.0683
www.eberlineservices.com

Internal Work Order

Analysis Code
Run Number

13-07149
Ra226
1

Notes
ALIQUOTED AND ADDED SPIKES AND TRACERS- DRIED FRACTIONS 4 AND 5 DOWN AND DIGESTED
DUE TO HIGH AMOUNT OF SOLIDS PRESENT- PH'D ALL SAMPLES- PRECIPITATED WITH BAAND PB
CARRIERS AND AMMONIUM SULFATE- DECANTED SAMPLES AND CENTRIFUGED- SUBMITTED
RADIUM PRECIP TO SEPARATIONS
FOLLOWED STEPS 12.1 TO 12.8 IN AP-006 REV 12 FOR RA 226 ANAL YSIS-(SYRINGE FIL TE RED
PRECIP-FILTERED-DRIED-OBTAIN FINAL WEIGHT)-SUBMIT TO COUNT ROOM.

74

Printed: 8/7/2013 10:34 AM

Page 1of1

Eberline Analytical
Oak Ridge Laboratory

Reagents Used in an Analysis

013376P
013930003

Ammonium Sulfate

014007002

1 mg/ml

JWOLFE

014008002

166 mg/ml

JWOLFE

014109P

Reagent Grade

JWOLFE

Reagent Grade

JWOLFE

009098P

Reagent Grade

JWOLFE

011383P

Reagent Grade

TS MITH

013575005

200 mg/ml

TS MITH

013416P

Perchloric Acid

_.flP'J
~A.,;c.~

1_01

'

-------------

---~----------

........____

-----

____________

-----

----------

---- ---

-------

-------~------------------------

---------------

-----

25
~~~~~~~~~JU.i.is~~~~..L~~~~~~:

==--{_m//1
----~ft.lL

P~rfi-r_ ----~-------.-eL.,__~---L~ __________

L"I O-:i.J.1.1AiJ1-1-~

---c-~C")- _ f '3.Q.lQ_Q~A 11~

~-kl.L-G-'="----~ _ _01__]"'_

lb~-- - -

--~-'==---- _Q~_::J_!J::___ _ 1 L __

__c,,,-

-tk~- _.., -'"----'

_l_~o-1L2~oALl::.J ----.U.~-~---- --~~- ----~~- _l<_t,,.~_ _"'-:--" ~


---- W,LL. \~03:.l:l..tt.(1-'4)-~') _\..AJ..&)_{L________u~'-l
.z..~~~s __AlfL--.._J_'i$__
------1, (\Q \\'? DJ~_7'-"4.Y1:\-(!-:--le }._____6_~ ~----- _J i'-1_~-- ~n...- .so_-______ "t1r.._ _:lro_

---ieL.k.1-1.

<___

--~~(olt1-J_2QJ3:?.'.l(x'i)_____~~..k_____.l~(~~--- --~~-!._
_ ~
_____l_j_l\al11 J.'J...o~ t'"'+Au.:}"':J_ _____-6 ms__________ 1J.1<2L______}_!'_ ~-~---- -~~

.,

__

J~
-----~ 't;/~ __f2ew'y._~1 __ ------~----- _D.J=-1~ ___ t'""'='==--- ---------------:
C---U1tLJ-- ----1'}1l<t.tJ_L(,.4.Lr)__ ---U~:~ -- __f!29_l!J__ ___ 1).___L______(d)&~ -~~
...,-~{-&'~- -l-'1.~.7//1)./1.lk"J,1_,J ~-- __ pJ'J;::--__ ---.2.L/:< -----uJ-;?;o ~
-----+U't/11. .-L'7;..tL-L.tr..ob':tJ----W-'2.J~'1~. . __e?.1~ _UJ. _ =-f4.'7i- c.- __

flJg_
\~~~i~~)
------i 1-l

l.l~~~V\= ~~~l=1t~~nl ~

.i2.
Jct>__

l t3. l 'J \)q_ \'"-\ l.t A-C") ____ ____J5 VY)_~ ______Ji,'i ~---- -z,~..:.__ -~____ _i q :+ t3 l ~t:>~tfL-~l"{)____!J_~_<L ________t~~- _ hrSf?~ ~~~) _ f.C> _
J_ihlt1-_
J_;, Q_}.J_~~ ~u'1j____6.fl\2____ J_ft_o_(o____ ~b< ~ ~ _~-- -~----
,
_ c- _ _

------------

----,-------------~-~ --------~--------- --~--~

------------------- - - - - - - -

- - - - - - - - - - --------

----"+--------- - .----------------"----------- . . . . . . . . ______


------------- ------------- ---
lI' - - -------------------- ------------- ---- --------------------- -------------
];

---------!------
~

- - - -.. -------------------- --- ----------------------- -----------

----....,____ _ _ _____;i._ _ _ ~------- - - - - - - - - - - - - - -.. - - - - - - -

~-------------- ..

___ ___.... ------------ ----


...

--~--------1-----------------...

----------~-

---------------

.....- - - - - - - - t - - - - - - - - - - - - - -

- - -----

..

- - - - - - - - - - ----------

------

- - -.. - - - - - -

--------j---

-----

----------------- --------

_ .. _ _------- --------

-----------------------

- - - - - - - -------

-------------
-----------------

---~---

----
-------------

----

-------1-------1

---------

______;. _______:_--?------- -------- -------------- ---------------- ---------- ----------------- - - - - - - - ----

---------------------

----

------!---------

RA-228 NOTES

Printed: 8/2/2013 8:37 AM

Page 1of1

~EBERLINE

SERVICES

Work Order Analysis Notes

#
1

Date

08/02/13 08: 36

Dept

PREP

Oak Ridge Laboratory

08/02/13 08: 37

PREP

Run Number

Notes

'*

Al::l6H:l0=FE8 Atl0 ill!BBEB Sl'l~l!!S )!l:l~B fl'tfl;el!RS- ORIE:O FR11:C: 1101qs 11:1~0 ii oorn~ 11:1~B BIOEim:"

DLIE =F0 111611 AUQl,,Jtff OF SOLIDS PRESENT- PH'D ALL SAMPLES- PRECIPITATED WI I A BA MB
vc:r ,,. uvc.u- _. .... _ ....
=~~
~!;lll,,IM i;IRl!;91P 'FO Sl!l"~R11:TIOlqS- -~, ..:l. I~
ALIQUOTED AND ADDED SPIKES AND TRACERS- DRIED FRACTIONS 4 AND 5 DOWN AND DIGESTED
DUE TO HIGH AMOUNT OF SOLIDS PRESENT- PH'D ALL SAMPLES- PRECIPITATED WITH BA AND PB
CARRIERS AND AMMONIUM SULFATE- DECANTED SAMPLES AND CENTRIFUGED- SUBMITTED
RADIUM PRECIP TO SEPARATIONS

c ......_.._ - ..

"2

Analysis Code

User
JWOLFE

JWOLFE

13-07149
Ra228
1

Internal Work Order

601 Scarboro Rd.


Oak Ridge, TN 37830
Voice: 865.481.0683
www.eberlineservices.com

...::..

'"'-

... 'Ft

--
~

Tt:..J

~\J.

t>s

Printed: 8/13/2013 7:05 PM

Page 1 of 1

4:EBER~~~c~

Oak Ridge Laboratory

Work Order Analysis Notes

Date

Dept

08/02/13 08:36

PREP

JWOLFE

08/02/13 08:37

PREP

JWOLFE

tt&0&13 12 39

PREP

LWALKER

PREP

LWALKER

08/13/13 19:05 I

User

601 Scarboro Rd.


Oak Ridge, TN 37830
Voice: 865.481.0683
www.eberlineservices.com

Internal Work Order

Analysis Code
Run Number

13-07149
Ra228
1

Notes

ALIQUOTED AND ADDED SPIKES AND TRACERS- DRIED FRACTIONS 4 AND 5 DOWN AND DIGESTED
DUE TO HIGH AMOUNT OF SOLIDS PRESENT- PH'D ALL SAMPLES- PRECIPITATED WITH BA AND PB
CARRIERS AND AMMONIUM SULFATE- DECANTED SAMPLES AND CENTRIFUGED- SUBMITTED
RADIUM PRECIP TO SEPARATIONS
ALIQUOTED AND ADDED SPIKES AND TRACERS- DRIED FRACTIONS 4 AND 5 DOWN AND DIGESTED
DUE TO HIGH AMOUNT OF SOLIDS PRESENT- PH'D ALL SAMPLES- PRECIPITATED WITH BA AND PB
CARRIERS AND AMMONIUM SULFATE- DECANTED SAMPLES AND CENTRIFUGED- SUBMITTED
RADIUM PRECIP TO SEPARATIONS
RECEIVED FILTERS BACK FROM COUNT ROOM-PUT BACK INTO C-TUBES-ADDED EDTA AND
SWIRLED-LET SIT OVERNIGHT TO DIGEST.
FOLLOWED STEPS 12.1TO12.7 IN AP-007REV18 (CHEMICAL CLEANUP FOR RA 228)

Page 1 of 1

Printed: 8/14/2013 5:51 AM

}!J EBE Rl.-.IN E;


~

SERVICES

Work Order Analysis Notes

Date

08/02/13 08 36

~2f aa/02113 08 37

Dept

I
I
I

User

PREP

PREP

JWOLFE

JWOLFE

I
""'-----

Internal Work Order

Analysis Code
Run Number

13-07149
Ra228
1

Notes

ALIQUOTED AND ADDED SPIKES AND TRACERS- DRIED FRACTIONS 4 AND 5 DOWN AND DIGESTED
DUE TO HIGH AMOUNT OF SOLIDS PRESENT- PH'D ALL SAMPLES- PRECIPITATED WITH BA AND PB
CARRIERS AND AMMONIUM SULFATE- DECANTED SAMPLES AND CENTRIFUGED- SUBMITTED
RADIUM PRECIP TO SEPARATIONS
ALIQUOTED AND ADDED SPIKES AND TRACERS- DRIED FRACTIONS 4 AND 5 DOWN AND DIGESTED
DUE TO HIGH AMOUNT OF SOLIDS PRESENT- PH'D ALL SAMPLES- PRECIPITATED WITH BA AND PB
CARRIERS AND AMMONIUM SULFATE- DECANTED SAMPLES AND CENTRIFUGED- SUBMITTED
RADIUM PRECIP TO SEPARATIONS
RECEIVED FILTERS BACK FROM COUNT ROOM-PUT BACK INTO C-TUBES-ADDED EDTA AND
SWIRLED-LET SIT OVERNIGHT TO DIGEST.

08/08/13 12:39

PREP

LWALKER

08/13/13 19:05

PREP

LWALKER

FOLLOWED STEPS 12.1 TO 12.7 IN AP-007 REV 18 (CHEMICAL CLEANUP FOR RA 228)

08/14/13 05:51

CHEM

TSMITH

Followed steps 12. 7 to 12.15 in AP-007 rev. 17 . ( Precipitated samples, hot bathed, centrifuged, and
discarded supernate. Dissolved precip, precipitated samples, hot bathed, centrifuged, and discarded
supernate. Dissolved precip, precipitated and filtered samples, obtained final weights, covered with aluminum
foil and took to count room l

1-
I'+

Oak Ridge Laboratory


601 Scarboro Rd.
Oak Ridge, TN 37830
Voice: 865.481.0683
www.eberlineservices.com

,:;

$'

Eberline Analytical
Oak Ridge Laboratory

Printed: 8/14/2013 7:01 AM

Page 1of1

Internal. Werk

Order

13-07149
AAalSrsc~e.

Run

Ra228

Reagents Used in an Analysis


Reagent
ID

Reagent
Name

Reagent
Concentration

Analyst

ID

OLFE

Ammonium Hydroxide

Reagent Grade

Ammonium Sulfate

200 mg/ml

JWOLFE

Barium Carrier

1 mg/ml

JWOLFE

166 mg/ml

JWOLFE

Reagent Grade

JWOLFE

013416P

Reagent Grade

JWOLFE

009098P

Reagent Grade

JWOLFE

011504033

ALKER

monium Sulfide

8/2/2013
8/13/2013

LWALKER
8/13/2013
~140080~~014109P
-r-~~~~~-~-~-~~----,~;:::;:::::~:::;:--~~~~-,;;;;;;;--~~;;;:;-;.;;~
LWALKER
8/13/2013
1-0-1306-50-0~6~-~~~~~~=::;:--~~~~LWALKER
um Hydroxide
8/13/2013

r-----~----+---------------

Yttrium Carrier
013955001
r---Olm._3_0_0_2--+-----------------+----------
Ammonium Oxalate
5%

8/13/2013
ITH

8/14/2013

013910007

Nitric Acid

lN

8/14/2013

013065009

Sodium Hydroxide

18M

8/14/2013

014110004

Nitric Acid

6N

8/14/2013

013065010

Sodium Hydroxide

lOM

/14/2013

L(J l{ l l o Ql_~

-c--- -

- -, --

----

-- r- .
--

--!----

-~-

---- - - - - -

---~

---------

'

__ ,,__
/

29
~

_________

:.

:(OT/

L11Yl/lf#t)J(:].~ __t!!&t:_ ____ ._Lt-L'L__ ~l-__ ~/I}___ c_


____ _______jg_/j?/I? __0Jl1JI 1/J:/J.i ,_'tJe~--- --'~ (2_ -~-- --/--f4~-- -~
------"-----~Lt
~---~--- _12Lt""L_. ~ _ -7'-/J C
-------~&u~ _ _______~--- ----li'!:>----#. _____fla:k__
2P '=- --,L-~ -~
---------
}Wilt/I) ___IJ_o?tlft&Y_]_ t[j_~____ _f2_tFr __tG --~-- .__
________

II 'n

___________ _J

------------- --------------

- - ---

------------+---- --------------

--------------- -

-----'-----..- - - - L - - - - -

- - - - L - - - - - t - - - - - - - - - - - ...- -

r~------l--------------l----------0------1---,-------

-------------o-------

,t
'

1------1-------

----.---------

~----1----------

------..---------+-1---------

-----~-----

---

--- -

----0----------- --

'

---<------- -- - - - - - - -

---j-----~-

- - -------

------

---~-------------1----------

--

--------

_ _::_--------~---+-~---+-----------1----------t----- - - - - - - - - - - - ----------------------~

_________,
- - - - - - - - -------''-------~----"-,__________________ ___.___
----+----------- -----

-------------------+----------If-------------------------------

--------

-----~------

1----------1-----

------ ----

------~-

------------1------1-----1-----------

-------+-------' ______________ ,____ __


i
---------------r
---

----------

-----------------~----------4'-

-----------"---~------'I---

--

a------0-------- - - -

--

-------1---

--1-----------

---

SECTION VIII

ANALYTICAL DATA (ISOTOPIC URANIUM)

Eberline Services
Oak Ridge Laboratory
Analysis Sheet

Printed: 81912013 6:54 AM


Page 1of3

13-07149
UUISO
Run 1

UUISO

Analysis Code

Run

7/22/2013

Lab Deadline I

8/13/2013

Date Received

Internal
Fraction

13-07149

Work Order

01

Sample
Desc

I
1

I LCS

---02 IMBL

Client
ID

Login
CPM

LCS

BLANK

I
I

Client I Engineering Management Support, Inc.

03

i DUP

04

TRG

D-81 TOT

PZ-302-AS TOT

45

07/17/13 10:43

46

07 /16/13 15:30

05

West Lake OU-1

1.0000E+OO
1.0000E+OO

--- -

TRG

PZ-302-AS DIS

II

~------

Sample
Aliquot

07/23/13 00:00
1.0000E+OO
--+-
I
07/23/13 00:00 I
1.0000E+OO

---------

Project

Sample
Date

46

07/16/13 15:30

1.0000E+OO

06

TRG

LR-100 TOT

47

07 /17 /13 10:23

1.0000E+OO

07

TRG

LR-100 DIS

47

07/17/13 10:23

1.0000E+OO

DO

D-81 TOT

45

07/17/13 10:43

1.0000E+OO

TRG

D-81 DIS

45

07/17/13 10:43

~--

Report Level

----

Activity Units

pCi

08

I
I

I
I

~-

09

Aliquot Units

1.0000E+OO

~---

Matrix
Method
Instrument Type

WA

10

TRG

PZ-204-SS TOT

43

07/17/13 11 :40

HASL 300, 4.5.2

11

TRG

PZ-204-SS DIS

43

07/17/13 11 :40

1.0000E+OO

Alpha Spectroscopy

12

TRG

LR-103 TOT

45

07/17/13 12:15

1.0000E+OO

45

07/17/13 12:15

41

07/17/13 13:09

Radiometric Tracer

U-232

13

TRG

LR-103 DIS

Radiometric Sol#

U-10a

14

TRG

PZ-111-KS TOT

Tracer Act (dpm/g)

19.042

15

TRG

1.0000E+OO

'

1.0000E+OO
1.0000E+OO
!----

PZ-111-KS DIS

41

07/17/13 13:09

1.0000E+OO

Carrier
Carrier Cone (mg/ml)
I

--~-

I
I
I

Cr~!I
Ci!<~

* SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only.

**Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.

Eberline Services
Oak Ridge Laboratory
Analysis Sheet

Printed: 81912013 6:54 AM


Page 2 of 3

13-07149

UUISO

Run 1

Internal
Fraction

Sample
Desc

01

LCS

Tracer
Aliquot(g)

0.6131

Tracer Total
ACT(dpm)

Radiometric
Tracer (pCi)

11.7 i

I Radiometric

Grav Filter
Tare(g)

Grav Carrier
Added(ml)

%Rec

0.00
---------

02

MBL

0.6051

11.5

Grav Filter
Final(g)

0.00

DUP

0.6057

11.5

04

TRG

0.6025

11.5

TRG

05

0.6027

0.00

11.5

TRG

0.6005

0.00

11.4

SAF
1*

0.00

I
I

---

06

Mean
%Rec

--i-----

f--

------

03

Grav
%Rec

Grav Filter
Net(g)

'

'

0.00

07

TRG

0.6011

11.4

0.00
--

08

DO

0.6039

11.5

0.00

09

TRG

0.6016

11.5

0.00

10

TRG

0.6021

11.5

0.00

11

TRG

0.6020

11.5

0.00

12

TRG

0.6010

11.4

0.00

13

TRG

0.5979

11.4 I

0.00

14

TRG

0.5994

11.4

0.00

15

TRG

0.5993

11.4

0.00

I---

I
~

I
I
I

-----

--~----

---

I
----

------

~------ ~~----~-

I
I

SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only.

Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.

SAF
2*

Eberline Services
Oak Ridge Laboratory
Analysis Sheet

Printed: 8/9/2013 6:54 AM


Page 3 of 3

13-07149

UUISO

Run 1

Internal
Fraction

Sample
Desc

01

LCS

02

MBL

Rough Prep
Date

Rough Prep
By

Prep
Date

Prep
By

SeptO
Date/Time

Sept1
By

JWOLFE

08/05/13 09:21 i

DUP

----..--

08/05/13 09:21 ;

--

JWOLFE
--..

TRG

JWOLFE

08/05/13 09:21

04

Sept1
Date/Time

-1

03

Sep to
By

08/05/13 09:21

~-----

..

---

JWOLFE
-

+---------~----------

05

TRG

06

TRG

07

TRG

08/05/13 09:21 I
;

08/05/13 09:21

JWOLFE

JWOLFE
- -----

08/05/13 09:21

JWOLFE
----

08

DO

08/05/13 09:21

09

TRG

08/05/13 09:21

10

TRG

08/05/13 09:21

JWOLFE

11

TRG

08/05/13 09:21

JWOLFE

12

TRG

I 08/05/13 09:21

JWOLFE

13

TRG

08/05/13 09:21

JWOLFE

JWOLFE
JWOLFE

14

TRG

08/05/13 09:21

JWOLFE
-

15

TRG

08/05/13 09:21 .
I

JWOLFE
----

I
.__j__
I

Qj1

SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only.

Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.

Eberline Services
Oak Ridge Laboratory

a:

""'"'

Nuclide

01

U-234

0
(J

.!/!

.;.,,
c::

c:c

::::>
::::>

LCS
Flag

95.04

OK

RPO
Flag

MDA
Flag

LCS

pCi/I

7.76E+OO

1.11E+OO

6.30E-02

BLANK

pCi/I

2.34E-01

1.14E-01

7.81E-02

D-81 TOT

pCi/I

1.88E+OO

4.00E-01

6.48E-02

PZ-302-AS TOT

pCi/I

2.35E+OO

5.89E-01

1.21E-01

OK

TRG

PZ-302-AS DIS

pCi/I

2.45E+OO

5.36E-01

9.42E-02

OK

U-234

TRG

LR-100 TOT

pCi/I

3.46E-01

3.25E-01

2.99E-01

OK

07

U-234

TRG

LR-100 DIS

pCi/I

3.82E-01

3.02E-01

2.95E-01

OK

08

U-234

DO

D-81 TOT

pCi/I

1.66E+OO

4.65E-01

1.19E-01

OK

U-234

TRG

D-81 DIS

pCi/I

2.10E+OO

5.18E-01

1.54E-01

OK

10

U-234

TRG

PZ-204-SS TOT

pCi/I

2.85E+OO

5.41E-01

7.75E-02

OK

11

U-234

TRG

PZ-204-SS DIS

pCi/I

2.42E+OO

4.73E-01

9.23E-02

OK

12

U-234

TRG

LR-103 TOT

pCi/I

8.26E-01

3.68E-01

1.51E-01

OK

U-234

TRG

LR-103 DIS

pCi/I .

1.85E-01

1.37E-01

1.15E-01

OK

LCS

--------

U-234

03

U-234

05
06

U-234

Error Estimate

MDA

8.17E+OO

OK
OK

OK

~-

~---

-------

09
~--

.E

~
0

Q.
Q.
:I
(/)

~I

13

----

14

U-234

TRG

PZ-111-KS TOT

pCi/1

7.02E+OO

1.15E+OO

7.95E-02

OK

15

U-234

TRG

PZ-111-KS DIS

pCi/I

8.15E+OO

1.SOE+OO

1.08E-01

OK

c:
Cll
E

Cll
Cl

--r----~

"'c:

"'

:i
Cl
c:
;:

~---

Cll
Cll

.E
Cl
c:

~--------

------- - - - - - - - - ~-------

Blank
Flag

OK

- - -------

TRG

U-234

Results

---

DUP

-------~

--~

MBL

r - - - - - !---~-------

----------

en

LCS
%R

Activity
Units

04

Sample
Desc

LCS
Known

Client
Identification

~---

Work Order: 13-07149-UUIS0-1

Lab
Fraction

02

c::

::i

Printed: 8/12/2013 2:25 PM

Page 1 of 3

Preliminary Data Report & Analytical Calculations

OK

Eberline Services
Oak Ridge Laboratory

a::

T"'"

Work Order: 13-07149-UUIS0-1

U-234

LCS

07/23/13 00:00

1.00E+OO

95.11

0.00

0.00

U-234

MBL

07/23/13 00:00

1.00E+OO

109.87

0.00

0.00

03

U-234

DUP

07/17/13 10:43

1.00E+OO

93.61

0.00

0.00

04

U-234

TRG

07/16/13 15:30

1.00E+OO

62.23

0.00

0.00

05

U-234

TRG

07/16/13 15:30

1.00E+OO

75.62

0.00

0.00

06

U-234

TRG

07/17/13 10:23

1.00E+OO

21.54

0.00

0.00

07

U-234

TRG

07/17/13 10:23

1.00E+OO

25.87

0.00

0.00

08

U-234

DO

07/17/13 10:43

1.00E+OO

56.19

0.00

0.00

U-234

TRG

07/17/13 10:43

1.00E+OO

61.66

0.00

0.00

U-234

TRG

07/17/13 11:40

1.00E+OO

88.76

0.00

0.00

11

U-234

TRG

07/17/13 11:40

1.00E+OO

86.08

0.00

0.00

12

U-234

TRG

07/17/13 12:15

1.00E+OO

38.24

0.00

0.00

U-234

TRG

07/17/13 12:15

1.00E+OO

57.62

0.00

0.00

14

U-234

TRG

07/17/13 13:09

1.00E+OO

77.94

0.00

0.00

15

U-234

TRG

07/17/13 13:09

1.00E+OO

56.31

0.00

0.00

01
02

Radiometric
%Rec

Mean
%Rec

Sample
Date

Nuclide

Sample
Aliquot

Grav

Sample
Desc

Lab
Fraction

%Rec

SAF

---

---

.!!!

la
c:

"'(

--

fl)

-::::>
::::>

-~

~--

09
~-

10
r------

~------

.E
t:'

13
~-

a.
a.
::s

(/)

jl
u

cCl)

E
Cl)

Cl

~-

~--

---------

Ill

c
Ill
:E

---~--

Cl

;::

--------

Cl)
Cl)

c
c

;,
w
11,,1!!1

~~~

f------- -

Printed: 8/12/2013 2:25 PM

Page 2 of 3

Preliminary Data Report & Analytical Calculations

Sep tO
Date/Time

Sept1
Date/Time

Eberline Services
Oak Ridge Laboratory

,:

Lab

01
------~

02

c::

Nuclide

Fraction

--

T"9

U-234

------
U-234

g
0

03

U-234

04

U-234

,!(!

c;;~

--------~

en

::::>

05

U-234

---

::::>

Work Order: 13-07149-UUIS0-1


I Sample
Desc

-l

Counting
Date/Time

LCS

-----

I
I

Halflife
(days)

Count

Counts

Bkg
CPM

Eff

Detect

Carrier

08/12113 05:37

A_Spec

Alpha_033

170 5.14 E+02

1.00 E-03

18.5

08/12/13 05:37

A_Spec

Alpha_034

170 1.80 E+01

0.00 E+OO

18.6

08/12/13 05:37

A_Spec

Alpha_035

170 1.21 E+02

1.00 E-03

18.3

08/12113 09:40

A_Spec

Alpha_048

170 9.27 E+01

2.00 E-03

16.8

08/12113 05:37

A_Spec

Alpha_037

170 1.25 E+02

2.00 E-03

17.8

08/12/13 05:37

A_Spec

Alpha_038

170 4.83 E+OO

1.00 E-03

17.2

Time

MBL

--r------

Printed: 8/12/2013 2:25 PM

Page 3 of 3

Preliminary Data Report & Analytical Calculations

L~~--

j::~

06

U-234

07

U-234

I T;;

08/12/13 05:37

A_Spec

Alpha_039

170 7.32 E+OO

4.00 E-03

19.7

08

U-234

I DO

08/12/13 05:37

A_Spec

Alpha_040

170 6.67 E+01

2.00 E-03

19

08/12/13 05:37

A_Spec

Alpha_041

170 9.36 E+01

8.00 E-03

19.2

08/12/13 05:37

A_Spec

Alpha_042

170 1.76 E+02

2.00 E-03

18.5

08/12/13 05:37

A_Spec

Alpha_043

170 1.57 E+02

0.00 E+OO

20

I TRG
I

----
f--------------i--

09

TRG

U-234

10

U-234

11

U-234

TRG
-
TRG
-

.5

a.
a.

:I

en

~I

U-234

TRG

08/12/13 05:37

A_Spec

Alpha_044

170 2.28 E+01

1.00 E-03

19.2

13

U-234

TRG

08/12/13 05:37

A_Spec

Alpha_045

170 7.66 E+OO

2.00 E-03

19.1

14

U-234

TRG

08/12/13 05:37

A_Spec

Alpha_046

170 3.69 E+02

1.00 E-03

17.9

15

U-234

08/12/13 05:37

A_Spec

Alpha_047

170 3.15 E+02

1.00 E-03

18.2

....c:

12

Cl>

E
Cl>

Cl

---

l'G

c:

l'G

:a:

..

--

Cl

.5

---------

Cl>
Cl>

.5

Cl

c:
w

tD
~ ....111:

fRG
-r--

-+

--------+-
------------r-----
I

------

-------

,:

c:
::i
ct:

Work Order: 13-07149-UUIS0-1

Lab
Fraction

Nuclide

Sample
Desc

Client
Identification

01

U-238

LCS

LCS

pCi/I

9.35E+OO

1.30E+OO

7.19E-02

02

U-238

MBL

BLANK

pCi/I

1.25E-01

8.17E-02

6.20E-02

U-238

DUP

D-81 TOT

pCi/I

1.30E+OO

3.16E-01

6.45E-02

Activity
Units

Results

Error Estimate

MDA

T""

03

Printed: 8/12/2013 2:25 PM

Page 1 of 3

Preliminary Data Report & Analytical Calculations

Eberline Services
Oak Ridge Laboratory

LCS
Known

7.96E+OO

LCS
%R

LCS
Flag

117.46

OK

RPO
Flag

MDA
Flag

Blank
Flag

OK
OK
OK

OK

OK

- -------

~
0

.!!,!

].
~

c:

q:

en

-::::>

::::>

...

.g
d

U-238

TRG

PZ-302-AS TOT

pCi/I

1.44E+OO

4.32E-01

1.52E-01

OK

05

U-238

TRG

PZ-302-AS DIS

pCi/I

1.39E+OO

3.73E-01

1.18E-01

OK

06

U-238

TRG

LR-100 TOT

pCi/I

1.18E-01

2.02E-01

3.41E-01

OK

--------

07

U-238

08

U-238
-~--

09

~
~

TRG

LR-100 DIS

pCi/I

7.75E-02

1.48E-01

2.73E-01

OK

DO

D-81 TOT

pCi/I

1.39E+OO

4.17E-01

1.48E-01

OK

TRG

D-81 DIS

pCi/I

1.80E+OO

4.68E-01

1.59E-01

OK

--

U-238
--

10

U-238

TRG

PZ-204-SS TOT

pCi/I

1.73E+OO

3.88E-01

1.02E-01

OK

11

U-238

TRG

PZ-204-SS DIS

pCi/I

1.SOE+OO

3.46E-01

9.19E-02

OK

12

U-238

TRG

LR-103 TOT

pCi/I

6.42E-01

3.19E-01

1.SOE-01

OK

tJ

13

U-238

TRG

LR-103 DIS

pCi/I

1.36E-01

1.18E-01

1.15E-01

OK

14

U-238

TRG

pCi/I

2.41E+OO

5.21E-01

1.14E-01

OK

pCi/I

3.47E+OO

7.77E-01

1.23E-01

OK

"

...
..
~
-~

Cl)

E;
't:

.E
0

Q.
Q.

:l

(/)

~I

04

c
Cl)
E
Cl)

Cl

15

----------1----
U-238

TRG

--------

PZ-111-KS TOT
-

_l
I

PZ-111-KS DIS

--

CIS

c
CIS
:ill
Cl

;::
Cl)
Cl)

o,
c
w
ti,:~i

~"lit

U)
~~.)

- - - - - -r - - - - - - - - - - -

,__ ______

Lab

--

LCS

07/23/13 00:00

1.00E+OO

95.11

0.00

0.00

U-238
02
________ ______
U-238
03

MBL

1.00E+OO

109.87

0.00

0.00

DUP

07/23/13 00:00
------
07/17/13 10:43

1.00E+OO

93.61

0.00

0.00

U-238

TRG

07/16/1315:30

1.00E+OO

62.23

0.00

0.00

U-238

TRG

07/16/13 15:30

1.00E+OO

75.62

0.00

0.00

.!!!

~
iii

c:

"(

TRG

07/17/13 10:23

1.00E+OO

21.54

0.00

0.00

TRG

07/17/13 10:23

1.00E+OO

25.87

0.00

0.00

U-238

DO

07/17/13 10:43

1.00E+OO

56.19

0.00

0.00

U-238

TRG

07/17/13 10:43

1.00E+OO

61.66

0.00

0.00

10

U-238

TRG

07/17/13 11:40

1.00E+OO

88.76

0.00

0.00

11

U-238

TRG

07/17/1311:40

1.00E+OO

86.08

0.00

0.00

12

U-238

TRG

07/17/13 12:15

1.00E+OO

38.24

0.00

0.00

U-238

TRG

07/17/13 12:15

1.00E+OO

57.62

0.00

0.00

14

U-238

TRG

07/17/13 13:09

1.00E+OO

77.94

0.00

0.00

15

U-238

TRG

07/17/13 13:09

1.00E+OO

56.31

0.00

0.00

-----------

05
--

---------

~----

- ~-~--i
07

-----------

08
09

SAF

-----

04

::>
::>

%Rec

Sep to
Date/Time

U-238

- U-238
--

-t

--+-----
r
-

----

.E

13
---------

a.
a.
:i

Cl)

.....c:

Q)

~I

E
Q)
Ol
nl

c:

nl

:ii:

--

,____

Ol

c:

;:::
Q)
Q)

.!:

Ol

c:

w
~ial
~~II

UJI
~~.J;

____

Sept1
Date/Time

""---

____..;,...

---------

CJ)

Mean
%Rec

Grav

U-238

-----------

Radiometric
%Rec

Sample
Date

01
~

Sample
Aliquot

Sample
Desc

-- ---------

a:

Work Order: 13-07149-UUIS0-1

Nuclide

Fraction

Printed: 8/12/2013 2:25 PM

Page 2 of 3

Preliminary Data Report & Analytical Calculations

Eberline Services
Oak Ridge Laboratory

--------

Eberline Services
Oak Ridge Laboratory

a:

Work Order: 13-07149-UUIS0-1

Lab
Fraction

Nuclide

Sample
Desc

Counting
Date/Time

01

U-238

LCS

U-238

02
T

Printed: 8/12/2013 2:25 PM

Page 3 of 3

Preliminary Data Report & Analytical Calculations

Halflife
(days)

Count
Time

Counts

Bkg
CPM

Eff

Detect

Carrier

08/12/13 05:37

A_Spec

Alpha_033

170 6.22 E+02

2.00 E-03

18.5

MBL

08/12/13 05:37

A_Spec

Alpha_034

170 9.66 E+OO

2.00 E-03

18.6

DUP

08/12/13 05:37

A_Spec

Alpha_035

170 8.38 E+01

1.00 E-03

18.3

08/12113 09:40

A_Spec

Alpha_048

170 5.70 E+01

0.00 E+OO

16.8

08/12/13 05:37

A_Spec

Alpha_037

170 7.10 E+01

0.00 E+OO

17.8

TRG

08/12/13 05:37

A_Spec

Alpha_038

170 1.66 E+OO

2.00 E-03

17.2

TRG

08/12/13 05:37

A_Spec

Alpha_039

170 1.49 E+OO

3.00 E-03

19.7

DO

08/12/13 05:37

A_Spec

Alpha_040

170 5.60 E+01

0.00 E+OO

19

TRG

08/12/13 05:37

A_Spec

Alpha_041

170 8.05 E+01

9.00 E-03

19.2

TRG

08/12/13 05:37

A_Spec

Alpha_042

170 1.07 E+02

6.00 E-03

18.5

08/12/13 05:37

A_Spec

Alpha_043

170 9.80 E+01

0.00 E+OO

20

08/12/13 05:37

A_Spec

Alpha_044

170 1.78 E+01

1.00 E-03

19.2

08/12/13 05:37

A_Spec

Alpha_045

170 5.66 E+OO

2.00 E-03

19.1

08/12/13 05:37

A_Spec

Alpha_046

170 1.27 E+02

0.00 E+OO

17.9

TRG
08/12/13 05:37
- ----- ,........ ...

A_Spec

Alpha_047

170 1.35 E+02

2.00 E-03

18.2

-----~-

03

U-238

--

.g
0

u
.!!!

"'
ct
I:

04

I TRG

U-238

--

en

05

::::>
::::>

06

U-238

07

U-238

TRG

U-238

08

U-238

09

U-238

10

U-238

-~~---

--

11

U-238

TRG

12

U-238

TRG
~-

.E

t!

0
0.
0.
:::l

"'-

13

TRG

U-238

---

14

U-238

15

U-238

c:

TRG

Q)

~I

E
Q)

Cl
CG
CG

:ii:
Cl

c:
't:
Q)
Q)

c:

'Ci
c:

w
11:1.~
11.'i~
~lJ
~.':nai,

----~--

--+

c:

~--

~-

+--~

~-------+-----

--

~-

Eberline Services
Oak Ridge Laboratory

Lab
Fraction

I
1

01

Work Order: 13-07149-UUIS0-1

Nuclide

Sample
Desc

Client
Identification

Activity
Units

U-235

LCS

LCS

pCi/I

1.19E+OO

3.22E-01

8.91E-02

U-235

MBL

BLANK

pCi/I

1.45E-01

1.01E-01

9.63E-02

Printed: 8/12/2013 2:25 PM

Page 1 of 3

Preliminary Data Report & Analytical Calculations

Results

Error Estimate

MDA

LCS
%R

LCS
Known

LCS
Flag

RPO
Flag

MDA
Flag

Blank
Flag

OK

------- ---------

02
T"9

03

8
.~

i;j
i::

q:

:::>

UJ

:::>

INV

OK

pCi/I

2.87E-01

1.54E-01

1.15E-01

PZ-302-AS TOT

pCi/I

6.21E-01

2.89E-01

1.31E-01

OK

TRG

PZ-302-AS DIS

pCi/I

4.62E-01

2.21E-01

1.46E-01

OK

U-235

TRG

LR-100 TOT

pCi/I

O.OOE+OO

2.45E-01

5.30E-01

OK

U-235

TRG

LR-100 DIS

pCi/I

3.11E-01

2.90E-01

2.69E-01

OK

U-235

DO

D-81 TOT

pCi/I

7.31E-01

3.13E-01

1.28E-01

OK

U-235

TRG

D-81 DIS

pCi/I

1.28E+OO

4.12E-01

1.56E-01

OK

U-235

TRG

PZ-204-SS TOT

pCi/I

4.40E-01

1.95E-01

1.20E-01

OK

U-235

TRG

PZ-204-SS DIS

pCi/I

2.85E-01

1.53E-01

1.14E-01

OK

U-235

TRG

LR-103 TOT

pCi/I

5.28E-01

3.16E-01

1.86E-01

OK

U-235

TRG

LR-103 DIS

pCi/I

1.19E-01

1.32E-01

1.79E-01

OK

U-235

TRG

PZ-111-KS TOT

pCi/I

8.18E-01

2.92E-01

9.80E-02

OK

U-235

TRG

PZ-111-KS DIS

pCi/I

9.90E-01

3.83E-01

1.91E-01

OK

U-235

DUP

D-81 TOT

04

U-235

TRG

05

U-235

06

- ----------

OK

------------ - ------

-----

07
t-----~-----

t-----

08
~-

,_

09
____

!------

10
-----

1---

11
12

----

.E

--

13
I

~:+-
------]
0

Q.
Q.

:s

(/)

QI

~I

QI

Cl
I'll

c
I'll
:!!

Cl

;::
QI
QI

.5

Cl

w
it:t,'JI
CF.~

!--------------

----~--

___L__
I

,_______j____ ----
------ -----r-I - ___ _. ----

I
I

--

..

1-

OK

Eberline Services
Oak Ridge Laboratory

a:

Lab

01

----

03

.!I!

~
iii
c:
c:(

-::::>
::::>

LCS

07/23/13 00:00

1.00E+OO

95.11

0.00

0.00

SAF

U-235

MBL

07/23/13 00:00

1.00E+OO

109.87

0.00

0.00

U-235

DUP

07/17/13 10:43

1.00E+OO

93.61

0.00

0.00

TRG

07/16/13 15:30

1.00E+OO

62.23

0.00

0.00

~-

04

Mean
%Rec

Grav
%Rec

Sample
Date

- f - - - - -

U-235

- - - - c-----

------c--

en

Sample
Aliquot

Radiometric
%Rec

Desc

------- - - -

----

Sample

U-235
~-

02
~

Work Order: 13-07149-UUIS0-1

Nuclide

Fraction

05

U-235

TRG

07/16/1315:30

1.00E+OO

75.62

0.00

0.00

U-235

TRG

07/17/13 10:23

1.00E+OO

21.54

0.00

0.00

U-235

TRG
---

07/17/13 10:23

1.00E+OO

25.87

0.00

0.00

DO

07/17/13 10:43

1.00E+OO

56.19

0.00

0.00

07/17/13 10:43

1.00E+OO

61.66

0.00

0.00

TRG

07/17/13 11:40

1.00E+OO

88.76

0.00

0.00

06
~------

---

07
--

~---------

08

U-235

- - - -- - - - - - - - - - - - - - - --

09

U-235

TRG

- - - - - --

10

U-235

------ --------

11

U-235

TRG

07/17/13 11:40

1.00E+OO

86.08

0.00

0.00

12

U-235

TRG

07/17/13 12:15

1.00E+OO

38.24

0.00

0.00

13

U-235

07/17/1312:15

1.00E+OO

57.62

0.00

0.00

TRG

07/17/13 13:09

1.00E+OO

77.94

0.00

0.00

TRG

07/17/13 13:09

1.00E+OO

56.31

0.00

0.00

- - - - -f-

.5

U-235

c..
c..

------- r------------

-------

Q)

----

:l

CJ)

~1
u

14

s:::
Q)
E

Cl

15

U-235
-

---

CG

s:::

CG

:ail

-------~

----

Cl

s:::

;::

- - - - - -------

Q)
Q)

.5

Cl

s:::

- - - -r---

TRG
- ----

1--------~i---

Printed: 8/12/2013 2:25 PM

Page 2 of 3

Preliminary Data Report & Analytical Calculations

~-

SeptO
Date/Time

Sep t1
Date/Time

0::

Lab

Fraction

01

Nuclide

Sample
Desc

Counting
Date/Time

U-235

LCS

02

U-235

MBL

03

U-235

DUP

- - - - - --

.!Q

::::>
::::>

Count
Time

Counts

Bkg
CPM

Eff

Detect

Carrier

08/12/13 05:37

A_Spec

Alpha_033

170 6.37 E+01

2.00 E-03

18.5

08/12/13 05:37

~-Spec

Alpha_034

170 9.00 E+OO

0.00 E+OO

18.6

A_Spec

Alpha_035

170 1.50 E+01

0.00 E+OO

18.3

T A _Spec

Alpha_048

170 1.98 E+01

1.00 E-03

16.8

A_Spec

Alpha_037

170 1.90 E+01

0.00 E+OO

17.8

A_Spec

Alpha_038

170 1.00 E+OO

0.00 E+OO

08/12/13 05:37

-------

U-235

TRG

08/12/13 09:40

05

U-235

06

U-235

TRG

I
i

----

CJ)

Halflife
(days)

>------------

f------~---

Work Order: 13-07149-UUIS0-1

- - - - f---

04

Printed: 8/12/2013 2:25 PM

Page 3 of 3

Preliminary Data Report & Analytical Calculations

Eberline Services
Oak Ridge Laboratory

08/12/13 05:37

I
I

TRG

08/12/13 05:37

17.2

~------

07

U-235

TRG

08/12/13 05:37

A_Spec

Alpha_039

170 4.83 E+OO

1.00 E-03

19.7

08

U-235

DO

08/12/13 05:37

A_Spec

Alpha_040

170 2.38 E+01

1.00 E-03

19

09

U-235

TRG

08/12/13 05:37

A_Spec

Alpha_041

170 4.63 E+01

4.00 E-03

19.2

10

U-235

TRG

08/12/13 05:37

A_Spec

Alpha_042

170 2.20 E+01

0.00 E+OO

18.5

11

U-235

TRG

08/12/13 05:37

A_Spec

Alpha_043

170 1.50 E+01

0.00 E+OO

20

12

U-235

TRG

08/12/13 05:37

A_Spec

Alpha_044

170 1.18 E+01

1.00 E-03

19.2

13

U-235

TRG

08/12/13 05:37

A_Spec

Alpha_045

170 4.00 E+OO

0.00 E+OO

19.1

14

U-235

TRG

08/12/13 05:37

A_Spec

Alpha_046

170 3.48 E+01

1.00 E-03

17.9

15

U-235

TRG

08/12/13 05:37

A_Spec

Alpha_047

170 3.10 E+01

0.00 E+OO

18.2

.E
0

c.
c.
:::s

"'....c
<II

c:

~I

<II
Cl

r----

('IS

('IS

-----~

--- - - -

~-------

Cl

;::

-----

<II
<II

=c

Cl

Clr~I
~!ii

...

UJ!

------

-- -----

-----

-------

+
I

- - ,__

Count Room Report


Client: Engineering Management Su

13-07149-UUIS0-1 (pCi/I) in WA
Tracer ID: U-1 Oa

Printed: 8/9/2013 6:54 AM


Page 1of1

/l1y\./'
:

.
1>"'"'

Internal
Fraction

Sample
Desc

Client
ID

Sample
Date

01

LCS

LCS

07/23/13 00:00

02

MBL

BLANK

07/23/13 00:00

Tracer
Aliquot(g)

Sample
Aliquot

Tracer
ACT(dpm)

1.0000

0.6131

11.6747

1.0000

0.6051

11.5223

II

Radiometric I
I
%Rec

Radiometric
Tracer (pCi)

0.00

SAF

SAF
2*

0.00
I

- -----------

03

DUP

D-81 TOT

07/17/13 10:43

1.0000

0.6057

11.5337 I

0.00

04

TRG

PZ-302-AS TOT

07/16/13 15:30

1.0000

0.6025

11.4728

0.00

05

TRG

PZ-302-AS DIS

07/16/13 15:30

1.0000

0.6027

11.4766

0.00

06

TRG

LR-100 TOT

07/17/13 10:23

1.0000

0.6005

11.4347

0.00

07

TRG

LR-100 DIS

07/17/13 10:23

1.0000

0.6011

11.4461

0.00 i

11.4995

0.00
0.00

08

DO

D-81 TOT

07/17/13 10:43

1.0000

0.6039

09

TRG

D-81 DIS

07/17/13 10:43

1.0000

0.6016

11.4557

10

TRG

PZ-204-SS TOT

07/17/1311:40

1.0000

0.6021

11.4652

0.00 i

11

TRG

PZ-204-SS DIS

07/17/13 11 :40

1.0000

0.6020

11.4633

0.00

12

TRG i
TRG

LR-103 TOT

07/17/13 12:15

1.0000

0.6010

11.4442

0.00

LR-103 DIS

07/17/13 12:15

1.0000

0.5979

11.3852

0.00 :

13

14
---~-----

15

TRG
!-------

--

PZ-111-KS TOT

----+-

TRG

----~-------------

PZ-111-KS DIS

07/17/13 13:09
--------

"

1.0000

~-----~--

0.5994

11.4138

0.00

0.5993

11.4119 I

o.oo

------~

07/17/13 13:09

1.0000

I
t

i
I

-r
I

- I

!
i

I
fJi:;:jl

"~
itt.~
())1

Eberline Services
Oak Ridge Laboratory

Isotope

U-234
U-238

Sol#

I
I

U-8a
U-8a

Page 1of1
Printed: 8/5/2013 9:21 AM

Spike and Tracer Worksheet

Activity
dpm/g

35.240
34.350

Solution
Date

Approx
Addition

8/5/2013

0.500

8/5/2013

Analysis Code

Date

Technician

UUISO

8/5/2013 9:20

JWOLFE

LCS

M$

LCSD

MSD

Volume
Used(g)

Volume
Used(g)

Volume
Used(g)

Volume
Used(g)

------

0.500

0.5144

Known
pCi

Error
Estimate

0.294

-u:so

MS

LCS ... ... .

8.17

0.5144

------------

Technician Initials

Added
pCi

0.00

Error
Estimate

0000
--

7.96

0.287

oooi

Known
pCi

Witness Initials

Error
Estimate

.....

Activity
dpmlg

Solution
Date

Volume
Used(g)

Approx
Addition

fraction

Isotope

Sol#

000

0.000

0.00

0.000

0000

0.00

0.000

0.00

ooool

01

U-232

U-10a

19.042

8/5/2013

o,6131

02

U-232

U-10a

19.042

8/5/2013

0.6051

0.6300

03

U-232

U-10a

19.042

8/5/2013

0.6057

0.6300

U-232

U-10a

19.042

8/5/2013

0.6025

0.6300

U-232

U-10a

19.042

8/5/2013

0.6027

0.6300

U-232

U-10a

19.042

8/5/2013

o.60()5

0.6300

U-232

U-10a

19.042

8/5/2013

0.601.1

0.6300

U-232

U-10a

19.042

8/5/2013

0.6039

0.6300

09

U-232

U-10a

19.042

8/5/2013

0;6016

0.6300

10

U-232

U-10a

19.042

8/5/2013

0.6021

0.6300

11

U-232

U-10a

19.042

8/5/2013

0.6020

0.6300

12

U-232

U-10a

19.042

8/512013

0.6010

0.6300

13

U-232

U-10a

19.042

8/5/2013

0.5979

0.6300

U-232

U-10a

19.042

8/5/2013

0.5994

0.6300

U-232

U-10a

19.042

8/5/2013

0.599~

0.6300

----------
-

04

05
06

07

II

08

i----~------

-------

15

---

i:il.~

tit1
(.~~

UJ!

Version 2.0 08/99

LCS

0.6300

~-

14

Balance Printer Tapes


Tracer

Error
Estimate

----

------t------r-------+------+-------1f--------+--------+--------1f--------+ -----+--------0------t

.. ................. Tracers

MSD

Added
pCi

''

Matrix Spike

Eberline Analytical
Oak Ridge Laboratory

Lab
Fraction
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15

Engineering Management Support, Inc.

----

Sample

Client ID
LCS
BLANK
D-81 TOT
PZ-302-AS TOT
PZ-302-AS DIS
LR-100TOT
LR-100 DIS
D-81 TOT
D-81 DIS
PZ-204-SS TOT
PZ-204-SS DIS
LR-103 TOT
LR-103 DIS
PZ-111-KS TOT
PZ-111-KS DIS

Analysis Code

Rpt Units

Lab Deadline

Technician

Thi SO

liters

8/13/2013

JWOLFE

Dilution Data

Muffle Data
.~~iq;

Type
LCS
MBL
DUP
TRG
TRG
TRG
TRG
DO
TRG
TRG
TRG
TRG
TRG
TRG
TRG

..

Pos.~~

.
.

No of Oils

Oil Factor

...

,.

"

Ratio

... :::

,.

...

.,

..

..

\.... 1:::; '


.. ., .
.

. .

...

..

.. . "........

.. : .<:
.
.

...

..

.;

...
.

.:

..

lfdit~
ft.1r.Ji.

Com~nts

Tectm;cian

Aliquot
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO

Aliquot

NetEq1;1iv.

"

Net Equiv

H-3 Solids Only


Water Added
(ml)

H3 Dist
Aliq

1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO.
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.ooooe+~
1.0000E+OO

1.ooooe+oo
1.ooooe+ao

__j

---

-----

1.0000E+OO

1.0000E+OO
1.0000E+OO

1.ooooe+00
1.0000E+OO

1.0000E+OO

1.0000E+Oa

-------

----

"

MS Aliquot Data

Aliquot Data

Printed: 8/5/2013 9:20 AM

Page 1of1

Aliquot Worksheet

"

.
..

._:JW;:i~ate

?, Ii)

16fill()

Sample Description:

Spectrum File:

Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

SPIKE
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000658
1307149A-UU
01
Shelf 2
U iso

Detector Name:

Alpha_033
Chamber Serial Number:

04026479A
Detector Serial Number:
91132
Env. Background:

System Bkgd 64781


Reagent Blank:

<not performed>
Sample Size:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

l.OOOE+OOO +/- O.OOOE+OOO liter

7:22:35 AM

8/12/2013
5:37:29 AM

8/12/2013
170.0 minutes
176.3 minutes

Tracer Certificate:

Tracer Quantity:

Effective Efficiency:

Counting Efficiency:

Chem. Recovery Factor:

U232 UU-lOA
0.613 mL
0.1758 +/- 0.0103
0.1848 +/- 0.0032 on 7/20/2013
0.9511 +/- 0.0580

Control Certificate Name:


NatU U-8A

Chem. Recov. of Control:


U-238
Peak Match Tolerance:

0.150 MeV

PEAK
Energy
(MeV)

Nuclide
U-232
U-234
U-235
U-238

5.285
4.741
4.405
4.161
T

Net
Pk Area
346.83
513.83
63.66
621.66

5.646925 +/-

AREA

2:31:30 PM

0.434635

REPORT

Pk Area
Error %

Ambient
Backgnd

Reagent
Backgnd

FWHM
(keV)

10.53
8.65
24.64
7.86

0.17
0.17
0.34
0.34

O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

26.2
36.8
3.7
25.8

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS

Nuclide

Id
Conf.

Energy
(keV)

U-232
U-234
U-235
U-238

0.998
0.997
0.997
0.996

5302.50*
4761.50*
4385.50*
4184.40*

Activity
(pCi/liter )
5.24E+OOO
7.76E+OOO
l.19E+OOO
9.35E+OOO

+/
+/
+/
+/

6.00E-001
l.llE+OOO
3.22E-001
l.30E+OOO

~fc}(r~

MDA
(pCi/liter
6.30E-002
6.30E-002
8.91E-002
7.19E-002

+/
+/
+/
+/

7.22E-003
7.22E-003
1. 02E-002
8.23E-003

0000065854.CNF

Live Time 10200.000 sec


Real Time 10579.500 sec
Start:
1 3447. 3(kev)
Stop : 1024 6496. 6(kev)
Acq. Start Mon Aug 12 05: 37: 29 2013

60

55

50

45

40

35
Vl

+-'
s:::
::s

8 30

25

1
1

20
15
10

3500
I

4500

4000

t'f1'
~"""'

ijijlta1

"''"

ROI Type: 1

5000
Energy(kev)

6000

5500
ROI Type: 3

6500

Channel Data Report

8/12/2013

Page

8:36:47 AM

*******************************************************
s p E C T R A L DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

01

Elapsed Live time:


Elapsed Real Time:

10200

10580

Channell------l-------l-------1-------1-------l-------l-------l-------I
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:

0
2
0
0
0
0
0
0
0
0
0
0
0
1
2
0
1
0
1
1
0
0
0
1
3
2
2
4
8
8
14
22
19
0
1
0
0
1
2
0
3
1
1
2
0
0

1
0
0
1
0
0
0
0
0
0
0
0
0
2
0
0
1
0
1
1
1
0
2
1
0
2
2
5
4
8
14
23
21
1
0
0
0
1
2
1
1
0
1
0
2
1

0
0
1
0
0
1
3
0
1
1
1
0
0
1
0
0
0
0
0
2
2
2
1
1
5
1
1
4
5
8
13
14
19
1
2
0
1
2
0
0
1
2
0
1
2
3

0
0
0
0
2
1
2
0
1
1
0
0
0
1
1
2
1
0
2
1
2
1
3
3
0
2
6
9
3
17
12
21
14
0
1
2
0
1
1
1
3
0
0
0
0
1

0
0
0
1
0
0
0
0
0
0
1
2
0
2
0
0
0
1
0
2
1
3
0
3
4
0
4
6
5
9
14
30
6
0
1
0
0
2
1
0
0
0
3
1
1
0

0
0
1
0
1
1
1
0
0
1
1
1
0
1
1
0
1
0
0
1
1
3
3
3
2
2
5
0
4
8
14
21
8
0
0
2
0
0
2
0
3
3
0
2
0
3

0
0
1
0
0
0
1
0
2
0
0
0
1
0
2
0
0
1
1
1
3
0
2
1
2
2
3
7
6
8
10
22
2
0
2
0
0
1
0
1
0
0
1
0
2
2

1
1
1
0
1
0
1
0
0
1
1
1
1
1
0
1
0
3
0
3
5
1
3
6
0
2
3
8
10
13
14
25
2
2
2
1
3
1
0
3
1
1
1
2
3
2

S1:S3

Channel Data Report


369:

8/12/2013
7

Sample Title:

Page

8:36:47 AM
0

01

Channell------l-------l-------l-------l-------1-------1-------1-------I
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:
625:
633:
641:
649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:

1
0
1
2
2
8
6
15
7
26
4
0
0
1
0
1
0
0
0
2
1
0
1
1
2
1
3
0
5
1
10
8
8
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

2
2
2
4
4
4
8
6
16
16
1
0
1
0
0
0
1
0
0
1
1
0
1
2
1
1
0
0
3
9
12
9
12
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

3
3
2
3
1
6
6
8
15
15
1
0
1
0
0
0
0
0
0
2
0
1
1
1
0
3
6
2
4
8
6
8
8
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

3
3
2
0
7
7
6
16
21
14
1
0
0
0
1
2
1
0
0
0
1
2
2
1
1
1
1
4
6
6
11
12
12
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
1
1
4
3
2
5
7
19
16
0
1
0
1
0
1
0
0
1
1
1
0
1
2
1
0
3
3
3
4
6
11
7
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
2
0
2
5
8
7
20
16
13
0
0
1
0
0
1
2
1
1
0
1
2
0
2
2
2
2
1
2
9
11
6
6
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

3
2
2
4
2
4
8
9
14
12
0
1
0
0
1
0
0
0
1
0
2
1
0
1
3
1
1
5
5
5
13
6
9
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

4
2
3
4
3
5
12
9
15
3
1
0
0
0
0
0
1
0
0
0
0
0
1
2
1
1
2
3
4
6
8
7
5
0
0
0
1
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0

1f!L4

Channel Data Report


801:

8/12/2013
0

Sample Title:

Page

8:36:47 AM
0

01

Channell------l-------l-------1-------1-------1-------l-------l-------I
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
1
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

81

.~~Apex-Alpha
Sample Description:
Spectrum File:
Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

BLANK
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000658
1307149A-UU
02
Shelf 2
U iso

Detector Name:

Alpha_034
Chamber Serial Number:

04026479B
Detector Serial Number:
91136
Env. Background:

System Bkgd 64782


Reagent Blank:

<not performed>
Sample Size:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

l.OOOE+OOO +/- O.OOOE+OOO liter


8/12/2013
7:22:35 AM
8/12/2013
5:37:30 AM
170.0 minutes
176.3 minutes

Tracer Certificate:

Tracer Quantity:

Effective Efficiency:

Counting Efficiency:

Chem. Recovery Factor:

U232 UU-lOA
0.605 mL

0.2039 +/- 0. 0113

0.1856 +/- 0.0032 on 12/16/2012


1. 0987 +/- 0.0637

Peak Match Tolerance:

0.150 MeV

PEAK
Energy
(MeV)

Nuclide
U-232
U-234
U-235
U-238

5.285
4.723
4.374
4.157

Net
Pk Area

AREA

REPORT

Pk Area
Error %

397.00
18.00
9.00
9.66

5:49:43 PM

Ambient
Backgnd

9.85
47.46
68.87
64.35

0.00
0.00
0.00
0.34

Reagent
Backgnd

FWHM
(keV)

O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

12.1
3.0
3.0
5.9

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS

Nuclide

Id
Conf.

Energy
(keV)

U-232
U-234
U-235
U-238

0.998
0.989
0.999
0.995

5302.50*
4761.50*
4385.50*
4184.40*

Activity
(pCi/liter )
5.17E+OOO
2.34E-001
l.45E-001
1.25E-001

+/
+/
+/
+/

5.60E-001
l.14E-001
1. OlE-001
8.17E-002

AG

8/t;tffj

MDA
(pCi/liter
7.81E-002
7.81E-002
9.63E-002
6.20E-002

+/+/+/+/-

8.46E-003
8.46E-003
1. 04E-002
6.72E-003

0000065855.CNF

Live Time 10200.000 sec


Real Time 10579.500 sec
start:
1 3439.l(kev)
Stop : 1024 6479. 9(kev)

Acq. Start Mon Aug 12 OS: 37: 30 2013

60
55

50

45

40

35

.....,
V)

s:::
::::s

8 30

25

20

15

10

d:,1

ll !_I\

!t i

A!~I

!t I
.

~'~ ~

ii'

ii

I i~ Mft tJV\ I~

")

3500

4000

4500

5000
Energy(kev)

6000

5500

lrul!
ii'~"'

ROI Type: 1

ROI Type: 3

Channel Data Report

8/12/2013

Page

8:36:56 AM

*******************************************************
s p E C T R A L DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

02

Elapsed Live time:


Elapsed Real Time:

10200
10580

Channell------1-------1-------1-------l-------l-------l-------l-------I
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:

0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
1
0
1
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
1
1
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
2
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2
0
0
1
0
1
0
1
0
0
1
0
0
0
0
1

m1:S

Channel Data Report


369:

8/12/2013
0

Sample Title:

8;}6i
0

w
1

Page
1

02

Channell------l-------l-------1-------1-------1-------l-------l-------I
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:
625:
633:
641:
649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:

0
0
1
0
0
0
0
0
0
0
0
1
0
0
1
0
0
1
0
0
0
2
1
0
2
0
1
3
1
3
10
10
7
5
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
2
0
0
0
0
0
0
0
0
0
0
1
0
0
1
0
0
0
1
0
0
1
1
0
3
5
2
6
9
19
3
0
0
0
0
0
0
0
0
0
1
0
0
0
0
1
0
0
0
0

0
0
0
0
0
0
0
0
0
0
1
0
0
0
1
0
0
0
1
2
1
0
2
0
3
0
0
4
4
6
10
4
13
3
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
1
0
0
0
1
0
0
0
0
1
0
0
1
0
0
1
1
0
1
0
1
1
1
3
3
4
8
12
6
24
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0

0
0
0
1
0
0
0
0
0
0
1
0
0
0
0
0
0
1
1
0
0
1
1
1
1
2
2
2
4
7
11
13
17
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
2
0
0
0
1
0
1
1
0
0
1
0
0
0
0
0
1
1
0
0
1
0
2
3
2
4
6
10
7
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
1
0
0
1
0
2
0
1
1
0
1
1
1
0
0
2
4
2
1
4
5
9
11
14
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
1
0
0
0
0
0
0
1
0
1
0
0
0
0
0
0
1
0
1
0
1
1
3
1
2
1
1
8
12
9
16
9
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

6189

Channel Data Report


801:

8/12/2013
0

Sample Title:

Page

8:36:56 AM
0

02

Channell------l-------l-------l-------l-------1-------1-------1-------I
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:

D-81 TOT-DUP
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000658
1307149A-UU
03
Shelf 2
U iso

Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:

Alpha_035
04026477A
58771
System Bkgd 64783
<not performed>

Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:

l.OOOE+OOO +/ O.OOOE+OOO liter


7/17/2013
7:22:35 AM
8/12/2013
5:37:32 AM
170.0 minutes
176.3 minutes

Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chem. Recovery Factor:

U232 UU-lOA
0.606 mL
0.1709 +/ 0.0102
0.1826 +/ 0.0032 on 12/16/2012
0.9361 +/ 0.0581

Peak Match Tolerance:

0.150 MeV

PEAK
Energy
(MeV)

Nuclide
U-232
U-234
U-235
U-238

5.279
4.733
4.389
4.154
T

Net
Pk Area

AREA

REPORT

Pk Area
Error %

333.15
120.83
15.00
83.83

5:49:42 PM

10.75
17.85
52.27
21. 43

Ambient
Backgnd
0.85
0.17
0.00
0.17

FWHM
(keV)

Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

13.7
3.4
2.9
5.1

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS

Nuclide

Id
Conf.

Energy
(keV)

U-232
U-234
U-235
U-238

0.996
0.994
1. 000
0.993

5302.50*
4761.50*
4385.50*
4184.40*

Activity
(pCi/liter )
5.18E+OOO
l.88E+OOO
2.87E-001
l.30E+OOO

+/
+/
+/
+/

6.04E-001
4.00E-001
1. 54E-001
3.16E-001

MDA
(pCi/liter
9.31E-002
6.48E-002
l.15E-001
6.45E-002

+/
+/
+/
+/

l.09E-002
7.56E-003
l.34E-002
7.53E-003

gfr>{r3

uU11

0000065850.CNF

Live Time 10200.000 sec


Real Time 10579.600 sec
start:
1 3463.4(kev)
stop : 1024 6473.5(kev)
Acq. Start Mon Aug 12 05: 37: 32 2013

60
55

50

45

40

35

Vl
.j...J

c:

:::J

8 30

25

20

15

10

3500
I

4000

4500

5000
Energy(kev)

5500

6000

t~

R-'

"'t..:Ji""'

ROI Type: 1

ROI Type: 3

Channel Data Report

8/12/2013

Page

8:37:06 AM

*******************************************************
s p E C T R A L DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

03

Elapsed Live time:


Elapsed Real Time:

10200

10580

Channell------l-------1-------1-------1-------l-------l-------l-------I
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
1
0
1
0
0
0
0
1
0
4
3
2
0
0
0
1
1
0
0
1
0
0
0
0
1
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
1
0
0
1
2
0
1
0
1
2
0
2
1
0
0
0
0
0
0
2
0
1
0
2
0

0
0
0
0
0
0
1
0
1
0
0
0
0
1
0
0
0
0
0
0
0
1
0
1
0
0
1
1
0
0
2
2
2
0
0
0
0
0
0
0
0
0
0
0
0
0

0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
2
0
0
2
1
3
0
2
6
0
0
0
0
2
0
1
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
1
0
0
0
1
0
0
0
0
0
1
1
0
1
1
0
1
0
1
1
2
1
3
0
0
0
0
0
1
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
1
0
1
1
1
0
0
0
1
0
0
1
1
0
2
2
0
1
0
0
0
1
0
0
0
0
0
0
1
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
1
2
0
3
1
1
3
1
0
0
0
0
0
1
0
0
0
0
0
1
0

0
1
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
1
1
0
0
1
0
0
1
1
2
1
0
0
2
0
1
0
0
1
1
0
0
0
0
0
1
1

li113

Channel Data Report


369:

8/12/2013
1

Sample Title:

Page

8:37:06 AM
1

03

Channell------l-------l-------l-------1-------1-------1-------l-------I
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:
625:
633:
641:
649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:

0
2
0
1
1
0
2
1
2
1
2
0
0
0
1
0
0
1
2
0
0
1
0
2
1
0
3
3
5
4
6
9
5
6
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
1
1
3
0
1
3
3
2
3
1
0
0
1
0
0
1
0
1
0
1
1
1
3
2
1
0
2
4
7
3
9
8
5
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

2
0
0
3
2
0
3
3
1
1
3
0
1
1
1
1
3
0
1
1
0
2
0
1
1
2
2
2
4
3
9
6
10
2
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
2
1
1
3
1
2
0
0
1
1
0
0
2
0
0
1
1
1
0
3
2
1
7
1
3
7
10
8
3
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
2
3
4
4
1
3
0
0
1
1
0
0
2
0
0
1
0
0
0
0
2
3
1
3
4
5
10
12
5
4
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
1
0
3
0
2
4
4
3
2
0
0
0
0
0
0
2
4
2
2
0
2
1
1
1
5
4
5
4
9
7
8
2
1
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
2
3
4
2
0
2
1
1
0
0
0
0
0
0
0
0
1
1
2
0
2
2
2
3
1
5
3
7
7
8
8
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
0
2
0
3
0
1
2
7
2
0
1
1
0
0
1
0
0
1
1
0
0
1
1
4
2
2
2
4
3
7
5
5
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

5114

Channel Data Report


801:

8/12/2013
0

Sample Title:

Page

8:37:06 AM
0

03

Channell------l-------l-------1-------1-------1-------l-------l-------I
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

lif115

Sample Description:

Spectrum File:

Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

PZ-302-AS TOT
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000659
1307149A-UU
04
Shelf 2
U iso

Detector Name:

Alpha_048
Chamber Serial Number:

02030596B
Detector Serial Number:
83111
Env. Background:

System Bkgd 64792


Reagent Blank:

<not performed>
Sample Size:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

l.OOOE+OOO +/- O.OOOE+OOO liter


7/16/2013
9:34:57 AM
8/12/2013
9:40:25 AM
170.0 minutes
170.0 minutes

Tracer Certificate:

Tracer Quantity:

Effective Efficiency:

Counting Efficiency:

Chem. Recovery Factor:

U232 UU-lOA
0.603 mL

0.1045 +/- 0.0077

0.1680 +/- 0.0030 on 12/16/2012


0.6223 +/- 0.0473

Peak Match Tolerance:

0.150 MeV

PEAK
Energy
(MeV)

Nuclide
U-232
U-234
U-235
U-238

5.273
4.723
4.421
4.143
T

Net
Pk Area
202.66
92.66
19.83
57.00

AREA

5:49:20 PM

REPORT

Pk Area
Error %

Ambient
Backgnd

Reagent
Backgnd

13.78
20.41
44.23
26.19

0.34
0.34
0.17
0.00

O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

FWHM
(keV)
7.0
7.4
3.0
7.0

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

Activity
(pCi/liter )

MDA
(pCi/liter

-------------------------------------------------------------------------------U-232
U-234
U-235
U-238

0.994
0.989
0.991
0.988

5302.50*
4761.50*
4385.50*
4184.40*

5.15E+OOO
2.35E+OOO
6.21E-001
l.44E+OOO

+/+/+/+/-

7.47E-001
5.89E-001
2.89E-001
4.32E-001

~I fo(f)

l.22E-001
l.21E-001
l.31E-001
l.52E-001

+/+/+/+/-

1. 76E-002
1. 76E-002
l.90E-002
2.20E-002

0000065901.CNF

Live Time
Real Ti me
start:
1
stop : 1024
Acq. Start

60

10200.000 sec
10200 .100 sec
3453. O(kev)

6472. l(kev)

Mon Aug 12 09:40:25 2013

55

50

45

40

35

Vl

.f-..1

c:

::l

8 30

25

20

15

10

3500
I

4000

4500

!~~

.......

t"""'

~.J

ROI Type: 1

5000
Energy(kev)

5500

6000

ROI Type: 3

Channel Data Report

8/12/2013

Page

12:43:31 PM

*******************************************************
s p E C T R A L DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

04

Elapsed Live time:


Elapsed Real Time:

10200
10200

Channell------l-------l-------l-------1-------1-------1-------l-------I
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
4
3
0
0
0
0
0
0
0
0
0
2
0
1
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
2
0
1
5
0
1
0
0
0
0
0
0
0
0
0
0
0
0
1
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
2
0
1
1
1
1
0
0
0
0
0
1
0
0
1
0
0
1
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2
1
3
1
0
0
0
0
0
0
0
0
1
1
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
1
1
2
0
0
0
0
0
1
0
0
0
1
1
0
0
0

1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
2
0
1
0
2
0
1
0
0
0
1
2
0
0
2
0
1
0
0

0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
1
0
0
0
0
0
0
0
0
0
2
0
3
1
1
4
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
1
1
0
2
1
0
1
0
0
0
0
0
0
0
0
0
1
1
0
0
0
iM.,
~

.1 ,i

Channel Data Report


369:

8/12/2013
0

Sample Title:

Page

12:43:31 PM
1

04

Channell------l-------l-------1-------1-------1-------l-------l-------I
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:
625:
633:
641:
649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:

0
1
1
0
1
1
1
0
2
1
0
0
0
2
0
0
0
0
0
0
0
0
0
1
1
2
3
1
2
2
1
10
5
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
1
0
0
1
1
0
2
4
2
1
2
0
0
0
2
0
1
0
0
0
0
0
1
0
2
0
2
1
2
5
9
8
1
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0

0
0
2
0
1
0
4
2
2
1
0
0
0
0
1
1
1
0
0
1
0
0
0
1
2
1
1
1
2
5
6
3
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
1
0
1
1
5
3
6
2
0
0
1
1
0
1
0
0
0
0
1
0
0
0
0
0
3
2
1
2
2
10
5
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
2
1
2
6
0
0
0
0
0
0
0
0
0
0
0
0
2
0
0
1
1
0
2
4
6
4
7
5
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
1
1
0
0
2
1
0
2
0
0
0
1
0
0
0
0
1
1
1
1
1
1
0
0
0
0
2
4
3
4
9
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
2
0
0
3
2
3
2
4
0
0
1
0
0
0
0
1
0
2
0
1
1
1
2
1
0
0
0
3
5
7
5
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
1
0
1
1
1
1
1
1
1
0
0
0
1
0
0
0
1
0
0
1
1
0
0
1
0
2
3
7
4
3
5
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

6119

Channel Data Report


801:

8/12/2013
0

Sample Title:

12:43:31
0

PM
0

Page
0

04

Channell------l-------l-------1-------1-------1-------l-------l-------I
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

61

~Apex-Alpha'"

Sample Description:

Spectrum File:

Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

PZ-302-AS DIS
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000658
1307149A-UU
05
Shelf 2
u iso

Detector Name:

Alpha_037
Chamber Serial Number:

04026478A
Detector Serial Number:
91133
Env. Background:

System Bkgd 62769


Reagent Blank:

<not performed>
Sample Size:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

l.OOOE+OOO +/O.OOOE+OOO liter

7 /16/2013
7:22:35 AM

8/12/2013
5:37:35 AM

170.0 minutes
176.3 minutes

Tracer Certificate:

Tracer Quantity:

Effective Efficiency:

Counting Efficiency:

Chem. Recovery Factor:

U232 UU-lOA
0.603 mL
0.1348 +/0.0089
0.1783 +/0.0033 on 1/26/2013
0.7562 +/0.0519

Peak Match Tolerance:

0.150 MeV

PEAK
Energy
(MeV)

Nuclide
U-232
U-234
U-235
U-238

5.274
4.726
4.417
4.147
T

Net
Pk Area

AREA

REPORT

Pk Area
Error %

261.49
124.66
19.00
71. 00

3:28:25 PM

12.13
17.58
46 .13
23.42

Ambient
Backgnd
0.51
0.34
0.00
0.00

Reagent
Backgnd

FWHM
(keV)

O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

5.4
8.1
2.9
4.9

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS

Nuclide

Id
Conf.

Energy
(keV)

Activity
(pCi/liter )

MDA
(pCi/liter

-------------------------------------------------------------------------------U-232
U-234
U-235
U-238

0.994
0. 991
0.993
0.990

5302.50*
4761.50*
4385.50*
4184.40*

5.15E+OOO
2.45E+OOO
4.62E-001
l.39E+OOO

+/+/+/+/-

6.67E-001
5.36E-001
2.21E-001
3.73E-001

1. 03E-001
9.42E-002
l.46E-001
l.18E-001

+/+/+/+/-

l.34E-002
l.22E-002
l.89E-002
l.52E-002

0000065845.CNF

Live Time :10200.000 sec


Real Time :10579.600 sec
Start:
1: 3463. 5(kev)

stop : 1024:6468.5(kev)

Acq. Start :Mon Aug 12 05:37:35 2013

60

55

50

45

40

35

V)

.f-J

c:

::::s

8 30

25

20

15

10

3500
I

4000

4500

5000
Energy(kev)

5500

6000

t.:m:i
..~..111,

ii",,)

r,J1

ROI Type: 1

ROI Type: 3

Channel Data Report

8/12/2013

Page

8:37:25 AM

*******************************************************
s p E C T R A L DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

05

Elapsed Live time:


Elapsed Real Time:

10200
10580

Channell------l-------l-------1-------1-------1-------l-------l-------I
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:

0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
1
0
0
0
0
0
1
0
1
0
2
0
3
0
1
1
1
0
1
1
0
0
0
1
0
0
0
0
1

0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
1
0
0
0
2
0
1
0
0
2
1
0
2
0
0
0
0
0
0
0
1
0
0
0
0
0

0
0
0
1
0
0
0
0
0
1
0
0
0
0
1
0
0
0
0
0
0
1
1
1
1
1
0
1
1
1
2
3
1
0
0
1
1
0
0
0
1
0
0
0
1
0

0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
1
0
0
1
1
0
1
2
3
1
0
0
0
0
0
0
1
0
1
1
0
0
0
1

0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
1
0
0
2
0
0
0
2
1
0
1
0
0
0
0
1
0
0
1
0
2
1
0

0
0
1
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
0
1
1
0
1
4
0
1
1
0
0
0
0
1
0
0
0
0
0
0

0
0
0
0
0
0
1
0
0
0
1
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
2
0
1
2
0
0
0
0
0
0
0
0
0
0
0
1
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
1
0
0
0
0
0
0
0
2
0
2
3
2
1
0
0
0
0
0
0
1
1
1
0
0
2
1
1

9123

Channel Data Report


369:

8/12/2013
2

Sample Title:

Page

8:37:25 AM
1

05

Channell------l-------l-------l-------1-------1-------1-------l-------I
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:
625:
633:
641:
649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:

0
0
0
0
0
1
1
1
6
1
1
0
0
2
1
0
1
0
0
0
0
0
1
1
0
4
2
3
3
3
4
5
8
5
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
2
0
1
4
1
2
3
4
2
0
0
0
1
0
0
0
0
0
1
1
0
2
1
1
1
2
2
0
3
8
8
8
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
1
1
0
2
1
0
1
3
1
1
0
1
0
0
0
0
1
0
0
0
1
3
1
1
3
1
4
2
3
6
8
4
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
1
3
5
4
2
3
1
0
1
0
0
0
0
0
1
3
1
1
0
0
0
2
1
1
1
1
8
4
3
10
1
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0

0
1
1
0
0
2
2
1
4
0
1
0
0
0
2
0
0
2
2
0
1
1
1
2
1
1
0
1
5
8
2
6
5
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
1
1
1
0
1
4
5
3
2
1
0
0
0
0
0
0
0
1
2
1
2
0
0
0
0
4
4
7
2
3
7
5
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

2
2
0
0
1
1
2
1
1
4
0
1
1
1
1
0
1
1
0
0
2
0
0
3
2
4
1
4
1
5
4
8
6
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

2
2
2
2
1
3
3
2
4
4
0
0
0
0
0
0
0
1
0
2
1
1
2
2
0
1
2
2
4
4
7
8
6
0
0
0
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

f:li12ii
"" .....

Channel Data Report


801:

8/12/2013
0

Sample Title:

Page

8:37:25 AM
0

05

Channell------l-------l-------l-------1-------1-------1-------l-------I
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
1
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0

Q125

Sample Description:

Spectrum File:

Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

LR-100 TOT
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000658
1307149A-UU
06
Shelf 2
u iso

Detector Name:

Alpha_038
Chamber Serial Number:

04026478B
Detector Serial Number:
91134
Env. Background:

System Bkgd 64785


Reagent Blank:

<not performed>
Sample Size:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

l.OOOE+OOO +/- O.OOOE+OOO liter

7/17/2013
7:22:35 AM

8/12/2013
5:37:37 AM

170.0 minutes
176.3 minutes

Tracer Certificate:

Tracer Quantity:

Effective Efficiency:

Counting Efficiency:

Chem. Recovery Factor:

U232 UU-lOA
0.600 mL
0.0371 +/- 0.0045
0.1722 +/- 0.0030 on 5/11/2013
0.2154 +/- 0.0263

Peak Match Tolerance:

0.150 MeV

PEAK
Energy
(MeV)

Nuclide
U-232
U-234
U-235
U-238

Net
Pk Area

5.285
4.732
4.397
4.173

AREA

REPORT

Pk Area
Error %

71.66
4.83
0.00
1. 66

5:13:35 PM

23.22
91.00
1960.0
169.38

Ambient
Backgnd

Reagent
Backgnd

FWHM
(keV)

0.34
0.17
0.00
0.34

O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

3.0
3.0
0.0
3.0

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

Activity
(pCi/liter )

MDA

(pCi/liter

-------------------------------------------------------------------------------U-232
U-234
U-235
U-238

0.998
0.994
0.999
0.999

5302.50*
4761.50*
4385.50*
4184.40*

5.13E+OOO
3.46E-001
O.OOE+OOO
1.18E-001

+/+/+/+/-

l.21E+OOO
3.25E-001
2.45E-001
2.02E-001

3.43E-001
2.99E-001
5.30E-001
3.41E-001

+/+/+/+/-

8.lOE-002
7.07E-002
1.25E-001
8.06E-002

0000065846.CNF

Live Time 10200.000 sec


Real Time 10579.600 sec
start:
1 3482. 5(kev)

stop : 1024 6501.G(kev)


Acq. Start Mon Aug 12 05: 37: 37 2013

60
55

50

45

40

35

V>

.f-1

c:

:::l

8 30

25

20

15

10

3500

,1

4000

4500

Cl!J
~"""

11'1\J!
~.JI

l.,il !.

1i,

ROI Type: 1

5000
Energy(kev)

5500

6000
ROI Type: 3

6500

Channel Data Report

8/12/2013

Page

8:37:32 AM

*******************************************************
s p E C T R A L DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

06

Elapsed Live time:


Elapsed Real Time:

10200
10580

Channell------l-------1-------1-------1-------l-------l-------l-------I
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
fi>il

:tli!i

Channel Data Report


369:

8/12/2013
0

Sample Title:

8:J'1:~i

Page
0

06

Channell------l-------1-------1-------1-------l-------l-------l-------I
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:
625:
633:
641:
649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
2
3
0
5
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0

0
0
0
0
1
0
0
0
0
0
0
1
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
2
0
1
3
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0

0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
0
0
1
0
4
1
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
0
0
3
2
3
3
3
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
1
1
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0

0
0
0
0
0
1
0
0
0
0
0
0
0
1
0
0
0
0
0
0
1
1
0
0
0
1
1
0
1
2
2
3
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
1
2
0
2
1
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
1
0
0
1
1
0
1
0
0
1
1
6
1
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

9129

Channel Data Report


801:

8/12/2013
0

Sample Title:

8:37iJi
0

Page
0

06

Channell------l-------l-------l-------1-------1-------1-------l-------I
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0

0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

c__
Sample Description:

Spectrum File:

Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

LR-100 DIS
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000658
1307149A-UU
07
Shelf 2
u iso

9(('1 //"';)

Detector Name:

Alpha_039
Chamber Serial Number:

060273 96A
Detector Serial Number:
83109
Env. Background:

System Bkgd 64786


Reagent Blank:

<not performed>
Sample Size:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

l.OOOE+OOO +/- O.OOOE+OOO liter


7/17/2013
7:22:35 AM
8/12/2013
5:37:38 AM
170.0 minutes
176.3 minutes

Tracer Certificate:

Tracer Quantity:

Effective Efficiency:

Counting Efficiency:

Chem. Recovery Factor:

U232 UU-lOA
0.601 mL

0.0508 +/- 0.0053

0.1965 +/- 0.0034 on 4/20/2013


0.2587 +/- 0.0272

Peak Match Tolerance:

0.150 MeV

PEAK
Energy
(MeV)

Nuclide
U-232
U-234
U-235
U-238

Net
Pk Area

5.275
4.752
4.392

REPORT

Pk Area
Error %

98.32
7.32
4.83
1.49

4 .115

AREA

2:01:25 PM

19.85
76.28
91.00
190.02

Ambient
Backgnd

Reagent
Backgnd

FWHM
(keV)

0.68
0.68
0.17
0.51

O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

3.3
3.0
3.0
3.0

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

Activity
(pCi/liter )

MDA
(pCi/liter

-------------------------------------------------------------------------------U-232
U-234
U-235
U-238

0.994
0.999
1.000
0.967

5302.50*
4761.50*
4385.50*
4184.40*

5.14E+OOO
3.82E-001
3.llE-001
7.75E-002

+/+/+/+/-

l.05E+OOO
3.02E-001
2.90E-001
l.48E-001

2.95E-001
2.95E-001
2.69E-001
2.73E-001

+/+/+/+/-

6.00E-002
6.00E-002
5.47E-002
5.55E-002

~131

0000065847.CNF

Live Time 10200.000 sec


Real Time 10579.500 sec
Start:
1 3449. 7(kev)

stop : 1024 6497. l(kev)

Acq. Start Mon Aug 12 05: 37: 38 2013

60
55

50

45

40

35

V)

+-'
s::::
:::s

8 30

25

20

15

10

~=>

.\11
I

3500

4000

4500

tlt!il
u~te

ROI Type: 1

5000
Energy(kev)

5500

6000
ROI Type: 3

6500

Channel Data Report

8/12/2013

Page

8:37:44 AM

*******************************************************
s p E C T R A L DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

07

Elapsed Live time:


Elapsed Real Time:

10200
10580

Channell------l-------1-------1-------1-------l-------l-------l-------I
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:

0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
1

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0

0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0

133

Channel Data Report


369:

8/12/2013
0

Sample Title:

8:37:4
0

Page

lit
0

07

Channell------l-------1-------1-------1-------l-------l-------l-------I
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:
625:
633:
641:
649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:

0
1
0
0
0
0
0
0
1
0
1
1
0
0
0
0
0
0
0
0
0
0
0
2
1
0
0
2
0
2
2
5
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
1
1
0
1
1
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
2
1
0
3
0
4
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
1
1
0
0
0
3
2
4
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
1
1
1
5
6
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
2
1
2
3
2
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0

0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
2
0
0
0
1
2
1
2
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
2
1
1
0
5
3
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
1
0
0
0
0
1
2
1
1
1
3
4
5
2
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
~

~ i~

~.J;;,~~

Channel Data Report


801:

8/12/2013
0

Sample Title:

Page

8:37:44 .lM
0

07

Channell------l-------l-------l-------l-------1-------1-------1-------I
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

51135

~~Apex-Alpha'"

Sample Description:

Spectrum File:

Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

D-81 TOT
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000658
1307149A-UU
08
Shelf 2
u iso

Detector Name:

Alpha_040
Chamber Serial Number:

06027396B
Detector Serial Number:
91135
Env. Background:

System Bkgd 64787


Reagent Blank:

<not performed>
Sample Size:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

1.000E+OOO +/- O.OOOE+OOO liter


7 /17 /2013
7:22:35 AM
8/12/2013
5:37:40 AM
170.0 minutes
176.3 minutes

Tracer Certificate:

Tracer Quantity:

Effective Efficiency:

Counting Efficiency:

Chem. Recovery Factor:

U232 UU-lOA
0.604 mL

0.1068 +/0.0078

0.1900 +/- 0.0033 on 12/16/2012


0.5619 +/- 0.0423

Peak Match Tolerance:

0.150 MeV

PEAK
Energy
(MeV)

Nuclide
U-232
U-234
U-235
U-238

5.277
4.735
4.393
4.149
T

Net
Pk Area

AREA

REPORT

Pk Area
Error %

207.49
66.66
23.83
56.00

5:49:33 PM

13.63
24.08
40.32
26.42

Ambient
Backgnd
0.51
0.34
0.17
0.00

FWHM
(keV)

Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

10.9
4.3
3.0
3.0

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS

Nuclide

Id
Conf.

Energy
(keV)

Activity
(pCi/liter )

MDA

(pCi/liter

-------------------------------------------------------------------------------U-232
U-234
U-235
U-238

0.995
0.995
1. 000
0.991

5302.50*
4761.50*
4385.50*
4184.40*

5.16E+OOO
1.66E+OOO
7.31E-001
1.39E+OOO

+/+/+/+/-

7.41E-001
4.65E-001
3.13E-001
4.17E-001

1.31E-001
1.19E-001
1.28E-001
l.48E-001

+/+/+/+/-

1.87E-002
1. 71E-002
1. 84E- 002
2.13E-002

B13S

0000065848.CNF

Live Time 10200.000 sec


Real Time 10579.500 sec
Start:
1 3459.0(kev)

Stop : 1024 6497 .3(kev)

Acq. Start Mon Aug 12 05: 37: 40 2013

60

55

50

45

40

35

V'l

-I-'

c:

::::I

8 30

25

20

15

10

3500
I

4500

4000

IQ!~
..

Jlil~ 1111

t;l<,)
~

....

ROI Type: 1

5000
Energy(kev)

6000

5500
ROI Type: 3

6500

Channel Data Report

8/12/2013

Page

8:37:51 AM

*******************************************************
s p E CTR AL DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

08

Elapsed Live time:


Elapsed Real Time:

10200
10580

Channell------l-------l-------l-------1-------1-------1-------l-------I
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:

0
0
0
0
0
0
0
0
0
1
1
0
0
0
0
0
0
1
0
0
0
0
0
0
1
1
0
0
0
2
1
1
1
1
1
0
1
2
0
0
1
0
0
0
0
0

0
0
0
0
0
0
0
0
1
0
2
1
0
0
0
1
0
0
0
0
2
1
1
0
1
0
2
0
0
1
0
2
0
0
0
0
0
0
0
0
0
2
0
0
0
0

2
0
0
1
0
0
0
0
0
1
0
1
0
1
0
0
1
0
0
1
0
0
0
0
0
1
0
0
0
0
0
2
0
0
0
0
0
1
1
0
2
0
0
0
0
1

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
1
0
0
1
0
1
0
1
1
1
0
0
0
0
1
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2
2
0
0
0
0
0
0
0
0
0
1
0
0
0
2
0
0
0
1
0
1
0
0
0
0
0
2
0
1

0
0
1
0
0
0
0
1
0
0
0
1
1
0
0
0
0
1
0
0
1
0
0
0
1
2
1
0
0
0
2
0
0
0
0
0
1
0
1
0
0
0
0
0
0
1

1
2
0
1
0
2
0
0
0
0
0
0
1
1
0
0
0
0
1
1
1
0
1
1
2
0
0
0
0
2
3
5
0
0
0
0
0
0
1
0
1
1
0
1
1
1

0
0
0
0
1
0
0
0
1
0
0
1
0
0
2
0
0
0
0
0
0
0
0
0
0
0
2
1
1
2
2
0
0
2
2
0
0
1
1
0
0
1
0
0
2
0
P.1

""' ...

Channel Data Report


369:

8/12/2013
1

Sample Title:

Page

8:37:51 AM
1

08

Channell------l-------l-------l-------l-------1-------1-------1-------I
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:
625:
633:
641:
649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:

0
1
0
0
0
1
1
0
0
1
0
1
0
1
1
0
0
0
0
0
1
2
1
0
0
3
4
1
2
2
6
8
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
1
0
1
0
0
2
1
0
1
1
0
0
0
2
0
0
1
0
0
1
0
4
1
2
0
4
4
3
1
11
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
1
1
0
1
1
3
3
0
0
3
0
0
0
0
0
0
1
1
1
1
1
2
0
2
0
0
2
3
3
6
8
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
1
0
4
1
3
0
0
0
0
0
0
1
0
0
0
0
2
1
0
0
1
0
1
2
1
2
7
5
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
0
0
0
0
1
0
3
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
2
3
4
4
3
7
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
1
5
0
3
2
1
0
1
0
0
1
0
1
0
1
0
0
0
1
2
1
0
2
5
0
4
2
9
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
0
2
1
0
2
2
2
0
0
0
0
0
0
1
1
0
0
0
0
1
0
2
0
0
1
3
1
7
10
9
7
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
1
2
1
1
1
1
2
0
0
2
1
0
0
0
0
1
0
0
1
5
0
1
1
4
4
2
5
6
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

s1-3s

Channel Data Report


801:

8/12/2013
0

Sample Title:

Page

8:37:51 AM
0

08

Channell------l-------l-------l-------1-------1-------1-------l-------I
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:

D-81 DIS
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000658
1307149A-UU
09
Shelf 2
U iso

Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:

Alpha_041
05026930A
91087
System Bkgd 64058
<not performed>

Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:

l.OOOE+OOO +/
O.OOOE+OOO liter
7/17/2013
7:22:35 AM
8/12/2013
5:37:42 AM
170.0 minutes
176.3 minutes

Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chem. Recovery Factor:

U232 UU-lOA
0.602 mL
0.1182 +/
0.0083
0.1917 +/
0.0033 on 8/10/2013
0.6166 +/
0.0445

Peak Match Tolerance:

0.150 MeV

PEAK
Energy
(MeV)

Nuclide
U-232
U-234
U-235
U-238

5.276
4.730
4.406
4.146
T

Net
Pk Area

AREA

REPORT

Pk Area
Error %

228.83
93.64
46.32
80.47

2:59:03 PM

12.96
20.43
29.04
22.09

Ambient
Backgnd
0.17
1. 36
0.68
1.53

FWHM
(keV)

Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

8.4
4.0
3.7
6.5

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS

Nuclide

Id
Conf.

Energy
(keV)

Activity
(pCi/liter )

MDA

(pCi/liter

-------------------------------------------------------------------------------U-232
U-234
U-235
U-238

0.995
0.993
0.997
0.989

5302.50*
4761.50*
4385.50*
4184.40*

5.14E+OOO
2.lOE+OOO
l.28E+OOO
l.80E+OOO

+/+/+/+/-

7.06E-001
5.18E-001
4.12E-001
4.68E-001

9.38E-002
1. 54E-001
1. 56E-001
1. 59E-001

+/+/+/+/-

l.29E-002
2. llE- 002
2.15E-002
2.18E-002

0000065849.CNF

Live Time 10200.000 sec


Real Time 10579.500 sec
Start:
1 3442.2(kev)
stop : 1024 6500.4(kev)
Acq. Start Mon Aug 12 05:37:42 2013

60

55

50

45

40

35

V)

.j....I

c:

:::::s

8 30

25
20
15
10

5
0
3500
.,.!l:il1.~1..,
~

4000

4500
ROI Type: l

5000
Energy(kev)

6000

5500
ROI Type: 3

6500

Channel Data Report

8/12/2013

Page

8:38:00 AM

*******************************************************
s p E CTR AL DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

09

Elapsed Live time:


Elapsed Real Time:

10200
10580

Channell------l-------l-------l-------1-------1-------1-------l-------I
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:

0
0
0
0
0
0
1
0
0
0
0
1
0
0
1
0
1
0
0
1
0
1
0
0
0
2
0
0
0
2
2
1
0
0
1
1
1
1
1
0
1
1
0
1
2
0

1
0
0
0
1
0
0
0
1
0
1
0
1
0
0
0
1
0
1
1
0
0
0
1
1
0
0
0
1
1
1
4
1
0
0
0
0
1
1
0
1
0
1
1
1
0

1
0
0
0
0
0
1
0
0
0
1
0
0
1
2
0
0
0
1
0
2
0
0
2
0
1
1
0
1
3
4
3
0
1
0
0
0
1
1
1
0
2
1
0
0
1

0
0
0
0
2
0
0
0
0
1
1
0
0
1
1
0
0
1
0
0
1
0
0
1
0
1
3
0
1
1
3
2
0
1
1
1
0
3
2
1
0
1
1
0
0
1

1
0
0
0
0
0
0
0
0
1
1
0
1
0
2
0
0
2
1
1
0
1
1
0
1
0
0
0
1
0
1
3
0
1
1
0
0
0
0
0
1
1
0
1
0
1

0
0
0
0
0
0
0
0
0
1
0
1
0
1
0
0
0
0
0
1
0
1
0
2
1
0
0
0
1
1
0
2
0
1
0
1
0
1
0
1
0
2
2
0
1
0

0
0
1
0
1
0
0
0
0
0
0
1
0
0
0
1
1
0
1
0
1
0
1
1
0
1
0
1
1
1
3
1
1
1
0
0
0
1
2
2
1
1
1
0
1
1

0
0
0
0
1
2
0
0
1
2
1
0
0
0
1
1
0
0
1
0
2
0
0
0
1
0
0
1
1
0
1
3
0
1
1
0
0
0
0
1
0
0
0
1
0
0

!H43

Channel Data Report


369:

8/12/2013
0

Sample Title:

8:3S:U
1

Page

Ml
0

09

Channell------l-------l-------l-------l-------1-------1-------l-------I
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:
625:
633:
641:
649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:

1
1
1
1
0
0
1
8
1
2
0
0
0
2
0
0
0
0
0
0
0
1
0
0
1
1
2
1
3
1
6
5
5
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0

0
1
0
1
1
2
3
2
2
2
1
0
0
0
0
0
0
1
1
0
1
0
1
0
0
0
0
3
1
4
4
4
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
1
3
2
2
0
0
1
1
0
0
0
0
0
0
0
0
0
2
0
1
2
4
6
3
5
11
2
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
1
0
1
0
1
0
2
3
1
0
0
0
1
1
0
0
1
0
0
2
0
0
0
1
2
1
3
3
7
8
8
2
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
1
0
0
1
0
1
4
2
1
0
0
1
0
1
0
1
0
1
0
0
0
0
1
1
2
3
2
2
5
2
5
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
0
0
1
2
1
4
2
4
0
0
0
0
0
0
1
0
0
0
1
0
1
0
0
0
0
1
1
6
4
7
10
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
0
4
0
1
1
0
1
3
0
0
0
1
1
0
2
0
0
0
0
0
0
2
1
0
3
0
3
5
8
8
12
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0

1
0
1
0
1
2
2
3
6
1
0
0
0
0
1
0
0
1
0
2
2
0
0
2
1
2
1
0
6
5
8
6
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1144

Channel Data Report


801:

8/12/2013
0

Sample Title:

Page

8:38:00 AM
0

09

Channell------l-------l-------1-------1-------1-------l-------l-------I
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

B145

Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:

PZ-204-SS TOT
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000658
1307149A-UU
10
Shelf 2
U iso

Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:

Alpha_042
05026930B
84185
System Bkgd 64788
<not performed>

Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:

O.OOOE+OOO liter
l.OOOE+OOO +/
7:22:35 AM
7/17/2013
5:37:43 AM
8/12/2013
170.0 minutes
176.3 minutes

Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chem. Recovery Factor:

U232 UU-lOA
0.602 mL
0.1639 +/
0.0099
0.1846 +/
0.0032 on 12/16/2012
0.8876 +/
0.0560

Peak Match Tolerance:

0.150 MeV

PEAK
Energy
(MeV)

Nuclide
U-232
U-234
U-235
U-238

5.279
4.724
4.424
4.154
T

AREA

REPORT

Pk Area
Error %

Net
Pk Area
317.49
175.66
22.00
106.98

5:49:29 PM

Ambient
Backgnd
0.51
0.34
0.00
1. 02

11. 01
14.81
42.73
19.06

FWHM
(keV)

Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

5.2
12.3
3.0
4.0

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS

Nuclide

Id
Conf.

Energy
(keV)

U-232
U-234
U-235
U-238

0. 996
0.990
0.989
0.993

5302.50*
4761.50*
4385.50*
4184.40*

Activity
(pCi/liter )

MDA

(pCi/liter

-------------------------------------------------------------------------------5.15E+OOO
2.85E+OOO
4.40E-001
l.73E+OOO

+/+/+/+/-

6.13E-001
5.41E-001
1.95E-001
3.88E-001

8.51E-002
7.75E-002
l.20E-001
l.02E-001

+/+/+/+/-

l.OlE-002
9.22E-003
l.43E-002
l.21E-002

0000065851.CNF

Live Time 10200.000 sec


Rea1 Ti me 105 79. 500 sec
start:
1 3450.2(kev)
stop : 1024 6505. 5(kev)
Acq. Start Mon Aug 12 05:37:43 2013

60

55

50

45

40

35

Vl

......
c
:::s

8 30

25

20

15

10

3500
I

4000

4500

11".J!,

ROI Type: 1

5000
Energy(kev)

6000

5500
ROI Type: 3

6500

Channel Data Report

8/12/2013

Page

8:38:07 AM

*******************************************************
s p E C T R A L DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

10

Elapsed Live time:


Elapsed Real Time:

10200
10580

Channell------l-------l-------l-------1-------1-------1-------l-------I
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
1
0
4
0
2
3
2
0
0
0
0
0
1
0
1
0
0
2
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
1
0
0
0
1
0
1
1
1
3
4
3
2
0
1
0
0
0
0
0
1
0
0
0
0
2

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2
1
0
1
0
0
1
0
2
1
1
1
0
0
0
0
0
0
1
0
0
0
0
0
0
1

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
0
0
0
0
1
0
1
2
0
2
3
1
4
0
1
0
0
0
1
0
0
2
0
0
3
2
0

0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
1
0
0
1
0
2
1
0
0
1
0
0
2
2
3
4
0
1
1
0
1
0
0
1
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2
1
0
0
2
5
2
1
0
0
0
1
0
0
0
0
1
0
0
0
0
0

0
0
0
0
0
0
0
1
0
1
0
0
0
0
0
0
0
0
0
0
0
1
1
0
1
0
1
2
1
3
1
6
1
0
0
0
0
0
0
1
0
1
1
0
1
0

0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
1
0
1
0
1
2
3
1
5
2
0
0
0
0
0
0
0
0
0
1
0
2
0
2

8148

Channel Data Report


369:

8/12/2013
0

Sample Title:

Page

8:38:07 AM
1

10

Channell------l-------1-------1-------1-------l-------l-------l-------I
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:
625:
633:
641:
649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:

0
1
0
1
1
5
4
6
5
3
0
3
1
1
1
0
1
0
1
0
1
0
0
2
0
2
1
3
5
3
6
13
6
0
1
0
0
0
0
0
0
0
0
0
0
0
0
2
0
0
0
0
0

0
0
1
1
1
3
2
2
5
2
0
0
0
1
0
0
1
1
1
1
1
0
0
0
0
1
2
4
6
11
11
8
4
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0

1
0
3
0
1
4
2
2
4
0
0
0
1
0
0
0
2
1
0
2
1
0
1
1
2
0
0
6
5
11
11
9
2
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
0
1
0
2
5
4
3
5
0
0
1
1
0
0
0
0
1
1
2
0
0
1
3
2
1
2
3
6
6
9
8
1
0
0
0
0
0
0
0
0
0
0
0
1
0
0
1
0
0
0
0
0

2
1
2
2
0
7
2
6
3
0
1
0
0
0
1
0
1
0
1
0
0
0
2
3
2
1
2
4
7
6
8
9
1
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0

1
1
2
4
1
6
4
5
2
0
0
0
0
2
1
0
1
0
1
1
1
1
4
0
1
1
1
3
7
2
7
6
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
1
0
0
6
2
6
5
7
0
0
1
0
1
0
1
1
1
0
3
0
3
0
0
0
0
1
4
9
5
11
6
0
0
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
0
1
0
6
4
3
2
2
0
0
0
0
1
0
0
0
0
0
1
2
4
1
2
0
0
4
4
6
13
12
5
0
0
0
0
1
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0

-f:l-149

Channel Data Report


801:

8/12/2013
0

Sample Title:

Page

8:38:07 AM
0

10

Channell------l-------l-------l-------l-------l-------1-------1-------1
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

Sample Description:

Spectrum File:

Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

PZ-204-SS DIS
\\OR-ALPHAl\Canberra\Apex.Alpha\Root\Data\00000658
1307149A-UU
11
Shelf 2
U iso

Detector Name:

Alpha_043
Chamber Serial Number:

04026481A
Detector Serial Number:
91088
Env. Background:

System Bkgd 57707


Reagent Blank:

<not performed>
Sample Size:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

O.OOOE+OOO liter
l.OOOE+OOO +/7:22:35 AM
7/17/2013
5:37:45 AM
8/12/2013
170.0 minutes
176.3 minutes

Tracer Certificate:

Tracer Quantity:

Effective Efficiency:

Counting Efficiency:

Chem. Recovery Factor:

U232 UU-lOA
0.602 mL

0.1724 +/0.0102

0.2003 +/0.0035 on 8/11/2013


0.8608 +/0.0533

Peak Match Tolerance:

0.150 MeV

PEAK
Energy
(MeV)

Nuclide
U-232
U-234
U-235
U-238

5.280
4.729
4.383
4.147
T

Net
Pk Area

AREA

REPORT

Pk Area
Error %

334.00
157.00
15.00
98.00

2:21:17 PM

10.74
15.69
52.27
19.90

Ambient
Backgnd
0.00
0.00
0.00
0.00

FWHM
(keV)

Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

39.5
8.9
3.0
6.6

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS

Nuclide

Id
Conf.

Energy
(keV)

Activity
(pCi/liter )

MDA
(pCi/liter

-------------------------------------------------------------------------------U-232
U-234
U-235
U-238

0.997
0.993
1. 000
0.990

5302.50*
4761.50*
4385.50*
4184.40*

5.15E+OOO
2.42E+OOO
2.85E-001
l.50E+OOO

+/+/+/+/-

6.00E-001
4.73E-001
1.53E-001
3.46E-001

9.24E-002
9.23E-002
l.14E-001
9.19E-002

+/+/+/+/-

1. OBE-002
1. 08E- 002
1.33E-002
l.07E-002

5151

0000065852.CNF

Live Ti me 10200. 000 sec


Real Time 10579.400 sec
Start:
1 3440. 3(kev)

Stop : 1024 6488.6(kev)


Acq. Start Mon Aug 12 05:37:45 2013

60
55

50

45

40

35

V)

.j..J

c:

:::J

8 30

25

20

15

10

3500

4000

4500

~~

ii-""'

lt.!l
r-.~

ROI Type: 1

5000
Energy(kev)

6000

5500
ROI Type: 3

Channel Data Report

8/12/2013

Page

8:38:15 AM

*******************************************************
s p E C T R A L DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

11

Elapsed Live time:


Elapsed Real Time:

10200
10579

Channell------l-------l-------1-------1-------1-------l-------l-------I
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
2
1
1
0
0
0
2
1
3
5
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
1
0
0
0
0
1
0
0
1
0
1
1
1
3
0
2
0
0
0
0
1
0
0
1
1
0
0
1
1

0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
2
2
0
3
0
1
1
4
3
0
0
0
0
0
0
0
1
0
0
0
0
1

0
0
0
0
0
1
0
0
1
0
0
0
0
1
0
0
0
0
0
0
0
0
0
1
0
1
0
1
2
1
2
5
1
1
0
0
1
0
1
1
0
1
0
0
0
2

0
0
0
0
0
0
0
0
2
0
0
0
0
1
1
0
1
0
1
1
0
0
2
0
0
0
0
0
3
4
1
2
0
1
0
1
1
0
0
0
0
0
1
0
0
1

0
0
0
0
0
1
0
0
0
0
0
0
0
1
0
0
1
0
0
0
0
0
0
0
1
0
0
0
1
1
3
3
0
2
0
0
1
0
0
0
2
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
1
1
3
1
2
3
0
0
0
0
0
1
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
1
1
0
1
0
0
2
2
4
0
0
0
0
0
0
0
0
0
0
0
0
0
0

!153

Channel Data Report


369:

8/12/2013
1

Sample Title:

8:3it1i
0

Page
0

11

Channell------l-------l-------1-------1-------1-------l-------l-------I
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:
625:
633:
641:
649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:

0
2
1
1
0
2
1
3
2
6
1
1
0
0
0
0
0
0
1
1
0
0
3
1
1
0
0
2
5
4
9
10
10
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
1
1
2
3
2
1
4
6
0
0
1
0
0
0
0
0
0
0
0
0
0
0
1
1
1
3
1
10
10
12
9
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
0
0
2
0
2
2
3
8
4
0
1
0
0
0
0
0
0
1
1
0
2
2
2
0
1
3
1
3
0
4
11
17
0
0
0
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
0
0
0
1
1
3
5
6
5
1
0
1
0
0
0
1
2
0
0
0
2
2
0
1
2
2
3
6
6
10
9
8
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
0
1
0
0
2
3
1
4
3
0
0
2
0
1
0
0
0
0
0
1
2
2
2
1
3
2
3
1
7
5
11
6
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
1
1
3
1
7
5
7
0
1
0
0
0
0
0
0
0
0
2
0
0
0
1
0
0
2
3
6
9
5
10
5
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
2
0
0
0
4
4
2
1
0
0
0
0
0
0
0
1
0
0
0
0
1
1
1
0
1
1
5
4
7
10
10
1
0
0
0
0
0
0
0
0
0
1
0
0
0
0
1
0
0
0
0
0

1
4
0
0
0
3
7
2
6
0
0
0
1
0
0
0
0
0
0
0
0
0
0
1
1
0
2
3
5
9
11
11
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

li154

Channel Data Report


801:

8/12/2013
0

Sample Title:

Page

8:38:15 AM
0

11

Channell------l-------l-------l-------1-------1-------1-------l-------I
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:

LR-103 TOT
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000658
1307149A-UU
12
Shelf 2
U iso

Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:

Alpha_044
04026481B
84168
System Bkgd 60396
<not performed>

Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:

1.000E+OOO +/
0.000E+OOO liter
7/17/2013
7:22:35 AM
8/12/2013
5:37:47 AM
170.0 minutes
176.3 minutes

Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chem. Recovery Factor:

U232 UU-lOA
0.601 mL
0.0734 +/
0.0064
0.1920 +/
0.0033 on 8/11/2013
0.3824 +/
0.0340

Peak Match Tolerance:

0.150 MeV

PEAK
Energy
(MeV)

Nuclide
U-232
U-234
U-235
U-238

5.256
4.709
4.385
4.143

Net
Pk Area

AREA

REPORT

Pk Area
Error %

142.00
22.83
11. 83
17.83

2:17:37 PM

16.51
41. 20
57.46
46.68

Ambient
Backgnd
0.00
0.17
0.17
0.17

Reagent
Backgnd

FWHM
(keV)

O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

4.7
3.0
3.0
3.0

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS

Nuclide

Id
Conf.

Energy
(keV)

Activity
(pCi/liter )

MDA

(pCi/liter

-------------------------------------------------------------------------------U-232
U-234
U-235
U-238

0.985
0.981
1.000
0.988

5302.50*
4761.50*
4385.50*
4184.40*

5.14E+OOO
8.26E-001
5.28E-001
6.42E-001

+/+/+/+/-

8.79E-001
3.68E-001
3.16E-001
3.19E-001

2.17E-001
1. 51E-001
1.86E-001
1. 50E-001

+/+/+/+/-

3. 71E-002
2.58E-002
3.19E-002
2.57E-002

0000065853.CNF

Live Time 10200.000 sec


Real Time 10579.400 sec
start:
1 3443.2(kev)
stop : 1024 6477. 3(kev)

Acq. Start Mon Aug 12 05:37:47 2013

60
55

50

45

40

35

V)

.j-J

s::::

::::s

8 30

25
20
15
10

5
0

i,;i Hf\I

3500

4500

4000

~!lllt

H-<

LI!!

"'.Ji

ROI Type: 1

5000
Energy(kev)

6000

5500
ROI Type: 3

Channel Data Report

8/12/2013

Page

8:3i:4ti ...

*******************************************************
s p E C T R A L DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

12

Elapsed Live time:


Elapsed Real Time:

10200
10579

Channell------l-------l-------1-------1-------1-------l-------l-------I
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:

0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
1
1

0
0
0
1
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
1
0
0
0
0
1
0
0
0
0
0
1

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
1
0
0
0
1
0
0
0
0
2
0
0
1
0
0
0
0

0
0
0
0
0
0
0
1
0
0
0
1

0
0
0
0
0
0
2
0
0
0
0
0
0
0
1
0
1
0
1
0
0
0
0
1

0
0
0
1
0
0
0
0
0
0

0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
1
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
1
0
0
0
1
0
0
1
0

0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
1
1

0
0
0
0
0
0
0
0
0
1

0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
1
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
1
0

0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1

0
0
0
0
0
0
0
0
2
1

0
1
0
0
1
0
0
0
1
0
0
0
0
0

fiH

Channel Data Report


369:

8/12/2013
0

Sample Title:

Page

8:38:22 AM
0

12

Channell------l-------l-------l-------1-------1-------1-------l-------I
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:
625:
633:
641:
649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:

0
0
1
0
0
0
0
0
2
0
0
0
0
1
0
0
0
1
0
0
0
1
0
1
0
2
1
0
3
4
2
6
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0

1
1
1
1
0
1
0
0
0
0
0
0
0
0
1
1
0
0
0
1
2
0
0
0
1
1
1
1
2
7
1
3
2
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
1
0
1
0
0
0
0
0
0
1
1
2
0
0
1
0
0
0
1
1
0
0
1
1
5
2
3
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
1
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
1
2
0
1
4
1
1
2
2
6
5
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
1
0
0
1
0
0
0
0
0
0
0
1
0
0
0
0
2
1
0
0
1
0
2
2
4
4
4
3
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
1
0
0
0
0
0
1
0
0
0
0
0
0
0
1
1
1
0
0
0
0
1
3
3
1
3
2
0
2
6
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0

0
0
0
0
1
1
0
0
1
3
0
1
1
0
1
1
1
2
0
1
0
2
0
0
0
1
1
2
1
3
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
0
0
1
1
0
0
0
0
0
0
0
0
0
0
0
0
1
1
1
0
3
1
0
0
1
2
7
1
1
6
4
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

m1S'9.

Channel Data Report


801:

8/12/2013
0

Sample Title:

Page

8:38:~#.

12

Channell------l-------l-------l-------l-------l-------1-------1-------1
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:

LR-103 DIS
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000658
1307149A-UU
13
Shelf 2
U iso

Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:

Alpha_045
04026482A
91131
System Bkgd 64789
<not performed>

Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:

O.OOOE+OOO liter
l.OOOE+OOO +/
7/17/2013
7:22:35 AM
8/12/2013
5:37:49 AM
170.0 minutes
170.0 minutes

Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chem. Recovery Factor:

U232 UU-lOA
0.598 mL
0.1100 +/
0.0080
0.1909 +/
0.0033 on 7/20/2013
0.5762 +/
0.0430

Peak Match Tolerance:

0.150 MeV

PEAK
Energy
(MeV)

Nuclide
U-232
U-234
U-235
U-238

5.281
4.774
4 .411
4.140
T

AREA

REPORT

Pk Area
Error %

Net
Pk Area
211. 66
7.66
4.00
5.66

2:31:26 PM

Ambient
Backgnd
0.34
0.34
0.00
0.34

13.48
72.63
109.57
85.23

FWHM
(keV)

Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

9.0
3.0
3.0
3.0

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS

Nuclide

Id
Conf.

Energy
(keV)

Activity
(pCi/liter )

MDA

(pCi/liter

-------------------------------------------------------------------------------U-232
U-234
U-235
U-238

0.997
0.999
0.995
0.986

5302.50*
4761.50*
4385.50*
4184.40*

5.llE+OOO
l.85E-001
l.19E-001
l.36E-001

+/+/+/+/-

7.27E-001
l.37E-001
l.32E-001
1.18E-001

l.15E-001
l.15E-001
1.79E-001
1.15E- 001

+/+/+/+/-

l.64E-002
1. 64E-002
2.54E-002
l.63E-002

0000065843.CNF

Live Time :10200.000 sec


Real Time :10200.100 sec
start:
1: 3453. ?(kev)
stop : 1024:6489.5(kev)
Acq. Start :Mon Aug 12 05:37:49 2013

60
55

50

45

40

35

Vl
.j-J

s::::
:::s

8 30

25

20

15

10

0
3500
~
ii-'"''

m
W,)

4000

4500

ROI Type: 1

5000
Energy(kev)

6000

5500
ROI Type: 3

Channel Data Report

8/12/2013

Page

8:38:28 AM

*******************************************************
s p E CTR AL DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

13

Elapsed Live time:


Elapsed Real Time:

10200
10200

Channell------1-------1-------1-------l-------l-------l-------l-------I
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:

0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1

0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
1
1
0
0
0

0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

8163

Channel Data Report


369:

8/12/2013
0

Sample Title:

Page

8:38:28 AM
0

13

Channell------l-------1-------1-------1-------l-------l-------l-------I
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:

625:
633:
641:
649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:

0
0
0
0
0
0
0
0
0
1
0
1
0
1
1
1
0
0
0
1
1
1
0
0
1
3
1
1
1
6
2
7
7
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
1
1
1
0
2
2
0
0
0
0
2
3
4
1
11
7
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
3
1
2
3
2
4
4
6
6
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
2
0
2
0
0
0
0
0
2
0
1
2
2
13
4
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
1
1
1
1
2
2
5
9
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
1
2
1
0
0
0
0
1
2
1
2
3
3
6
5
9
7

3
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
1
0
0
0
1
0
0
0
0
1
0
3
2
1
0
0
2
0
0
1
2
3
5
2
1
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0

0
0
0
0
0
0
0
0
1
0
0
0
0
1
0
1
1
0
0
1
0
1
1
3
0
2
0
0
6
7
5
4
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

8164

Channel Data Report


801:

8/12/2013
0

Sample Title:

S;~ii
0

tf
0

Pg~

13

Channell------l-------l-------l-------l-------l-------1-------1-------1
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1!1165

Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:

PZ-111-KS TOT
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000658
1307149A-UU
14
Shelf 2
u iso

Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:

Alpha_046

04026482B

58762

System Bkgd 64790

<not performed>

Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:

l.OOOE+OOO +/- O.OOOE+OOO liter

7:22:35 AM

7/17/2013
5:37:51 AM

8/12/2013
170.0 minutes

170.0 minutes

Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chem. Recovery Factor:

U232 UU-lOA
0.599 mL

0.1395 +/0.1789 +/0.7794 +/-

Peak Match Tolerance:

0.150 MeV

0.0091

0.0031 on 12/16/2012
0.0527

5:49:23 PM

-------------------------------------------------PEAK

AREA

REPORT

-------------------------------------------------Energy
(MeV)

Nuclide

Pk Area
Error %

Net
Pk Area

Reagent
Backgnd

Ambient
Backgnd

FWHM

(keV)

-------------------------------------------------------------------------------U-232
U-234
U-235
U-238

5.270
4. 715
4.408
4.139

269.00
368.83
34.83
127.00

0.00
0.17
0.17
0.00

11. 97
10.21
33.31
17.46

O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

23.9
28.7
3.7
5.4

Tracer Peak used for Effective Efficiency

-------------------------------------------------NUCLIDE ANALYSIS RESULTS

-------------------------------------------------Nuclide

Id
Conf.

Energy
(keV)

U-232
U-234
U-235
U-238

0.992
0.985
0.996
0.986

5302.50*
4761.50*
4385.50*
4184.40*

Activity
(pCi/liter )

MDA

(pCi/liter

-------------------------------------------------------------------------------5.12E+OOO
7.02E+OOO
8.18E-001
2.41E+OOO

+/+/+/+/-

6.56E-001
1.15E+OOO
2.92E-001
5.21E-001

1.14E- 001
7.95E-002
9.80E-002
1.14E- 001

+/+/+/+/-

1.46E-002
l.02E-002
1.25E-002
l.45E-002

9166

0000065842.CNF

Live Time :10200.000 sec


Real Ti me :10200 .100 sec
Start:
1:3453.?(kev)
stop : 1024: 6515. 4(kev)
Acq. Start : Mon Aug 12 05: 37: 51 2013

60
55

50

45

40

35

Vl

.1-J

s:::

::::I

8 30

25
20
15
10

5
0

3500

4000

4500

t:r!ll

......

m
""J

ROI Type: 1

5000
Energy(kev)

6000

5500
ROI Type: 3

6500

Channel Data Report

8/12/2013

8:38:l~

...

Page

*******************************************************
s p E CTR AL DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

14

Elapsed Live time:


Elapsed Real Time:

10200
10200

Channell------l-------l-------1-------1-------1-------l-------l-------I
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:

0
0
0
0
0
0
0
0
0
0
0
1
2
0
0
0
0
1
0
0
0
0
0
0
0
0
1
4
2
5
8
2
2
0
0
0
0
0
0
0
0
1
0
0
0
2

0
1
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
1
0
1
0
0
0
0
1
1
1
3
1
3
4
0
0
1
0
0
0
1
1
0
1
0
3
0
0
1

0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
2
3
2
5
1
0
0
1
0
0
0
0
2
1
1
0
2
0
1
1

0
0
0
1
0
0
0
0
0
0
1
0
0
0
0
0
0
0
1
1
0
0
0
0
0
1
0
1
5
3
4
2
0
1
1
0
0
1
0
0
0
1
0
1
0
2

0
0
0
0
0
1
0
0
1
0
0
0
0
0
1
0
0
0
0
0
1
1
1
0
1
3
0
1
1
4
4
1
0
0
0
1
0
3
0
1
0
3
1
0
1
0

0
0
0
0
0
1
1
0
0
0
0
0
1
0
1
0
1
0
0
0
1
1
0
0
0
1
0
2
4
3
2
0
0
0
0
0
0
0
0
0
0
1
0
1
2
0

0
0
0
0
1
0
0
0
1
0
0
0
0
0
1
0
0
0
1
1
3
0
1
0
2
1
0
0
3
4
2
0
1
0
0
2
1
0
1
0
1
0
0
0
2
1

0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
1
0
0
1
2
0
1
3
1
3
2
3
1
0
0
0
0
0
0
0
0
1
1
1
0
1
2
1

....

Channel Data Report


369:

8/12/2013
1

Sample Title:

Page

8:38:34 AM
2

14

Channell------l-------l-------1-------1-------1-------l-------l-------I
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:
625:
633:
641:
649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:

1
0
4
3
4
5
11
12
6
1
0
0
0
0
0
0
0
2
0
0
0
1
0
2
1
0
6
5
3
6
12
5
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

2
1
2
2
3
5
7
12
8
1
0
0
0
0
0
1
1
0
0
0
1
0
0
0
2
1
0
6
5
10
8
5
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
2
5
2
4
11
8
11
5
0
0
1
0
0
1
1
0
2
1
0
1
3
2
1
2
1
2
2
2
11
9
6
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
3
0
5
12
10
14
10
4
0
0
0
0
0
0
0
0
0
0
2
0
1
0
0
1
6
1
4
6
8
9
3
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0

2
1
4
4
5
8
9
9
2
0
0
0
0
0
0
1
0
0
0
0
0
2
0
0
0
1
2
1
5
2
13
2
0
0
0
0

0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0

0
5
4
5
8
7
7
10
1
0
0
0
0
1
0
0
0
1
1
0
0
0
0
3
2
2
1
5
2
8
4
2
0
0
0
0
0

0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0

0
2
1
5
3
7
12
15
0
0
0
0
1
0
0
1
0
2
0
1
0
1
1
1
0
3
4
2
9
8
8
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

3
2
4
4
2
3
16
6
1
1
0
0
0
0
0
0
0
0
0
1
1
0
2
1
1
1
3
3
8
10
6
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

Channel Data Report


801:

8/12/2013
0

Sample Title:

..

Page

a:lt;U
0

14

Channell------l-------l-------l-------l-------1-------1-------1-------I
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:

PZ-111-KS DIS
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000658
1307149A-UU
15
Shelf 2
U iso

Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:

Alpha_047
02030596A
91086
System Bkgd 64791
<not performed>

Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:

l.OOOE+OOO +/- O.OOOE+OOO liter


7:22:35 AM
7/17/2013
5:37:53 AM
8/12/2013
170.0 minutes
170.0 minutes

Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:

Chem. Recovery Factor:

U232 UU-lOA
0.599 mL
0.1026 +/- 0.0077
0.1822 +/- 0.0032 on 12/16/2012
0.0432

0.5631 +/-

Peak Match Tolerance:

0.150 MeV

5:49:21 PM

-------------------------------------------------PEAK

AREA

REPORT

-------------------------------------------------Energy
(MeV)

Nuclide

Pk Area
Error %

Net
Pk Area

Reagent
Backgnd

Ambient
Backgnd

FWHM
(keV)

-------------------------------------------------------------------------------U-232
U-234
U-235
U-238

5.260
4.716
4.428
4 .133

197.83
314.83
31.00
134.66

13.94
11. 05
35.77
16.92

0.17
0.17
0.00
0.34

O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

5.3
10.8
3.7
3.4

Tracer Peak used for Effective Efficiency

-------------------------------------------------NUCLIDE ANALYSIS RESULTS

-------------------------------------------------Nuclide

Id
Conf.

Energy
(keV)

U-232
U-234
U-235
U-238

0.987
0.985
0.987
0.982

5302.50*
4761.50*
4385.50*
4184.40*

Activity
(pCi/liter )

MDA
(pCi/liter

-------------------------------------------------------------------------------1. 58E-002
5.12E+OOO
8.15E+OOO
9.90E-001
3.47E+OOO

+/- 7.51E-001
+/- l.50E+OOO
+/- 3.83E-001
+/- 7.77E-001

1. 08E-001 +/-

l.08E-001 +/ 1. 58E- 002


l.91E-001 +/- 2.81E-002
l.23E-001 +/- 1. 81E- 002

0000065844.CNF

Live Time 10200.000 sec


Real Time 10200.100 sec
Start:
1 3457 .9(kev)

Stop : 1024 6467. 7(kev)

Acq. Start Mon Aug 12 05: 37: 53 2013

60
55

50

45

40

35

Vl

.f-J

s::::

:::s

8 30

25

20

15

10

3500
I

4000

4500

5000
Energy(kev)

6000

5500

WI
I~~~

,,

l'J

ROI Type: 1

ROI Type: 3

Channel Data Report

8/12/2013

Page

8:38:40 AM

*******************************************************
s P E C T R A L DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

15

Elapsed Live time:


Elapsed Real Time:

10200
10200

Channell------l-------l-------l-------1-------1-------1-------l-------I
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:

0
0
0
0
0
0
0
0
1
1
0
0
0
0
0
0
0
0
1
1
1
0
0
0
0
0
2
2
0
2
1
3
1
1
0
0
0
0
0
0
1
1
0
1
2
1

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
2
3
4
2
2
1
0
0
1
1
0
0
1
0
0
0
3
2
0

0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
2
0
2
1
1
1
3
0
2
3
0
1
1
0
0
0
0
1
0
0
0
0
2
0
0
2

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
0
0
0
1
4
1
0
0
3
2
1
9
5
1
0
0
0
1
0
0
0
1
0
1
0
0
2

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2
0
0
1
1
1
2
1
0
1
2
5
5
2
2
1
1
0
0
1
0
0
0
0
0
1
1
0
0

1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
0
1
1
0
2
1
0
1
1
2
0
9
2
0
0
0
0
0
0
1
0
2
1
0
1
0
1

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2
0
0
0
0
0
0
2
0
3
1
4
1
4
2
0
0
0
0
0
0
0
1
0
1
1
0
1
1
0

0
0
0
0
0
0
1
0
0
1
0
1
1
0
0
1
0
0
0
0
0
0
0
0
1
0
1
1
3
1
4
0
1
0
0
0
0
0
1
0
0
0
0
0
0
0

511

Channel Data Report


369:

8/12/2013
2

Sample Title:

Page

8:38:40 AM
1

15

Channell------l-------l-------l-------1-------1-------1-------l-------I
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:
625:
633:
641:
649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:

1
1
2
5
6
4
5
7
6
5
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2
1
3
4
3
3
6
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
2
1
4
3
4
9
6
5
8
0
0
0
1
0
0
0
0
1
1
0
1
0
2
1
4
1
5
3
2
4
4
5
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0

4
1
0
2
1
4
5
8
4
6
0
0
0
0
0
0
0
0
0
0
0
1
0
1
1
0
2
4
5
4
2
2
6
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
1
0
1
2
8
6
12
12
9
0
1
0
0
0
0
0
0
0
0
0
1
0
1
2
0
1
2
6
4
3
3
5
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

3
0
2
5
4
3
6
8
5
4
0
0
0
1
0
0
0
0
1
1
0
0
1
1
1
1
0
2
0
4
6
1
3
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
3
3
2
3
7
5
5
6
5
0
0
0
0
0
1
0
0
0
0
0
0
1
0
0
0
3
2
1
3
2
5
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
1
1
1
4
10
9
6
5
0
0
0
0
0
0
1
1
0
1
0
0
0
1
0
1
0
2
2
4
5
3
6
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
5
3
4
3
11
6
4
2
2
0
0
1
0
0
0
0
0
1
0
2
0
2
1
3
1
1
6
8
4
5
5
7
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

f!H74

Channel Data Report


801:

8/12/2013
0

Sample Title:

Page

8:38:40 AM
0

15

Channell------l-------1-------1-------1-------l-------l-------l-------I
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0

Page 1 of 2
8/12/2013 6:43:21 AM

QA SUMMARY REPORT
Review Of QA Results - Pulser Check
Date
Time

: 8/12/2013
: 6:43:21 AM

CHAMBER
Alpha 001
Alpha 002
Alpha 003
Alpha 004
Alpha 005
Alpha 006
Alpha 007
Alpha 008
Alpha 009
Alpha 010
Alpha 011
Alpha 012
Alpha 013
Alpha 014
Alpha 015
Alpha 016
Alpha 017
Alpha 018
Alpha 019
Alpha 020
Alpha 021
Alpha 022
Alpha 023
Alpha 024
Alpha 025
Alpha 026
Alpha 027
Alpha 028
Alpha 029
Alpha 030
Alpha 031
Alpha 032
Alpha 033
Alpha 034
Alpha 035
Alpha 036
Alpha 036
Alpha 037
Alpha 038
Alpha 039
Alpha 040
Alpha 041

DEVICE
21f
21f
21f
21f
21f
2lf
21f
21f
21f
21f
21f
2lf
2lf
2lf
21f
21f
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
Alpha AnalystlOODC
Alpha AnalystlOODC
Alpha Analystl OODC
Alpha Analystl OODC
Alpha AnalystlOODC
Alpha AnalystlOODC
Alpha AnalystlOODC
Alpha AnalystlOODC
Alpha AnalystlOODC
Alpha Analystl OODC

PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
Peak Energy
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
'"'v
'1.,-"
ALL
ALL
u
ALL
ALL
ALL
ALL
ALL
ALL
Peak CPS
Peak CPS
Peak CPS
PeakFWHM
Peak CPS
ALL
ALL
ALL
ALL
ALL

FLAG
Not Done
Not Done
Passed
Passed
Not Done
Not Done
Not Done
Not Done
Not Done
Passed
Passed
Passed
Passed
Passed
Action
Not Done
Not Done
Passed
Passed
Not Done
Not Done
Passed
Passed
Passed
Passed
Not Done
Passed
Not Done
Passed
Not Done
Passed
Not Done
Action
Action
Action
Action
Action
Passed
Passed
Passed
Passed
Passed

DATE

8/12/2013 5:20:50 AM
8/12/2013 5:20:50 AM

8/12/2013
8/12/2013
8/12/2013
8/12/2013
8/12/2013
8/12/2013

5:20:51 AM
5:20:52 AM
5:20:53 AM
5:20:53 AM
5:20:54 AM
5:20:55 AM

8/10/2013 11:23:01 AM
8/12/2013 5:20:55 AM

8/12/2013
8/12/2013
8/12/2013
8/12/2013

5:20:56 AM
5:20:57 AM
5:20:57 AM
5:20:58 AM

8/12/2013 5:20:59 AM
8/12/2013 5:20:59 AM
8/12/2013 5:21:00 AM
8/12/2013 5:21:01 AM
8/12/2013 5:21:02 AM
8/9/2013 5:06:44 AM
8/12/2013 5:21:05 AM
8/12/2013 5:21:05 AM
8/12/2013 5:21:06 AM
8/12/2013 5:21:09 AM
8/12/2013 5:21:10 AM
8/12/2013 5:21:12 AM
8/12/2013 5:22:26 AM

!11

Page 2 of 2

Review of QA Results - Pulser Check


8/12/2013 6:43:21 AM

CHAMBER
Alpha 042
Alpha 043
Alpha 044
Alpha 045
Alpha 046
Alpha 047
Alpha 048

DEVICE
Alpha AnalystlOODC
Alpha AnalystlOODC
Alpha Analyst! OODC
Alpha AnalvstlOODC
Alpha AnalystlOODC
Alpha AnalystlOODC
Alpha Analyst! OODC

PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
ALL

APPROVED BY:

APPROVAL DATE:

FLAG
Passed
Passed
Passed
Passed
Passed
Passed
Passed

DATE
8/12/2013 5:21:15 AM
8/12/2013 5:22:23 AM
8/12/2013 5:22:22 AM
8/12/2013 5:21:19 AM
8/12/2013 5:21:21 AM
8/12/2013 5:21:22 AM
8/12/2013 5:21:24 AM

6/12/12

Library Listing Report

Page

12:17:04 PM

*************************************************************************
L I B R A R Y L I S T I N G R E P 0 R T
*****
*****
*************************************************************************
Nuclide Library Title:

Uranium

Nuclide Library Description:


Nuclide
Name

Half-Life
(Seconds)

U-232
U-234
U-235
U-238

2.174E+009
7.731E+Ol2
2.221E+Ol6
1. 410E+Ol 7

Energy
(keV )

U-232,-234,-235,-238
Energy
Uncert. (keV
0.000
0.000
0.000
0.000

5302.500*
4761.500*
4385.500*
4184.400*

Yield
(%)
99.8000
99.8000
80.9000
100.2300

Yield
Uncert . (Abs . +- )
0.0000
0.0000
0.0000
0.0000

key line

TOTALS:

Nuclides

Energy Lines

1178

SECTION IX

ANALYTICAL DATA (ISOTOPIC THORIUM)

Eberline Services
Oak Ridge Laboratory
Analysis Sheet

Printed: 8112/2013 5:48 AM


Page 1of3

13-07149
Th ISO
Run 1

13-07149

Work Order

Internal
Fraction

Sample
Desc

Client
ID

Login
CPM

Sample
Date

Sample
Aliquot

ThiSO

Analysis Code

01

LCS

i 07 /23/13 00:00

LCS

1.0000E+OO
-

----

Run
Date Received I

02

MBL

BLANK

03

DUP

D-81 TOT

04

TRG

05

West Lake OU-1

7/22/2013

07/23/13 00:00

1.0000E+OO

45

07/17/13 10:43

1.0000E+OO

PZ-302-AS TOT

46

07 /16/13 15:30

1.0000E+OO

TRG

PZ-302-AS DIS

46

07/16/13 15:30

1.0000E+OO

06

TRG

LR-100 TOT

47

07/17/13 10:23

1.0000E+OO

07 /17/13 10:23

1.0000E+OO

07/17/13 10:43

1.0000E+OO

07/17/13 10:43

1.0000E+OO

07/17/13 11 :40

1.0000E+OO

~--

Lab Deadline I

8/13/2013

Client I Engineering Management Support, Inc.


Project I

Report Level

07

TRG

LR-100 DIS

47

Activity Units

pCi

08

DO

D-81 TOT

45

09

TRG

D-81 DIS

45

10

TRG

PZ-204-SS TOT

43

11

TRG

PZ-204-SS DIS

43

07/17/13 11 :40

1.0000E+OO

12

TRG

LR-103 TOT

45

07/17/13 12:15

1.0000E+OO

Aliquot Units
Matrix
Method

WA

HASL 300, 4.5.2

Instrument Type

Alpha Spectroscopy

Radiometric Tracer

Th-229

13

TRG

LR-103 DIS

45

07/17/13 12:15

1.0000E+OO

Radiometric Sol#

Th-18a

14

TRG

PZ-111-KS TOT

41

07/17/13 13:09

1.0000E+OO

Tracer Act (dpm/g)

22.466

15

TRG

PZ-111-KS DIS

41

07/17/13 13:09

1.0000E+OO

Carrier
Carrier Cone (mg/ml)

t!fll
1-

00

Q~

SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only_

Actual mass exceeded the calibration curve range_ Results should be qualified as appropriate.

Eberline Services
Oak Ridge Laboratory
Analysis Sheet

Printed: 811212013 5:48 AM


Page 2 of 3

13-07149

Th ISO

Run 1

Internal
Fraction

Sample
Desc

01

LCS

Tracer
Aliquot(g)

o.4782

Tracer Total
ACT(dpm)

10.7

Radiometric i Grav Carrier


%Rec
i Added{ml)

Radiometric
Tracer (pCi)

0.00

-~------

02

MBL

0.2381-t

5.3

0.00

03

DUP

0.2355

5.3

0.00

04

TRG

0.2340

-1

5.3

0.00

Grav Filter
Tare (g)

Grav Filter
Final{g)

Grav Filter
Net(g)

TRG

0.2352

SAF

Mean
%Rec

SAF
2*

1*

. ---

---~

---

--

'

05

Grav
%Rec

------

-------

f----

5.3

0.00
I

06

TRG

0.2345

5.3

0.00
-----

07

TRG

0.2339

5.3

0.00

08

DO

0.2339

5.3

0.00

09

TRG

0.2321

5.2

0.00

10

TRG

0.2323

5.2

0.00

11

TRG

0.2340

5.3

0.00

-------

--

---

12

TRG

0.2307

5.2

0.00

13

TRG

0.2327

5.2

0.00

14

TRG

0.2333

5.2

0.00

15

TRG

0.2323

5.2

0.00

II

I
i

----

I
i

---

I
I

~l;ll!
UWI"'

00
i--"~

SAF1

-----

is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only.

Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.

-----

Eberline Services
Oak Ridge Laboratory
Analysis Sheet

Printed: 8/12/2013 5:48 AM


Page 3 of 3

13-07149

Th ISO

Run 1

Internal
Fraction

Sample
Desc

01

LCS

Rough Prep
Date

Rough Prep
By

04
05

JWOLFE

SeptO
Date/Time

JWOLFE

------

08/05/13 09:20

JWOLFE

TRG

I 08105113 09:20

JWOLFE

TRG

08/05/13 09:20

JWOLFE

08/05/13 09:20

JWOLFE

I 08105113 09:20

JWOLFE

1 08/05/13 09:20

JWOLFE

TRG
TRG

08

DO

TRG

10

TRG

08/05/13 09:20

JWOLFE

11

TRG

I 08/05/13 09:20

JWOLFE

12

TRG

08/05/13 09:20

JWOLFE

13

TRG

08/05/13 09:20

JWOLFE

TRG

08/05/13 09:20

JWOLFE

08/05/13 09:20

JWOLFE

TRG

15

08/05/13 09:20

--

'

-- --

I
I

l__
I

--

09

1
-

14

Sep t1
By

07

Sep t1
Date/Time

=-f-=

----

06

Sep to
By

08/05/13 09:20
------

DUP

08/05/13 09:20
---

MBL

03

Prep
By

---

02

Prep
Date

JWOLFE
--

- -

I
I
-~

!l2JI
Qw.idi1

SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only.

**Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.

Eberline Services
Oak Ridge Laboratory

(
~
.g
0

(.)

.!(!

<ac:

<:(

"""""

en

-I

.c

Sample
Desc

Client
Identification

Activity
Units

01

TH-228

LCS

LCS

pCi/I

4.65E+OO I

6.99E-01

1.13E-01

02

TH-228

MBL

BLANK

pCi/I

5.87E-02 I

1.29E-01 I

2.44E-01

TH-228

DUP

D-81 TOT

pCi/I

4.31 E-02 I

5.50E-02 I

8.19E-02

03

...

....c:
Cll

E
Cll

Cl

ca
c:
ca
:i1

c:

Cll
Cll

.5

Cl

c:

w
~~I
~iHJih

4.87E+OOI

LCS
%R

LCS
Flag

95.61

OK

RPO

OK

NA

OK

1.69E-011

1.19E-011

1.11E-01

OK

05

TH-228

TRG

PZ-302-AS DIS

pCi/I

6.72E-03 I

4.22E-02 I

1.02E-01

OK

06

TH-228

TRG

LR-100 TOT

pCi/I

-1.60E-031

8.50E-021

1.98E-01

OK

07

TH-228

TRG

LR-100 DIS

pCi/I

4.57E-021

6.87E-021

1.11E-01

OK

08

TH-228

DO

D-81 TOT

pCi/I

6.31 E-02 I

6.90E-02 I

8.24E-02

OK

09

TH-228

TRG

D-81 DIS

pCi/I

6.92E-02 I

8.39E-02 I

1.30E-01

OK

TH-228

TRG

PZ-204-SS TOT

pCi/I

9.05E-02 I

7 .22E-02 I

6.50E-02

OK

14
15

OK

OK

pCi/I

13

Blank
Flag

MDA
Flag

Flag

PZ-302-AS TOT

--------1----------+------~--~--~---+-~------1~--~--t~~~~~-+~~~~~+-~~~~~+--~~~~+-~~~~-t-~----1----~---t-~--~---1

TH-228

TRG

PZ-204-SS DIS

pCi/I

1.22E-021

7.10E-021

1.61E-01

OK

TH-228

TRG

LR-103 TOT

pCi/I

5.89E-02 I

8.58E-02 I

1.43E-01

OK

TH-228

~I
TRG

LR-103 DIS

pCi/I

1.69E-02

6.32E-02/

1.33E-01

TH-228

PZ-111-KS TOT

pCi/I

1.94E-02

6.28E-02

1.30E-01

OK

TRG

---~z-111-K_s DIS

pCitl

-3.39E-04

3.58E-02

1.osE-01

OK

__--;;_;;;

-I

-------i-----1---------------
1------+--------L____,_______
1

1--------------+------- _

OK

1--------+-----------------L--+-
~1--------------1---1-~-----------

Cl

;::

TRG

12

Q.
Q.
::I
(/)

LCS
Known

MDA

TH-228

11

IError Estimate

04

10

cj

Results

-j--------------t-----,

f--------------t--

.5

Work Order: 13-07149-ThlS0-1

Nuclide

Lab

Fraction

Printed: 8/13/2013 8:54 AM

Page 1 of 3

Preliminary Data Report & Analytical Calculations

Lab
Fraction

01

Work Order: 13-07149-ThlS0-1

Nuclide

Sample
Desc

Sample
Date

TH-228

LCS

07/23/13 00:00

Sample
Aliquot

1.00E+OO

a::

8
.!!!
(I)

~
Ill

~I

02
~

TH-228

-.r:.
....

MBL

~~i
05

06

Mean
%Rec

Grav
%Rec

SAF

0.00

0.00

---------

1.00E+OO

I
48.42!

0.00

0.00

0.00

0.00

0.00

0.00

DUP

07/17/13 10:43

1.00E+OO

96.95

TH-228

TRG

07/16/13 15:30

1.00E+OO

74.151

TH-228

TRG

07/16/13 15:30

1.00E+OO

101.841

0.00

0.00

TRG

07/17/13 10:23

1.00E+OO

73.691

0.00

0.00

TH-228

TRG

TH-228

DO

07/17/13 10:23

1.00E+OO

93.451

0.00

0.00

07/17/13 10:43

1.00E+OO

95.13

0.00

0.00

-
TH-228

TRG

07/17/13 10:43

1.00E+OO

114.28

0.00

0.00

TH-228

TRG

07/17/13 11:40

1.00E+OO

117.11

0.00

0.00

TH-228

TRG

07/17/13 11:40

1.00E+OO

81.10

0.00

0.00

TH-228

TRG

07/17/13 12:15

1.00E+OO

83.25

0.00

0.00

TH-228

TRG

07/17/13 12:15

1.00E+OO

103.65

0.00

0.00

TH-228

TRG

07/17/13 13:09

1.00E+OO

92.39

0.00

0.00

TH-228

TRG

07/17/13 13:09

1.00E+OO

113.75

0.00

0.00

~-

10
11

---

------~

12
~----

13
f--------------

0
0.
0.

:I

...s::

(/)

14
~-

15
-------~

--
I

Q)

I: I
~I
o,

E
Q)

Cl

-------

Ill

s::

Ill

::!!:

------

---------

------------

!t!ltl1
!!>~$.

I
--

09

t::

Sep t1
Date/Time

SeptO
Date/Time

--------

----~---

07/23/13 00:00

- -------

08
1----

118.131

TH-228

TH-228
--

07
1---

- ------

~---

-- -- ---

----------!--

tn

Radiometric
%Rec

---~----

i::

Printed: 8/13/2013 8:54 AM

Page 2of3

Preliminary Data Report & Analytical Calculations

Eberline Services
Oak Ridge Laboratory

c:

::i

ll::

Lab
Fraction

Nuclide

01

TH-228

02
~

03
--~

~
0
u
.!!,!

"'c:

"'(

04

en

.c

I-

05
06
07

Printed: 8/13/2013 8:54 AM

Page 3 of 3

Preliminary Data Report & Analytical Calculations

Eberline Services
Oak Ridge Laboratory

Work Order: 13-07149-ThlS0-1

-+
1

Sample
Desc

Counting
Date/Time

LCS

Halflife
(days)

Count
Time

Bkg
CPM

Counts

Carrier

08/12/13 12:55

A_Spec

Alpha_004

170.02 4.02 E+02

2.30 E-02

19.4

08/12/13 12:55

A_Spec

Alpha_010

170.02 2.11 E+OO

11.70 E-02

19.7

-------

------ -

TH-228

MBL

TH-228

DUP

__________________(_____

08/12/13 12:55

A_Spec

Alpha_011

170 3.15 E+OO

5.00 E-03

20.5

08/12/13 12:55

A_Spec

Alpha_012

170 9.15 E+OO

5.00 E-03

19.9

08/12/13 12:55

A_Spec

Alpha_013

9.00 E-03

18.7

08/12/13 12:55

A_Spec

Alpha_014

170 -7.99 E-02

2.40 E-02

18.5

08/12/13 12:55

A_Spec

Alpha_015

170 2.32 E+OO

4.00 E-03

14.8

DO

08/12/13 12:55

A_Spec

Alpha_019

170 3.66 E+OO

2.00 E-03

16.6

TRG

08/12/13 12:55

A_Spec

Alpha_022

170 4.45 E+OO

1.50 E-02

15.3

08/12/13 12:55

A_Spec

Alpha_023

170 6.66 E+OO

2.00 E-03

17.1

1.40 E-02

17.1

I ---
--- ---------- --- ----l--

TH-228

Eff

Detect

-------

TRG

--+-----

--~~-2~-rG
TH-228

TRG
-

---~-

TH-228

TRG
-

---~

08

TH-228

09

TH-228

10

TH-228

11

TH-228

l~G

12

TH-228

TRG

170.02 4.70 E-01

TRG

170 6.20 E-01

08/12/13 12:55

A_Spec

Alpha_024

08/12/13 12:55

A_Spec

Alpha_025

170.02 3.13 E+OO

1.10 E-02

17.4

13

TH-228

TRG

08/12/13 12:55

A_Spec

Alpha_027

170.02 1.11 E+OO

1.70 E-02

17.3

14

TH-228

TRG

08/12/13 12:55

A_Spec

Alpha_029

170.02 1.28 E+OO

1.60 E-02

19.5

15

TH-228

TRG

08/12/13 12:55

A_Spec

Alpha_031

170.02 -2.01 E-02

6.00 E-03

14.2

-=~
Q.
Q.

::s

fl)

....c:

.....
c:
.S!

- -

Cl)

E
Cl)
Cl

ns
ns

r::

:E
Cl

r::

;:
Cl)
Cl)

.5

Cl

r::

w
~i:il
~

....

Eberline Services
Oak Ridge Laboratory

~
s:::

::s

I
I

Nuclide

01

02

- ----1--.
03 i

--()4
.g

en

.!(!

"'s:::
ct

.c

Desc

Client
Identification

Activity
Units

TH-230

LCS

LCS

pCi/I

4.95E+OO

7.33E-01

8.51E-02

TH-230

MBL

BLANK

pCi/I

3.98E-01

2.38E-01

2.0SE-01

TH-230

DUP

D-81 TOT

t-

pCi/I

2.65E-01

1.24E-01

5.57E-02

pCi/I

4.29E-01

1.90E-01

7.51E-02

pCi/I

2.60E-01

1.27E-01

6.67E-02

pCi/I

5.53E-01

2.31E-01

1.10E-01

0
.E
~
0

c..
c..

:I

....c:

CJ)

MDA

LCS
Known

5.45E+OO

LCS
%R

LCS
Flag

90.74

OK

RPO
Flag

MDA
Flag

Blank
Flag

OK

Cl>
Cl

ns
c:
ns

:!:
Cl

c:
;:
Cl>
Cl>

.5

Cl

INV

=+

OK
OK

TH-230

TRG

PZ-302-AS DIS

TH-230

TRG

LR-100 TOT

TRG

LR-100 DIS

pCi/I

4.10E-01

1.93E-01

1.0SE-01

OK

DO

D-81 TOT

pCi/I

3.70E-01

1.71E-01

1.01E-01

OK

TRG

D-81 DIS

pCi/I

3.03E-01

1.SOE-01

1.18E-01

OK

TRG

PZ-204-SS TOT

pCi/I

2.94E-01

1.33E-01

7.94E-02

OK

11

TH-230

TH-230

TRG

PZ-204-SS DIS

pCi/I

5.51E-01

2.31E-01

1.26E-01

OK

12

TH-230

TRG

LR-103 TOT

pCi/I

5.20E-01

2.17E-01

1.04E-01

OK

13

TH-230

TRG

LR-103 DIS

pCi/I

5.53E-01

2.04E-01

1.09E-01

OK

TH-230

TRG

PZ-111-KS TOT

pCi/I

4.23E-01

1.71E-01

7.06E-02

OK

TH-230

TRG

PZ-111-KS DIS

4.SSE-01

1.96E-01

8.63E-02

OK

~fJ=
-

OK
OK

~-------

14
~------

15

---f-!Ci/I
I

----- --------

-------+-

I
I
-----~---!-----~---

c:

OK

PZ-302-AS TOT

Cl>

"""'"'

Error Estimate

TRG

10

~~!1

Results

TH-230

-----~

~I

Sample

_____J

eJH_. :::::

Work Order: 13-07149-ThlS0-1

-------1

a::

Lab
Fraction

Printed: 8/13/2013 8:54 AM

Page 1of3

Preliminary Data Report & Analytical Calculations

------~---1
!

OK

Lab
Fraction

Nuclide

01

TH-230

Work Order: 13-07149-ThlS0-1


I Sample
i

-----

~I

__J ______

""""

~
0

.!(!

~
Cii
i:::

'<I:

TH-230
TH-230

en

.c

05

TH-230

---

06

07

t.i
.E

;:::
0

a.
a.

:::i
(/)

....c:

1.00E+OO

0.00

MBL

--------

0.00

0.00

DUP

------

I TRG

07/17/13 10:43

1.00E+OO

07/16/1315:30

1.00E+OO

07/16/13 15:30

!---------

TRG
- -

-----

-------~---

3
5

0.00

0.00

0.00

0.00

1.00E+OO

74.151
------+-
101.841

0.00

0.00

07/17/13 10:23

1.00E+OO

73.69

0.00

0.00

07/17/13 10:23

1.00E+OO

93.45

0.00

0.00

07/17/13 10:43

1.00E+OO

95.13

0.00

0.00

07/17/13 10:43

1.00E+OO

114.28

0.00

0.00

07/17/1311:40

1.00E+OO

117.11

0.00

0.00

'

HTG
TRG

TH-230

DO

1~-RG-

~-

11

TH-230

-+~~--

07/17/1311:40

1.00E+OO

81.10

0.00

0.00

12

TH-230

-~ TRG_

07/17/13 12:15

1.00E+OO

83.25

0.00

0.00

13

TH-230

TRG

07/17/13 12:15

1.00E+OO

103.65

0.00

0.00

14

TH-230

TRG

07/17/13 13:09

1.00E+OO

92.39

0.00

0.00

07/17/13 13:09

1.00E+OO

113.75

0.00

0.00

- - - -- - - - -

15
-----

~-----

TH-230

+---

! TRG

I
--r----

=G---
I

------

t~~~

-----+-----
------1---

II

I
i

--

--~------~

Q)
Q)

Cl

0.00

TH-230

c:

c:
w

118.13

SAF

10

"'c:

.5

Mean
%Rec

Grav
%Rec

TH-230

GI

Cl

;:

II
----- -

-----------~--:---

'"'.,J\

07/23/13 00:00

J
1

09

Cl

il>~!lt.

1.00E+OO

-----+----
i

TH-230

GI

"'
::!!!

07/23/13 00:00

Radiometric
%Rec

!------------------ ---------

c--

lti.l!~I

LCS

+------

08

(3 '

04

------~

jl

Sample
Aliquot

TH-230

03

Sample
Date

-t -------

f----

Desc

02

Printed: 8/13/2013 8:54 AM

Page 2 of 3

Preliminary Data Report & Analytical Calculations

Eberline Services
Oak Ridge Laboratory

- .. --

--

-----

Ii
Ii
I

Sep to
Date/Time

Sept1
Date/Time

01

Work Order: 13-07149-ThlS0-1

~
_ o_D=~-2 __
Lab
Fraction

a:

""""

,___~~_J

04
~

.!/2
~

i'a

i::

ct

-..c:

05

TH-230

A_Spec

ML

08112113 ,,,..

[ __

A_soec

I.,,

._,101

110.02I1.43 . . .1

DUP

08/12/1312:55

----!----

A_Spec

1Alpha_o111

TRG

08/12/13 12:55

A_Spec

c.i

.E

I-

"

17011.98 E+01

11.00 E-03

20.~

Alpha_012

17012.38 E+01

11.00 E-03

19.9

A_Spec

Alpha_013I

170.0211.87 E+01

2.00 E-03

18.7

A_Spec

Alpha_014

17012.83 E+01

4.00 E-03

18.5

A_Spec

Alpha_015

17012.13 E+01

4.00 E-03

14.8

A_Spec

Alpha_019

170 I2.20 E+01

0.00 E+OO

16.6

A_Spec

Alpha_022

170 2.00 E+01

1.20 E-02

08/12/13 12:55 ---~

A_Spec

Alpha_023

170 2.22 E+01

5.00 E-03

17.1

08/1211312:55

A_Spec

Alpha_024

170 2.88 E+01

7.00 E-03

17.1

TH-230

13

Q.
Q.

15 I

::J
(/)

08/12/1312:55

TRG
TRG

--~8/12/1-; 12:5;---r-

-t
I

A_Spec

IA1pha_0251

170.0212.83 E+01

14.00 E-03

17.4

TH~~-0- +TRG

08/12/1312:55

A_Spec

Alpha_027

170.02 3.73 E+01

1.00 E-02

17.3

TRG

08/12/13 12:55

A_Spec

IA1pha_029I

170.0212.87 E+01

12.00 E-03

19.5

I TRG I

08/12/13 12:55

A_Spec

IA1pha_0311

170.0212.95 E+01

13.00 E-03

14.2

TH-230

+-----------r----<C-----

(l)

Cl

cu

--r

c:
cu
:ii:
Cl
c:

;::

(l)
(l)

c:
w

!----+-----------+-----

---j----
1

r,J;\11

if-"

15.3

08/12/13 12:55

(l)

Cl

TRG

.5

I1.00

: : : :: : t

DO

TH-230

12

19.4

1.00 E-02

-02

08/12/13 12:55

TRG

~-230

t0

....c:

TRG

TH~230
TH-230

170.0214.27 E+02

Eff

CPM

-+-------

~--

11

Alpha_0041

TH-230

-fo+

Bkg

Counts

Carrier

08/12/1312:55

~~ii ~:~- ::
I

-~

30

TH-230

08

Count
Time

Detect

LCS

TH-230

!-------+----------~--

CJ)

Halflife
(days)
I

____ TH-23~-

Counting
Date/Time

Sample
Desc

Nuclide

Printed: 8/13/2013 8:54 AM

Page 3 of 3

Preliminary Data Report & Analytical Calculations

Eberline Services
Oak Ridge Laboratory

Eberline Services
Oak Ridge Laboratory

Lab

01
Q:

TH-232

03

04

.!!!

~
'iii

Activity
Units

LCS

LCS

pCi/I

4.44E+OO

6.72E-01

6.92E-02

BLANK

pCi/I

1.01E-01

1.27E-01

1.91E-01

D-81 TOT

pCi/I

3.77E-02

4.58E-02

5.56E-02

Results

IError Estimate

MDA

LCS
Known

4.87E+OO

LCS
%R

LCS
Flag

91.26

OK

RPO
Flag

MDA
Flag

MBL

OK
OK

~-

DUP

NA

OK

-----

TRG

PZ-302-AS TOT

pCi/I

2.18E-01

1.34E-01

1.08E-01

OK

TRG

PZ-302-AS DIS

pCi/I

5.33E-02

5.54E-02

5.81E-02

OK

.c

TRG

LR-100 TOT

pCUI

-1.32E-02

4.04E-02

1.10E-01

OK

TH-232

TRG

LR-100 DIS

pCi/I

3.51E-02

5.40E-02

8.01E-02

OK

08

TH-232

DO

D-81 TOT

pCi/I

4.47E-02

5.81E-02

8.03E-02

OK

09

TH-232

TRG

D-81 DIS

pCi/I

3.77E-02

5.25E-02

7.94E-02

OK

TH-232

TRG

PZ-204-SS TOT

pCi/I

3.29E-02

4.59E-02

6.94E-02

OK

TH-232

TRG

PZ-204-SS DIS

pCi/I

6.02E-02

7.71E-02

1.14E-01

OK

LR-103 TOT

pCi/I

5.SOE-02

7.26E-02

1.10E-01

OK

LR-103 DIS

pCl/I

8.SOE-02

7.91E-02

9.75E-02

OK

PZ-111-KS TOT

pCi/I

-1.75E-02

3.18E-02

9.71E-02

OK

PZ-111-KS DIS

pCi/I

2.46E-03

3.44E-02

9.83E-02

OK

TH-232

~~~:~+=:=:
.....

ti)

07

---------

~-

-----

10
11

f----~
12
---~~

.E

~
0

c..
c..

:::s
en

....c:

13
1---------

E
Q)
Cl

ns
c:
ns
:?:

TH-232

r------

-------

TRG

TH-232

TRG

- - - - - - - - f--

15
f-------------

TRG
!---~

- - - - - - - - - r----- - - - - -

14
-------

Q)

.~I
0

TH-232
-------

----

~=tTRG

--

--~

~~-~~~~=--

Cl

c:

-
-

;:::
Q)
Q)

.5

Cl

c:

w
fJ\~
.....

----~

-------

Blank
Flag

---

TH-232

---------

Client
Identification

-t---t---
02

Sample
Desc

TH-232
--------

Work Order: 13-07149-ThlS0-1

Nuclide

Fraction

Printed: 8/13/2013 8:54 AM

Page 1of3

Preliminary Data Report & Analytical Calculations

I
I

=r=

OK

a::

8
.!(!

~
cuc::
ct

Sample
Date

01

TH-232

LCS

01123113 00:00

1.00E+OO

118.13

0.00

0.00

07/23/13 00:00

1.00E+OO

48.42

0.00

0.00

07/17/13 10:43

1.00E+OO

96.95

0.00

0.00

07/16/13 15:30

1.00E+OO

74.15

0.00

0.00

04

~----

en

-I.c:

_ _2H-23-=-----r- MBL _- - - - -
TH-232
TI<-232

i DUP

SAF

I
!

TRG

-~-------

Radiometric
%Rec

Mean
%Rec

Sample
Desc

-----

Sample
Aliquot

Grav
%Rec

Nuclide

03

~---

Work Order: 13-07149-ThlS0-1

Lab
Fraction

02
~

Printed: 8/13/2013 8:54 AM

Page 2 of 3

Preliminary Data Report & Analytical Calculations

Eberline Services
Oak Ridge Laboratory

----

~~---

"

05

TH-232

TRG

07/16/13 15:30

1.00E+OO

101.84

0.00

0.00

06

TH-232

TRG

07/17/13 10:23

1.00E+OO

73.69

0.00

0.00

I
I

---

f--------

07

TH-232

TRG

07/17/13 10:23

1.00E+OO

93.45

0.00

0.00

08

TH-232

DO

07/17/13 10:43

1.00E+OO

95.13

0.00

0.00

TRG

07/17/13 10:43

1.00E+OO

114.28

0.00

0.00

~----

09

TH-232

- -- - - -

10

TH-232

TRG

07/17/13 11 :40

1.00E+OO

117.11

0.00

0.00

11

TH-232

TRG

07/17/13 11:40

1.00E+OO

81.10

0.00

0.00

12

TH-232

TRG

07/17/13 12:15

1.00E+OO

83.25

0.00

0.00

13

TH-232

TRG

07/17/13 12:15

1.00E+OO

103.65

0.00

0.00

14

TH-232

TRG

07/17/13 13:09

1.00E+OO

92.39

0.00

0.00

15

TH-232

TRG

07/17/13 13:09

1.00E+OO

113.75

0.00

0.00

~-

.5
0

Q.
Q.

::I
fl)

....c:
Q)

~I

Q)

Cl
<'<I

c:
<'<I
:!:
Cl
c:

c:
Q)

~----

~------

Q)

.!:

Cl

w
~

~"

U:li
(;!~

----

~~_-_

SeptO
Date/Time

Sept1
Date/Time

01
!---------

Sample
Desc

Counting
Date/Time

TH-232

LCS

TH-232

~1

~0

.!!!

~
c:

q:

0
en

..c

A_Spec

Alpha_004

170.02 3.84 E+02

5.00 E-03

19.4

MBL

08/12/13 12:55

A_Spec

Alpha_010

170.02 3.64 E+OO

8.00 E-03

19.7

DUP

08/12/13 12:55

A Spec

Alpha_011

170 2.83 E+OO

1.00 E-03

20.5

TH-232

TRG

08/12/13 12:55

A_Spec

Alpha_012

170 1.21 E+01

5.00 E-03

19.9

TH-232

TRG

08/12/13 12:55

A_Spec

Alpha_013

170.02 3.83 E+OO

1.00 E-03

18.7

TRG

08/12/13 12:55

A_Spec

Alpha_014

170 -6.80 E-01

4.00 E-03

18.5

TH-232

TRG

08/12/13 12:55

A_Spec

Alpha_015

170 1.83 E+OO

1.00 E-03

14.8

TH-232

DO

08/12/13 12:55

A_Spec

Alpha_019

170 2.66 E+OO

2.00 E-03

16.6

TH-232

TRG

08/12/13 12:55

A_Spec

Alpha_022

170 2.49 E+OO

3.00 E-03

15.3

TH-232

TRG

08/12/13 12:55

A_Spec

Alpha_023

170 2.49 E+OO

3.00 E-03

17.1

TH-232

TRG

08/12/13 12:55

A_Spec

Alpha_024

170 3.15 E+OO

5.00 E-03

17.1

TRG

08/12/13 12:55

A_Spec

Alpha_025

170.02 3.00 E+OO

0.00 E+OO

17.4

TRG

08/12/13 12:55

A_Spec

Alpha_027

170.02 5.81 E+OO

7.00 E-03

17.3

A_Spec

Alpha_029

170.02 -1.19 E+OO 17.00 E-03

19.5

A_Spec

Alpha_031

170.02 1.50 E-01

14.2

f--------------

07
~

08

--=I -

-~9

10

+--=

j,...........-------------

TH-232

----

f-

06
----~

Eff

08/12/13 12:55

TH-232

05
.......--.----~

Bkg
CPM

Counts

Carrier

-------

04

-----

Count
Time

Detect

------------

03

----~---

Halflife
(days)

----

02

r-----

Work Order: 13-07149-ThlS0-1

Nuclide

Lab
Fraction

Printed: 8/13/2013 8:54 AM

Page 3 of 3

Preliminary Data Report & Analytical Calculations

Eberline Services
Oak Ridge Laboratory

__

-- f-------------

11

--

12

TH-232

- - - r---------------

t.i
.E

13
---~

~0

a.
a.
:::i

Cl)

.....c:

14
-

15

Cl

-----~

C'O

c:
C'O

:E

---

Cl

c:

;:
QI

QI

c:
c:

c,

w
!'.!!~
~""''

CJ()

It""

08/12/13 12:55

TRG

---

TH-232
__________
,._________

08/12/13 12:55

TRG

5.00 E-03

- ---- ---+-
----------r
I

E
QI

TH-232

--------~

QI

i:

TH-232
-----------

~--

==--=---1~ .

~------

f--

I
I

Count Room Report


Client: Engineering Management Su

Printed: 8112/2013 5:48 AM


Page 1of1

13-07149-ThlS0-1 (pCi/I) in WA
Tracer ID: Th-18a

..,/\- \v-"

x-6

Sample
Desc

Client
ID

01

LCS

LCS

02

MBL

BLANK

03

DUP

D-81 TOT

Internal
Fraction

Sample
Date

Sample
Aliquot

07/23/13 00:00

1.0000

I 07/23/13 00:00

1.0000

I
I

--

I
I

~-

ra~/17/13 10:43

1.0000

04

TRG

PZ-302-AS TOT

I 07/16/13 15:30

1.0000

05

TRG

PZ-302-AS DIS

la7/16/13 15:30

1.0000

I
!
I

~\

-<

06

TRG

LR-100 TOT

07

TRG

08
09

0.00

0.2381

5.3492

0.00

0.2355

5.2907

0.00

5.2570

0.00

5.2840

0.00

0.2345

5.2683

0.00

0.2339

5.2548

0.00

0.2339

5.2548

0.00

0.2321

5.2144

0.00

0.2323

5.2189

0.00

0.2340

5.2570

0.00

0.2307

5.1829

0.00

0.2327

5.2278

0.00

0.2333

5.2413

0.00

0.2323

5.2189

0.00

LR-100 DIS

07/17/1310:23

1.0000

DO

D-81 TOT

07/17/13 10:43

1.oooo-1-

TRG

D-81 DIS

07/17/13 10:43

1.0000

SAF
1*

%Rec

0.2352

1.0000

PZ-204-SS TOT

IRadiometric

~--

07/17/13 10:23

TRG

Radiometric
Tracer (pCi)

10.7432

'

10

Tracer
ACT(dpm)

0.4782

1 0.2340

Tracer
Aliquot(g)

07/17/1311:40

1.0000
I

11

TRG

PZ-204-SS DIS

07/17/13 11 :40

-""~-

12

TRG

LR-103 TOT

07/17/13 12:15

1.0000

13

TRG

LR-103 DIS

07/17/13 12:15

1.0000

14

TRG

PZ-111-KS TOT

15

TRG

PZ-111-KS DIS

1.0000

07/17/13 13:09

1.0000

07/17/1313:09

1.0000

I
I.

I
I

'
I
I

f~~))
~.,~.

(.l!JI
11'1,'l!

SAF
2*

Eberline Services
Oak Ridge Laboratory

lCS ~ llll~trix Spikes


Isotope

Activity
dpm/g

Sol#

Th-228 I
Th-230

Solution
Date

103.560

Th-8b
Th-1b

23.525

8/5/20131
I

Th-8b

103.560

..
fraction

01

'i;i)

Isotope

Sol#

Th-229

Th-18a

'

Approx
Addition

8/5/201..:L_

Th-232

8/5/2013[

Analvsis Code

Date

Technician

Th ISO

8/5/2013 9:18

JWOLFE

LC$.

.NIS

LCSD

MSD

Volume
Used(g)

Volume
Used(g)

Volume
Used(g)

Volume
Used(g)

O.'f~'l

0.100

111.

Tracers
Activity
dpm/g

','

22.466 I

Volume
Used(g)

Solution
Date

0.00

0.000

0.00

0.000

o.ooj

0.000

0.00

0.000

o.ooi

0.000

Error
Estimate

0.147

4.87

0.175

----r-
oooJ

0.000

0.00

0.000

22 .466

8/5/2~~ 3

0.2381
,'

03

Th-229

22 .466

81512013

0.2lJS5

0.2200

04

Th-229

Th-18a

22.4661

8/5/2013

o.~~~o -.

0.2200

05

Th-229

Th-18a

22.466t-;5/2013

(l.236:.!i

0.2200

06

Th-229

Th-18a

22 .466 I

8/5/2013

0.23:11:5.

0.2200

07

Th-229

Th-18a

22.4661

8/5/2013

-0.2~3~-

0.2200

08

Th-229

Th-18a

22.466

8/5/2013

o\23~~

0.2200

09

Th-229

Th-18a

22.466

8/5/2013

o.23~1

0.2200

0.2200

' '

;,;.'"

...

,/

. <i,,

-.a33'J

.:

10

Th-229

Th-18a

22.466

8/5/2013

0.2~3

0.2200

11

Th-229

Th-18a

22.466

8/5/2013

0:2Mo"1~

0.2200

'':', "I:'./

12
13
14
15

Th-229

Th-18a

22.466

8/5/2013

0.2~01

0.2200

Th-229

Th-18a

22.4661

8/5/2013

0)~27.

0.2200

Th-229

Th-18a

22.466

8/5/2013

Th-18a

22.466

8/5/2013

I
I Th-229

(1~333

0.2200

(),2323 '

0.2200

-.

II

'

..

~-l~

tie!

..

~ ~

Version 2.0 08/99

'. ..
.. \..

......

. I

Matrix Spike

,~

"

.. -. "' .. '

Error
Estimate

0.000

LCS

Tracer

Added
pCi

---

0.2200

Th-18a

0000

Balance Printer Tapes

Th-18a

0.00,

I
I
o.oolI

Known
pCi

Error
Estimate
--

:,,",

Approx
Addition

Q.4782-_

8/5/2013

Added
pCi

0.175

5.45

0.1043f ..

0.100

Error
Estimate

MSD

LCSD

MS

LCS

Known
pCi

4.87

Q.51~

0.500
--

Witness Initials

- -

Th-229

02

Page 1of1
Printed: 8/5/2013 9:20 AM

Spike and Tracer Worksheet

Eberline Analytical
Oak Ridge Laboratory

Lab
Fraction
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15

Engineering Management Support, Inc.

Client ID
LCS
BLANK
D-81 TOT
PZ-302-AS TOT
PZ-302-AS DIS
LR-100 TOT
LR-100 DIS
D-81 TOT
D-81 DIS
PZ-204-SS TOT
PZ-204-SS DIS
LR-103 TOT
LR-103 DIS
PZ-111-KS TOT
PZ-111-KS DIS

Printed: 8/5/2013 9:22 AM

Page 1 of 1

Aliquot Worksheet

Rpt Units

Lab Deadline

Technician

UUISO

liters

8/13/2013

JWOLFE

Dilution Data

Muffle Data
Ratio

Sample
Type
LCS
MBL
DUP
TRG
TRG
TRG
TRG
DO
TRG
TRG
TRG
TRG
TRG
TRG
TRG

Analysis Code

No of Dils

.. Post/Pre ..

..

Oil ractor

Aliquot Data
Ratio

.
.

.
:

...
.
:

.2

.,':

-:.

:.
,,

.:

::

Aliquot
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO ...:
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO ::.

MS Aliquot Data
Aliquot

illetEquiv
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
.1.0000E+OO
1.QOOOE+OO
1.000GE+OO
t.OQOOE+OO
1.000UE+OO
1.0000E+OO

illetEqll~v

H-3 Solids Only


HJ Dist
Aliq

Water Added
(ml)

:.

..

.
.

-.:
:

. .

I
~~~

.......

[i:J
~~"

Comments

Techn~;an

'

1:

~ Jt.i:)ui

Dale

~Q

Sample Description:

Spectrum File:

Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

SPIKE
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000659
1307149A-TH
01
Shelf 2
Th iso

Detector Name:

Alpha_004
Chamber Serial Number:

Detector Serial Number:


4
Env. Background:

System Bkgd 64765


Reagent Blank:

<not performed>
Sample Size:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

l.OOOE+OOO +/- O.OOOE+OOO liter


8/12/2013
7:20:26 AM
8/12/2013 12:55:09 PM
170.0 minutes
170.0 minutes

Tracer Certificate:

Tracer Quantity:

Effective Efficiency:

Counting Efficiency:

Chem. Recovery Factor:

Th229 TH-18A
0.478 mL

0.2292 +/- 0.0133

0.1940 +/- 0.0036 on 12/15/2012 11:26:46 AM


1.1813 +/- 0. 0718

Control Certificate Name:


NatTh Th-8

Chem. Recov. of Control:


TH-232
0.185048 +/Peak Match Tolerance:
0.175 MeV

PEAK
Energy
(MeV)

Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232

5.856
5.361
4. 871
4.622
3.953

Net
Pk Area

AREA

REPORT

Pk Area
Error %

25.15
402.09
418.64
427.30
384.15

0.015336

Ambient
Backgnd
0.85
3.91
1.36
1. 70
0.85

39.85
9.83
9.60
9.50
10.01

FWHM
(keV)

Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

2.9
12.4
5.1
15.2
12.5

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS

Nuclide

Id
Conf.

Energy
(keV)

TH-227
TH-228
TH-229
TH-230
TH-232

1.000
0.992
1. 000
0.987
0.990

5850.00*
5400.00*
4872.00*
4672.00*
3997.00*

Activity
(pCi/liter )
2.98E-001
4.65E+OOO
4.86E+OOO
4.95E+OOO
4.44E+OOO

+/+/+/+/+/-

1. 24E- 001
6.99E-001
5.52E-001
7.33E-001
6.72E-001

MDA
(pCi/liter
7.lOE-002
l.13E-001
7.96E-002
8.51E-002
6.92E-002

+/+/+/+/+/-

8.06E-003
l.28E-002
9.05E-003
9.66E-003
7.86E-003

fG

8(lJ/t~

9195

0000065907.CNF
Live Time 10201.000 sec
Rea1 Ti me 10201. 000 sec
start:
1 3493.l(kev)
stop : 1024 6486. 9(kev)
Acq. Start Mon Aug 12 12:55:09 2013

55

50

45

40

35

Vl

-I-'

c:

:::J

8 30

25

20

15

10

5
Q f'

1rn1 Ill!' u11uomqn)All"m111 1

3500

rn;ff1UJ!ID!!!!!lllll!n!f!l!U11111 1111 1111)(!q![1111

4000

4500

(il!!il

11

w: 1 P11

rrrn111m1:1w1 1w 111

5000
Energy(kev)

1111~vu1v1nn 1 11

lfj\ '1

5500

fiw1 '11m111111m

6000

Jliw11t!1

ROI Type: 1

"If.

ROI Type: 3

!l!JijOI!

n1111111u

ll un

11

'1

6500

Channel Data Report

8/12/2013

Page

4:30:57 PM

*******************************************************
s p E C T R A L DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

01

Elapsed Live time:


Elapsed Real Time:

10201
10201

Channell------l-------l-------l-------l-------1-------1-------1-------I
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:

10201
0
2
0
0
0
0
0
1
1
0
1
0
1
1
1
3
1
1
6
7
10
12
0
2
0
1
1
1
2
0
1
1
0
0
1
1
1
2
1
2
2
5
4
2
4

10201
0
2
2
1
0
2
0
0
0
2
0
1
0
1
2
5
1
2
7
5
11
7
1
0
0
0
0
0
1
0
0
2
0
2
2
0
1
3
1
0
2
3
1
3
4

0
0
0
1
1
2
1
0
0
2
1
1
1
1
2
2
2
5
5
6
7
12
7
0
0
0
1
1
0
0
0
0
0
0
0
0
2
2
0
1
3
0
0
0
3
2

0
1
0
0
0
0
2
1
1
2
1
1
0
1
1
4
3
2
6
2
13
4
10
1
0
1
0
0
1
1
1
0
0
1
0
0
1
2
0
0
1
1
4
2
1
3

0
0
0
0
0
0
1
0
2
1
0
0
1
4
3
3
2
2
4
5
9
15
6
0
1
0
0
0
0
1
0
1
0
0
1
0
0
0
1
0
2
1
1
0
2
2

0
0
0
0
0
0
0
0
1
0
0
0
2
1
0
2
3
2
4
8
8
11
2
0
0
1
0
1
1
0
0
2
1
0
1
0
1
2
1
0
1
2
2
1
3
2

0
1
0
0
0
0
1
1
3
0
0
1
2
0
3
1
3
6
9
5
7
8
6
0
1
2
0
0
0
0
0
0
1
1
2
1
2
0
2
1
3
1
4
1
0
3

0
0
0
3
0
1
0
0
0
1
2
2
1
5
2
2
2
7
3
6
17
6
4
0
0
0
0
1
1
0
0
1
0
0
2
1
2
2
1
1
0
1
0
0
2
4

8197

Channel Data Report


369:

8/12/2013
6

Sample Title:

4:30:57
3

PM
1

Page
5

01

Channell------l-------l-------1-------1-------1-------l-------l-------I
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:
625:
633:
641:
649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:

4
5
6
12
9
1
7
1
3
4
8
4
3
5
3
0
5
2
0
3
0
1
2
1
0
1
3
2
3
5
5
2
5
2
5
17
6
1
0
1
2
1
2
1
2
7
7
7
1
0
0
0
0

3
6
3
10
12
1
3
4
4
5
7
2
5
2
3
5
1
2
2
0
2
0
0
0
0
1
0
0
0
0
4
2
6
4
9
10
3
2
0
1
3
0
4
5
4
2
6
4
2
0
0
0
0

2
9
6
15
10
2
4
3
2
4
8
8
7
3
2
2
2
1
1
1
2
0
0
0
0
2
0
1
0
1
3
5
7
5
17
11
1
2
1
0
0
0
1
1
0
8
6
2
1
0
0
0
0

5
9
12
17
7
3
2
4
3
6
8
5
3
6
4
0
0
2
0
2
0
0
1
1
0
0
1
3
2
2
4
2
4
10
8
20
1
1
0
1
0
0
1
2
1
5
5
1
0
1
0
1
0

6
7
7
18
3
1
1
5
3
7
5
7
0
4
2
4
4
2
0
1
0
0
1
2
1
2
1
1
2
0
2
4
3
6
10
14
1
0
1
0
1
1
1
0
3
4
4
0
0
0
0
0
1

4
3
13
6
4
0
3
3
2
7
13
7
4
2
6
4
1
1
4
1
1
1
0
1
1
1
2
0
3
2
3
4
2
7
8
11
0
1
0
0
0
0
0
2
3
7
4
1
0
0
0
0
0

3
3
9
17
3
3
4
4
1
5
6
9
3
4
0
5
4
3
3
2
0
0
3
1
1
1
1
5
1
1
8
5
5
4
15
7
0
1
1
4
0
1
1
2
4
5
8
0
0
0
0
0
0

4
5
5
14
6
1
1
7
10
7
11
7
6
6
1
4
2
2
2
0
1
0
0
0
0
2
2
0
1
6
4
7
2
9
17
5
1
0
1
1
0
2
1
2
2
3
6
1
0
0
0
0
0

Channel Data Report


801:

8/12/2013
0

Sample Title:

4:30:57
0

PM
0

Page
0

01

Channell------l-------l-------l-------1-------1-------1-------l-------I
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
0
0
1
1
0
0
1
0
0
1
0
0
0
0
1
2
4
0
0
1
0
0
0
0
0

1
1
0
0
1
0
0
0
0
1
0
1
0
0
1
1
1
6
4
2
1
0
0
0
0
0
0

0
0
0
0
0
1
0
0
1
0
0
0
0
1
0
0
3
6
4
0
1
0
0
0
1
0
0

0
0
0
0
0
0
0
0
1
0
0
0
0
2
0
1
3
8
4
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
1
0
0
1
1
0
1
0
1
2
5
3
0
0
0
0
0
0
1
1

0
0
0
0
1
0
0
0
0
0
1
0
1
0
0
2
0
5
3
4
1
0
0
0
0
0
0

0
1
0
1
0
0
1
0
0
0
0
1
2
0
1
2
3
2
0
0
1
0
2
1
0
0
0

0
0
1
0
0
0
0
1
1
2
0
0
0
0
0
1
5
2
0
1
0
0
0
0

Sample Description:
Spectrum File:
Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

BLANK
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000659
1307149A-TH
02
Shelf 2
Th iso

Detector Name:

Alpha_OlO
Chamber Serial Number:

Detector Serial Number:


10
Env. Background:

System Bkgd 64766


Reagent Blank:

<not performed>
Sample Size:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

1.000E+OOO +/- O.OOOE+OOO liter


8/12/2013
7:20:26 AM
8/12/2013 12:55:04 PM
170.0 minutes
170.0 minutes

Tracer Certificate:

Tracer Quantity:

Effective Efficiency:

Counting Efficiency:

Chem. Recovery Factor:

Th229 TH-18A
0.238 mL

0.0952 +/- 0.0108

0.1967 +/- 0.0036 on 12/15/2012 11:26:40 AM


0.4842 +/- 0.0556

Peak Match Tolerance:

0.175 MeV

PEAK
Energy
(MeV)

Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232

Net
Pk Area

5.823
5.410
4 .871
4.620
3.928

AREA

REPORT

Pk Area
Error %

4.28
2 .11
86.62
14.30
3.64

Ambient
Backgnd
2.72
2.89
2.38
1. 70
1. 36

125 .11
217.70
21.40
55.32
123.16

FWHM
(keV)

Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

2.9
2.9
3.4
2.9
2.9

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS

Nuclide

Id
Conf.

Energy
(keV)

TH-227
TH-228
TH-229
TH-230
TH-232

0.996
0.999
1. 000
0.986
0.976

5850.00*
5400.00*
4872.00*
4672.00*
3997.00*

Activity
(pCi/liter )
1.22E-001
5.87E-002
2.42E+OOO
3.98E-001
1. OlE-001

+/+/+/+/+/-

1.55E-001
1.29E-001
5.38E-001
2.38E-001
1.27E-001

8{ F~/13

MDA
(pCi/liter
2.45E-001
2.44E-001
2.29E-001
2.05E-001
1.91E-001

+/+/+/+/+/-

5.44E-002
5.42E-002
5.lOE-002
4.55E-002
4.24E-002

0000065910.CNF

Live Time 10201.000 sec


Rea1 Ti me 10201. 000 sec
start:
1 3505.?(kev)
stop : 1024 6498.0(kev)
Acq. Start Mon Aug 12 12: 55: 04 2013

60
55
50
45
40
35
V)

.f-J

c::

:::li

8 30

25
20
15
10
5
0

IA

!,

4000
t!'.!ll
i"JI
Jf.il';)
lt"l<fli

4500
ROI Type: 1

5000
Energy(kev)

I
11

fi

5500

6000
ROI Type: 3

6500

Channel Data Report

8/12/2013

Page

4:31:04 PM

*******************************************************
s P E C T R A L DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

02

Elapsed Live time:


Elapsed Real Time:

10201
10201

Channell------l-------l-------l-------l-------1-------1-------1-------I
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:

10201
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
1

10201
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0

0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
1
0

0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
1
0
0
0
0

0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0

;8-262

Channel Data Report


369:

8/12/2013
0

Sample Title:

Page

4:31:04 PM
0

02

Channell------l-------l-------l-------l-------1-------1-------1-------I
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:
625:
633:
641:
649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:

0
0
1
0
0
0
1
0
0
0
0
3
3
1
3
1
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
1
0
0
0
0
1
1
0
4
0
0
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
0
0
0
0
0
0
0
1
0
0
0
0
2
0
0
0

0
1
0
0
0
1
0
1
0
1
2
1
2
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1

0
0
0
0
1
0
3
1
3
2
2
2
0
2
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
1
0
0
0
0
0
0
1
0
0
0
0
0
0

1
0
0
2
0
1
0
1
2
1
1
2
1
2
1
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
1
0
0
3
2
0
1
0
1
2
3
1
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
0
0
0
0
1
1
2
0
0
2
0
1
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
0
0
1
0
0
0
1
0
0
1
0
0
1
2
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
1

.fi2ti3

Channel Data Report


801:

8/12/2013
0

Sample Title:

4:31:04
0

Page

PM
0

02

Channell------l-------1-------1-------1-------l-------l-------l-------I
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
1
0
0
0
0
0
0
0

0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0

0
0
0
0
0
0
0
1
1
0
0
0
0
0
0
0
1
0
0
0
1
0
0
0

Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:

D-81 TOT-DUP
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000659
1307149A-TH
03
Shelf 2
Th iso

Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:

Alpha_Oll
11

System Bkgd 64767


<not performed>

Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:

1.000E+OOO +/- O.OOOE+OOO liter


7/17/2013
7:20:26 AM
8/12/2013 12:55:05 PM
170.0 minutes
170.0 minutes

Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chem. Recovery Factor:

Th229 TH-18A
0.235 mL
0.1988 +/- 0.0161
0.2051 +/- 0.0035 on 7/20/2013
0.9695 +/- 0.0803

Peak Match Tolerance:

0.175 MeV

PEAK
Energy
(MeV)

Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232

5.940
5.348
4.880
4.608
3.915

Net
Pk Area

AREA

REPORT

Pk Area
Error %

2.15
3.15
178.83
19.83
2.83

2:50:46 PM

161. 66
126.67
14.66
44.23
120.53

FWHM
(keV)

Ambient
Backgnd

Reagent
Backgnd

0.85
0.85
0.17
0.17
0.17

O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

2.6
2.6
4.2
2.6
2.6

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS

Nuclide

Id
Conf.

Energy
(keV)

TH-227
TH-228
TH-229
TH-230
TH-232

0.959
0.986
1.000
0.979
0. 965

5850.00*
5400.00*
4872.00*
4672.00*
3997.00*

MDA
(pCi/liter

Activity
(pCi/liter )
2.95E-002
4.31E-002
2.39E+OOO
2.65E-001
3.77E-002

+/+/+/+/+/-

4.78E-002
5.50E-002
3.80E-001
1.24E-001
4.58E-002

AG

g( r2{r3

8.20E-002
8.19E-002
5.59E-002
5.57E-002
5.56E-002

+/+/+/+/+/-

1.30E-002
1.30E-002
8.87E-003
8.84E-003
8.83E-003

0000065911.CNF

Live Time 10200.000 sec


Real Time 10200.000 sec
Start:
1 3640. l(kev)

Stop : 1024 6315. 3(kev)

Acq. Start Mon Aug 12 12:55:05 2013

60
55

50

45

40

35

V)
.j-..1

c:

::::s

8 30

25

20

15

10

M AH '.

4000

4500

a!~

,,,,1

ROI Type: 1

~I

5000
Energy(kev)

/,

.l.i

5500
ROI Type: 3

!.

6000

Channel Data Report

8/12/2013

4:31:1~

Page

Mt

*******************************************************
s p E C T R A L DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

03

Elapsed Live time:


Elapsed Real Time:

10200
10200

Channell------l-------l-------1-------1-------1-------l-------l-------I
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:

10200
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0

10200
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0

0
0

0
0
0

0
0
0

0
0
0

0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0

0
0
0
0
0
0

0
0
0
0
0
0
0
0

0
0
1

0
0
0
0
0
0
0
0

1
0
0
0
0

0
0
0
0
0
0
0

0
0
0

0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
1

0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
1
0
0
0
0

0
0
0
0
0
0

0
0
0
0
0
0

0
0
0
0
0
0

0
0
0
0
0
0

0
0
0
0
0
0
0

0
0
0

0
0
0
0
0
0
0

0
1
0
0
0
0

0
0
0
0

1
0

0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
1
1
0

0
0
0

0
0
0
0
0
0
0
0

0
0
0
0

1
0
0
0
0
0

2
0

0
0
0

1
0
0
0

0
1
0
0
0
0
0

0
0
0
0

1
1
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0

1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

126&7

Channel Data Report


369:

8/12/2013
0

Sample Title:

4:31:10
0

Page

PM
0

03

Channell------l-------l-------l-------1-------1-------1-------l-------I
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:
625:
633:
641:
649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:

0
0
0
0
1
0
2
1
0
2
1
6
2
4
0
2
0
0
1
0
0
1
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
1
0
0
2
0
0
1
3
2
3
1
3
3
1
1
1
0
0
1
1
1
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0

0
1
0
0
0
1
1
3
0
2
8
5
3
2
1
1
2
1
0
1
3
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
2
1
0
0
1
3
1
3
3
2
2
2
0
0
1
2
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
1
1
0
2
0
1
2
2
0
2
1
0
0
1
0
0
1
1
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
3
0
1
1
3
2
3
2
1
0
0
1
2
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0

0
0
0
0
1
0
0
1
2
0
6
2
0
0
2
0
1
1
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
2
0
0
0
4
4
3
6
2
2
0
2
0
2
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

.,. ...
~

Channel Data Report


801:

8/12/2013
0

Sample Title:

4:31:10
0

Page

PM
0

03

Channell------l-------1-------1-------1-------l-------l-------l-------I
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
1
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
1
0
0
1
0
1
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0

Sample Description:

Spectrum File:

Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

PZ-302-AS TOT
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000659
1307149A-TH
04
Shelf 2
Th iso

Detector Name:

Alpha_012
Chamber Serial Number:

Detector Serial Number:


12
Env. Background:

System Bkgd 64768


Reagent Blank:

<not performed>
Sample Size:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

1.000E+OOO +/- O.OOOE+OOO liter


7/16/2013
7:20:26 AM
8/12/2013 12:55:06 PM
170.0 minutes
170.0 minutes

Tracer Certificate:

Tracer Quantity:

Effective Efficiency:

Counting Efficiency:

Chem. Recovery Factor:

Th229 TH-18A
0.234 mL

0.1475 +/- 0.0136

0.1989 +/- 0.0034 on 12/11/2011


0.7415 +/- 0.0698

Peak Match Tolerance:

0.175 MeV

PEAK
Energy
(MeV)

Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232

5.824
5.358
4.866
4.595
3.946

Net
Pk Area
5.83
9.15
131. 83
23.83
12.15

AREA

2:21:56 PM

REPORT

Pk Area
Error %

Ambient
Backgnd

Reagent
Backgnd

FWHM
(keV)

82.55
68.23
17.08
40.32
58.49

0.17
0.85
0.17
0.17
0.85

O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

3.0
3.0
3.3
3.0
3.0

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS

Nuclide

Id
Conf.

Energy
(keV)

TH-227
TH-228
TH-229
TH-230
TH-232

0.997
0.991
1. 000
0. 969
0.987

5850.00*
5400.00*
4872.00*
4672.00*
3997.00*

Activity
(pCi/liter )
1. 08E-001
1. 69E-001
2.38E+OOO
4.29E-001
2.18E-001

+/+/+/+/+/-

9.lOE-002
1.19E-001
4.31E-001
1.90E-001
1.34E-001

MDA
(pCi/liter
7.71E-002
1. llE- 001
7.53E-002
7.51E-002
1.08E-001

+/+/+/+/+/-

1.40E-002
2.00E-002
1.37E-002
1.36E-002
1.95E-002

AG.

8/r3/r~
1m

0000065912.CNF

Live Time 10200.000 sec


Real Time 10200.000 sec
Start:
1 3502.?(kev)

Stop : 1024 6535. 3(kev)

Acq. Start Mon Aug 12 12:55:06 2013

60
55

50

45

40

35

Vl

.f.-1

s::::
:::::s

8 30

25

20

15

10

5
qi !;~

0
4000

4500

~i~

11\:J!

""''

...... ~ll

ROI Type: 1

5000
Energy(kev)

1~H

/;lji,

If:

~d

6000

5500
ROI Type: 3

6500

Channel Data Report

8/12/2013

Page

4:31:17 PM

*******************************************************

S P E C T R A L
R E P 0 R T
DAT A
*****
*****

*******************************************************

Sample Title:

04

Elapsed Live time:


Elapsed Real Time:

10200

10200

Channell------l-------1-------1-------1-------l-------l-------l-------I
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
12 9:
13 7:
14 5:
153:
161:
169:
1 77:
185:
193:
201:
209:
21 7:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:

10200
0
0
0
0
0
1
0
0
0
0
0
0
1
0
2
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
1
0

10200
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2
1
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
1
1
1
0
0
0
0
0
0
0
0
0
1
0
0
0
1
0
0
1
0
0
0
0
0
0
1
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
1
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
1
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
1
1
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
1
0
1
0
0
0

Channel Data Report


369:

8/12/2013
0

Sample Title:

4:31:17
0

Page

PM
0

04

Channell------l-------l-------1-------1-------1-------l-------l-------I
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:
625:
633:
641:
649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:

1
0
0
1
0
1
1
2
1
2
0
1
0
1
1
1
1
0
0
1
0
0
0
0
0
0
0
0
0
1
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0

1
1
1
0
0
0
2
0
3
2
2
1
2
1
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
0
1
0
1
0
1
2
0
2
4
1
0
0
2
2
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
2
1
2
3
3
1
1
1
0
0
2
1
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
1
0
0
1
0
1
3
2
2
3
1
0
0
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
0
0

0
0
0
1
1
1
4
2
3
1
3
3
4
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
1
2
1
1
0
4
4
1
1
2
5
2
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0

1
1
0
0
0
2
0
1
1
1
1
2
1
1
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

6J213

Channel Data Report


801:

8/12/2013
0

Sample Title:

Page

4:31:1T Mt
0

04

Channe 1 I- - - - - - I - - - - - - - I - - - - - - - I - - - - - - - I - - - - - - - I - - - - - - - I - - - - - - - I - - - - - - - I
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0

1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

Sample Description:
Spectrum File:
Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

PZ-302-AS DIS
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000659
1307149A-TH
05
Shelf 2
Th iso

Detector Name:

Alpha_Ol3
Chamber Serial Number:

Detector Serial Number:


13
Env. Background:

System Bkgd 64769


Reagent Blank:

<not performed>
Sample Size:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

l.OOOE+OOO +/- O.OOOE+OOO liter


7/16/2013
7:20:26 AM
8/12/2013 12:55:07 PM
170.0 minutes
170.0 minutes

Tracer Certificate:

Tracer Quantity:

Effective Efficiency:

Counting Efficiency:

Chem. Recovery Factor:

Th229 TH-18A
0.235 mL

0.1903 +/- 0.0158

0.1869 +/0.0035 on 12/15/2012 11:26:45 AM


1.0184 +/- 0.0864

Peak Match Tolerance:

0.175 MeV

PEAK
Energy
(MeV)

Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232

5.814
5.436
4.865
4. 611
4. 011

Net
Pk Area

AREA

REPORT

Pk Area
Error %

0.30
0.47
170.98
18.66
3.83

Ambient
Backgnd

Reagent
Backgnd

1. 70
1.53
1. 02
0.34
0.17

O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

988.92
627 .11
15.04
45.85
102.72

FWHM
(keV)
2.8
2.8
5.7
2.8
5.7

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

TH-227
TH-228
TH-229
TH-230
TH-232

0.993
0.993
1.000
0.980
0.999

5850.00*
5400.00*
4872.00*
4672.00*
3997.00*

Activity
(pCi/liter )
4.29E-003
6.72E-003
2.39E+OOO
2.60E-001
5.33E-002

+/+/+/+/+/-

4.24E-002
4.22E-002
3.88E-001
l.27E-001
5.54E-002

8/t:J/f:i

MDA
(pCi/liter
1. 05E- 001
l.02E-001
8.81E-002
6.67E-002
5.81E-002

+/+/+/+/+/-

1. 71E-002
l.65E-002
1.43E-002
l.08E-002
9.42E-003

0000065913.CNF

Live Ti me 10201. 000 sec


Real Time 10201.000 sec
start:
1 3547 .5(kev)

stop : 1024 6438. l(kev)

Acq. Start Mon Aug 12 12: 55: 07 2013

60
55

50

45

40

35

V>

+-'
s::::
::3

8 30

25

20

15

10

~
~

I!''
iJ

4000

4500

~~
ll'li1:1i

ROI Type: 1

5000
Energy(kev)

5500

6000

ROI Type: 3

Channel Data Report

8/12/2013

Page

4:31:24 PM

*******************************************************
s p E CTR AL DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

05

Elapsed Live time:


Elapsed Real Time:

10201
10201

Channell------l-------l-------l-------1-------1-------1-------l-------I
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:

10201
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
1
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0

10201
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
1
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
1
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
1
0
1
0
0
0
2
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0

821

Channel Data Report


369:

8/12/2013
1

Sample Title:

Page

4:31:24 PM
0

05

Channell------l-------1-------1-------1-------l-------l-------l-------I
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:
625:
633:
641:
649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:

1
1
0
0
0
1
0
0
4
2
0
3
1
2
0
1
0
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0

0
0
0
0
0
1
1
5
1
3
6
1
3
2
2
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
1
0
0
0
0
0
3
2
5
8
1
3
6
0
2
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
1
0
1
2
1
1
5
2
4
0
3
0
0
0
0
0
0
1
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
1
0
1
0
0
0
3
1
1
3
4
5
1
1
0
1
1
0
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
1
1
3
4
1
3
1
1
1
0
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1

0
0
0
0
0
1
0
0
1
4
4
1
0
0
3
1
1
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
1
1
1
0
1
1
3
2
3
3
2
1
1
0
1
0
0
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
1
0
0
0
0
0

-6l21S

Channel Data Report


801:

Pagei

8/12/2013
0

Sample Title:

05

Channell------l-------1-------1-------1-------l-------l-------l-------I
809:
81 7:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
93 7:
94 5:
953:
961:
969:
977:
985:
993:
1001:
1009:
101 7:

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
1
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

.1219

Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:

LR-100 TOT
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000660
1307149A-TH
06
Shelf 2
Th iso

Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:

Alpha_014
14
System Bkgd 64770
<not performed>

Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:

O.OOOE+OOO liter
l.OOOE+OOO +/7/17/2013
7:20:26 AM
8/12/2013 12:55:08 PM
170.0 minutes
170.0 minutes

Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chem. Recovery Factor:

Th229 TH-18A
0.235 mL
0.1360 +/0.0131
0.1846 +/0.0034 on 12/15/2012 11:26:44 AM
0.7369 +/0.0722

Peak Match Tolerance:

0.175 MeV

PEAK
Energy
(MeV)

Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232

5. 771
5.288
4.882
4.606
3. 963

Net
Pk Area
0.28
-0.08
121.81
28.32
-0.68

AREA

REPORT

Pk Area
Error %
13 02. 3

Ambient
Backgnd
2. 72
4.08
1.19
0.68
0.68

5312.3
17.86
37.34
304.44

FWHM
(keV)

Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

2.9
2.9
8.8
2.9
0.0

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS

Nuclide

Id
Conf.

Energy
(keV)

TH-227
TH-228
TH-229
TH-230
TH-232

0.968
0.936
0.999
0.978
0.994

5850.00*
5400.00*
4872.00*
4672.00*
3997.00*

MDA
(pCi/liter

Activity
(pCi/liter )
5.61E-003
-l.60E-003
2.38E+OOO
5.53E-001
-l.32E-002

+/+/+/+/+/-

7.30E-002
8.50E-002
4.50E-001
2.31E-001
4.04E-002

-Ac;

l.72E-001
l.98E-001
1. 29E-001
l.lOE-001
l.lOE-001

g/ P{IJ

+/+/+/+/+/-

3.24E-002
3.73E-002
2.43E-002
2.08E-002
2.07E-002

0000066015. CNF

Live Time
Real Time
start:
1
Stop : 1024
Acq. Start

60

10200.000 sec
10200.000 sec
3507. 9(kev)
6512.2(kev)
Mon Aug 12 12: 55 :08 2013

55

50

45

40

35

Vl

......
c
:::i;

8 30
25

20

15
10
5
0

"I\

4000
~1;,!

f"I,,)
1"11,::P

R"''

4500
ROI Type: 1

5000
Energy(kev)

,I

I\!

5500

6000
ROI Type: 3

6500

Channel Data Report

8/12/2013

Page

4:31:31 PM

*******************************************************
s P E C T R A L DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

06

Elapsed Live time:


Elapsed Real Time:

10200
10200

Channell------l-------1-------1-------1-------l-------l-------l-------I
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:

10200
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
0
0
0
0
0
0
0
0
0
0
0
1

10200
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
1
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
1
1
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
1
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
1
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
1
0
0
2
0
0
0
0
0

1!1222

Channel Data Report


369:

8/12/2013
0

Sample Title:

4:31:31
0

Page

PM
0

06

Channell------l-------1-------1-------1-------l-------l-------l-------I
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:
625:
633:
641:
649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:

0
0
0
0
0
0
3
1
0
1
2
1
3
0
1
1
0
2
1
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0

0
0
1
0
0
0
1
1
0
1
5
2
0
0
0
0
1
0
3
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
1
0
1
1
1
1
0
2
2
3
1
0
2
1
0
1
1
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
1
0
2
1
1
0
3
0
3
2
2
1
0
1
1
0
0
1
0
0
0
0
1
0
1
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
3
0
0
0
0
1
0
0

0
1
0
1
0
0
1
4
5
0
0
0
2
0
0
2
0
0
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

2
0
0
0
0
0
0
3
4
1
2
2
0
1
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
0
1
1
0
0
0
1
1
2
0
1
2
1
2
1
1
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0

0
1
1
0
0
0
2
3
1
2
2
0
1
0
0
1
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
1
0
0
0
0
1
0
0
0
0
0

B223

Channel Data Report


801:

8/12/2013
0

Sample Title:

Page

4:31:31 PM
0

06

Channell------l-------l-------1-------1-------1-------l-------l-------I
809:
817:
825:
833:
841:
84 9:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
94 5:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
1
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0

Sample Description:

Spectrum File:

Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

LR-100 DIS
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000659
1307149A-TH
07
Shelf 2
Th iso

Detector Name:

Alpha_Ol5
Chamber Serial Number:

Detector Serial Number:


15
Env. Background:

System Bkgd 64771


Reagent Blank:

<not performed>
Sample Size:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

l.OOOE+OOO +/- O.OOOE+OOO liter


7:20:26 AM
7/17/2013
8/12/2013 12:55:09 PM
170.0 minutes
170.0 minutes

Tracer Certificate:

Tracer Quantity:

Effective Efficiency:

Counting Efficiency:

Chem. Recovery Factor:

Th229 TH-18A
0.234 mL

0.1381 +/- 0.0132

0.1477 +/- 0.0027 on 7/20/2013


0.9345 +/- 0.0908

Peak Match Tolerance:

0.175 MeV

PEAK
Energy
(MeV)

Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232

5.872
5.400
4.866
4.618
3.924

Net
Pk Area
-0.85
2.32
123.32
21.32
1.83

AREA

6:27:27 PM

REPORT

Pk Area
Error %
246.69
149.12
17. 71
43.23
152.56

Ambient
Backgnd
0.85
0.68
0.68
0.68
0.17

FWHM
(keV)

Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

0.0
6.0
3.0
3.0
3.0

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS

Nuclide

Id
Conf.

Energy
(keV)

TH-227
TH-228
TH-229
TH-230
TH-232

0.997
1.000
1. 000
0.985
0.973

5850.00*
5400.00*
4872.00*
4672.00*
3997.00*

Activity
(pCi/liter )
-l.68E-002
4.57E-002
2.38E+OOO
4.lOE-001
3.51E-002

+/+/+/+/+/-

4.15E-002
6.87E-002
4.45E-001
l.93E-001
5.40E-002

MDA
(pCi/liter
l.18E-001
l. llE- 001
l.09E-001
1. 08E-001
8.0lE-002

+/+/+/+/+/-

2.21E-002
2.08E-002
2.04E-002
2.03E-002
l.50E-002

f\G

1fr~{t')

8225

0000065909.CNF

Live Time 10200.000 sec


Real Time 10200.000 sec
start:
1 3490. B(kev)

stop : 1024 6558. B(kev)

Acq. Start Mon Aug 12 12: 55: 09 2013

60
55

50

45

40

35

V'I

......
c:
:::::5

8 30

25

20

15

10

0
3500

\l

4000

4500

~~I

N
j'I;,)

ROI Type: 1

5000
Energy(kev)

5500

6000
ROI Type: 3

6500

Channel Data Report

8/12/2013

Page

4:31:51 PM

*******************************************************
s p E CTR AL DAT A RE P 0 R T *****
*****
*******************************************************
Sample Title:

07

Elapsed Live time:


Elapsed Real Time:

10200

10200

Channell------l-------l-------l-------l-------1-------1-------1-------I
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:

10200
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0

10200
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
1
0
0

0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
3

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

@227

Channel Data Report


369:

8/12/2013
0

Sample Title:

4:31:51
0

Page

PM
1

07

Channell------l-------l-------l-------l-------1-------1-------1-------I
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:
625:
633:
641:
649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:

2
0
1
0
1
0
0
1
1
2
1
0
2
1
0
1
3
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
1
0
0
0
2
0
3
4
0
1
1
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0

1
0
0
0
0
1
3
0
4
1
0
2
0
0
1
0
0
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
1
0
1
2
0
3
2
3
0
1
2
1
2
0
2
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
0
0
0
0
0
0
0
0
0
0
0
0

0
1
0
0
3
1
1
3
5
1
3
0
0
0
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
1
0
0
0
2
0
1
0
1
2
0
0
2
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
1
1
0
0
2
1
6
4
1
2
0
0
1
0
1
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0

1
0
0
1
1
2
0
0
3
4
3
1
0
0
3
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

8228

Channel Data Report


801:

8/12/2013
0

Sample Title:

4:31:51
0

Page

PM
0

07

Channell------l-------l-------l-------1-------1-------1-------l-------I
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0

Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:

D-81 TOT
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000659
1307149A-TH
08
Shelf 2
Th iso

Detector Name:
Chamber Serial Number:

Detector Serial Number:


Env. Background:
Reagent Blank:

Alpha_Ol9
19

System Bkgd 64773

<not performed>

Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:

l.OOOE+OOO +/- O.OOOE+OOO liter

7/17/2013
7:20:26 AM

8/12/2013 12:55:35 PM

170.0 minutes

170.0 minutes

Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chem. Recovery Factor:

Th229 TH-18A

0.234 mL

0.1578 +/- 0.0142

0.1659 +/- 0.0029 on 2/17/2013


0.9513 +/- 0.0873

Peak Match Tolerance:

0.175 MeV

PEAK
Energy
(MeV)

Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232

5.768
5.295
4.869
4.622
3.982

Net
Pk Area

AREA

REPORT

Pk Area
Error %

5.64
3.66
141.00
22.00
2.66

10:45:23 AM

93.45
107.87
16.56
42.73
128.85

Ambient
Backgnd

Reagent
Backgnd

FWHM
(keV)

1. 36
0.34
0.00
0.00
0.34

O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

5.0
3.3
6.0
6.7
3.3

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

TH-227
TH-228
TH-229
TH-230
TH-232

0.965
0.944
1.000
0.987
0.999

5850.00*
5400.00*
4872.00*
4672.00*
3997.00*

Activity
(pCi/liter )
9.73E-002
6.31E-002
2.38E+OOO
3.70E-001
4.47E-002

+/+/+/+/+/-

9.26E-002
6.90E-002
4.20E-001
1. 71E-001
5.81E-002

~c.\C'-'

MDA

(pCi/liter
l.18E-001
8.24E-002
l.OlE-001
l.OlE-001
8.03E-002

+/+/+/+/+/-

2.09E-002
1.45E-002
l.78E-002
l.78E-002
1. 42E- 002

0000065914.CNF

Live Time 10200.000 sec


Real Time 10200.000 sec
start:
1 3279.3(kev)
stop : 1024 6687 .O(kev)

Acq. Start Mon Aug 12 12: SS: 3S 2013

60
55

50

45

40

35

VI

.j..J

c::

:::J

8 30

25

20

15

10

j\

}.

3500

4000

(jt:!I

r-,11
~..,JI
i.~'

l,Ji\ 11,i,

I.

\ i

ROI Type: 1

4500

5000
Energy(kev)

5500

6000
ROI Type: 3

6500

Channel Data Report

8/12/2013

4:31:58 PM

Page

*******************************************************
s p E C T R A L DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

08

Elapsed Live time:


Elapsed Real Time:

10200
10200

Channell------l-------l-------l-------l-------1-------1-------1-------I
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:

10200
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

10200
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0

0
1
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
0
0
0
0
0
0

0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0

0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
1
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0

0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0

&!1232

Channel Data Report


369:

8/12/2013
0

Sample Title:

4:31:58
0

PM
0

Page
0

08

Channell------l-------l-------l-------1-------1-------1-------l-------I
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:
625:
633:
641:
649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:

1
0
0
1
0
0
1
1
1
2
1
5
2
1
2
1
2
1
0
2
0
0
0
0
0
0
0
1
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
0
0
0
0
0

0
0
0
1
1
1
1
1
1
0
2
9
1
1
1
0
1
0
1
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2
0
0
0
0
0
0

0
0
0
0
0
0
1
3
1
2
2
1
3
0
0
0
1
2
0
0
0
0
0
0
1
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
1
0
1
0
0
0
0
0

0
0
0
0
0
1
1
0
1
2
2
3
2
3
1
1
0
1
3
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
1
0
0
1
2
4
1
1
0
1
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
2
1
3
2
0
0
3
2
0
1
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
1
1
0
1
4
3
1
2
1
1
0
0
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
1
1
0
0
0
1
2
2
3
3
5
1
1
2
2
1
2
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0

1233

Channel Data Report


801:

8/12/2013
0

Sample Title:

4:31:58
0

PM
0

Page
0

08

Channelj------1-------1-------1-------l-------l-------l-------l-------I
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0

0
0
0
0
0
0
0
0
0
0
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

Sample Description:
Spectrum File:
Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

D-81 DIS
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000659
1307149A-TH
09
Shelf 2
Th iso

Detector Name:

Alpha_022
Chamber Serial Number:

Detector Serial Number:


22
Env. Background:

System Bkgd 64774


Reagent Blank:

<not performed>
Sample Size:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

l.OOOE+OOO +/- O.OOOE+OOO liter


7/17/2013
7:20:26 AM
8/12/2013 12:55:36 PM
170.0 minutes
170.0 minutes

Tracer Certificate:

Tracer Quantity:

Effective Efficiency:

Counting Efficiency:

Chem. Recovery Factor:

Th229 TH-18A
0.232 mL

0.1750 +/- 0.0152

0.1531 +/- 0.0029 on 12/15/2012


1.1428 +/- 0.1013

Peak Match Tolerance:

0.175 MeV

PEAK
Energy
(MeV)

Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232

5.785
5.308
4.890
4.611
4.036

Net
Pk Area

AREA

REPORT

Pk Area
Error %

3.64
4.45
155.13
19.96
2.49

1:57:26 PM

123.16
120.09
15.85
46.42
138.29

Ambient
Backgnd
1.36
2.55
1. 87
2.04
0.51

FWHM
(keV)

Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

3.1
3.1
4.8
3.1
3.1

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS

Nuclide

Id
Conf.

Energy
(keV)

TH-227
TH-228
TH-229
TH-230
TH-232

0.978
0.957
0.998
0.980
0.992

5850.00*
5400.00*
4872.00*
4672.00*
3997.00*

Activity
(pCi/liter )
5.67E-002
6.92E-002
2.36E+OOO
3.03E-001
3.77E-002

+/
+/
+/
+/
+/

7.04E-002
8.39E-002
4.0lE-001
l.50E-001
5.25E-002

hG.
8f f3(f3

MDA
(pCi/liter
l.07E-001
l.30E-001
l.15E-001
l.18E-001
7.94E-002

+/+/+/+/+/-

l.81E-002
2.21E-002
1. 96E-002
2.0lE-002
1. 35E- 002

0000065915.CNF

Live Time 10200.000 sec


Real Ti me 10200. 000 sec
start:
1 3421.S(kev)
stop : 1024 6608.B(kev)
Acq. Start Mon Aug 12 12: 55: 36 2013

60
55
50
45
40
35
V'l

.......
c:
~

8 30

25
20
15
10

5
0

hI r.

f '\

3500

4000

4500

ti!~

r'IJi
~""~
en

\1~ !\ V.\1\

Ail

!i

\ I

I.I

IH

ROI Type: 1

5000
Energy(kev)

5500

6000
ROI Type: 3

6500

Channel Data Report

8/12/2013

Page

4:32:05 PM

*******************************************************
s p E C T R A L DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

09

Elapsed Live time:


Elapsed Real Time:

10200
10200

Channell------l-------1-------1-------1-------l-------l-------l-------I
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:

10200
0
0
0
0
1
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1

10200
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0

0
1
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0

0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1

E237

Channel Data Report


369:

8/12/2013
0

Sample Title:

4:32:05
0

Page

PM
0

09

Channell------l-------l-------1-------1-------1-------l-------l-------I
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:
625:
633:
641:
649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:

0
1
0
0
1
0
0
1
0
1
4
6
2
1
0
2
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0

0
0
0
0
1
0
0
0
1
4
2
7
3
0
1
3
0
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0

0
0
0
2
1
1
1
0
0
1
3
2
3
1
1
1
0
0
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
2
0
7
1
2
2
2
1
1
0
0
0
1
1
0
0
1
0
0
0
0
0
0
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
0
0
0
1
1
2
0
4
2
2
4
1
2
1
1
1
0
0
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0

1
0
1
0
1
0
0
1
1
2
4
9
3
3
2
1
1
0
1
0
0
1
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0

0
0
0
1
0
1
0
0
1
2
0
2
0
2
1
3
0
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
1
0
1
4
3
0
2
1
1
1
0
2
1
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
0
0
0
0
0
0
0
0

.,..,,..
'5

Channel Data Report


801:

8/12/2013
0

Sample Title:

4:32:05
0

Page

PM
0

09

Channell------l-------l-------l-------l-------1-------1-------1-------I
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
1
0
0
1
0
0
0
0
0
0
0
0
0
0

Sample Description:

Spectrum File:

Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

PZ-204-SS TOT
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000659
1307149A-TH
10
Shelf 2
Th iso

Detector Name:

Alpha_023
Chamber Serial Number:

Detector Serial Number:


23
Env. Background:

System Bkgd 64775


Reagent Blank:

<not performed>
Sample Size:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

l.OOOE+OOO +/- O.OOOE+OOO liter


7/17/2013
7:20:26 AM
8/12/2013 12:55:37 PM
170.0 minutes
170.0 minutes

Tracer Certificate:

Tracer Quantity:

Effective Efficiency:

Counting Efficiency:

Chem. Recovery Factor:

Th229 TH-18A
0.232 mL

0.2003 +/- 0.0163

0.1710 +/- 0.0030 on 7/20/2013


1.1711 +/- 0.0974

Peak Match Tolerance:

0.175 MeV

PEAK
Energy
{MeV)

Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232

5.818
5.345
4.884
4.600
4.015

Net
Pk Area

AREA

REPORT

Pk Area
Error %

1.15
6.66
177.66
22.15
2.49

6:18:25 PM

Ambient
Backgnd

Reagent
Backgnd

0.85
0.34
0.34
0.85
0.51

O.OOE+OOO
0.00E+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

249.58
78.18
14.72
42.57
138.29

FWHM
{keV)
6.2
3.1
4.6
3.1
3.1

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
{keV)

Activity
(pCi/liter )

MDA

(pCi/liter

-------------------------------------------------------------------------------TH-227
TH-228
TH-229
TH-230
TH-232

0.995
0.984
0.999
0.974
0.998

5850.00*
5400.00*
4872.00*
4672.00*
3997.00*

1.56E-002
9.05E-002
2.36E+OOO
2.94E-001
3.29E-002

+/+/+/+/+/-

3.91E-002
7.22E-002
3.76E-001
l.33E-001
4.59E-002

A6

~/ 13(t3

8.14E-002
6.50E-002
6.36E-002
7.94E-002
6.94E-002

+/+/+/+/+/-

l.30E-002
l.03E-002
l.OlE-002
1.26E-002
l. llE-002

0000065916.CNF

Live Time 10200.000 sec


Real Time 10200.000 sec
start:
1 3403.0(kev)
stop : 1024 6588.3(kev)
Acq. Start Mon Aug 12 12: 55: 37 2013

60
55

50

45

40

35

VI

+-'
c:
::s

8 30

25

20

15

10

......

"'
"'

I=

3500
Q';li
ti'\)
.i::u~
jji,,,.Jli,

1q1i1

1,\

11//,,\,'

4000

4500
ROI Type: 1

5000
Energy(kev)

5500

6000
ROI Type: 3

6500

Channel Data Report

8/12/2013

Page

4:32:11 PM

*******************************************************
s P E C T R A L DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

10

Elapsed Live time:


Elapsed Real Time:

10200
10200

Channell------l-------l-------1-------1-------1-------l-------l-------I
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:

10200
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0

o
0
1
0
0
0
0

10200
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
1
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
1

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
1
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0

:242

Channel Data Report


369:

8/12/2013
1

Sample Title:

4:32:11
0

Page

PM
1

10

Channell------l-------l-------1-------1-------1-------l-------l-------I
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:
625:
633:
641:
649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:

0
0
0
0
1
1
0
0
1
1
0
4
3
1
1
2
1
0
1
2
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0

1
0
0
0
2
1
0
2
1
0
4
2
1
1
3
3
0
0
2
0
1
0
0
0
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
2
0
1
1
3
1
3
4
0
2
1
0
0
0
1
1
0
0
0
0
0
0
0
0
0
0
0
1
0
1
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
1
1
2
5
2
1
2
3
2
2
1
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
2
0
0
0
0
1
0
3
5
0
8
1
1
4
1
1
1
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
0
0
0
0
0
0
1
4
1
6
3
3
0
3
2
0
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
3
2
5
2
1
1
1
2
0
0
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
0
0
1
1
1
0
3
4
2
5
3
1
1
1
3
2
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0

9243

Channel Data Report


801:

8/12/2013
0

Sample Title:

4:32:11
0

PM
0

Page
0

10

Channell------l-------l-------1-------1-------1-------l-------l-------I
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0

0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

Sample Description:

Spectrum File:

Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

PZ-204-SS DIS
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000659
1307149A-TH
11

Shelf 2
Th iso

Detector Name:

Alpha_024
Chamber Serial Number:

Detector Serial Number:


24
Env. Background:

System Bkgd 64776


Reagent Blank:

<not performed>
Sample Size:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

1.000E+OOO +/- O.OOOE+OOO liter


7/17/2013
7:20:26 AM
8/12/2013 12:55:38 PM
170.0 minutes
170.0 minutes

Tracer Certificate:

Tracer Quantity:

Effective Efficiency:

Counting Efficiency:

Chem. Recovery Factor:

Th229 TH-18A
0.234 mL

0.1387 +/- 0.0133

0.1710 +/- 0.0032 on 12/15/2012


0.8110 +/- 0.0792

Peak Match Tolerance:

0.175 MeV

PEAK
Energy
(MeV)

Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232

5.809
5.374
4.865
4.600
3.866

Net
Pk Area
-1.72
0.62
123.96
28.81
3.15

AREA

2:02:15 PM

REPORT

Pk Area
Error %
137.81
583.27
17.77
37.39
126.67

Reagent
Backgnd

Ambient
Backgnd
2.72
2.38
2.04
1.19
0.85

FWHM
(keV)

O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

3.1
3.1
3.4
6.2
3.1

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS

Nuclide

Id
Conf.

Energy
(keV)

TH-227
TH-228
TH-229
TH-230
TH-232

0.991
0.997
1. 000
0.974
0. 914

5850.00*
5400.00*
4872.00*
4672.00*
3997.00*

Activity
(pCi/liter )
-3.38E-002
1.22E-002
2.38E+OOO
5.51E-001
6.02E-002

+/+/+/+/+/-

4.70E-002
7.lOE-002
4.47E-001
2.31E-001
7. 71E-002

MDA
(pCi/liter
1. 68E-001
1. 61E-001
1.50E-001
1.26E-001
1.14E-001

+/+/+/+/+/-

3.16E-002
3.02E-002
2.81E-002
2.37E-002
2.15E-002

g.f l3/t3
5245

0000065917.CNF

Live Time 10200.000 sec


Real Time 10200.000 sec
start:
1 3411.G(kev)
stop : 1024 6597.0(kev)
Acq. Start Mon Aug 12 12: 55: 38 2013

60
55

50

45

40

35

V'l

.f-J

c:

:::J

8 30

25

20

15

10

,._
~
~

f='

Mi tll.1\ I!

3500

4000

4500

G!!I

I'll

ROI Type: 1

5000
Energy(kev)

\!,

I,

5500

6000
ROI Type: 3

6500

Channel Data Report

8/12/2013

Page

4:32:20 PM

*******************************************************
s P E C T R A L DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

11

Elapsed Live time:


Elapsed Real Time:

10200
10200

Channell------l-------1-------1-------1-------l-------l-------l-------I
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:

10200
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
1

10200
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0

0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
1
1
1
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
1
0
1
0
0
0
0
0
0
0
0
0
1
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
1

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
1
0
0
1

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

l\l247

Channel Data Report


369:

8/12/2013
0

Sample Title:

4:32:20
0

Page

PM
1

11

Channell------l-------l-------l-------1-------1-------1-------l-------I
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:
625:
633:
641:
649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:

0
0
0
0
0
0
3
1
1
1
3
6
3
3
1
0
1
1
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
1
1
0
0
0
0
1
3
3
1
1
1
1
0
1
0
1
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
0
1
1
0
0
1
1
0
1
0
1
3
2
3
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0

1
0
0
0
1
1
0
0
0
2
4
2
4
0
2
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
0
0
0
3
0
0
1
2
1
2
2
0
1
0
2
0
0
1
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0

0
0
1
0
2
1
1
0
1
3
4
2
2
5
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
2
0
3
3
4
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0

1
1
0
0
0
2
0
1
5
3
0
2
0
0
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

m2

Channel Data Report


801:

8/12/2013
0

Sample Title:

4:32:20
0

PM
0

Page
0

11

Channell------l-------l-------l-------l-------1-------1-------1-------I
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
0
0
0
0
0
0
0
0

0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0

~~Apex-Alpha"'

Sample Description:
Spectrum File:
Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

LR-103 TOT
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000659
1307149A-TH

12

Shelf 2

Th iso

Detector Name:

Alpha_025
Chamber Serial Number:

Detector Serial Number:


25

Env. Background:

System Bkgd 64777

Reagent Blank:

<not performed>

Sample Size:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

1.000E+OOO +/- O.OOOE+OOO liter

7/17/2013
7:20:26 AM

8/12/2013 12:55:39 PM

170.0 minutes
170.0 minutes

Tracer Certificate:

Tracer Quantity:

Effective Efficiency:

Counting Efficiency:

Chem. Recovery Factor:

Th229 TH-18A
0.231 mL
0.1445 +/- 0.0136
0.1736 +/- 0.0032 on 12/15/2012
0.8325 +/- 0.0799

Peak Match Tolerance:

0.175 MeV

PEAK
Energy
(MeV)

Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232

5.755
5 .411
4.847
4.646
3.893

Net
Pk Area

AREA

REPORT

Pk Area
Error %

1. 81
3.13
127.32
28.32
3.00

1:57:27 PM

193.79
144.41
17.42
37.34
130.67

Ambient
Backgnd
1.19
1. 87
0.68
0.68
0.00

Reagent
Backgnd

FWHM
(keV)

O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

3.1
3.1
4.6
3.1
3.1

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

TH-227
TH-228
TH-229
TH-230
TH-232

0.954
0.999
0.997
0.996
0.945

5850.00*
5400.00*
4872.00*
4672.00*
3997.00*

Activity
(pCi/liter )
3.41E-002
5.89E-002
2.35E+OOO
5.20E-001
5.50E-002

+/+/+/+/+/-

6.64E-002
8.58E-002
4.33E-001
2.17E-001
7.26E-002

J4

8/fJ/fJ

MDA
(pCi/liter
l.24E-001
1.43E-001
1.04E-001
1. 04E-001
1. lOE-001

+/+/+/+/+/-

2.29E-002
2.63E-002
1. 92E- 002
l.91E-002
2.03E-002

0000065918.CNF

Live Time 10201.000 sec


Rea1 Ti me 10201. 000 sec
start:
1 3405. 9(kev)
Stop : 1024 6615. S(kev)
Acq. Start Mon Aug 12 12: 55: 39 2013

55

45
40
35
Vl
.j....I

c:

::::l

8 30

25
20
15
10
5
0

~
I

3500

4000

4500

~11:~

i".)
!.!'II
Rm~'

I !) I

ROI Type: 1

5000
Energy(kev)

5500

6000
ROI Type: 3

6500

Channel Data Report


369:

8/12/2013
0

Sample Title:

4:32:28
0

Page

PM
1

12

Channell------l-------1-------1-------1-------l-------l-------l-------I
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:
625:
633:
641:
649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:

0
0
0
0
0
2
0
1
2
3
2
1
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
1
0
0

2
0
0
0
0
1
0
0
2
3
1
0
2
2
2
1
0
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
1
0
0
2
1
1
1
1
2
4
3
2
0
1
0
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
1
1
1
2
2
2
0
2
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
1
0
0
1
1
0
1
4
4
3
5
0
0
0
1
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0

1
0
0
0
1
1
0
2
3
1
2
2
1
2
2
0
0
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
2
1
1
3
2
4
3
3
1
0
2
0
0
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
1
0
0
0
0
0
0
0
0

0
1
1
1
1
2
1
3
4
3
2
2
0
1
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
&"""
..; ,Ji

Channel Data Report


801:

8/12/2013
0

Sample Title:

4:32:28
0

Page

PM
0

12

Channell------l-------l-------1-------1-------1-------l-------l-------I
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0

Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:

LR-103 DIS
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000659

1307149A-TH

13

Shelf 2

Th iso

Detector Name:
Chamber Serial Number:

Detector Serial Number:


Env. Background:
Reagent Blank:

Alpha_027

27

System Bkgd 64778

<not performed>

Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:

l.OOOE+OOO +/- O.OOOE+OOO liter

7/17/2013
7:20:26 AM

8/12/2013 12:55:40 PM

170.0 minutes

170.0 minutes

Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chem. Recovery Factor:

Th229 TH-18A

0.233 mL

0.1791 +/- 0.0153

0.1728 +/- 0.0032 on 12/15/2012


1.0365 +/- 0.0906

Peak Match Tolerance:

0.175 MeV

PEAK
Energy
(MeV)

Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232

5.878
5.319
4.874
4.601
3.926

Net
Pk Area

AREA

REPORT

Pk Area
Error %

1. 30
1.11
159.15
37.30
5.81

2:27:41 PM

273.47
374.31
15.58
32.94
90.54

Ambient
Backgnd

Reagent
Backgnd

FWHM

(keV)

1. 70
2.89
0.85
1. 70
1.19

O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

3.2
3.2
5.1
3.2
3.2

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

Activity
(pCi/liter )

MDA

(pCi/liter

-------------------------------------------------------------------------------TH-227
TH-228
TH-229
TH-230
TH-232

0. 996
0.966
1. 000
0.974
0.974

5850.00*
5400.00*
4872.00*
4672.00*
3997.00*

l.98E-002
1.69E-002
2.37E+OOO
5.53E-001
8.60E-002

+/+/+/+/+/-

5.42E-002
6.32E-002
3.96E-001
2.04E-001
7.91E-002

l.12E-001
1. 33E-001
8.90E-002
1. 09E-001
9.75E-002

+/+/+/+/+/-

l.87E-002
2.23E-002
1.49E-002
1.82E-002
l.63E-002

rs/r3/t3
8255

0000065919.CNF

Live Time 10201.000 sec


Real Time 10201.000 sec
start:
1 3402 .4(kev)
stop : 1024 6658. l(kev)
Acq. Start Mon Aug 12 12: 55 :40 2013

55

45
40
35
VI
.j....I

c::
::::J

8 30

25
20
15
10

5
0

1,1,\

3500

4000

4500

~~~

Nli

!,

ROI Type: 1

5000
Energy(kev)

5500

6000
ROI Type: 3

6500

Channel Data Report

8/12/2013

Page

4:32:35 PM

*******************************************************
s p E C T R A L DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

13

Elapsed Live time:


Elapsed Real Time:

10201
10201

Channell------l-------l-------1-------1-------1-------l-------l-------I
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:

10201
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
1

0
1
0
0
2
0
0
0
0

10201
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

o.

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
1
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
1

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
1

1
1
0
1
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
1
0
0
0
0
0
0
0
0
0
1
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
1
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
f\l?

-'""

Channel Data Report


369:

8/12/2013
0

Sample Title:

4:32:35
1

Page

PM
0

13

Channell------l-------l-------1-------1-------1-------l-------l-------I
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:
625:
633:
641:
649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:

0
1
0
2
0
0
0
3
2
3
3
4
2
2
3
2
1
2
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
1
0
1
2
3
1
1
3
6
3
2
3
1
2
2
0
1
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0

0
0
1
0
0
0
0
0
1
1
2
1
3
0
1
0
2
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

2
2
0
0
0
0
2
0
0
2
1
1
3
1
0
0
1
0
1
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0

0
1
0
0
1
3
2
1
0
5
1
1
1
1
2
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
1
1
0
1
1
1
2
5
3
2
4
3
2
0
1
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
1
0
1
0
2
1
0
5
5
0
2
2
4
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
1
1
0
1
0
1
1
5
2
2
1
0
0
1
0
0
0
0
1
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
fil

.y

Channel Data Report


801:

8/12/2013
0

Sample Title:

4:32:35
0

PM
0

Page
0

13

Channell------l-------l-------l-------1-------1-------1-------l-------I
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0

0
0
0
0
0
0
0
0
0
0
1
1
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0

1
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
1
1
0
1
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
1
1
1
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
1
0
1
0
0
0

S259

Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:

PZ-111-KS TOT
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000659
1307149A-TH
14
Shelf 2
Th iso

Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:

Alpha_029
29
System Bkgd 64779
<not performed>

Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:

l.OOOE+OOO +/- O.OOOE+OOO liter


7/17/2013
7:20:26 AM
8/12/2013 12:55:40 PM
170.0 minutes
170.0 minutes

Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chem. Recovery Factor:

Th229 TH-18A
0.233 mL
0.1797 +/- 0.0153
0.1945 +/- 0.0036 on 12/15/2012
0.9239 +/- 0.0804

Peak Match Tolerance:

0.175 MeV

PEAK
Energy
(MeV)

Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232

5.798
5.356
4.879
4.641
3.949

Net
Pk Area
3.32
1.28
160.15
28.66
-1.19

AREA

2:30:02 PM

REPORT

Pk Area
Error %

Ambient
Backgnd

119. 77
323.54
15.54
36.86
180.58

0.68
2.72
0.85
0.34
1.19

FWHM
(keV)

Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

3.1
3.1
13.2
4.7
0.0

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS

Nuclide

Id
Conf.

Energy
(keV)

TH-227
TH-228
TH-229
TH-230
TH-232

0.986
0.990
1. 000
0.995
0.988

5850.00*
5400.00*
4872.00*
4672.00*
3997.00*

Activity
(pCi/liter )
5.03E-002
l.94E-002
2.37E+OOO
4.23E-001
-1. 75E-002

+/+/+/+/+/-

6.08E-002
6.28E-002
3.96E-001
1. 71E-001
3.18E-002

PG

g,{r.3 (c~

MDA
(pCi/liter
8.55E-002
l.30E-001
8.87E-002
7.06E-002
9.71E-002

+/+/+/+/+/-

1.43E-002
2.17E-002
1.48E-002
1.18E-002
1.62E-002

0000065920.CNF

Live Time 10201.000 sec

Real Time 10201.000 sec

start:
1 3413. 5(kev)

stop : 1024 6597. 5(kev)

Acq. Start Mon Aug 12 12:55:40 2013

55

50

45

40

35

VI

+-'

c:

:::I

8 30

25

20

15

10

,\1

3500

4000

4500

11.ili~

11"'1,)

m
i-'"""'

ROI Type: 1

5000
Energy(kev)

5500

6000
ROI Type: 3

6500

Channel Data Report

8/12/2013

Page

4:32:42 PM

*******************************************************
s p E C T R A L DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

14

Elapsed Live time:


Elapsed Real Time:

10201
10201

Channell------l-------l-------l-------l-------1-------1-------1-------I
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:

10201
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

10201
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
1

0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
1
0

0
0
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
1

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
1
0

Channel Data Report


369:

8/12/2013
0

Sample Title:

4:32:42
0

Page

PM
0

14

Channell------l-------1-------1-------1-------l-------l-------l-------I
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:
625:
633:
641:
649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:

1
0
0
0
0
0
0
1
4
1
4
4
4
0
0
2
0
2
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0

0
0
0
0
0
2
1
1
0
3
2
6
2
5
0
0
2
2
2
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
0
2
0
1
4
1
1
1
3
2
5
0
1
2
1
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
1
0
1
0
0
0
0
3
2
2
3
1
1
1
1
2
2
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
2
0
2
0
1
0
2
5
3
2
3
3
1
1
0
0
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
1
1
0
0
3
0
3
3
2
1
3
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
1
0
0

0
0
0
1
1
0
2
1
1
1
0
2
3
2
2
0
1
0
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
1
0
0
1
2
0
0
2
7
1
1
2
1
0
0
0
3
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0

.;:.

Channel Data Report


801:

8/12/2013
0

Sample Title:

4:32:42
0

Page

PM
0

14

Channell------l-------l-------l-------l-------1-------1-------1-------I
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
1
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0

Sample Description:

Spectrum File:

Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

PZ-111-KS DIS
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000659
1307149A-TH
15
Shelf 2
Th iso

Detector Name:

Alpha_031
Chamber Serial Number:

Detector Serial Number:


31
Env. Background:

System Bkgd 64780


Reagent Blank:

<not performed>
Sample Size:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

l.OOOE+OOO +/- O.OOOE+OOO liter


7/17/2013
7:20:26 AM
8/12/2013 12:55:41 PM
170.0 minutes
170.0 minutes

Tracer Certificate:

Tracer Quantity:

Effective Efficiency:

Counting Efficiency:

Chem. Recovery Factor:

Th229 TH-18A
0.232 mL

0.1613 +/- 0.0144

0.1418 +/- 0.0034 on 6/13/2013


1.1375 +/- 0.1054

Peak Match Tolerance:

0.175 MeV

PEAK
Energy
(MeV)

Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232

5.921
5.441
4 .871
4.634
3. 912

Net
Pk Area
6.32
-0.02
143.15
29.49
0.15

AREA

3:23:29 PM

REPORT

Pk Area
Error %
82.73
10563.
16.44
36.46
1398.6

FWHM
(keV)

Ambient
Backgnd

Reagent
Backgnd

0.68
1. 02
0.85
0.51
0.85

O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO

3.1
3.1
7.1
3.1
3.1

Tracer Peak used for Effective Efficiency

NUCLIDE ANALYSIS RESULTS

Nuclide

Id
Conf.

Energy
(keV)

TH-227
TH-228
TH-229
TH-230
TH-232

0.974
0.991
1. 000
0.993
0.963

5850.00*
5400.00*
4872.00*
4672.00*
3997.00*

Activity
(pCi/liter )
l.07E-001
-3.39E-004
2.36E+OOO
4.85E-001
2.46E-003

+/
+/
+/
+/
+/

9.02E-002
3.58E-002
4.14E-001
1. 96E-001
3.44E-002

MDA
(pCi/liter
9.52E-002
l.06E-001
9.88E-002
8.63E-002
9.83E-002

+/+/+/+/+/-

1.67E-002
l.86E-002
l.73E-002
l.51E-002
l.72E-002

~-

rs/rJ/fJ
8265

0000065921.CNF

Live Time 10201.000 sec


Rea1 Ti me 10201. 000 sec
start:
1 3388.9(kev)

stop : 1024 6594. 6(kev)

Acq. Start Mon Aug 12 12: 55: 41 2013

60
55

50

45

40

35

VI
.j.....I

c=

::::s

8 30

25
20
15
10
~

I=

5
~
~

I='

3500

4000

4500

~.,

r,,,
rn
m

ii, i~

ROI Type: 1

5000
Energy(kev)

5500

6000
ROI Type: 3

6500

Channel Data Report

8/12/2013

Page

4:32:49 PM

*******************************************************
s P E C T R A L DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

15

Elapsed Live time:


Elapsed Real Time:

10201

10201

Channell------l-------l-------l-------l-------1-------1-------1-------I
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:

10201
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
1
0
0
0
0
0
0

10201
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0

0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
1
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
1
~

"7
;

Channel Data Report


369:

8/12/2013
0

Sample Title:

4:32:49
0

Page

PM
0

15

Channell------l-------l-------l-------l-------1-------1-------1-------I
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:
625:
633:
641:
649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:

1
0
0
2
0
0
1
0
1
1
1
3
2
1
1
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
1
0
0

0
1
0
0
1
1
2
0
0
1
4
3
5
0
0
2
0
0
0
4
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0

1
0
0
1
0
0
0
0
0
2
3
3
2
0
2
1
0
1
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0

0
0
0
0
1
0
2
0
1
3
1
1
2
2
1
1
0
1
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
0
0
0
0
1
2
1
1
2
5
4
1
3
2
0
0
2
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0

0
0
0
2
1
0
0
0
2
2
7
4
0
0
1
1
0
0
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
1
0
0
1
2
0
1
1
2
3
4
0
2
0
0
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
0
0
1
1
1
1
1
1
4
6
1
2
2
1
0
4
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

5268

Channel Data Report


801:

8/12/2013
0

Sample Title:

4:32:49
0

PM
0

Page
0

15

Channell------l-------1-------1-------1-------l-------l-------l-------I
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0

0
0

0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
1
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
1
0
0
0
0
1
0
0
0
0

0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
0
0
1
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0

Page 1 of 2
8/12/2013 6:43:21 AM

~jtApex-Alpha ]
QA SUMMARY REPORT
Review Of QA Results - Pulser Check
Date
Time

: 8/12/2013
: 6:43:21 AM

CHAMBER
Alpha 001
Alpha 002
Alpha 003
Alpha 004
Alpha 005
Alpha 006
Alpha 007
Alpha 008
Alpha 009
Alpha 010
Alpha 011
Alpha 012
Alpha 013
Alpha 014
Alpha 015
Alpha 016
Alpha 017
Alpha 018
Alpha 019
Alpha 020
Alpha 021
Alpha 022
Alpha 023
Alpha 024
Alpha 025
Alpha 026
Alpha 027
Alpha 028
Alpha 029
Alpha 030
Alpha 031
Alpha 032
Alpha 033
Alpha 034
Alpha 035
Alpha 036
Alpha 036
Alpha 037
Alpha 038
Alpha 039
Alpha 040
Alpha 041

DEVICE
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
21f
21f
21f
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
Alpha AnalystlOODC
Alpha Analyst 1OODC
Alpha AnalystlOODC
Alpha Analyst! OODC
Alpha Analyst! OODC
Alpha Analyst 1OODC
Alpha Analyst! OODC
Alpha Analyst! OODC
Alpha Analyst! OODC
Alpha Analyst! OODC

PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
Peak Energy
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
tJV
ALL
'{;'
ALL
(]
ALL
ALL
ALL
ALL
ALL
ALL
ALL
Peak CPS
Peak CPS
Peak CPS
PeakFWHM
Peak CPS
ALL
ALL
ALL
ALL
ALL

FLAG
Not Done
Not Done
Passed
Passed
Not Done
Not Done
Not Done
Not Done
Not Done
Passed
Passed
Passed
Passed
Passed
Action
Not Done
Not Done
Passed
Passed
Not Done
Not Done
Passed
Passed
Passed
Passed
Not Done
Passed
Not Done
Passed
Not Done
Passed
Not Done
Action
Action
Action
Action
Action
Passed
Passed
Passed
Passed
Passed

DATE

8/12/2013 5:20:50 AM
8/12/2013 5:20:50 AM

8/12/2013
8/12/2013
8/12/2013
8/12/2013
8/12/2013
8/12/2013

5:20:51 AM
5:20:52 AM
5:20:53 AM
5:20:53 AM
5:20:54 AM
5:20:55 AM

8/10/2013 11:23:01 AM
8/12/2013 5:20:55 AM

8/12/2013
8/12/2013
8/12/2013
8/12/2013

5:20:56 AM
5:20:57 AM
5:20:57 AM
5:20:58 AM

8/12/2013 5:20:59 AM
8/12/2013 5:20:59 AM
8/12/2013 5:21:00 AM
8/12/2013 5:21:01 AM
8/12/2013 5:21:02 AM
8/9/2013 5:06:44 AM
8/12/2013 5:21:05 AM
8/12/2013 5:21:05 AM
8/12/2013 5:21:06 AM
8/12/2013 5:21:09 AM
8/12/2013 5:21:10 AM
8/12/2013 5:21:12 AM
8/12/2013 5:22:26 AM

Page 2 of 2

Review of QA Results - Pulser Check


8/12/2013 6:43:21 AM

CHAMBER
Alpha 042
Alpha 043
Alpha 044
Alpha 045
Alpha 046
Alpha 047
Alpha 048

DEVICE
Alpha AnalystlOODC
Alpha Analyst 1OODC
Alpha AnalystlOODC
Alpha AnalystlOODC
Alpha AnalystlOODC
Alpha Analystl OODC
Alpha AnalystlOODC

PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
ALL

APPROVED BY:

APPROVAL DATE:

FLAG
Passed
Passed
Passed
Passed
Passed
Passed
Passed

DATE
8/12/2013 5:21:15 AM
8/12/2013 5:22:23 AM
8/12/2013 5:22:22 AM
8/12/2013 5:21:19 AM
8/12/2013 5:21:21 AM
8/12/2013 5:21:22 AM
8/12/2013 5:21:24 AM

6/12/12

Library Listing Report

Page

12:16:29 PM

*************************************************************************
*****
L I B R A R Y L I S T I N G R E P 0 R T
*****
*************************************************************************
Nuclide Library Title:

Thorium

Nuclide Library Description:


Nuclide
Name

Half-Life
(Seconds)

TH-227
TH-228
TH-229
TH-230
TH-232

6.873E+008
6.034E+007
2.487E+Oll
2.379E+012
4.434E+017

* =

Th-227,-228,-229,-230,-232
Energy
uncert. {keV

Energy
(keV )

0.000
0.000
0.000
0.000
0.000

5850.000*
5400.000*
4872.000*
4672.000*
3997.000*

Yield
( %)
97.5000
99.9400
99.5200
99.8200
100.0000

Yield
Uncert . (Abs . +- )
0.0000
0.0000
0.0000
0.0000
0.0000

key line

TOTALS:

Nuclides

Energy Lines

8272

SECTIONX

ANALYTICAL DATA (RADIUM-226)

Eberline Services
Oak Ridge Laboratory
Analysis Sheet

Printed: 817/2013 10:34 AM


Page 1of3

13-07149
Ra226
Run 1

13-07149

Internal
Fraction

Sample
Desc

Client
ID

Ra226
1

01

LCS

LCS

07/23/13 00:00

1.0000E+OO

02

MBL

BLANK

07/23/13 00:00

1.0000E+OO

Date Received I

7/22/2013

03

DUP

D-81 TOT

45

07/17/13 10:43

1.0000E+OO

Lab Deadline I

8/13/2013

04

TRG

PZ-302-AS TOT

46

07/16/13 15:30

1.0000E+OO

05

TRG

PZ-302-AS DIS

46

07/16/13 15:30

1.0000E+OO

West Lake OU-1

06

TRG

LR-100 TOT

47

07/17/13 10:23

1.0000E+OO

Work Order
Analysis Code

Run

Client I Engineering Management Support, Inc.


Project I

Login
CPM

Sample
Date

Sample
Aliquot

Report Level

07

TRG

LR-100 DIS

47

07/17/13 10:23

1.0000E+OO

Activity Units

pCi

08

DO

D-81 TOT

45

07/17/13 10:43

1.0000E+OO

09

TRG

D-81 DIS

45

07/17/13 10:43

1.0000E+OO

WA

10

TRG

PZ-204-SS TOT

43

07/17/1311:40

1.0000E+OO

E903.0

11

TRG

PZ-204-SS DIS

43

07/17/13 11 :40

1.0000E+OO

Alpha Spectroscopy

12

TRG

LR-103 TOT

45

07/17/13 12:15

1.0000E+OO

Ba-133

13

TRG

LR-103 DIS

45

07/17/13 12:15

1.0000E+OO

Radiometric Sol#

Ba-6a

14

TRG

PZ-111-KS TOT

41

07/17/13 13:09

1.0000E+OO

Tracer Act (dpm/g)

991.12

15

TRG

PZ-111-KS DIS

41

07/17/13 13:09

1.0000E+OO

Aliquot Units
Matrix
Method
Instrument Type
Radiometric Tracer

Carrier
Carrier Cone (mg/ml)

itil~

~~
~~~Rli

* SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only.

**Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.

Eberline Services
Oak Ridge Laboratory
Analysis Sheet

Printed: 81712013 10:34 AM


Page 2 of 3

13-07149

Ra226

Run 1

Internal
Fraction

Sample
Desc

Tracer Total
ACT(dpm)

Tracer
Aliquot(g)

Radiometric
Tracer (pCi)

Radiometric GravCa"ier
%Rec
Added(ml)

Grav Filter
Tare (g)

Grav Filter
Final (g)

Grav Filter
Net(g)

Grav
%Rec

Mean
%Rec

SAF
1*

SAF
2*

01

LCS

0.9174

909.3

404.0

98.64

0.0229

0.0296

0.0067

98.64

2.40

1.00

02

MBL

0.9114

903.3

414.1

101.77

0.0230

0.0295

0.0065

101.77

2.34

1.00

03

DUP

0.9088

900.7

413.9

102.01

0.0225

0.0302

0.0077

102.01

2.69

1.00

04

TRG

0.9069

898.8

369.8

91.33

0.0227

0.0301

0.0074

91.33

2.61

1.00

05

TRG

0.9085

900.4

296.5

73.10

0.0227

0.0289

0.0062

73.10

2.23

1.00

06

TRG

0.9097

901.6

387.5

95.41

0.0229

0.0301

0.0072

95.41

2.55

1.00

07

TRG

0.9089

900.8

369.4

91.03

0.0224

0.0294

0.0070

91.03

2.50

1.00

08

DO

0.9075

899.4

425.3

104.97

0.0227

0.0303

0.0076

104.97

2.66

1.00

09

TRG

0.9080

899.9

426.5

105.21

0.0225

0.0299

0.0074

105.21

2.61

1.00

10

TRG

0.9048

896.8

348.6

86.30

0.0228

0.0307

0.0079

86.30

2.74

1.00

11

TRG

0.9036

895.6

411.9

102.10

0.0226

0.0297

0.0071

102.10

2.53

1.00

12

TRG

0.9110

902.9

384.1

94.44

0.0226

0.0312

0.0086

94.44

2.91

1.00

0.0088

89.42

2.96

1.00

13

TRG

0.9075

899.4

362.3

89.42

0.0225

0.0313

14

TRG

0.9057

897.7

410.4

101.50

0.0228

0.0299

0.0071

101.50

2.53

1.00

15

TRG

0.9097

901.6

429.9

105.85

0.0226

0.0297

0.0071

105.85

2.53

1.00

~~!!II

* SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only.

Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.

Eberline Services
Oak Ridge Laboratory
Analysis Sheet

Printed: 8nt2013 10:34 AM


Page 3 of 3

13-07149

Ra226

Run 1

Internal
Fraction

Sample
Desc

01

Rough Prep
Date

Rough Prep
By

Prep
Date

Prep
By

Sep to
Date/Time

SeptO
By

LCS

08/02/13 08:18

JWOLFE

08/06/13 09:39

TSMITH

02

MBL

08/02/13 08:18

JWOLFE

08/06/13 09:39

TS MITH

03

DUP

08/02/13 08: 18

JWOLFE

08/06/13 09:39

TSMITH

04

TRG

08/02/13 08:18

JWOLFE

08/06/13 09:39

TSMITH

05

TRG

08/02/13 08: 18

JWOLFE

08/06/13 09:39

TS MITH

06

TRG

08/02/13 08: 18

JWOLFE

08/06/13 09:39

TSMITH

07

TRG

08/02/13 08:18

JWOLFE

08/06/13 09:39

TS MITH

08

DO

08/02/13 08: 18

JWOLFE

08/06/13 09:39

TSMITH

09

TRG

08/02/13 08:18

JWOLFE

08/06/13 09:39

TS MITH

10

TRG

08/02/13 08: 18

JWOLFE

08/06/13 09:39

TSMITH

11

TRG

08/02/13 08: 18

JWOLFE

08/06/13 09:39

TSMITH

12

TRG

08/02/13 08: 18

JWOLFE

08/06/13 09:39

TSMITH

Sep t1
Date/Time

Sep t1
By

'
-

-----

13

TRG

08/02/13 08: 18

JWOLFE

08/06/13 09:39

TSMITH

14

TRG

08/02/13 08:18

JWOLFE

08/06/13 09:39

TS MITH

15

TRG

08/02/13 08:18

JWOLFE

08/06/13 09:39

TS MITH

--

;;~

1"1)

* SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only.

**Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.

J~

::i

.g

0
(,)

.!!

~
Ill

c:
ct

Work Order: 13-07149-Ra226-1

Nuclide

Sample
Desc

Client
Identification

01

RA-226

LCS

LCS

pCUI

1.15E+01

1.37E+OO

1.62E-01 !

02

RA-226

MBL

BLANK

pCi/I

-2.15E-02

8.91E-02

2.88E-01 I

03

RA-226

DUP

D-81 TOT

04

RA-226

TRG

PZ-302-AS TOT

05

RA-226

Lab
Fraction

ns

07

RA-226

TRG

LR-100 DIS

08

RA-226

DO

D-81 TOT

Error Estimate

MDA

i
I

LCS
Known

1.02E+01

3.87E-01

3.16E-01

pCi/I

8.47E-01

4.02E-01

3.35E-01

pCi/I

3.41E-01

2.60E-01

2.63E-01 1

RA-226

~---J

pCi/I

I
!

I
II
I

3.25E-01
2.33E-01

2.96E-01

2.82E-01

8.35E-01

3.54E-01

OK

I
3.10E-01 1

OK

1.19E-01 I

OK

OK

3.81E-01

2.11E-01 i

OK

t-TRG
I

PZ-204-SS TOT

pCi/I

8.76E-01

4.00E-01

2.56E-01

OK

---

11

RA-226

TRG

PZ-204-SS DIS

pCl/1

5.81E-01

2.89E-01

1.53E-01

OK

12

RA-226

TRG

LR-103 TOT

pCi/I

7.11E-01

3.59E-01

2.93E-01

OK

LR-103 DIS

pCi/I

1.05E+OO

4.72E-01

3.49E-01

OK

pCi/I

2.15E-01

1.93E-01

2.s1E-01 I

pCl/I

3.70E-01

2.31E-01

1.85E-01 I

13
t

Q.
Q.

::I
(/)

....c
Q)

~I

(,)

E
Q)
O'l

RA-226

TRG

14

RA-226

15

RA-226

I TRG

PZ-111-KS TOT

TRG

PZ-111-KS DIS

-----+

ns
c
ns

:z
c

Q)
Q)

c,
c
w
;~1

!'..)

+!
I
I

O'l

;::

-t-

OK

--~

-t

II
!

Blank
Flag

OK

OK

pCi/I

MDA
Flag

OK

pCi/I

OK

NA

3.61E-01

112.89

RPO
Flag

OK
-

'

5.79E-01

LCS
Flag

OK

8.39E-01

pCi/I

LCS
%R

pCi/I

D-81 DIS

TRG
--

10

LR-100 TOT

TRG

RA-226

PZ-302-AS DIS

TRG

RA-226

~-

Results

06

09

Activity
Units

CD
N
N

Printed: 8/8/2013 8:43 AM

Page 1of3

Preliminary Data Report & Analytical Calculations

Eberline Services
Oak Ridge Laboratory

OK

Eberline Services
Oak Ridge Laboratory

Lab

Fraction

01

Printed: 8/8/2013 8:43 AM

Page 2 of 3

Preliminary Data Report & Analytical Calculations

Work Order: 13-07149-Ra226-1

Sample
Aliquot

Radiometric
%Rec

Grav
%Rec

Mean
%Rec

Sept1
Date/Time

SeptO
Date/Time

Nuclide

Sample
Oesc

Sample
Date

RA-226

LCS

07/23/13 00:00

1.00E+OO

98.64

0.00

98.64

8/6/2013 9:39

RA-226

MBL

07/23/13 00:00

1.00E+OO

100.00

0.00

101.77

8/6/2013 9:39

RA-226

DUP

07/17/13 10:43

1.00E+OO

100.ool

o.ool
i

102.01

8/6/2013 9:39\

RA-226

TRG

07/16/13 15:30

1.00E+OO

91.33 1

0.00

91.33

8/6/2013 9:391

SAF

-------

02

c:

ii!

""""

------------- f---

03

--~

---------

.g

8
.!!!
].
~

04

(C)

'---------- ------ -----

05----
,_____

RA-226

TRG

07/16/13 15:30

I 1.00E+OO

73.10

0.00

73.10

8/6/2013 9:3-;r

06

RA-226

TRG

07/17/13 10:23

1.00E+OO

95.41

0.00

95.41

8/6/2013 9:39t

1-------

RA-226

TRG

07/17/13 10:23

1.00E+OO

91.03

0.00

91.03

8/6/2013 9:3r

0.00

104.97

8/6/2013 9:3+

ca

07

.E

RA-226

09

RA-226

TRG

07/17/13 10:43

1.00E+OO

100.ool

o.ool

105.21

8/6/2013 9:39

10

RA-226

TRG

07/17/1311:40

1.00E+OO

86.30

0.00

86.30

8/6/2013 9:39

11

RA-226

TRG

07/17/13 11:40

1.00E+OO

100.00

0.00

102.10

8/6/2013 9:39

12

RA-226

TRG

07/17/13 12:15

1.00E+OO

94.44

0.00

94.44

8/6/2013 9:39

13

RA-226

TRG

07/17/13 12:15

1.00E+OO

89.42

0.00

89.42

8/6/2013 9:39

RA-226

TRG

07/17/13 13:09

1.00E+OO

100.ool

0.00

101.50

8/6/2013 9:39

o.oo[

105.85

8/6/2013 9:39

DO

07/17/13 10:43

1.00E+OO

100.ool
I

14

----------

:I

15

en
....

c
E
Cl)

RA-226

TRG

07/17/13 13:09

1.00E+OO

100.00

Cl)

Cl

----

--

Ill

c
Ill
::!!:
Cl
c
;:::

__j___

---

---

---------------

i
i
i

~r~

r,J!
'""-l

(.l(.1,

~~--

__ ,_______

-r-
I

-----

Cl)
Cl)

.5
Cl
c

08

-------

c.
c.

i: I
0 I

-t

N
N

~-----

.!!!

---

-------i----
I

--

Eberline Services
Oak Ridge Laboratory

Lab

01
r:i::

.g
8
.!!!

~I

~ i
c:t I

"""""
<D
N
N

~i:
~
::l

RA-226

~
0

Q.
Q.

::s

CJ)

'l:

E
Ql
en
C'CS
c
C'CS
:ii:
en
c
;::
Ql
Ql

'Ci
c
w

Alpha_022

170 -5.30 E-01

DUP

08/07/1316:06

A_Spec

Alpha_023

170 2.01 E+01

RA-226

RA-226

) TRG

06

Bl

s-~~~~--1 ~;~-226

09

RA-226

10

RA-226

13
14

15

DO

______i__ ------
: TRG
I

r TR~

Eff

CPM

16.6

11.00 E-03
[9.00 E-03

15.3

11.10 E-02

17.1

-r

A_Spec

08/07/13 16:06

TRG

TRG
_ _ _ _ _ _ _ _ _ j____________

Alpha_024

170 1.91 E+01

11.10 E-02

A_Spec

Alpha_025

170 7.32 E+OO

14.00 E-03

08/07/1316:06

A_Spec

Alpha_027

170 1.41 E+01

11.10 E-02

08/07/1316:06

A_Spec

Alpha_029

170 9.66 E+OO

12.00 E-03

08/07/13 16:06

A_Spec

Alpha_031

170 5.96 E+OO

/1.20 E-02

14.2

08/07/13 16:06

A Spec

Alpha 033

170 2.23 E+01

14.00 E-03

18.5

08/07/13 16:06

A_Spec

Alpha_034

170 1.93

17.4

E+01~.oo E-03 I
I

19.5

18.6

TRG

08/07/13 16:06

A_Spec

Alpha_035

17011.58 E+01

11.00 E-03

18.3

RA-226

TRG

08/07/13 16:06

A_Spec

Alpha_036

17011.66 E+01

18.00 E-03

19.1
17.2

RA.226

--~ _,.:~ -

RA-226

TRG

08/07/1316:06

A_Spec

Alpha_038

170 2.06 E+01

18.00 E-03

0810711316'06

A_Spee

Alpha_039

170 6.30 E+OO

11.00--E--0-2--------'--------------"
19.7

Alpha_040

17011.05 E+01

13.00 E-03

08/07/13 16:06

--

A_Spec

t
!----+----------= ~ _J_-

._,_______---------+-----------j-----f

I
:

-+----

17.3

RA-226

l---~-2;;-----1-~;~j

17.1

08/07/13 16:06

-------+------ ______

l--------------------+---------1---II

(..~jl

170 2.97 E+02

A_Spec

05

Bkg

Ql

Alpha_019

I
I

08/07/13 16:06

RA-226

<.i

A_Spec

Counts

MBL

04

11

.5

08/07/1316:06

Count
Time

Carrier

Detect

I----+-------------+----------- ~--

(/)

ifl

--+-- --

Halflife
(days)

---------,--------- ---

.,
.!:;
1::
.,

i LCS

----

03

Counting
Date/Time

+-----
I

RA-226

1----

cu

a::

I Sample
Desc

RA-226

02

Work Order: 13-07149-Ra226-1

Nuclide

Fraction

Printed: 8/8/2013 8:43 AM

Page 3 of 3

Preliminary Data Report & Analytical Calculations

19

1-~----------1
I

I
i

----+-------------1

Count Room Report


Client: Engineering Management Su

Printed: 817/2013 10:34 AM


Page 1of1

13-07149-Ra226-1 (pCi/I) in WA
Tracer ID: Ba-Ga

M\.

/..
"'

'

y
(1

">

'

SAF

SAF

98.64

2.40

1.00

414.1000

101.77

2.34

1.00

900.7299

413.9000

102.01

2.69

1.00

0.9069

898.8467 I

369.8000

91.33

2.61

1.00

1.0000

0.9085

900.4325

296.5000

73.10

2.23

1.00

07/17/13 10:23

1.0000

0.9097

901.6219

387.5000

95.41

2.55

1.00

LR-100 DIS

07/17/13 10:23

1.0000

0.9089

900.8290

369.4000

91.03

2.50

1.00

DO

D-81 TOT

07/17/13 10:43

1.0000

0.9075

899.4414

425.3000

104.97

2.66

1.00

09

TRG

D-81 DIS

07/17/13 10:43

1.0000

0.9080

899.9370

426.5000

105.21

2.61

1.00

10

TRG

PZ-204-SS TOT

07/17/1311:40

1.0000

0.9048

896.7654

348.6000

86.30

2.74

1.00

11

TRG

PZ-204-SS DIS

07/17/13 11 :40

1.0000

0.9036

895.5760

411.9000

102.10

2.53

1.00

12

TRG

LR-103 TOT

07/17/13 12:15

1.0000

0.9110

902.9103

384.1000

94.44

2.91

1.00

13

TRG

LR-103 DIS

07/17/13 12:15

1.0000

0.9075

899.4414

362.3000

89.42

2.96

1.00

14

TRG

PZ-111-KS TOT

07/17/13 13:09

1.0000

0.9057

897.6574

410.4000

101.50

2.53

1.00

15

TRG

PZ-111-KS DIS

07/17/13 13:09

1.0000

0.9097

901.6219

429.9000

105.85

2.53

1.00

Internal
Fraction

Sample
Desc

Client
ID

Sample
Date

Sample
Aliquot

Tracer
ACT(dpm)

01

LCS

LCS

07/23/13 00:00

1.0000

0.9174

909.2535

404.0000

02

MBL

BLANK

07/23/13 00:00

1.0000

0.9114

903.3068

03

DUP

D-81 TOT

07/17/13 10:43

1.0000

0.9088

04

TRG

PZ-302-AS TOT

07/16/13 15:30

1.0000

05

TRG

PZ-302-AS DIS

07/16/13 15:30

06

TRG

LR-100 TOT

07

TRG

08

Tracer
Aliquot (g)

Radiometric
Tracer (pCi)

Radiometric
%Rec

I
~-l~

Eberline Services
Oak Ridge Laboratory

Page 1of1
Printed: 812/2013 8:18 AM

Spike and Tracer Worksheet


Technician

Analysis Code

Date

Ra226

8/2/2013 8:17

;;;:Les

MS

LCSD

Msl>

Volume
Used(g)

Volume
Used(g)

Volume
Used(g)

Volume
Used(g)

Technician Initials

Witness Initials

JWOLFE

MS

LCS
Known
pCi

10.22

Error
Estimate

0.470

Added
pCi

0.00

i
I

MSC
Error
Estimate

Known
pCi

0.000

Error
Estimate

0.00

Added
pCi

0.000

O.OOi

----t---

------1
Balance Printer Tapes>
Solution
Date

Volume
Used(g)

81212013 .

o.9174

1.0200

8/2/2013 .

0.9114

1.0200

:~.908s

81212013

. ,,,;,,

8/2/2013

1.0200

o,9oas

1.0200

:p.9097 I

8/2/20131

8/2/2013
81212013

....

~.

LCS

,., ~

' ,,

'I

i '

1.0200
1.0200

IJ.9075
.

1.0200
---I

o.soso

1.0200

.. .

1.0200

8/2/2013

0.9036

1.0200

8/2/2013;

0.9110

1.0200

8/2/20131

. U075

812120131

. . o.9Gs1

1.0200

o.9bs1

1.0200

8/2120131

Version 2.0 08/99

'. 0.9089

09048 I

8/2/20131 1

Tracer

. ' ' i>

i'~

8/212013 I

1.0200

;;

<>~9969

8/212013R

;'31

Approx
Addition

1.0200

Error
Estimate

Matrix Spike

0.000

Eberline Analytical
Oak Ridge Laboratory

Analysis Code

01
02
03
04
05
06
07
08
09
10
11
12
13
14
15

liters

Sample

Muffle Data

Client ID

Type

Ratio
Postll?re

LCS
BLANK
D-81 TOT
PZ-302-AS TOT
PZ-302-AS DIS
LR-100 TOT
LR-100 DIS
D~81 TOT
D-81 DIS
PZ-204-SS TOT
PZ-204-SS DIS
LR-103 TOT
LR-103 DIS
PZ-111-KS TOT
PZ-111-KS DIS

LCS
MBL
DUP
TRG
TRG
TRG
TRG
DO
TRG
TRG
TRG
TRG
TRG
TRG
TRG

Engineering Management Support, Inc.

c:ti~l

II"'~

00
l"1t,il

Comments

Technician:

NoofQ!ls
;''.",

..

"

';

. ...

:;>

JWOLFE
Aliquot Data

.. 1.

"

..

':

.,\',.

"

"

::. I

'
;

',

.''"' v.

"

,::

"

..

. :'
(~

., . . .,.:

.. "!:

. "',..'"""

::.

:.:

..

. i

,;.
.~

...

:
,.

'"
,

"

.:

,."':.

"

. ~

"

.: .

..

H .:.

'

''....
;;

MS Aliquot Data

1.0000E+OO . 1.000QE+OO
1.0000E+OO "; f.OOOOE+OO
1.0000E+OO
1'.0000E+OO
1.0000E+OO
1.00QOE+OO
1.0000E+OO 1;,oQOOE+OO
1.0000E+OO . 1~0000E+OO
1.0000E+OO
;LOOOOE+OO
1.0000E+OO . 1.<l!JOOE+OO
1.0000E+OO .. iooooE+OO
1.0000E+OO : 1{0000E+OO
1.0000E+OO ;, {OOOOE+OO
1.0000E+OO
f.OooQE+OO
1.0000E+OO tOOGOE+OO
1.0000E+OO
f (JOOOE+OO
1.0000E+OO ,(OOOOE+OO

,.

"

')

..

"

'

H-3 Solids Only

"

f J~!i)tEquiv

..

I..

....

"? '.""
,, ". ,.

'

Aliquot

Ratio

"

I:,

:,

..

"

Off: Factor

,::,:

:.

".'

...

"

8/13/2013

. '>

"!: ;

Technician

Dilution Data

I<

Lab Deadline

'''.' ;.l

Rpt Units

Ra226

Lab
Fraction

Printed: 8/2/2013 8:19 AM

Page 1of1

Aliquot Worksheet

Water Added
(ml)

Netequlv ~

Aliquot

,,,

>,,

...
"
,',

''

... \ . "

7 ..

"!:

"

.,

'

,.

'"!:,~
.,,,

':

H3 Dist
Aliq

'

'

.,

...

t ,

,L;
::

',

--

',,1:~'

": :! D

"

.:.'::<

..

.,

.:.:::

.:::::.
..

"

'" :: :'"""~." \

,.

,.

...

~" ii

. .:.:. <.;;:";.:""'

'

" "

,,:

I
<

\.
<:! ....()
~_))ate: --0-'~

12

.......-"""_ . .

Eberline Services - Oak Ridge


Version 1.0 9/1999

Printed: 8/6/2013 11 :29 AM


Page 1 of 1

Gravimetric Worksheet

Gravimetric
Carrier

Analysis
Code

Work Order

Carrier Cone
(mg/ml)

Technician

Ra226
TRetec Engineering Management Support, Inc. Sample
Fraction

Client ID

Type

01
02
03
04
05
06
07
08
09
10
11
12
13
14
15

LCS
BLANK
DUP
PZ-302-AS TOT
PZ-302-AS DIS
LR-100 TOT
LR-100 DIS
D-81 TOT
D-81 DIS
PZ-204-SS TOT
PZ-204-SS DIS
LR-103 TOT
LR-103 DIS
PZ-111-KS TOT
PZ-111-KS DIS

LCS
MBL
DUP
TRG
TRG
TRG
TRG
DO
TRG
TRG
TRG
TRG
TRG
TRG
TRG

---

f-

TS MITH

Filter Data

Carrier Data
Carrier Added
(ml)

Filter Tare
(g)

0.0229
0.0230
0.0225
0.0227
0.0227
0.0229
0.0224
0.0227
0.0225
0.0228
0.0226
0.0226
0.0225
0.0228
0.0226

Gravimetric

..

Filter ~et
" ~{g}

Filter Final
(g)

%
Recovery

/ '' ~po6f

0.0296
0.0295
0.0302
0.0301
0.0289
0.0301
0.0294
0.0303
0.0299
0.0307
0.0297
0.0312
0.0313
0.0299
0.0297

. . \

(tQo6 $
1

-~. .0~001t

: c:fmo.14
.~...

...

u~no?(l
(l:q(l16

..
..

.
.

Q~0074

..
.

Q.00~2

:0..00.12

-O'ioo19

- . q~oo;:1
o.ooss
.O,.ooss.
. (f.ol)7t

o.OQ71

..

.. :

.['

i .

f'

.....
_;
.
;..........
.

Technician:
~,Ji

~~

Date:

~/~_!]__

'

Sample Description:

Spectrum File:

Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

SPIKE
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000654
1307149A-RA
01
Shelf 2
Ra

Detector Name:

Alpha_Ol9
Chamber Serial Number:

Detector Serial Number:


19
Env. Background:

System Bkgd 64043


Reagent Blank:

<not performed>
Sample Size:

Generic Mult. Factor:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

l.OOOE+OOO +/O.OOOE+OOO liter


2.400E+OOO
Generic Div. Factor:
8/7/2013
1:10:08 PM
8/7 /2013
4:06:13 PM
170.0 minutes
170.0 minutes

Chem. Recovery Factor:

Counting Efficiency:

Effective Efficiency:

0.9864 +/0.1659 +/0.1637 +/-

0.0000

0.0029 on 2/17/2013
0.0029

Control Certificate Name:


Ra226 Ra-Sb

Chem. Recov. of Control:


RA-226
0.470344 +/Peak Match Tolerance:

0.350 MeV

PEAK
Nuclide

Energy
(MeV)

RA-224
RA-226

5.528
4.706

Net
Pk Area

AREA

10:45:23 AM

0.031846

REPORT

Pk Area
Error %

470.15
296.83

l.OOOE+OOO

9.05
11. 38

Ambient
Backgnd
0.85
0.17

Reagent
Backgnd

FWHM
(keV)

O.OOE+OOO
O.OOE+OOO

6.1
8.8

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

RA-224
RA-226

0.968
0.992

5685.50*
4785.00*

Activity
(pCi/liter )
l.92E+001 +/
l.15E+001 +/

l.86E+OOO
l.37E+OOO

MDA
(pCi/liter
2.45E-001 +/
l.62E-001 +/

8.48E-003
5.62E-003

0000065496.CNF

Live Time 10200.000 sec


Real Time 10200.000 sec
start:
1 3279.3(kev)
stop : 1024 6687. O(kev)
Acq. Start wed Aug 07 16: 06: 13 2013

60
55

50

45

40

35

Vl
.j-J

s:::

:::s

8 30
25

20

15
10
5
0~~'1L.4'-UJ!L-W.~--"-"-.=.!U----LJ._J-'-J..l-.__-L-"--U.-4-._.__-'---'--'"-'--+-J--"--'----J--J---+_...~_,_.__........_+"-_,___.__._--'"-'-'-+---'-"'--~

3500
~!l!
r-.~
(~)

U'i\

ROI Type: 1

4000

4500

5000
Energy(kev)

5500

6000

6500

Channel Data Report

8/8/2013

Page

5:36:24 AM

*******************************************************
s P E C T R A L DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

01

Elapsed Live time:


Elapsed Real Time:

10200
10200

Channell------l-------l-------l-------1-------1-------1-------l-------I
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:

10200
0
2
0
0
2
0
2
0
1
0
1
1
2
3
1
1
2
0
3
2
2
3
1
3
2
1
1
2
2
4
3
3
0
3
2
2
7
5
1
6
5
4
9
2
1

10200
0
1
0
1
0
1
1
0
1
1
2
3
1
0
0
2
2
1
2
1
1
3
2
3
4
1
2
1
6
4
5
1
4
5
2
2
5
3
2
1
2
1
4
4
2

0
1
0
0
1
1
0
1
0
2
1
1
2
1
1
0
3
2
1
0
3
0
0
3
3
3
1
0
4
2
5
4
1
4
5
2
5
7
4
1
6
4
5
4
2
5

2
0
1
0
0
2
1
1
1
3
0
1
0
2
1
1
2
3
3
1
1
1
1
4
2
3
4
2
2
0
2
0
4
2
3
4
2
3
1
5
3
3
2
1
8
5

0
0
0
1
1
1
0
3
3
1
0
3
0
2
3
1
4
1
2
2
1
0
0
1
3
3
5
2
3
2
3
0
4
1
1
6
1
4
2
2
4
1
3
3
3
4

2
2
1
4
1
3
1
2
1
0
2
1
2
0
0
1
3
2
1
2
1
6
3
3
1
1
2
5
3
2
3
1
4
1
5
1
3
3
2
3
2
2
0
6
4
4

1
1
0
4
2
2
0
2
1
0
0
1
0
1
4
0
1
1
2
1
2
1
3
1
5
4
4
3
2
3
3
3
3
0
3
4
4
2
3
1
0
1
1
6
3
4

1
1
2
1
1
0
1
0
0
0
3
2
1
3
1
2
1
2
1
1
0
1
1
3
2
1
1
2
0
4
4
2
3
2
4
5
3
4
5
2
3
7
3
2
6
3

Channel Data Report


369:

8/8/2013
3

Sample Title:

Page

5:36:24 AM
3

01

Channell------l-------l-------l-------1-------1-------1-------l-------I
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:
625:
633:
641:
649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:

2
7
2
6
6
2
7
5
4
2
2
4
3
3
4
0
2
3
2
5
6
3
2
6
1
2
7
2
3
6
5
4
3
6
5
3
2
6
5
6
10
3
5
8
5
1
4
5
2
4
3
6
3

4
6
6
1
1
2
4
3
5
5
2
1
3
2
2
3
3
2
3
3
4
4
5
2
7
3
3
5
3
1
6
4
7
6
4
6
1
8
4
6
2
5
0
3
6
1
2
6
2
4
6
4
1

3
2
2
2
4
5
2
7
1
2
2
3
2
4
4
2
4
7
2
2
2
4
1
3
6
3
2
6
6
4
5
2
6
5
5
5
2
4
9
5
2
10
3
4
3
4
5
5
5
4
5
5
5

5
4
1
3
7
5
3
6
5
2
4
6
2
0
3
3
5
4
6
2
2
5
1
7
5
5
5
5
7
2
4
2
4
2
7
11
4
5
7
4
3
6
6
6
4
4
3
3
5
2
2
3
3

4
6
5
8
5
5
3
4
8
2
1
4
4
1
4
4
2
1
4
2
3
3
2
3
8
5
4
2
3
5
7
3
8
2
4
5
4
5
6
5
3
6
4
5
3
6
6
5
3
3
3
8
2

2
0
3
3
5
6
7
4
2
5
2
1
2
6
3
3
1
3
3
2
4
4
6
5
4
9
3
4
3
1
3
1
8
4
3
8
6
2
5
7
4
7
3
2
1
1
4
5
5
4
5
2
6

3
3
6
8
7
3
6
9
4
3
1
1
2
2
6
2
1
3
0
1
5
2
5
3
5
3
10
10
5
4
9
5
5
9
3
2
8
4
7
4
6
6
5
1
1
5
2
2
4
1
2
0
0

1
4
7
4
2
3
2
6
9
1
4
5
7
3
2
1
4
6
3
5
4
8
3
5
3
4
7
2
6
2
8
7
6
8
5
5
3
2
3
0
5
8
3
2
0
3
6
5
4
4
2
1
6

""
G

Channel Data Report


801:

8/8/2013
3

Sample Title:

Page

5:36:24 AM
6

01

Channell------l-------1-------1-------1-------l-------l-------l-------I
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

9
7
4
4
3
4
3
6
6
3
7
6
2
2
2
3
2
2
6
2
6
1
1
5
0
2
3

1
7
0
9
7
2
5
8
3
2
6
3
2
3
1
3
0
2
1
1
2
2
3
5
1
4
1

6
4
8
2
5
6
12
3
6
2
6
1
3
2
4
1
1
2
3
3
3
2
2
4
1
5
5

6
4
3
3
3
2
5
1
7
6
1
3
1
2
1
2
0
3
0
4
2
2
0
1
1
1
1

4
7
3
6
5
4
5
6
3
6
3
2
3
3
1
3
4
2
1
3
3
1
3
2
2
2
1

5
5
2
1
4
1
7
4
3
2
2
3
1
2
2
5
1
4
2
2
1
4
3
2
2
2
4

4
2
2
2
1
3
2
7
3
5
4
1
5
1
7
2
3
0
4
1
1
2
1
4
2
2
1

8
5
5
3
5
6
2
3
2
6
1
3
2
4
2
1
4
3
6
3
3
2
1
1

5288

Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:

BLANK
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000654
1307149A-RA
02
Shelf 2
Ra

Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:

Alpha_022
22
System Bkgd 64044
<not performed>

Sample Size:
Generic Mult. Factor:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:

l.OOOE+OOO +/- O.OOOE+OOO liter


2.340E+OOO
Generic Div. Factor:
8/7/2013
1:10:08 PM
8/7/2013
4:06:14 PM
170.0 minutes
170.0 minutes

Chem. Recovery Factor:


Counting Efficiency:
Effective Efficiency:

1.0000 +/0.1531 +/0.1531 +/-

Peak Match Tolerance:

Energy
(MeV)

RA-224
RA-226

1:57:26 PM

0.350 MeV

PEAK

Nuclide

0.0000
0.0029 on 12/15/2012
0.0029

l.OOOE+OOO

Net
Pk Area

5.640
4.764

-0.55
-0.53

AREA

REPORT

Pk Area
Error %
555.92
415.13

Ambient
Backgnd

Reagent
Backgnd

FWHM
(keV)

2.55
1.53

O.OOE+OOO
O.OOE+OOO

3.1
3.1

NUCLIDE ANALYSIS RESULTS

Nuclide

Id
Conf.

Energy
(keV)

RA-224
RA-226

0.997
0.999

5685.50*
4785.00*

Activity
(pCi/liter )
-2.34E-002 +/- l.30E-001
-2.15E-002 +/- 8.91E-002

MDA
(pCi/liter
3.57E-001 +/- l.33E-002
2.88E-001 +/- l.07E-002

6289

0000065452.CNF

Live Time :10200.000 sec


Real Time :10200.000 sec
Start:
1:3421.S(kev)

Stop : 1024:6608.B(kev)

Acq. Start :wed Aug 07 16:06:14 2013

60

55

50

45

40

35

V)

.j-1

c:

::::s

8 30

25

20

15

10

..,,
"'

3500
ROI Type: 1

4000

4500

5000
Energy(kev)

5500

6000

6500

Channel Data Report

8/8/2013

Page

5:36:30 AM

*******************************************************
s p E CTR AL DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

02

Elapsed Live time:


Elapsed Real Time:

10200
10200

Channell------l-------l-------1-------1-------1-------l-------l-------I
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:

10200
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

10200
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

fil2Q
... .;;; 1

Channel Data Report


369:

8/8/2013
0

Sample Title:

Page

5:36:30 AM
0

02

Channell------l-------1-------1-------1-------l-------l-------l-------I
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:
625:
633:
641:
649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
1
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

m2s2

Channel Data Report


801:

8/8/2013
0

Sample Title:

Page

5:36:30 AM
0

02

Channell------l-------l-------l-------l-------1-------1-------1-------I
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

5293

~~Apex-Alpha'"

Sample Description:

Spectrum File:

Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

D-81 TOT-DUP
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000654
1307149A-RA
03
Shelf 2
Ra

Detector Name:

Alpha_023
Chamber Serial Number:

Detector Serial Number:


23
Env. Background:

System Bkgd 64045


Reagent Blank:

<not performed>
Sample Size:

Generic Mult. Factor:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

l.OOOE+OOO +/- O.OOOE+OOO liter


Generic Div. Factor:
2.690E+OOO
1:10:08 PM
7/17/2013
4:06:15 PM
8/7 /2013
170.0 minutes
170.0 minutes

Chem. Recovery Factor:

Counting Efficiency:

Effective Efficiency:

1. 0000 +/-

0 .1710 +/0.1710 +/-

Peak Match Tolerance:

Energy
(MeV)

RA-224
RA-226

6:18:25 PM

0.350 MeV

PEAK

Nuclide

0.0000
0.0030 on 7/20/2013
0.0030

l.OOOE+OOO

Net
Pk Area

5.541
4.601

AREA
Pk Area
Error %"

12.45
20.13

61.85
46.00

REPORT
Ambient
Backgnd
2.55
1. 87

FWHM
(keV)

Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO

3.1
3.1

NUCLIDE ANALYSIS RESULTS

Nuclide

Id
Conf.

Energy
(keV)

RA-224
RA-226

0.973
0.957

5685.50*
4785.00*

Activity
(pCi/liter )
5.50E-001 +/- 3.40E-001
8.39E-001 +/- 3.87E-001

MDA
(pCi/liter
3.70E-001 +/- l.28E-002
3.16E-001 +/- l.09E-002

0000065453.CNF

Live Time :10200.000 sec


Real Time :10200.000 sec
Start:
1: 3403 .O(kev)

Stop : 1024:6588.3(kev)

Acq. start :wed Aug 07 16:06:15 2013

60
55

50

45

40

35

VI

.f-J

c:

8 30

25

20

15

10

~
I

3500

4000

~.!ii
f\~

U11

ROI Type: l

4500

M~,

1: IM

5000
Energy(kev)

5500

,H

6000

6500

Channel Data Report

8/8/2013

Page

5:36:36 AM

*******************************************************
s p E C T R A L DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

03

Elapsed Live time:


Elapsed Real Time:

10200
10200

Channell------l-------l-------l-------1-------1-------1-------l-------I
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:

10200
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
1
0
0
0

10200
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
1
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
1
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
1
0
0
0
0
0
0
0

0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0

0
0
0
1
0
0
0
0
1
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
1
0
0
0

8295

Channel Data Report


369:

8/8/2013
1

Sample Title:

Page

5:36:36 AM
0

03

Channell------l-------1-------1-------1-------l-------l-------l-------I
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:
625:
633:
641:
649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:

1
3
0
0
0
0
0
0
0
1
0
0
0
1
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
1

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
1
0

1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
1
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0

0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
1
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
1
1
0
0
0
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
1
0
0
2
0
1
0
0
0
0
0
0
0
0
1
0

0
1
0
0
1
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

82

Channel Data Report


801:

8/8/2013
0

Sample Title:

Page

5:36:36 AM
0

03

Channell------l-------l-------l-------1-------1-------1-------l-------I
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
1
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0

0
0
0
0
0
0
0
0
0
1
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0

82

~---====555'1t'Ap ex-A Ip ha

Sample Description:

Spectrum File:

Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

PZ-302-AS TOT
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000654
1307149A-RA
04
Shelf 2
Ra

Detector Name:

Alpha_024
Chamber Serial Number:

Detector Serial Number:


24
Env. Background:

System Bkgd 64046


Reagent Blank:

<not performed>
Sample Size:

Generic Mult. Factor:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

l.OOOE+OOO +/- O.OOOE+OOO liter


2.610E+OOO
Generic Div. Factor:
1:10:08 PM
7/16/2013
8/7/2013
4:06:16 PM
170.0 minutes
170.0 minutes

Chem. Recovery Factor:

Counting Efficiency:

Effective Efficiency:

0.9133 +/0.1710 +/0.1562 +/-

Peak Match Tolerance:

Energy
(MeV)

RA-224
RA-226

2:02:15 PM

0.350 MeV

PEAK

Nuclide

0.0000

0.0032 on 12/15/2012
0.0029

1.000E+OOO

Net
Pk Area

5.565
4.580

AREA

REPORT

Pk Area
Error %

7.64
19.13

77.95
47.31

Ambient
Backgnd
1.36
1.87

FWHM
(keV)

Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO

3.1
3.1

NUCLIDE ANALYSIS RESULTS

Nuclide

Id
Conf.

Energy
(keV)

RA-224
RA-226

0.981
0.947

5685.50*
4785.00*

Activity
(pCi/liter )
3.58E-001 +/- 2.80E-001
8.47E-001 +/- 4.02E-001

z4G

g(g/rJ

MDA
(pCi/liter
3.22E-001 +/- 1.18E-002
3.35E-001 +/- 1.23E-002

0000065454.CNF

Live Time :10200.000 sec


Real Time :10200.000 sec
Start:
1:3411.G(kev)
Stop : 1024: 6597 .O(kev)
Acq. Start :wed Aug 07 16:06:16 2013

60
55

50

45

40

35

VI

.j....I

s:::

:::J

8 30

25

20

15

10

,\ l:1
I

3500

4000

a
(,.~

;tll!
~

ROI Type: 1

4500

5000
Energy(kev)

5500

i1

6000

6500

Channel Data Report

8/8/2013

Page

5:36:42 AM

*******************************************************

s P E C T R A L DAT A R E P 0 R T *****

*****
*******************************************************

Sample Title:

04

Elapsed Live time:


Elapsed Real Time:

10200
10200

Channell------l-------l-------1-------1-------1-------l-------l-------I
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:

10200
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
1
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
1
0
0
0

10200
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
1
0
0
0
0
0
1
0
0
0
0
0
0
0
0
1

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
1
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
1
0
0
0
0
0
0
0
1
0
0
0

0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
1
1
0
0
0
0
0

0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
1
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
1
0
0
1
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
1
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
1
0
0
0
0

83f.J1

Channel Data Report


369:

8/8/2013
1

Sample Title:

Page

5:36:42 AM
0

04

Channell------l-------1-------1-------1-------l-------l-------l-------I
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:
625:
633:
641:
649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
1

0
0
1
1
0
0
0
1
0
0
0
0
0
1
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0

0
1
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
1
0
0
0
0
1
0
0
0
0
0
0
0
0
0
1
0
1
0
0
0
0
1
1
0
1

0
0
0
0
0
0
0
2
1
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
1
0
0
0
0
0
0
0
0
0
0
1
0
0
0
1
0
0
0
0
0
1
0

0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
1
0
0
0
0
1
0
0
1
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
1
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
1
0
0
0
0
0
0
1
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
1
0
0

G3:fi2

Channel Data Report


801:

8/8/2013
0

Sample Title:

Page

5:36:42 AM
0

04

Channell------l-------l-------l-------1-------1-------1-------l-------I
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
1
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0

Sample Description:

Spectrum File:

Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

PZ-302-AS DIS
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000654
1307149A-RA
05
Shelf 2
Ra

Detector Name:

Alpha_025
Chamber Serial Number:

Detector Serial Number:


25
Env. Background:

System Bkgd 64047


Reagent Blank:

<not performed>
Sample Size:

Generic Mult. Factor:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

1.000E+OOO +/- O.OOOE+OOO liter


2.230E+OOO
Generic Div. Factor:
7/16/2013
1:10:08 PM
8/7/2013
4:06:17 PM
170.0 minutes
170.0 minutes

Chem. Recovery Factor:

Counting Efficiency:

Effective Efficiency:

0.7310 +/0.1736 +/0.1269 +/-

Peak Match Tolerance:

Energy
(MeV)

RA-224
RA-226

1:57:27 PM

0.350 MeV

PEAK
Nuclide

0.0000

0.0032 on 12/15/2012
0.0024

l.OOOE+OOO

Net
Pk Area

5.481
4.610

AREA

REPORT

Pk Area
Error %

2.13
7.32

Ambient
Backgnd

Reagent
Backgnd

1. 87
0.68

O.OOE+OOO
O.OOE+OOO

191.21
76.28

FWHM
(keV)
3.1
4.7

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

RA-224
RA-226

0.947
0.961

5685.50*
4785.00*

Activity
(pCi/liter )
1.05E-001 +/- 2.0lE-001
3.41E-001 +/- 2.60E-001

lt.G

g(g/r'!J

MDA
(pCi/liter
3.74E-001 +/- 1.37E-002
2.63E-001 +/- 9.60E-003

0000065455.CNF

Live Time :10200.000 sec


Real Time :10200.000 sec
start:
1: 3405. 9(kev)
stop : 1024: 6615. S(kev)
Acq. start :wed Aug 07 16:06:17 2013

60
55
50
45
40
35
Vl
.j..J

c:

:::Ji

8 30

25
20
15
10

5
0

,!

3500
~;!Ii

(,,Ji
Ill'~

U1

1,1

.\fi

ROI Type: 1

4000

4500

5000
Energy(kev)

5500

6000

6500

Channel Data Report

8/8/2013

Page

5:36:50 AM

*******************************************************
s p E C T R A L DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

05

Elapsed Live time:


Elapsed Real Time:

10200
10200

Channell------l-------1-------1-------1-------l-------l-------l-------I
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:

10200
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
1
0
0
0
0
0

10200
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
1
0
1
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
1
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0

1
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
2
0
0
0
0
0
0

8386

Channel Data Report


369:

8/8/2013
0

Sample Title:

Page

5:36:50 AM
0

05

Channell------l-------l-------1-------1-------1-------l-------l-------I
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:
625:
633:
641:
649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0

0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
1
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

El 357

Channel Data Report


801:

8/8/2013
0

Sample Title:

Page

5:36:50 AM
0

05

Channell------l-------l-------l-------l-------1-------1-------1-------I
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
1
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
1
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
1

0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0

Sample Description:

Spectrum File:

Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

LR-100 TOT
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000654
1307149A-RA
06
Shelf 2
Ra

Detector Name:

Alpha_027
Chamber Serial Number:

Detector Serial Number:


27
Env. Background:

System Bkgd 64048


Reagent Blank:

<not performed>
Sample Size:

Generic Mult. Factor:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

1.000E+OOO +/- O.OOOE+OOO liter


2.550E+OOO
Generic Div. Factor:
7/17/2013
1:10:08 PM
8/7/2013
4:06:18 PM
170.0 minutes
170.0 minutes

Chem. Recovery Factor:

Counting Efficiency:

Effective Efficiency:

0.9541 +/0.1728 +/0.1648 +/-

Peak Match Tolerance:

Energy
(MeV)

RA-224
RA-226

2:27:41 PM

0.350 MeV

PEAK
Nuclide

0.0000

0.0032 on 12/15/2012
0.0031

1.000E+OOO

Net
Pk Area

5.475
4.636

AREA

REPORT

Pk Area
Error %

0.96
14.13

373.51
56.03

Ambient
Backgnd

Reagent
Backgnd

2.04

O.OOE+OOO
O.OOE+OOO

1. 87

FWHM
(keV)
3.2
3.2

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

RA-224
RA-226

0.944
0. 971

5685.50*
4785.00*

Activity
(pCi/liter )
4.17E-002 +/
5.79E-001 +/

1.56E-001
3.25E-001

MDA
(pCi/liter
3.38E-001 +/
3.lOE-001 +/

1.24E-002
1.14E-002

0000065456.CNF

Live Time :10200.000 sec


Real Time :10200.000 sec
start:
1: 3402 .4(kev)
Stop : 1024: 6658. l(kev)
Acq. Start :wed Aug 07 16:06:18 2013

60
55
50
45
40
35
VI
.j.....I

c:

::::s

8 30

25
20
15
10
5
0

,\i,1,11,

3500
~~

(,,Ji
lf"..AI'

~!!~

1.

ROI Type: 1

4000

4500

5000
Energy(kev)

5500

6000

6500

Channel Data Report

8/8/2013

Page

5:36:56' 11.M

*******************************************************
s p E CTR AL DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

06

Elapsed Live time:


Elapsed Real Time:

10200
10200

Channell------l-------1-------1-------1-------l-------l-------l-------I
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:

10200
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
1

0
0
0
0
0
0
0
0
1
0
0
1
0
0
0

10200
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
1
0
0
0
0
0
0
0
1

0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1

0
0
0
1
0
0
0
0
0
1
0
1

0
0

0
0
0
0
0
0
1
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

5311

Channel Data Report


369:

8/8/2013
0

Sample Title:

Page

5:36:55 AM
0

06

Channell------l-------1-------1-------1-------l-------l-------l-------I
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:
625:
633:
641:
649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:

0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
1
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
1
0
0
0
0
0
1
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
1
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
2
1
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0

0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
1
0
0
0
0
0
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

312

Channel Data Report


801:

8/8/2013
0

Sample Title:

Page

5:36:56 AM
0

06

Channell------l-------l-------l-------l-------1-------1-------1-------I
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
1
0
0
0
0
0
0
0
0
0
1
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
1
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
1
0
0
0
0
0
0
0
0
2
1
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
1
1
0
0
0
0
0
0
0
0
0
0
0

9313

Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:

LR-100 DIS
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000654
1307149A-RA
07
Shelf 2
Ra

Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:

Alpha_029
29
System Bkgd 64049
<not performed>

Sample Size:
Generic Mult. Factor:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:

1.000E+OOO +/- O.OOOE+OOO liter


2.500E+OOO
Generic Div. Factor:
7/17/2013
1:10:08 PM
8/7 /2013
4:06:19 PM
170.0 minutes
170.0 minutes

Chern. Recovery Factor:


Counting Efficiency:
Effective Efficiency:

0.9103 +/0.1945 +/0.1771 +/-

Peak Match Tolerance:

Energy
(MeV)

RA-224
RA-226

2:30:02 PM

0.350 MeV

PEAK
Nuclide

0.0000
0.0036 on 12/15/2012
0.0033

1.000E+OOO

Net
Pk Area

5.508
4.558

AREA

REPORT

Pk Area
Error %

2.96
9.66

153 .11
64.35

Ambient
Backgnd

Reagent
Backgnd

FWHM
(keV)

2.04
0.34

O.OOE+OOO
O.OOE+OOO

3.1
3.1

NUCLIDE ANALYSIS RESULTS


Nuclide

Id
Conf.

Energy
(keV)

RA-224
RA-226

0.960
0.935

5685.50*
4785.00*

Activity
(pCi/liter )
1.17E-001 +/- 1.80E-001
3.61E-001 +/- 2.33E-001

MDA
(pCi/liter
3.09E-001 +/- 1.llE-002
1.79E-001 +/- 6.44E-003

&314

0000065458.CNF

Live Time :10200.000 sec


Real Time :10200.000 sec
start:
1:3413.S(kev)

Stop : 1024: 6597. S(kev)

Acq. start :wed Aug 07 16:06:19 2013

60

55

50

45

40

35

Vl

-1-'

s::::

8 30

25

20

15

10

,1,

3500
!l.':i!!ll
( ~

...

jj..01Jll.

';,.il"ll

ii

~ ~i\

J i,!.

ROI Type: 1

4000

4500

5000
Energy(kev)

5500

6000

6500

Channel Data Report

8/8/2013

Page

5:37:05 AM

*******************************************************
s p E CTR AL DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

07

Elapsed Live time:


Elapsed Real Time:

10200
10200

Channell------l-------l-------l-------l-------1-------1-------1-------I
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:

10200
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0

10200
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
1
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
0
0
0
0
1
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
1
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
1
0
0
0

8316

Channel Data Report


369:

8/8/2013
0

Sample Title:

Page

5:37:05 AM
0

07

Channell------l-------l-------l-------l-------1-------1-------1-------I
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:
625:
633:
641:
649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:

0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0

0
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
1
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
1
0
0
0
0
0
0
0

0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
1
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0

0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
1
0
0
1
1
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
1
0
0
0
II?"'
W"'"'i
I

Channel Data Report


801:

8/8/2013
0

Sample Title:

Page

5:37:015 .AM
0

07

Channell------1-------1-------1-------l-------l-------l-------l-------I
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
1
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0

!JJ318

---='pex-Alpha'"

Sample Description:

Spectrum File:

Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

D-81 TOT
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000654
1307149A-RA
08
Shelf 2
Ra

Detector Name:

Alpha_031
Chamber Serial Number:

Detector Serial Number:


31
Env. Background:

System Bkgd 64050


Reagent Blank:

<not performed>
Sample Size:

Generic Mult. Factor:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

Chem. Recovery Factor:

Counting Efficiency:

Effective Efficiency:

1.000E+OOO +/- O.OOOE+OOO liter


2.660E+OOO
Generic Div. Factor:
7/17/2013
1:10:08 PM
8/7/2013
4:06:19 PM
170.0 minutes
170.0 minutes
1.0000 +/0.1418 +/0.1418 +/-

Peak Match Tolerance:

Energy
(MeV)

RA-224
RA-226

3:23:29 PM

0.350 MeV

PEAK

Nuclide

0.0000

0.0034 on 6/13/2013
0.0034

1.000E+OOO

Net
Pk Area

5.468
4.634

AREA

REPORT

Pk Area
Error %

2.32
5.96

149.12
95.01

FWHM
(keV)

Ambient
Backgnd

Reagent
Backgnd

0.68
2.04

O.OOE+OOO
O.OOE+OOO

3.1
3.1

NUCLIDE ANALYSIS RESULTS

Nuclide

Id
Conf.

Energy
(keV)

RA-224
RA-226

0.940
0. 971

5685.50*
4785.00*

Activity
(pCi/liter )
1.22E-001 +/- 1.82E-001
2.96E-001 +/- 2.82E-001

MDA
(pCi/liter
2.97E-001 +/- l.41E-002
3.87E-001 +/- 1.84E-002

0000065457.CNF

Live Time :10200.000 sec


Real Time :10200.000 sec
start:
1: 3388. 9(kev)
stop : 1024:6594.6(kev)
Acq. Start :wed Aug 07 16: 06: 19 2013

60
55
50
45
40
35
Vl
.f-1

s::::
:::s

8 30

25
20
15
10
5

,I ,111,
I

3500

4000

~~
(,,JI

f'IJI
,,~

ROI Type: 1

4500

11,

5000
Energy(kev)

5500

6000

6500

Channel Data Report

8/8/2013

Page

5:37:11 AM

*******************************************************
s p E CTR AL DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

08

Elapsed Live time:


Elapsed Real Time:

10200
10200

Channell------l-------l-------1-------1-------1-------l-------l-------I
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:

10200
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0

10200
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
1
0
1
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
1
0
0
1
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
.fi~M

ii

~.5Li

Channel Data Report


369:

8/8/2013
0

Sample Title:

Page

5:37:11 AM
1

08

Channell------l-------l-------1-------1-------1-------l-------l-------I
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:
625:
633:
641:
649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:

0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0

0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0

0
1
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
1
0
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
1
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

li322

Channel Data Report


801:

8/8/2013
0

Sample Title:

Page

5:37:11 AM
0

08

Channell------l-------l-------l-------1-------1-------1-------l-------I
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0

0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0

Sample Description:

Spectrum File:

Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

D-81 DIS
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000654
1307149A-RA
09
Shelf 2
Ra

Detector Name:

Alpha_033
Chamber Serial Number:

04026479A
Detector Serial Number:
91132
Env. Background:

System Bkgd 64051


Reagent Blank:

<not performed>
Sample Size:

Generic Mult. Factor:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

l.OOOE+OOO +/- O.OOOE+OOO liter


2.610E+OOO
Generic Div. Factor:
7/17/2013
1:10:08 PM
8/7/2013
4:06:44 PM
170.0 minutes
170.0 minutes

Chem. Recovery Factor:

Counting Efficiency:

Effective Efficiency:

1. 0000 +/-

0 .1848 +/0.1848 +/-

Peak Match Tolerance:

Energy
(MeV)

RA-224
RA-226

2:31:30 PM

0.350 MeV

PEAK

Nuclide

0.0000

0.0032 on 7/20/2013
0.0032

l.OOOE+OOO

Net
Pk Area

5.489
4.613

AREA

REPORT

Pk Area
Error %

5.15
22.32

94.34
42.22

Ambient
Backgnd
0.85
0.68

FWHM
(keV)

Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO

3.0
3.0

NUCLIDE ANALYSIS RESULTS

Nuclide
RA-224
RA-226

Id
Conf.

Energy
(keV)

0.951

5685.50*
4785.00*

0. 962

Activity
(pCi/liter )
2.04E-001 +/- l.93E-001
8.35E-001 +/- 3.54E-001

MDA
(pCi/liter
2.37E-001 +/- 8.17E-003
2.llE-001 +/- 7.25E-003

0000065459.CNF

Live Time :10200.000 sec


Real Time :10200.000 sec
start:
1: 3447. 3(kev)
stop : 1024:6496.6(kev)
Acq. start :wed Aug 07 16:06:44 2013

60
55
50
45
40

35
Vl
.f-1

c:

:::::s

8 30

25
20
15
10
5
0

q
I

3500

4000

n::inlll

t"4l

11:..111

ROI Type: 1

4500

I.

'

,I,

'.!

5000
Energy(kev)

'

5500

6000

6500

Channel Data Report

8/8/2013

Page

5:37:18 .AM

*******************************************************
s p E CTR AL DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

09

Elapsed Live time:


Elapsed Real Time:

10200
10200

Channell------l-------l-------l-------l-------l-------1-------1-------1
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
1
0
0
1
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
1
1
1
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
1

1
1
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
1
1
0
0
0
0
0
0
0
0
0
0
1
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
1

83

Channel Data Report


369:

8/8/2013
0

Sample Title:

Page

5:37:18 AM
1

09

Channell------l-------1-------1-------1-------l-------l-------l-------I
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:
625:
633:
641:
649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:

0
0
0
0
1
0
0
0
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2
0
0
0
0
0
0
0
0
0
0
0
1

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
2
0
0
0
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
1
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0

0
0
0
0
0
1
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
1
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1

83

Channel Data Report


801:

8/8/2013
0

Sample Title:

Page

5:37:18 AM
0

09

Channell------l-------l-------1-------1-------1-------l-------l-------I
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
1
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

~~Apex-Alpha'"

Sample Description:

Spectrum File:

Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

PZ-204-SS TOT
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000654
1307149A-RA
10
Shelf 2
Ra

Detector Name:

Alpha_034
Chamber Serial Number:

04026479B
Detector Serial Number:
91136
Env. Background:

System Bkgd 64052


Reagent Blank:

<not performed>
Sample Size:

Generic Mult. Factor:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

1.000E+OOO +/- O.OOOE+OOO liter


2.740E+OOO
Generic Div. Factor:
1:10:08 PM
7/17/2013
4:06:45 PM
8/7/2013
170.0 minutes
170.0 minutes

Chem. Recovery Factor:

Counting Efficiency:

Effective Efficiency:

0.8630 +/0.1856 +/0.1601 +/-

Peak Match Tolerance:

Energy
(MeV)

RA-224
RA-226

5:49:43 PM

0.350 MeV

PEAK

Nuclide

0.0000

0.0032 on 12/16/2012
0.0028

1.000E+OOO

Net
Pk Area

5.556
4.614

8.83
19.32

AREA

REPORT

Pk Area
Error %

Ambient
Backgnd

Reagent
Backgnd

FWHM
(keV)

66.70
45.50

0.17
0.68

O.OOE+OOO
O.OOE+OOO

3.0
3.0

NUCLIDE ANALYSIS RESULTS

Nuclide
RA-224
RA-226

Id
Conf.

Energy
(keV)

0.978

5685.50*
4785.00*

0. 962

Activity
(pCi/liter )
4.24E-001 +/- 2.83E-001
8.76E-001 +/- 4.00E-001

MDA
(pCi/liter
2.00E-001 +/- 6.85E-003
2.56E-001 +/- 8.73E-003

0000065460.CNF

Live Time :10200.000 sec


Real Time :10200.100 sec
start:
1: 3439. l(kev)
Stop : 1024:6479.9(kev)
Acq. Start :wed Aug 07 16:06:45 2013

60
55
50
45
40
35
Vl
.j-.1

8 30
25
20
15
10

5
0

.~ ~ M Al

3500
~

to.JI
tl.~

~ r.

1~f; :~~

~\

11i

ROI Type: 1

4000

4500

5000
Energy(kev)

5500

6000

Channel Data Report

8/8/2013

Page

5:37:24 AM

*******************************************************
s p E C T R A L DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

10

Elapsed Live time:


Elapsed Real Time:

10200

10200

Channell------l-------1-------1-------1-------l-------l-------l-------I
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:

0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
1
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
2
1
1
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
1
0
0
0
0

0
0
0
0
0
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
1
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
1
0
0
0
0
1
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
0
0

0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
1
0
0
0
0
1
0
0
0
0
1
0
0
1
0
0
0
0
0
0
0
0

1
0
0
0
0
0
0
0
1
0
2
0
0
0
0
0
0
0
0
0
1
1
0
2
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
1
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

m331

Channel Data Report


369:

8/8/2013
0

Sample Title:

Page

5:37:24 AM
0

10

Channell------l-------l-------l-------1-------1-------1-------l-------I
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:
625:
633:
641:
649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:

0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
1
0
0
0
0
0
0
0
1
0
0
0
0
1
0
0
0
0
1
0
0
1
0
0
0
0
0
0
0
2
0
0
0
0
0
0
0

0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
1
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2
0
0
0

0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
1
0
0
1
0
0

0
0
0
1
0
1
0
0
0
0
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
1
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
1
0
0
0
0
0
0
1
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0

1
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
1
0
0
0
0
0
0
0
0

~~7~
u;..,..,.:;.

Channel Data Report


801:

8/8/2013
0

Sample Title:

Page

5:37:24 AM
0

10

Channell------l-------l-------l-------1-------1-------1-------l-------I
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
0
0
0
1
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
1
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
0
1
0
0
0
0

1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0

0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
1

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0

5333

Sample Description:

Spectrum File:

Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

PZ-204-SS DIS
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000654
1307149A-RA
11

Shelf 2
Ra

Detector Name:

Alpha_035
Chamber Serial Number:

04026477A
Detector Serial Number:
58771
Env. Background:

System Bkgd 64053


Reagent Blank:

<not performed>
Sample Size:

Generic Mult. Factor:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

Chem. Recovery Factor:

Counting Efficiency:

Effective Efficiency:

l.OOOE+OOO +/- O.OOOE+OOO liter


Generic Div. Factor:
2.530E+OOO
7/17/2013
1:10:08 PM
4:06:39 PM
8/7/2013
170.0 minutes
170.0 minutes
1. 0000 +/-

0 .1826 +/0.1826 +/-

Peak Match Tolerance:

Energy
(MeV)

RA-224
RA-226

5:49:42 PM

0.350 MeV

PEAK

Nuclide

0.0000

0.0032 on 12/16/2012
0.0032

l.OOOE+OOO

Net
Pk Area

5.518
4.675

15.66
15.83

AREA

REPORT

Pk Area
Error %

Ambient
Backgnd

Reagent
Backgnd

FWHM
(keV)

50.15
49.57

0.34
0.17

O.OOE+OOO
O.OOE+OOO

2.9
4.4

NUCLIDE ANALYSIS RESULTS

Nuclide

Id
Conf.

Energy
(keV)

RA-224
RA-226

0.964
0.984

5685.50*
4785.00*

Activity
(pCi/liter )
6.09E-001 +/- 3.06E-001
5.81E-001 +/- 2.89E-001

MDA
(pCi/liter
l.86E-001 +/- 6.38E-003
l.53E-001 +/- 5.25E-003

0000065461.CNF

Live Time :10200.000 sec


Real Time :10200.000 sec
Start:
1:3463.4(kev)
Stop : 1024: 6473. S(keV)
Acq. Start :wed Aug 07 16:06:39 2013

60
55
50
45
40
35
V'l
.j....I

c:

8 30
25
20
15
10

5
i

~\'I\

3500

'li'
(,,Ji
(..,.)

ui

!;

l .~ f, ~ li\I\

!1

MI

P\

ROI Type: 1

4000

4500

5000
Energy(kev)

5500

6000

Channel Data Report

8/8/2013

Page

5:37:31 AM

*******************************************************
s p E CTR AL DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

11

Elapsed Live time:


Elapsed Real Time:

10200

10200

Channell------l-------l-------l-------1-------1-------1-------l-------I
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:

0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
1
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
1
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
1
0
0
0

0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
1
3
0
0
0
0
0
0
0
0
0

!336

Channel Data Report


369:

8/8/2013
0

Sample Title:

Page

5:37:31 AM
0

11

Channell------l-------l-------1-------1-------1-------l-------l-------I
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:
625:
633:
641:
649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:

0
0
1
0
0
0
2
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
0
0
0
0
0
1
0
1
0
0
0

0
0
0
1
0
0
1
0
0
0
0
0
1
0
0
1
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
1
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
1
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
1
1
0
0
1
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0

0
1
0
0
0
1
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
1
0
0
1
0
0
0
0
0
2
0
0
0
0

0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
1
0
0
0
0
0
0

0
0
0
0
0
0
1
0
0
0
0
0
0
0
1
0
0
0
0
0
1
0
0
1
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0

0
0
0
1
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
0
0
0
0
0
0
0
0
0
0
1
0
1
0
0
0

E3

Channel Data Report


801:

8/8/2013
0

Sample Title:

Page

5:37:31 AM
0

11

Channell------l-------l-------1-------1-------1-------l-------l-------I
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0

0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0

0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1338

Sample Description:

Spectrum File:

Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

LR-103 TOT
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000654
1307149A-RA
12
Shelf 2
Ra

Detector Name:

Alpha_036
Chamber Serial Number:

04026477B
Detector Serial Number:
84167
Env. Background:

System Bkgd 64054


Reagent Blank:

<not performed>
Sample Size:

Generic Mult. Factor:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

1.000E+OOO +/- O.OOOE+OOO liter


Generic Div. Factor:
2.910E+OOO
1:10:08 PM
7/17/2013
4:06:41 PM
8/7/2013
170.0 minutes
170.0 minutes

Chem. Recovery Factor:

Counting Efficiency:

Effective Efficiency:

0.9444 +/0.1910 +/0.1804 +/-

Peak Match Tolerance:

Energy
(MeV)

RA-224
RA-226

2:31:37 PM

0.350 MeV

PEAK

Nuclide

0.0000
0.0033 on 7/20/2013
0.0031

1.000E+OOO

Net
Pk Area

5.559
4.583

AREA

REPORT

Pk Area
Error %

3.32
16.64

119. 77
50.29

0.68
1. 36

FWHM
(keV)

Reagent
Backgnd

Ambient
Backgnd

O.OOE+OOO
O.OOE+OOO

3.0
5.9

NUCLIDE ANALYSIS RESULTS

Nuclide

Id
Conf.

Energy
(keV)

RA-224
RA-226

0.979
0.948

5685.50*
4785.00*

Activity
(pCi/liter )
1.50E-001 +/- 1.80E-001
7.llE-001 +/- 3.59E-001

/tY

g{&/r'!J

MDA
(pCi/liter
2.55E-001 +/- 8.72E-003
2.93E-001 +/- 9.99E-003

0000065462.CNF

Live Time :10200.000 sec

Real Time :10200.000 sec

Start:
1:3452.9(kev)

Stop : 1024:6474.2(kev)

Acq. start :wed Aug 07 16:06:41 2013

60
55

50

45

40

..,,

35

.j..J

c:

8 30

25

20

15

10

0
it:'~~
11'.1,,J!

H11;,~~A1~,U
I

3500

4000

ROI Type: 1

4500

5000
Energy(kev)

5500

6000

Channel Data Report

8/8/2013

Page

5:37:38 AM

*******************************************************

s P E C T R A L DAT A R E P 0 R T *****

*****
*******************************************************

Sample Title:

12

Elapsed Live time:


Elapsed Real Time:

10200
10200

Channell------l-------1-------1-------1-------l-------l-------l-------I
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:

0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
1
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
1
0
0
1
0
1
0
0
0
0
0
1
0
0
1
0
0
0
0
0
0
0
0
1
0
0
0
1
0
0
0
0
0
0
0
1
0
0
0
0
0
0
1

0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
1
0
0
0
0
1
0
0

0
0
0
0
0
0
0
1
0
0
0
1
0
0
1
0
0
0
0
0
0
0
2
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
2
0
0

1
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
1
1
1
0
0
0
1
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
1

0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
2
0
0
1
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0

(!341

Channel Data Report


369:

8/8/2013
0

Sample Title:

Page

5:37:38 AM
0

12

Channell------l-------l-------l-------l-------1-------1-------1-------I
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:
625:
633:
641:
649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:

1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0

0
0
0
0
0
1
0
0
0
1
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
1
0
0
0
0

0
0
0
1
0
0
0
1
0
0
0
0
1
1
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
1
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0

0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
2
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
1

!1342

Channel Data Report


801:

8/8/2013
0

Sample Title:

Page

5:37:38 AM
0

12

Channell------l-------l-------l-------1-------1-------1-------l-------I
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

1
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
1
0
0
0
0
0
0
1
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
1
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0

1
0
0
1
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0

~~Apex-Alpha"'

Sample Description:

Spectrum File:

Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

LR-103 DIS
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000654
1307149A-RA
13
Shelf 2
Ra

Detector Name:

Alpha_038
Chamber Serial Number:

04026478B
Detector Serial Number:
91134
Env. Background:

System Bkgd 64055


Reagent Blank:

<not performed>
Sample Size:

Generic Mult. Factor:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

l.OOOE+OOO +/- O.OOOE+OOO liter


2.960E+OOO
Generic Div. Factor:
7/17/2013
1:10:08 PM
8/7/2013
4:06:43 PM
170.0 minutes
170.0 minutes

Chem. Recovery Factor:

Counting Efficiency:

Effective Efficiency:

0.8942 +/0.1722 +/0.1539 +/-

Peak Match Tolerance:

Energy
(MeV}

RA-224
RA-226

5:13:35 PM

0.350 MeV

PEAK

Nuclide

0.0000

0.0030 on 5/11/2013
0.0027

l.OOOE+OOO

Net
Pk Area

5.543
4.608

AREA

REPORT

Pk Area
Error %

10.15
20.64

64.46
44.77

Ambient
Backgnd
0.85
1.36

FWHM
(keV}

Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO

3.0
3.0

NUCLIDE ANALYSIS RESULTS

Nuclide

Id
Conf.

Energy
(keV}

RA-224
RA-226

0.974
0.960

5685.50*
4785.00*

Activity
(pCi/liter }
5.48E-001 +/- 3.53E-001
l.05E+OOO +/- 4.72E-001

MDA
(pCi/liter
3.23E-001 +/- l.llE-002
3.49E-001 +/- l.20E-002

0000065463.CNF

Live Time :10200.000 sec


Real Ti me :10200. 000 sec
Start:
1: 3482. 5(kev)

Stop : 1024:6501.G(kev)

Acq. start :wed Aug 07 16:06:43 2013

60

55

50

45

40

35

Vl
.j-J

c:

8 30

25

20

15

10

0
3500

4000

t:F!Jt
t ,JI
~u;,,

UI\

ROI

Type: 1

4500

5000
Energy(kev)

!\

?. I

!~

5500

6000

6500

Channel Data Report

8/8/2013

Page

5:37:44 AM

*******************************************************
s p E C T R A L DAT A R E P 0 R T *****
*****
*******************************************************
Sample Title:

13

Elapsed Live time:


Elapsed Real Time:

10200
10200

Channell------1-------1-------1-------l-------l-------l-------l-------I
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0

0
0
0
1
0
0
0
0
0
0
2
0
0
0
0
0
0
0
1
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
1
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
1
0
0
0
0
0
0
0
0
1
0
1
0
0
0
1
1
0
0
0

0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0

0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0

0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0

BJ

Channel Data Report


369:

8/8/2013
0

Sample Title:

Page

5:37:44 AM
0

13

Channell------l-------l-------1-------1-------1-------l-------l-------I
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:
625:
633:
641:
649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:

0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
1
0
0
0
0
0
0

0
0
0
0
0
1
1
0
0
0
0
0
0
1
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
1
0
0
0
1
0
1
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
1
0
1
0
0
1
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
1
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

1
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
1
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
1
0
0
0
0
0
1
0
0
0
1
0
0
0
0
0
0
0

6347

Channel Data Report


801:

8/8/2013
0

Sample Title:

Page

5:37:44 AM
0

13

Channell------l-------l-------1-------1-------1-------l-------l-------I
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0

0
0
1
0
0
1
0
1
1
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0

0
0
0
0
1
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0

Sample Description:

Spectrum File:

Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

PZ-111-KS TOT
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000654
1307149A-RA
14
Shelf 2
Ra

Alpha_039
Detector Name:

Chamber Serial Number:

06027396A
Detector Serial Number:
83109
Env. Background:

System Bkgd 64056


Reagent Blank:

<not performed>
l.OOOE+OOO +/- O.OOOE+OOO liter
Generic Div. Factor:
2.530E+OOO
1:10:08 PM
7/17/2013
4:06:47 PM
8/7/2013
170.0 minutes
170.0 minutes

Sample Size:

Generic Mult. Factor:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

Chem. Recovery Factor:

Counting Efficiency:

Effective Efficiency:

1.0000 +/0.1965 +/0.1965 +/-

Peak Match Tolerance:

Energy
(MeV)

RA-224
RA-226

2:01:25 PM

0.350 MeV

PEAK

Nuclide

0.0000

0.0034 on 4/20/2013
0.0034

l.OOOE+OOO

REPORT

Pk Area
Error %

Net
Pk Area

5.573
4.555

AREA

4.66
6.30

94.59
89.57

FWHM
(keV)

Ambient
Backgnd

Reagent
Backgnd

0.34

O.OOE+OOO
O.OOE+OOO

1. 70

3.0
3.0

NUCLIDE ANALYSIS RESULTS

Nuclide

Id
Conf.

Energy
(keV)

RA-224
RA-226

0.984
0.933

5685.50*
4785.00*

Activity
(pCi/liter )
l.68E-001 +/- l.59E-001
2.15E-001 +/- l.93E-001

MDA
(pCi/liter
l.73E-001 +/- 5.88E-003
2.51E-001 +/- 8.51E-003

0000065464.CNF

Live Time :10200.000 sec


Real Time :10200.000 sec
Start:
1: 3449 .?(kev)
stop : 1024: 6497. l(kev)
Acq. start :wed Aug 07 16:06:47 2013

60
55
50
45
40
35
VI
.f-J

c:

::::s

8 30

25
20
15
10

5
0
~
("1JI

U"ll
liil"!lll

!~ f}
I

3500

4000

ROI Type: 1

4500

5000
Energy(kev)

5500

6000

6500

Channel Data Report

8/8/2013

Page

5:37:51 AM

*******************************************************

s P E C T R A L DAT A R E P 0 R T *****

*****
*******************************************************

Sample Title:

14

Elapsed Live time:


Elapsed Real Time:

10200
10200

Channell------l-------l-------l-------l-------1-------1-------1-------I
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0

0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
1
0
0
0
1
0
0
0
0
0
0
0
1
0
0
0
0
0

0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0

9351

Channel Data Report


369:

8/8/2013
0

Sample Title:

Page

5:37:51 .lM
0

14

Channell------l-------l-------l-------1-------1-------1-------l-------I
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:
625:
633:
641:
649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:

0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0

1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0

o
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
1
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
1
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

mJ

Channel Data Report


801:

8/8/2013
0

Sample Title:

Page

5:37:51 AM
0

14

Channell------l-------l-------l-------1-------1-------1-------l-------I
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0

~~Apex-Alpha"'

Sample Description:

Spectrum File:

Batch Identification:

Sample Identification:

Sample Geometry:

Procedure Description:

'-

PZ-111-KS DIS
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000654
1307149A-RA
15
Shelf 2
Ra

Detector Name:

Alpha_040
Chamber Serial Number:

06027396B
Detector Serial Number:
91135
Env. Background:

System Bkgd 64057


Reagent Blank:

<not performed>
Sample Size:

Generic Mult. Factor:

Sample Date/Time:

Acquisition Date/Time:

Acquisition Live Time:

Acquisition Real Time:

Chem. Recovery Factor:

Counting Efficiency:

Effective Efficiency:

1.000E+OOO +/- O.OOOE+OOO liter


Generic Div. Factor:
2.530E+OOO
1:10:08 PM
7/17/2013
4:06:49 PM
8/7/2013
170.0 minutes
170.0 minutes
1.0000 +/0.1900 +/0.1900 +/-

Peak Match Tolerance:

Energy
(MeV)

RA-224
RA-226

5:49:33 PM

0.350 MeV

PEAK

Nuclide

0.0000

0.0033 on 12/16/2012
0.0033

1.000E+OOO

Net
Pk Area

5.535
4.603

AREA

REPORT

Pk Area
Error %

1.15
10.49

249.59
62.21

Ambient
Backgnd
0.85
0.51

FWHM
(keV)

Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO

3.0
0.0

NUCLIDE ANALYSIS RESULTS

Nuclide

Id
Conf.

Energy
(keV)

RA-224
RA-226

0. 971
0.958

5685.50*
4785.00*

Activity
(pCi/liter )
4.30E-002 +/- 1.07E-001
3.70E-001 +/- 2.31E-001

MDA
(pCi/liter
2.24E-001 +/- 7.63E-003
1.85E-001 +/- 6.30E-003

8(811)

0000065465.CNF

Live Time :10200.000 sec


Real Time :10200.000 sec
start:
1:3459 .O(kev)
Stop : 1024:6497.3(kev)
Acq. Start :wed Aug 07 16: 06: 49 2013

60
55

50

45

40

35

Vl

......
c:

::s

8 30

25

20

15

10

3500
I

Cit!'

(,iJ!
u~

U1

ROI Type: 1

j~

i\ ;~Al I,

4000

4500

5000
Energy(kev)

5500

6000

6500

Channel Data Report

8/8/2013

Page

5:37:5S AM

*******************************************************
s P E C T R A L DAT A RE P 0 R T *****
*****
*******************************************************
Sample Title:

15

Elapsed Live time:


Elapsed Real Time:

10200
10200

Channell------l-------1-------1-------1-------l-------l-------l-------I
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:

0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
1
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
1
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
1
0
0

0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
1
0
0
0
1
0
0
0
0
0
0
0
0
0
0

63

Channel Data Report


369:

8/8/2013
1

Sample Title:

Page

5:37:58 AM
0

15

Channell------l-------l-------l-------1-------1-------1-------l-------I
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:
625:
633:
641:
649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:

0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
1

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1

0
0
0
0

0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1

0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
1

0
0
0
0
0
0
0
0
0
0

B3

Channel Data Report


801:

8/8/2013
0

Sample Title:

Page

5:37:58 AM
0

15

Channell------l-------l-------l-------1-------1-------1-------l-------I
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
1
0
1
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0

0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0

0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0

8358

Page 1 of 2
8/7/2013

6:51 :42 AM

~1i'Apex-Alpha ]
QA SUMMARY REPORT

Review Of QA Results - Pulser Check


Date
Time

: 8/7/2013
: 6:51 :42 AM

CHAMBER
Alpha 001
Alpha 002
Alpha 003
Alpha 004
Alpha 005
Alpha 006
Alpha 007
Alpha 008
Alpha 009
Alpha 010
Alpha 011
Alpha 012
Alpha 013
Alpha 014
Alpha 015
Alpha 016
Alpha 017
Alpha 018
Alpha 019
Alpha 020
Alpha 021
Alpha 022
Alpha 023
Alpha 024
Alpha 025
Alpha 026
Alpha 027
Alpha 028
Alpha 029
Alpha 030
Alpha 031
Alpha 032
Alpha 033
Alpha 034
Alpha 035
Alpha 036
Alpha 037
Alpha 038
Alpha 039
Alpha 040
Alpha 041
Alpha 042

DEVICE
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
21f
21f
21f
2lf
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
Alpha Analyst! OODC
Alpha Analyst! OODC
Alpha Analyst! OODC
Alpha AnalystlOODC
Alpha AnalystlOODC
Alpha AnalystlOODC
Alpha AnalystlOODC
Alpha AnalystlOODC
Alpha AnalystlOODC
Alpha Analyst! OODC

PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
Peak Energy
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
PeakFWHM
ALL
ALL
ALL
ALL

FLAG
Not Done
Not Done
Passed
Passed
Not Done
Not Done
Not Done
Not Done
Not Done
Passed
Passed
Passed
Passed
Passed
Action
Not Done
Not Done
Passed
Passed
Passed
Not Done
Passed
Passed
Passed
Passed
Not Done
Passed
Not Done
Passed
Not Done
Passed
Not Done
Passed
Passed
Passed
Passed
Not Done
Action
Passed
Passed
Passed
Passed

DATE

817/2013 5:32:16 AM
817/2013 5:32:17 AM

817/2013
817/2013
817/2013
817/2013
817/2013
817/2013

5:32:18 AM
5:32:18 AM
5:32:19 AM
5:32:20 AM
5:32:21 AM
5:32:22 AM

817/2013 5:32:23 AM
817/2013 5:32:24 AM
8/2/2013 5:14:08 AM
817/2013
817/2013
817/2013
817/2013

5:32:24
5:32:25
5:32:26
5:32:27

AM
AM
AM
AM

817/2013 5:32:28 AM
817/2013 5:32:28 AM
817/2013 5:32:29 AM
817/2013
817/2013
817/2013
817/2013

5:32:30 AM
5:32:32 AM
5:32:33 AM
5:32:35 AM

817/2013
817/2013
817/2013
817/2013
817/2013

5:32:37 AM
5:32:38 AM
5:32:41 AM
5:32:43 AM
5:32:45 AM

Page 2 of 2

Review of QA Results - Pulser Check


8/7/2013

CHAMBER
Alpha 043
Alpha 044
Alpha 045
Alpha 046
Alpha 047
Alpha 048

DEVICE
Alpha Analyst I OODC
Alpha AnalystlOODC
Alpha AnalystlOODC
Alpha AnalystlOODC
Alpha Analyst I OODC
Alpha AnalystlOODC

PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL

FLAG
Not Done
Not Done
Passed
Passed
Passed
Passed

APPROVED BY:

APPROVAL DATE:

'g( 1!17

6:51:42AM

DATE

8/7/2013
8/7/2013
8/7/2013
8/7/2013

5:32:48
5:32:50
5:32:53
5:32:55

AM
AM
AM
AM

6/12/12

Library Listing Report

Page

12:16:17 PM

*************************************************************************
*****
L I B R A R Y L I S T I N G R E P 0 R T
*****
*************************************************************************
Nuclide Library Title:

Radium
Ra-226, Po-218, Rn-222

Nuclide Library Description:


Nuclide
Name

Half-Life
(Seconds}

P0-218
RN-222
RA-226

5.049E+Ol0
5.049E+010
5.049E+010

* =

Energy
Uncert. (keV

Energy
(keV )

0.000
0.000
0.000

6003.000*
5490.000*
4785.000*

Yield
( %)
99.9800
99.9200
100.0000

Yield
Uncert. (Abs. + - )
0.0000

0.0000

0.0000

key line

TOTALS:

Nuclides

Energy Lines

8361

SECTION XI

ANALYTICAL DATA (RADIUM-228)

Eberline Services
Oak Ridge Laboratory
Analysis Sheet

Printed: 811412013 7:01 AM


Page 1of3

13-07149
Ra228
Run 1

Ra228

Analysis Code
Run
Date Received

Internal
Fraction

13-07149

Work Order

Client
ID

Sample I
Desc

01

LCS

02

MBL

7/22/2013

03

Login
CPM

Sample
Date

Sample
Aliquot

07/23/13 00:00

1.0000E+OO

I 07/23/13 00:00

1.0000E+OO

45

07/17/13 10:43

1.0000E+OO

46

07/16/13 15:30

1.0000E+OO

LCS

BLANK

!1

I ---,.-----

DUP

D-81 TOT
----~-

Lab Deadline I

8/13/2013

04

TRG:

05

TRG

West Lake OU-1

06

TRG

07

PZ-302-AS TOT

'

PZ-302-AS DIS

46

07/16/13 15:30

1.0000E+OO

LR-100 TOT

47

07/17/13 10:23

1.0000E+OO

TRG

LR-100 DIS

47

07/17/13 10:23

1.0000E+OO

08

DO

D-81 TOT

45

07/17/13 10:43

1.0000E+OO

09

TRG

D-81 DIS

45

07/17/13 10:43

1.0000E+OO

WA

10

TRG

PZ-204-SS TOT

43

07/17/13 11 :40

1.0000E+OO

E904.0

11

TRG

PZ-204-SS DIS

43

07/17/1311:40

1.0000E+OO

Alpha/Beta GPC

12

TRG

LR-103 TOT

45

07/17/13 12:15

1.0000E+OO

Radiometric Tracer

Ba-133

13

TRG

LR-103 DIS

45

07/17/13 12:15

1.0000E+OO

Radiometric Sol#

Ba-Ga

14

TRG

PZ-111-KS TOT

41

07/17/13 13:09

1.0000E+OO

Tracer Act (dpm/g)

991.12

15

TRG

PZ-111-KS DIS

41

07/17/13 13:09

1.0000E+OO

Carrier

Yttirum

Client I Engineering Management Support, Inc.


Project I
Report Level

Activity Units

pCi

----

Aliquot Units
Matrix
Method
Instrument Type

Carrier Cone (mg/ml)

I
I

34
-

~!Ii

* SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only.
w~.i1

**Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.

Eberline Services
Oak Ridge Laboratory
Analysis Sheet

Printed: 811412013 7:01 AM


Page 2 of 3

13-07149

Ra228
Run 1
Radiometric I Grav Carrier
% Rec
I Added (ml)

I Grav Filter
I
Net (g)

Internal
Fraction

Sample
Desc

01

LCS

0.9174

909.3

404.0

98.641

2.000

0.0901

0.1486

0.0585

86.03

84.86

1.00

1.00

02

MBL

0.9114

903.3

414.1

101.77

2.000

0.0915

0.1477

0.0562

82.65

84.11

1.00

1.00

0.0566

83.24

84.91

1.00

1.00

Tracer
Aliquot(g)

Tracer Total
ACT(dpm)

Radiometric
Tracer (pCi)

Grav Filter
Tare (g)

Grav Filter
Final (g)

Grav
%Rec

Mean
%Rec

SAF

I
I

SAF

--

03

DUP

0.9088

900.7

413.9

102.01

2.000

0.0918

0.1484

04

TRG

0.9069 i

898.8

369.8

91.33

2.000

0.0917t

0.1462

0.0545

80.15

73.20

1.00

1.00

05

TRG

0.9085

900.4

296.5

73.10

2.000

0.0916

0.1486

0.0570

83.82

61.28

1.00

1.00

06

TRG

0.9097

901.6

387.5

95.41

2.000

0.0916

0.1501

0.0585

86.03

82.08

1.00

1.00

07

TRG

0.9089

900.8

369.4

91.03

2.000

0.0915

0.1477

0.0562

82.65

75.24

1.00

1.00

08

DO

0.9075

899.4

425.3

104.97

2.000

0.0916

0.1471

0.0555

81.62

85.68

1.00

1.00

09

TRG

0.9080

899.9

426.5

105.21

2.000

0.0921

0.1473

0.0552

81.18

85.41

1.00

1.00

10

TRG

0.9048

896.8

348.6

86.30

2.000

0.09161

0.1471

0.0555

81.62

70.43

1.00

1.00

11

TRG

0.9036

895.6

411.9

102.10

2.000

0.0913

0.1395

0.0482

70.88

72.37

1.00

1.00

12

TRG

0.9110

902.9

384.1

94.44

2.000

0.0917

0.1464

0.0547

80.44

75.97

1.00

1.00

13

TRG

0.9075

899.4

362.3

89.42

2.000

0.0912

0.1481

0.0569

83.68

74.83

1.00

1.00

14

TRG

0.9057

897.7

410.4

101.50

2.000

0.0915

0.1482

0.0567

83.38

84.63

1.00

1.00

15

TRG

0.9097

901.6

429.9

105.85

2.000

0.0913

0.1471

0.0558

82.06

86.86

1.00

1.00

0
w

* SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only.

**Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.

Eberline Services
Oak Ridge Laboratory
Analysis Sheet

Printed: 811412013 7:01 AM


Page 3 of 3

13-07149

Ra228

Run 1

Internal
Fraction

Sample
Desc

Rough Prep
Date

Rough Prep
By

Prep
Date

Prep
By

Sep tO
Date/Time

Sep tO
By

Sep t1
Date/Time

Sep t1
By

01

I LCS

08/02/13 08:19

JWOLFE

08/06/13 09:40

TSMITH

08/14/13 04:03

TS MITH

02

MBL

08/02/13 08:19

JWOLFE

08/06/13 09:40

TS MITH

08/14/13 04:03

TSMITH

03

DUP

~
05

TRG

08/02/13 08:19

JWOLFE

08/06/13 09:40

TSMITH

08/14/13 04:03

TSMITH

08/14/13 04:03

TSMITH

08/02/13 08:19

JWOLFE

08/06/13 09:40

TSMITH

--

08/02/13 08: 19

JWOLFE

08/06/13 09:40

TSMITH

08/14/13 04:03

TSMITH

--

06

TRG

08/02/13 08:19

JWOLFE

08/06/13 09:40

TSMITH

08/14/13 04:03

TS MITH

07

TRG

08/02/13 08:19

JWOLFE

08/06/13 09:40

TSMITH

08/14/13 04:03

TSMITH

08

DO

08/02/13 08: 19

JWOLFE

08/06/13 09:40

TS MITH

08/14/13 04:03

TS MITH

TRG

08/02/13 08:19

JWOLFE

08/06/13 09:40

TSMITH

08/14/13 04:03

TSMITH

10

TRG

08/02/13 08: 19

JWOLFE

08/06/13 09:40

TS MITH

08/14/13 04:03

TSMITH

11

TRG

08/02/13 08: 19

JWOLFE

08/06/13 09:40

TS MITH

08/14/13 04:03

TSMITH

12

TRG

08/02/13 08: 19

JWOLFE

08/06/13 09:40

TS MITH

08/14/13 04:03

TSMITH

13

TRG

08/02/13 08: 19

JWOLFE

08/06/13 09:40

TSMITH

08/14/13 04:03

TS MITH

14

TRG

08/02/13 08: 19

JWOLFE

08/06/13 09:40

TSMITH

08/14/13 04:03

TSMITH

15

TRG

08/02/13 08:19

JWOLFE

08/06/13 09:40

TSMITH

08/14/13 04:03

TSMITH

~-

09

r--

--

~-

--~-

iilm~

* SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only.

t::ll

** Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.

Eberline Services
Oak Ridge Laboratory

(
t:

~1

~I

~,

Work Order: 13-07149-Ra228-1

Lab
Fraction

Nuclide

Sample
Desc

Client
Identification

Activity
Units

01

RA-228

LCS

LCS

pCi/I

7.81E+OO

8.58E-01

1.09E+OO

02

RA-228

MBL

BLANK

pCi/I

9.52E-01

5.17E-01

9.85E-01

03

RA-228

DUP

D-81 TOT

pCi/I

9.69E-01

5.75E-01

1.12E+OO

Results

89.51

OK

RPO
Flag

MDA
Flag

OK

NA

OK

pCi/I

1.26E+OO

6.43E-01

1.23E+OO

OK

05

RA-228

TRG

PZ-302-AS DIS

pCi/I

1.43E+OO

8.10E-01

1.57E+OO

. OK

cu
0:::

06

RA-228

TRG

LR-100 TOT

pCi/I

-1.70E-01

5.97E-01

1.30E+OO

OK

07

RA-228

TRG

LR-100 DIS

pCi/I

5.12E-01

6.53E-01

1.34E+OO

OK

08

RA-228

DO

D-81 TOT

pCi/I

1.22E+OO

6.26E-01

1.21E+OO

OK

09

RA-228

TRG

D-81 DIS

pCi/I

1.15E+OO

5.93E-01

1.14E+OO

OK

10

RA-228

TRG

PZ-204-SS TOT

pCi/I

1.97E-01

8.04E-01

1.69E+OO

OK

11

RA-228

TRG

PZ-204-SS DIS

pCi/I

1.34E+OO

7.63E-01

1.48E+OO

OK

12

RA-228

TRG

LR-103 TOT

pCi/I

7.25E-01

7.62E-01

1.SSE+OO

OK

13

RA-228

TRG

LR-103 DIS

pCi/I

1.99E+OO

7.43E-01

1.37E+OO

OK

14

RA-228

TRG

PZ-111-KS TOT

pCi/I

5.25E-01

6.27E-01

1.28E+OO

OK

PZ-111-KS DIS

pCUI

5.68E-01

5.67E-01

1.15E+OO

OK

---

::l

15

RA-228

TRG

Cl)

E
Cl)
ns
'
c:
ns

:E
c:
'
;:

-~-~-~----

- -------

Cl)
Cl)

c:
'Ci
c:

---------~-----

--

--

--

---- -

Blank
Flag

OK

PZ-302-AS TOT

.....c:

u~

LCS
Flag

TRG

(/)

(;I~

8.73E+OO

LCS
%R

RA-228

LCS
Known

04

co

c.
c.

~lr~

MDA

~I

Error Estimate

---+~

Printed: 8/14/2013 10:47 AM

Page 1of3

Preliminary Data Report & Analytical Calculations

OK

Printed: 8/14/2013 10:47 AM

Page 2of3

Preliminary Data Report & Analytical Calculations

Eberline Services
Oak Ridge Laboratory

Work Order: 13-07149-Ra228-1

Sample
Aliquot

Radiometric
%Rec

Grav
%Rec

Mean
%Rec

Sep. to
Date/Time

Sep t1
Date/Time

Lab
Fraction

Nuclide

Sample
Desc

Sample
Date

01

RA-228

LCS

07/23/13 00:00

1.00E+OO

98.64

86.03

84.86

1.00

8/6/2013 9:40

8/14/2013 4:03

02

RA-228

MBL

07/23/13 00:00

1.00E+OO

101.77

82.65

84.11

1.00

8/6/2013 9:40

8/14/2013 4:03

RA-228

DUP

07/17/13 10:43

1.00E+OO

102.01

83.24

84.91

1.00

8/6/2013 9:40

8/14/2013 4:03

SAF

a::

03

---
~

0
(.)

.~

~
cu

c:
<t

co

N
N

cu

04

-- ----------

RA-228

TRG

07/16/13 15:30

1.00E+OO

91.33

80.15

73.20

1.00

8/6/2013 9:40

8/14/2013 4:03

RA-228

TRG

07/16/13 15:30

1.00E+OO

73.10

83.82

61.28

1.00

8/6/2013 9:40

8/14/2013 4:03

RA-228

TRG

07/17/13 10:23

1.00E+OO

95.41

86.03

82.08

1.00

8/6/2013 9:40

07

RA-228

TRG

07/17/13 10:23

1.00E+OO

91.03

82.65

75.24

1.00

8/6/2013 9:40

8/14/2013 4:03

8/14/2013 4:03

08

RA-228

DO

07/17/13 10:43

1.00E+OO

104.97

81.62

85.68

1.00

8/6/2013 9:40

8/14/2013 4:03

TRG

07/17/13 10:43

1.00E+OO

105.21

81.18

85.41

1.00

8/6/2013 9:40

8/14/2013 4:03

TRG

07/17/13 11:40

1.00E+OO

86.30

81.62

70.43

1.00

8/6/2013 9:40

8/14/2013 4:03

TRG

07/17/1311:40

1.00E+OO

102.10

70.88

72.37

1.00

8/6/2013 9:40

8/14/2013 4:03

--r---

os4

--

----

06

0::: ~-+

------- -----------------

_1;t
09

I
RA-228

- - - - - - ------

11

RA-228

RA-228

c..i

~
0

Q.
Q.

:::i
(/)

....c:

12

RA-228

TRG

07/17/13 12:15

1.00E+OO

94.44

80.44

75.97

1.00

8/6/2013 9:40

8/14/2013 4:03

13

RA-228

TRG

07/17/13 12:15

1.00E+OO

89.42

83.68

74.83

1.00

8/6/2013 9:40

8/14/2013 4:03

14

RA-228

TRG

07/17/13 13:09

1.00E+OO

101.50

83.38

84.63

1.00

8/6/2013 9:40

8/14/2013 4:03

RA-228

TRG

07/17/13 13:09

1.00E+OO

105.85

82.06

86.86

1.00

8/6/2013 9:40

8/14/2013 4:03

------

15
----

Q)

~I

E
Q)
Cl

cu
cu
:iE

----------

c:

- ----

1----~---

--------

- - - -------------

~'!I~

t ..ii
C~'.I

Eberline Services
Oak Ridge Laboratory

Work Order: 13-07149-Ra228-1

Oesc

Counting
Date/Time

RA-228

LCS

02

RA-228

03

Lab
Fraction

Nuclide

01

Printed: 8/14/2013 10:47 AM

Page 3 of 3

Preliminary Data Report & Analytical Calculations

Sample

Halflife
(days)

Count
Time

Counts

Bkg
CPM

Eff

Detect

Carrier

08/14/13 07:52

L84110R

A1

120

618 1.083333333

0.4776

M8L

08/14/13 07:52

L84110R

A2

120

158 0.833333333

0.4699

RA-228

DUP

08/14/13 07:52

L84110R

A3

120

201 1.166666667

0.4809

04

RA-228

TRG

08/14/13 07:52

L84110R

A4

120

187

0.4732

05

RA-228

TRG

08/14/13 07:52

L84110R

81

120

204 1.166666667

0.4754

06

RA-228

TRG

08/14/13 07:52

L84110R

82

120

156 1.383333333

0.4658

07

RA-228

TRG

08/14/13 07:52

L84110R

83

120

180 1.266666667

0.4713

08

RA-228

DO

08/14/13 07:52

L84110R

84

120

241 1.366666667

0.4773

09

RA-228

TRG

08/14/13 07:52

L84110R

C1

120

211 1.166666667

0.4705

10

RA-228

TRG

08/14/13 07:52

LB4110R

C2

120

222 1.766666667

0.4676

11

RA-228

TRG

08/14/13 07:52

LB4110R

C3

120

235 1.383333333

0.4614

12

RA-228

TRG

08/14/13 07:52

L84110R

C4

120

250

1.75

0.4714

13

RA-228

TRG

08/14/13 07:53

L84110A

A3

120

266 1.316666667

0.4719

14

RA-228

TRG

08/14/13 07:53

LB4110A

02

120

206

1.45

0.4682

RA-228

TRG

08/14/13 07:53

L84110A

04

120

186

1.25

0.4741

-----

i::

8
.~

1ii

co

r---

N
N

""
0:::

---

--

~
0

c..
c..

-------

::s

15

t/)

jl
o.

....c:

~-----

---~---

Ql

E
Ql

Cl
rel

~----

c:

rel

::ill

----

---~-

t--

---------- ---

----------- --

'~

-~-------~----

,.....----

Count Room Report


Client: Engineering Management Su

Printed: 811412013 7:01 AM


Page 1of1

13-07149-Ra228-1 (pCi/I) in WA
Tracer ID: Ba-6a

Internal
Fraction

Sample
Desc

Client
ID

Sample
Date

Sample
Aliquot

01

LCS

LCS

07/23/13 00:00

1.0000

Tracer
Aliquot (g)

0.9174

Tracer
ACT(dpm)

909.2535

Radiometric
Tracer(pCi)

404.0000

Radiometric
%Rec

SAF
1

SAF

98.64

1.00

1.00

-----

02

MBL

BLANK

07/23/13 00:00

1.0000

0.9114

903.3068

414.1000

101.77

1.00

1.00

03

DUP

D-81 TOT

07/17/13 10:43

1.0000

0.9088

900.7299

413.9000

102.01

1.00

1.00

04

TRG

PZ-302-AS TOT

07/16/13 15:30

1.0000

0.9069

898.8467

369.8000

91.33

1.00

1.00

05

TRG

PZ-302-AS DIS

07/16/13 15:30

1.0000

0.9085

900.4325

296.5000

73.10

1.00

1.00

06

TRG

LR-100 TOT

07/17/13 10:23

1.0000

0.9097

901.6219

387.5000

95.41

1.00

1.00

07

TRG

LR-100 DIS

07/17/13 10:23

1.0000

0.9089

900.8290

369.4000

91.03

1.00

1.00

08

DO

D-81 TOT

07/17/13 10:43

1.0000

0.9075

899.4414

425.3000

104.97

1.00

1.00

09

TRG

D-81 DIS

07/17/13 10:43

1.0000

0.9080

899.9370

426.5000

105.21

1.00

1.00

10

TRG

PZ-204-SS TOT

07/17/1311:40

1.0000

0.9048

896.7654

348.6000

86.30

1.00

1.00

11

TRG

PZ-204-SS DIS

07/17/1311:40

1.0000

0.9036

895.5760

411.9000

102.10

1.00

1.00

12

TRG

LR-103 TOT

07/17/13 12:15

1.0000

0.9110

902.9103

384.1000

94.44

1.00

1.00

13

TRG

LR-103 DIS

07/17/13 12:15

1.0000

0.9075

899.4414

362.3000

89.42

1.00

1.00

14

TRG

PZ-111-KS TOT

07/17/13 13:09

1.0000

0.9057

897.6574

410.4000

101.50

1.00

1.00

15

TRG

PZ-111-KS DIS

07/17/13 13:09

1.0000

0.9097

901.6219

429.9000

105.85

1.00

1.00

-~

il:'!l1i

Eberline Services
Oak Ridge Laboratory

---Date

Analysis Code

Ra228
Isotope

Ra-228 I

Sol#

Ra-11

I
I

Activity
dpm/g

37.690

Solution
Date

8/2/2013

Approx
Addition

LCS

MS

:LCSEI.

MSEI

Volume
Used(g)

Volume
Used(g)

Volume
Used(g)

Volume
Used(g)

0.5141

0.530

Activity
dpm/g

Volume
Used(g)

Approx
Addition

fraction

Isotope

Sol#

01

Ba-133

Ba-6a

991.120

8/2/2013

0.9174

1.0200

02

Ba-133

Ba-6a

991.120

8/2/2013

0.9114

1.0200

03

Ba-133

Ba-6a

991.120

8/2/2013

0.9088

1.0200

04

Ba-133

Ba-6a

991.120

8/2/2013

0.9069

1.0200

05

Ba-133

Ba-6a

991.120

8/2/2013

0.9085

1.0200

06

Ba-133

Ba-6a

991.120

8/2/2013

0.9097

1.0200

07

Ba-133

Ba-6a

991.120

8/2/2013

0.9089

1.0200

08

Ba-133

Ba-6a

991.120

8/2/2013

0.9075

1.0200

09

Ba-133

Ba-6a

991.120

8/2/2013

0.9080

1.0200

10

Ba-133

Ba-6a

991.120

8/2/2013

0.9048

1.0200

11

Ba-133

Ba-6a

991.120

8/2/2013

0.9036

1.0200

12

Ba-133

Ba-6a

991.120

8/2/2013

0.9110

1.0200

13

Ba-133

Ba-6a

991.120

8/2/2013

0.9075

1.0200

14

Ba-133

Ba-6a

991.120

8/2/2013

0.9057

1.0200

15

Ba-133

Ba-6a

991.120

8/2/2013

0.9097

1.0200

--

;'~'

l::ll'1
(0

Version 2.0 08/99

Witness Initials

JWOLFE
LCS
Known
pCi

8.73

:
Solution
Date

Technician

8/2/2013 8:18

Tracet:St

t....~

Page 1of1
Printed: 8/2/2013 8:19 AM

Spike and Tracer Worksheet

Error
Estimate

0.445

'MS
Added
pCi

000

M~EI

LCSEI

E"or
Estimate

0.000

Known
pCi

o.ool

Error
Estimate

0.000

Balance Printer Tapes

..

Tracer

Added
pCi

Error
Estimate

0.00

LCS

Matrix Spike

0.000

:_

-.

Eberline Analytical
Oak Ridge Laboratory

Lab
Fraction

Sample

, Engineering Management Support, Inc.

Type

Client ID

01
02
03
04
05
06
07
08
09
10
11
12
13
14
15

LCS
BLANK
D-81 TOT
PZ-302-AS TOT
PZ-302-AS DIS
LR-100 TOT
LR-100 DIS
D-81 TOT
D-81 DIS
-
PZ-204-SS TOT
PZ-204-SS DIS
LR-103 TOT
LR-103 DIS
PZ-111-KS TOT
PZ-111-KS DIS

- -- -

Comnffinfs

~JI

Technician:

Printed: 8/2/2013 8:19 AM


Page 1of1

Aliquot Worksheet

Analysis Code

Rpt Units

Lab Deadline

Technician

Ra228

liters

8/13/2013

JWOLFE

Muffle Data

Dilution Data

- :,::-11 Ratio
: - - PostJPre

No of Dils

LCS t
MBL i

-_ - -

Aliquot

I~~~ I; \ ;_ l
TRG I
TRG I
DO f~
TRG I
TRG
TRG I

Oil Factor

Aliquot Data

Net Equiv

- 11
Aliq

--+-----+

-------------+---------1

---- --1 ------ --l

. \iliDa

-Oate

1-I~t,ii)

Eberline Services - Oak Ridge


Version 1.0 9/1999

Work Order

Analysis

Code

Gravimetric
Carrier

Carrier Cone

Ra228

Yttirum

34.0000

TRetec Engineering Management Support, Inc. Sample

Carrier Data

Fraction

Client ID

Type

Carrier Added
(ml)

01
02
03
04
05
06
07
08
09
10
11
12
13
14
15

LCS
BLANK
DUP
PZ-302-AS TOT
PZ-302-AS DIS
LR-100 TOT
LR-100 DIS
D-81 TOT
D-81 DIS
PZ-204-SS TOT
PZ-204-SS DIS
LR-103 TOT
LR-103 DIS
PZ-111-KS TOT
PZ-111-KS DIS

LCS
MBL
DUP
TRG
TRG
TRG
TRG
DO
TRG
TRG
TRG
TRG
TRG
TRG
TRG

f------

~-

Printed: 8/14/2013 7:00 AM


Page 1 of 1

Gravimetric Worksheet

2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000

0.0901
0.0915
0.0918
0.0917
0.0916
0.0916
0.0915
0.0916
0.0921
0.0916
0.0913
0.0917
0.0912
0.0915
0.0913

Gravimetric
Filter Ne~

Filter Final
(g)

o.1486
0.1477
0.1484
0.1462
0.1486
0.1501
0.1477
0.1471
0.1473
0.1471
0.1395
0.1464
0.1481
0.1482
0.1471

(gl.

,,

0.05$2 :

o.o5s6

ctos4.$;

- '(t0$7()
0.0585
.
0.0562
~.0555
... - 0.055~

.. .

O~SPP

: o.Q482

.,

0~054'7

d~0569

..

o.o5a1
-

.:::

0.0558
-

:
-

.:: .

--.

'
-:

!ltm11fll1

~~~

Technician-. _ _ _ _ _
-6//1"
___::__ _ __

Date:

__1 I '1

i)

%
Recovery

'

-~0585

~-

f-

c:lJi~I

TSMITH

Filter Data
Filter Tare
(g)

...--

t,r,Ji
"".Ji

Technician

_:

.
.

86.03
82.65
83.24
80.15
83.82
86.03
82.65
81.62
81.18
81.62
70.88
80.44
83.68
83.38
82.06

C
Sheet1

~/l'ttc

c;e

Detector ID Sample ID Alpha Beta Count Time Voltage


TOD
A3
1307149-13 16
266
120
1400 8/14/13 9:53
D2
1307149-14 10
206
120
1400 8/14/13 9:53
D4
1307149-15 15
186
120
1400 8/14/13 9:53

VJ
...J

>

Page 1

Sheet1

Flt~}

<If)

Detector ID Sample ID Alpha Beta Count Time Voltage


TOD
C1
1307149-09 11
211
120
1400 8/14/13 9:52
C2
1307149-10
9
222
120
1400 8/14/13 9:52
C3
1307149-11
17
235
120
1400 8/14/13 9:52
C4
1307149-12
7
250
120
1400 8/14/13 9:52
A1
1307149-01
18
618
120
1400 8/14/13 9:52
A2
1307149-02 17
158
120
1400 8/14/13 9:52
A3
1307149-03
8
201
120
1400 8/14/13 9:52
A4
1307149-04 13
187
120
1400 8/14/13 9:52
81
1307149-05
9
204
120
1400 8/14/13 9:52
82
1307149-06 10
156
120
1400 8/14/13 9:52
83
1307149-07 11
180
120
1400 8/14/13 9:52
84
1307149-08
6
241
120
1400 8/14/13 9:52

iwi~

Page 1

Eberline Analytical
Oak Ridge Laboratory

Printed: 8/14/2013 6:53 AM

Page 1of1

GPC Detector Report


(ALL Backgrounds)

('___
Detector

Alpha/Beta

Calibration Date

Count Date

Bkg CPM

PFW

LCL

Mean

UCL

LB4110A - Al

Alpha

11/18/2007

8/14/2013

5.00E-02

-2.13E+Ol

2.82E-01

2.19E+Ol

LB4110A - A2

Alpha

11/18/2007

8/14/2013

8.33E-02

-1.81E+Ol

2.54E-01

1.86E+Ol

LB4110A - A3

Alpha

11/18/2007

8/14/2013

1.00E-01

-1.76E+Ol

2.16E-01

l.80E+Ol

LB4110A - A4

Alpha

11/18/2007

8/14/2013

6.67E-02

-1.87E+Ol

2.36E-01

1.92E+Ol

LB4110A - Bl

Alpha

11/18/2007

8/14/2013

8.33E-02

-9.68E-02

7.51E-02

2.47E-01

LB4110A - B2

Alpha

11/18/2007

8/14/2013

6.67E-02

-7.81E-02

7.22E-02

2.22E-01

LB4110A - B3

Alpha

11/18/2007

8/14/2013

6.67E-02

-6.29E-02

5.34E-02

1. 70E-01

LB4110A - B4

Alpha

11/18/2007

8/14/2013

1.67E-02

-1.40E-01

7.88E-02

2.98E-01

LB4110A - Cl

Alpha

11/18/2007

8/14/2013

5.00E-02

-l.49E-01

8.86E-02

3.26E-01

LB4110A - C2

Alpha

11/18/2007

8/14/2013

8.33E-02

-1.77E-01

8.67E-02

3.50E-01

LB4110A - C3

Alpha

11/18/2007

8/14/2013

1.00E-01

-1. 72E-01

1.00E-01

3.72E-01
1.99E-01

LB4110A - C4

Alpha

11/18/2007

8/14/2013

1.33E-01

-6.27E-02

6.83E-02

LB4110A - Dl

Alpha

11/18/2007

8/14/2013

1.67E-02

-5.36E-02

8.33E-02

2.20E-01

LB4110A - D2

Alpha

11/18/2007

8/14/2013

5.00E-02

-6.98E-02

6.06E-02

1.91E-01

LB4110A - D3

Alpha

11/18/2007

8/14/2013

6.67E-02

-4.85E-02

7.07E-02

1.90E-01

LB4110A - D4

Alpha

11/18/2007

8/14/2013

6.67E-02

-5.72E-02

7.03E-02

1.98E-01

LB4110R - Al

Alpha

11/24/2006

8/14/2013

5.00E-02

-9.81E-02

1.0lE-01

3.00E-01

LB4110R - A2

Alpha

11/24/2006

8/14/2013

3.33E-02

-8.92E-02

7.63E-02

2.42E-01

LB4110R - A3

Alpha

11/24/2006

8/14/2013

8.33E-02

-7.32E-02

7.73E-02

2.28E-01

LB4110R - A4

Alpha

11/24/2006

8/14/2013

1. l 7E-01

-5.27E-02

7.09E-02

1.94E-01

LB4110R - Bl

Alpha

11/24/2006

8/14/2013

5.00E-02

-9.41E-02

6.16E-02

2.17E-01

5.00E-02

-6.94E-02

6.33E-02

1.96E-01

LB4110R - B2

C~lll

Alpha

11/24/2006

8/14/2013

LB4110R - B3

Alpha

11/24/2006

8/14/2013

6.67E-02

-6.49E-02

6.99E-02

2.05E-01

LB4110R - B4

Alpha

11/24/2006

8/14/2013

6.67E-02

-6.38E-02

7.02E-02

2.04E-01

LB4110R - Cl

Alpha

11/24/2006

8/14/2013

6.67E-02

-7.67E-02

7.36E-02

2.24E-01

LB4110R - C2

Alpha

11/24/2006

8/14/2013

6.67E-02

-7.54E-02

7.lOE-02

2.17E-01

LB4110R - C3

Alpha

11/24/2006

8/14/2013

1.67E-02

-8.79E-02

8.43E-02

2.57E-01

LB4110R - C4

Alpha

11/24/2006

8/14/2013

6.67E-02

-6.18E-02

8.12E-02

2.24E-Ol

LB4110R - Dl

Alpha

11/24/2006

8/14/2013

O.OOE+OO

-1.03E-Ol

7.0lE-02

2.43E-01

LB4110R - D2

Alpha

11/24/2006

8/14/2013

O.OOE+OO

-7.79E-02

6.96E-02

2.17E-Ol

LB4110R - D3

Alpha

11/24/2006

8/14/2013

O.OOE+OO

-8.29E-02

6.93E-02

2.22E-01

-7.53E-02

7.41E-02

2.23E-Ol

-1.56E-02

9.58E-02

2.07E-01

LB4110R - D4

Alpha

11/24/2006

8/14/2013

O.OOE+OO

LB5100 - 1

Alpha

7/10/2006

10/26/2007

5.00E-02

fJt/lf/;L-

Eberline Analytical
Oak Ridge Laboratory

Detector

Alpha/Beta

Calibration Date

Count Date

Bkg CPM

PFW

LCL

Mean

UCL

Beta

11/18/2007

8/14/2013

8.53E+OO

-2.89E+02

7.63E+OO

3.04E+02

LB4110A - A2

Beta

11/18/2007

8/14/2013

3.42E+OO

-3.03E+Ol

2.59E+OO

3.55E+Ol

LB4110A - A3

Beta

11/18/2007

8/14/2013

1.32E+OO.

-5.0lE+Ol

2.63E+OO

5.54E+Ol

LB4110A - A4

Beta

11/18/2007

8/14/2013

7.37E+OO

-3.24E+Ol

3.22E+OO

3.88E+Ol

LB4110A - Bl

Beta

11/18/2007

8/14/2013

1.37E+OO

-1.04E+01

3.23E+OO

1.68E+Ol

1.07E+OO

-7.62E+OO

2.00E+OO

1.16E+Ol

Beta

11/18/2007

8/14/2013

LB4110A - B3

Beta

11/18/2007

8/14/2013

1.25E+OO

1.16E-01

1.36E+OO

2.60E+OO

LB4110A - B4

Beta

11/18/2007

8/14/2013

1.02E+OO

-7.61E+OO

1.97E+OO

1.16E+Ol

LB4110A - Cl

Beta

11/18/2007

8/14/2013

1.30E+OO

-5.38E+OO

2.12E+OO

9.62E+OO
2.15E+OO

LB4110A - C2

Beta

11/18/2007

8/14/2013

1.25E+OO

3.81E-01

1.27E+OO

LB4110A - C3

Beta

11/18/2007

8/14/2013

1.55E+OO

4.72E-01

l.46E+OO

2.45E+OO

LB4110A - C4

Beta

11/18/2007

8/14/2013

1.47E+OO

-1.75E+OO

2.lOE+OO

5.95E+OO

LB4110A - Dl

Beta

11/18/2007

8/14/2013

2.17E+OO

-2.31E+OO

2.56E+OO

7.43E+OO

LB4110A - D2

Beta

11/18/2007

8/14/2013

l.45E+OO.

-6.40E-01

1.56E+OO

3.76E+OO

LB4110A - D3

Beta

11/18/2007

8/14/2013

4.92E+OO

1.29E+OO

4.48E+OO

7.66E+OO

1.25E+OO

-4.23E-01

1.37E+OO

3.16E+OO

LB4110A - D4

~t~

LB4110A - Al

LB4110A - B2

t ~

Printed: 8/14/2013 6:53 AM

Page 1of1

GPC Detector Report


(ALL Backgrounds)

Beta

11/18/2007

8/14/2013

LB4110R - Al

Beta

11/24/2006

8/14/2013

1.08E+OO.

-6.08E+01

3.66E+OO

6.81E+Ol

LB4110R - A2

Beta

11/24/2006

8/14/2013

8.33E-01

-4.83E+Ol

2.0lE+OO

5.23E+Ol

LB4110R - A3

Beta

8/14/2013

1.17E+OO

-4.47E+Ol

2.73E+OO

5.02E+01

11/24/2006

LB4110R - A4

Beta

11/24/2006

8/14/2013

1.00E+OO.

-4.46E+Ol

1.99E+OO

4.86E+Ol

LB4110R - Bl

Beta

11/24/2006

8/14/2013

1.17E+OO

-4.69E+Ol

2.02E+OO

5.lOE+Ol

LB4110R - B2

Beta

11/24/2006

8/14/2013

1.38E+oo.

-4.69E+Ol

2.05E+OO

5.lOE+Ol
5.20E+Ol

LB4110R - B3

Beta

11/24/2006

8/14/2013

1.27E+OO.

-4.67E+Ol

2.65E+OO

LB4110R - B4

Beta

11/24/2006

8/14/2013

1.37E+OO

-4.70E+01

1.92E+OO

5.09E+Ol

LB4110R - Cl

Beta

11/24/2006

8/14/2013

1.17E+OO

-4.68E+Ol

2.96E+OO

5.27E+Ol

LB4110R - C2

Beta

11/24/2006

8/14/2013

1.77E+oo.

-4.68E+Ol

2.71E+OO

5.22E+Ol

LB4110R - C3

Beta

11/24/2006

8/14/2013

l.38E+OO

-4.72E+Ol

2.52E+OO

5.23E+Ol

LB4110R - C4

Beta

11/24/2006

8/14/2013

1.75E+OO.

-5.33E+Ol

2.95E+OO

5.92E+Ol

LB4110R - Dl

Beta

11/24/2006

8/14/2013

O.OOE+OO

-4.44E+01

5.55E+OO

5.55E+Ol

LB4110R - D2

Beta

11/24/2006

8/14/2013

O.OOE+OO

-4.77E+Ol

1.87E+OO

5.15E+Ol

LB4110R - D3

Beta

11/24/2006

8/14/2013

O.OOE+OO

-5.llE+Ol

5.52E+OO

6.22E+Ol

LB4110R - D4

Beta

11/24/2006

8/14/2013

O.OOE+OO

-4.74E+Ol

2.23E+OO

5.19E+Ol

LB5100 - 1

Beta

7/10/2006

10/26/2007

4.52E+OO

-3.19E-01

1.58E+OO

3.48E+OO

~I f'1t1-

Eberline Analytical
Oak Ridge Laboratory

~~
11:.,,,,Ji

.....~
U'!

Printed: 8/14/2013 6:53 AM

Page 1 of 1

GPC Detector Report


(ALL Efficiencies)
Detector

Alpha/Beta

Calibration Date

Count Date

Eff

PFW

LCL

Mean

UCL

LB4110A - Al

Alpha

11/18/2007

8/14/2013

0.2512

-0.0128

0.2159

0.4446

LB4110A - A2

Alpha

11/18/2007

8/14/2013

0.1976

-0.0503

0.1741

0.3986

0.2062

-0.0736

0.1634

0.4004

-0.0521

0.1821

0.4162

LB4110A - A3

Alpha

LB4110A - A4

Alpha

11/18/2007

8/14/2013

0.2163

LB4110A - Bl

Alpha

11/18/2007

8/14/2013

0.2161

0.1943

0.2243

0.2543

LB4110A - B2

Alpha

11/18/2007

8/14/2013

0.2080

0.1923

0.2213

0.2502

11/18/2007

8/14/2013

LB4110A - B3

Alpha

11/18/2007

8/14/2013

0.2305

0.1279

0.2323

0.3366

LB4110A - B4

Alpha

11/18/2007

8/14/2013

0.2253

0.2088

0.2364

0.2639

LB4110A - Cl

Alpha

11/18/2007

8/14/2013

0.2185

0.1976

0.2207

0.2439

8/14/2013

0.2271

0.1971

0.2252

0.2532

0.2234

0.2494

0.2755

LB4110A - C2

Alpha

LB4110A - C3

Alpha

11/18/2007

8/14/2013

0.2512

LB4110A - C4

Alpha

11/18/2007

8/14/2013

0.2224

0.1969

0.2256

0.2544

8/14/2013

0.2246

0.2028

0.2328

0.2628

0.2277

0.2580

0.2884

0.2634

0.2958

11/18/2007

LB4110A - Dl

Alpha

LB4110A - D2

Alpha

11/18/2007

8/14/2013

0.2532

LB4110A - D3

Alpha

11/18/2007

8/14/2013

0.2557

0.2309

11/18/2007

LB4110A - D4

Alpha

11/18/2007

8/14/2013

0.1884

0.1642

0.1992

0.2342

LB4110R - Al

Alpha

11/24/2006

8/14/2013

0.2327

0.1983

0.2385

0.2786

LB4110R - A2

Alpha

11/24/2006

8/14/2013

0.2088

0.1851

0.2201

0.2551

0.2141

0.1924

0.2243

0.2563

0.2118

0.2453

0.2789

LB4110R - A3

Alpha

LB4110R - A4

Alpha

11/24/2006

8/14/2013

0.2384

LB4110R - Bl

Alpha

11/24/2006

8/14/2013

0.2190

0.1832

0.2257

0.2681

LB4110R - B2

Alpha

11/24/2006

8/14/2013

0.2072

0.1754

0.2169

0.2585

11/24/2006

8/14/2013

LB4110R - B3

Alpha

11/24/2006

8/14/2013

0.2453

0.2015

0.2438

0.2861

LB4110R - B4

Alpha

11/24/2006

8/14/2013

0.2154

0.1882

0.2312

0.2742

LB4110R - Cl

Alpha

11/24/2006

8/14/2013

0.2126

0.1833

0.2150

0.2466

LB4110R - C2

Alpha

11/24/2006

8/14/2013

0.2208

0.1932

0.2245

0.2558

LB4110R - C3

Alpha

11/24/2006

8/14/2013

0.2345

0.2034

0.2394

0.2754

LB4110R - C4

Alpha

11/24/2006

8/14/2013

0.2093

0.1826

0.2222

0.2618

LB4110R - Dl

Alpha

11/24/2006

8/14/2013

0.0000

0.0035

0.1992

0.3949

LB4110R - D2

Alpha

11/24/2006

8/14/2013

0.0000

0.0047

0.2265

0.4484

LB4110R - D3

Alpha

11/24/2006

8/14/2013

0.0000

0.0046

0.2225

0.4404

LB4110R - D4

Alpha

11/24/2006

8/14/2013

0.0000

0.0023

0.1793

0.3564

LB5100 - 1

Alpha

7/10/2006

10/26/2007

0.3368

F
p

0.3332

0.3455

0.3578

~ f(Cfl'--'

Eberline Analytical
Oak Ridge Laboratory

~t~
ui.~ti~

~::lr~

c__

Detector

Alpha/Beta

Calibration Date

Count Date

Eff

LB4110A - Al

Beta

11/18/2007

8/14/2013

PFW

LCL

Mean

UCL

0.5501

0.2112

0.5625

0.9138

0.1621

0.4648

0.7676

LB4110A - A2

Beta

11/18/2007

8/14/2013

0.4861

LB4110A - A3

Beta

11/18/2007

8/14/2013

0.4623

0.0901

0.4572

0.8243

LB4110A - A4

Beta

11/18/2007

8/14/2013

0.5187

0.1429

0.4892

0.8355

LB4110A - Bl

Beta

11/18/2007

8/14/2013

0.5074

0.4634

0.5297

0.5961

LB4110A - B2

Beta

11/18/2007

8/14/2013

0.5085

0.4632

0.5268

0.5904

LB4110A - B3

Beta

11/18/2007

8/14/2013

0.5253

0.3169

0.5314

0.7459

LB4110A - B4

Beta

11/18/2007

8/14/2013

0.5471

0.4918

0.5538

0.6158

LB4110A - Cl

Beta

11/18/2007

8/14/2013

0.5013

0.4511

0.5026

0.5542

LB4110A - C2

Beta

11/18/2007

8/14/2013

0.4973

0.4293

0.5010

0.5728

LB4110A - C3

Beta

11/18/2007

8/14/2013

0.6105

0.5291

0.5907

0.6523

LB4110A - C4

Beta

11/18/2007

8/14/2013

0.5262

0.4578

0.5248

0.5918

LB4110A - Dl

Beta

11/18/2007

8/14/2013

0.5361

0.4784

0.5530

0.6275

LB4110A - D2

Beta

11/18/2007

8/14/2013

0.5635

0.4887

0.5871

0.6855

LB4110A - 03

Beta

11/18/2007

8/14/2013

0.6122

0.5374

0.6149

0.6924

LB4110A - D4

Beta

11/18/2007

8/14/2013

0.4431

0.3845

0.4719

0.5592

LB4110R - Al

Beta

11/24/2006

8/14/2013

0.5579

0.4743

0.5672

0.6601

0.5014

0.4158

0.5085

0.6013

0.4503

0.5384

0.6264

LB4110R - A2

Beta

LB4110R - A3

Beta

11/24/2006

8/14/2013

0.5143

LB4110R - A4

Beta

11/24/2006

8/14/2013

0.5879

0.5032

0.5914

0.6797

0.5302

0.4463

0.5422

0.6380

0.4247

0.5195

0.6144

LB4110R - Bl

;,;Ji

Printed: 8/14/2013 6:53 AM

Page 1 of 1

GPC Detector Report


(ALL Efficiencies)

Beta

11/24/2006

11/24/2006

8/14/2013

8/14/2013

LB4110R - B2

Beta

11/24/2006

8/14/2013

0.5048

LB4110R - B3

Beta

11/24/2006

8/14/2013

0.6049

0.4939

0.5917

0.6895

LB4110R - B4

Beta

11/24/2006

8/14/2013

0.5211

0.4540

0.5489

0.6438

LB4110R - Cl

Beta

11/24/2006

8/14/2013

0.4606

0.4159

0.5015

0.5871

LB4110R - C2

Beta

11/24/2006

8/14/2013

0.5183

0.4440

0.5283

0.6126

LB4110R - C3

Beta

11/24/2006

8/14/2013

0.5685

0.4755

0.5706

0.6656

LB4110R - C4

Beta

11/24/2006

8/14/2013

0.4916

0.4258

0.5249

0.6241

LB4110R - Dl

Beta

11/24/2006

8/14/2013

0.0000

0.0076

0.4763

0.9450

LB4110R - 02

Beta

11/24/2006

8/14/2013

0.0000

0.0092

0.5352

1.0613

LB4110R - 03

Beta

11/24/2006

8/14/2013

0.0000

0.0089

0.5198

1.0308

LB4110R - 04

Beta

11/24/2006

8/14/2013

0.0000

0.0044

0.4279

0.8514

LB5100 - 1

Beta

7/10/2006

10/26/2007

0.4428

0.4555

0.4731

0.4906

fJ' tv\.,..

SECTION XII

BARIUM-133 ANALYTICAL TRACER DATA

0-
VAX/VMS Peak Search Report Generated
Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level

8(1'/l:J

DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP_130714901 GE2 BAFIL 194399.CN


PEAK Vl6.9 PEAKEFF V2.2
SPIKE
7-AUG-2013 00:00:00.
1307149-01
FILTER
GE2
0 00:15:00.00
25
3.00000
No

Pk It

Energy

Area

Bkgnd

1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31

28.25
30.98
35.05
52.18
61.76
65.83
77.17
81.10
93.19
111.82
115.92
162.03
185.80
238.59
276.83
295.50
302.86
307.32
317.94
333.82
337.94
356.03
378.29
383.76
386.99
391.06
437.17
468.07
511. 26
860.92
911. 57

52
2033
515
70
184
114
18
799
26
200
29
30
21
54
64
12
116
24
13
72
20
529
10
140
215
51
94
19
32
7
9

166
115
113
74
50
55
50
52
83
60
62
89
108
36
26
21
49
19
11
16
13
18
16
25
18
19
11
7
6
2
0

3
3
3
0
1
1
2
2
0
1
1
0
0
0
0
3
3
0
0
1
1
0
0
1
1
1
0
0
0
0
0

7-AUG-2013 07:46:15.77

Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian

FWHM Channel
1.66
1.37
1.68
1. 54
1.46
1.47
1. 64
1. 45
2.65
1. 55
1. 56
3.16
1.98
1. 48
2.00
2.15
1. 53
1. 31
2.89
1. 81
1. 82
1.51
3.07
1. 86
1.71
1. 86
1. 81
1. 80
5.04
1.47
2.06

28.36
31.09
35.17
52.29
61. 87
65.95
77.28
81.21
93.30
111.93
116.04
162.14
185.91
238.70
276.94
295.61
302.97
307.42
318.05
333.93
338.05
356.14
378.40
383.87
387.10
391.17
437.28
468.18
511. 36
861. 02
911.67

Left

Pw

26
26
26
49
57
57
76
76
90
107
107
158
182
235
273
292
292
306
315
330
330
351
375
380
380
380
433
464
505
858
909

15
15
15
7
13
13
11
11
7
15
15
9
9
9
7
15
15
5
7
12
12
10
6
15
15
15
9
7
12
6
6

7-AUG-2013 07:30:54.
1.00000E+OO filter
0
BAFIL
0 00:15:00.31 0.0%
4096
10.00000
Cts/Sec %Err

5.80E-02
2.26E+OO
5.73E-01
7.77E-02
2.05E-01
1.27E-01
2.05E-02
8.87E-01
2.89E-02
2.23E-01
3.24E-02
3.30E-02
2.28E-02
6.00E-02
7.08E-02
1.29E-02
1.29E-01
2.67E-02
1.45E-02
7.99E-02
2.20E-02
5.88E-01
1.15E-02
1.55E-01
2.39E-01
5.71E-02
l.04E-01
2.13E-02
3.56E-02
7.28E-03
1. OOE-02

46.5
2.3
5.6
23.6
9.5
13.3
54.1
3.8
61. 5
9.2
43.4
60.4
93.9
24.2
18.3
90.4
12.0
34.3
49.9
14.4
41. 3
4.6
67.6
10.2
7.3
21. 7
12.2
32.3
23.4
56.0
33.3

Fit
1.llE+Ol

2.21E+OO
2.41E+OO
2.43E+OO

4.72E+OO

7.69E-01

2.39E+Ol

Summary of Nuclide Activity


Sample ID : 1307149-01

Acquisition date

Total number of lines in spectrum


Number of unidentified lines
Number of lines tentatively identified by NID

31
27
4

Page :
2
7-AUG-2013 07:30:54

12.90%

Nuclide Type : FISSION


Nuclide
BA-133

Hlife
10.SOY

Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
4.040E+02

Total Activity

---------

4.040E+02

Wtd Mean
Decay Corr
pCi/filter
4.040E+02

Decay Corr
2-Sigma
2-Sigma Error %Error Flags
0.769E+02
19.03

---------

4.040E+02

Nuclide Type : NATURAL


Nuclide
Hlif e
TH-234 4.47E+09Y

Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
6.326E+02

Total Activity
Grand Total Activity :
Flags: "K"
"E"

=
=

---------

Wtd Mean
Decay Corr
pCi/filter
6.326E+02

---------

6.326E+02

6.326E+02

l.037E+03

1.037E+03

Keyline not found


Manually edited

Decay Corr
2-Sigma
2-Sigma Error %Error Flags
1.340E+02
21.18

"M"
"A"

Manually accepted
Nuclide specific abn. limit

Nuclide Line Activity Report


Sample ID : 1307149-01

Acquisition date

Page :
3
7-AUG-2013 07:30:54

Nuclide Type: FISSION


Nuclide
BA-133

Energy
81.00
302.84
356.01

%Abn
33.00*
17.80
60.00

Final Mean for

Uncorrected Decay Corr 2-Sigma


%Ef f
pCi/filter pCi/filter %Error
4.040E+02 19.03
1. 799E+Ol
4.040E+02
2.589E+02 38.36
7.560E+OO 2.589E+02
7.170E+OO 3.695E+02
3.696E+02 17.71

3 Valid Peaks

Status
OK
OK
OK

4.040E+02+/- 7.689E+Ol ( 19.03%)

Nuclide Type: NATURAL


Nuclide
TH-234

Energy
63.29

%Abn
3.80*

Final Mean for


Flag:

11

* 11

Keyline

Uncorrected Decay Corr 2-Sigma


%Eff
pCi/filter pCi/filter %Error
2.305E+Ol 6.326E+02
6.326E+02 21.18

1 Valid Peaks

Status
OK

6.326E+02+/- 1.340E+02 ( 21.18%)

Combined Activity-MDA Report


Sample ID : 1307149-01
- - - -

Acquisition date

Page :
4
7-AUG-2013 07:30:54

Identified Nuclides

Nuclide
BA-133
TH-234

Activity
(pCi/filter)

Act error

MDA

(pCi/filter)

MDA error

Act/MDA

4.040E+02
6.326E+02

7.689E+Ol
1.340E+02

1.867E+Ol

1.443E+02

3.179E+OO
1.192E+Ol

21. 643
4.385

Act error

MDA

(pCi/ filter)

MDA error

Act/MDA

6.561E+OO
l.195E+02
3.886E+OO
l.806E+OO
3.277E+Ol
1.036E+Ol

9.788E+OO
1.727E+02
7.674E+OO
3.201E+OO
5.038E+Ol
1.902E+Ol

l.503E+OO
l.983E+Ol
1.461E-01
6.602E-02
5.688E+OO
1.472E+OO

-0.391
0.018
2.696
0.791
0.263
1.070

Non-Identified Nuclides

Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241

Key-Line
Activity K.L.
(pCi/filter)Ided
-3.827E+OO
3.114E+OO
2.069E+Ol
2.531E+OO
1.327E+Ol
2.035E+Ol

VAX/VMS Peak Search Report Generated


Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level

Bt11~

DK,A.100: [GA,MMA.SCUSR.ARCHIVE]SMP_130714902 GE2 BAFIL 194401. CN


PEAK Vl6.9 PEAKEFF V2.2
BLAWK
7-AUG-2013 00:00:00.
1307149-02
FILTER
GE2
0 00:15:00.00
25
3.00000
No

Pk It

Energy

Area

Bkgnd

1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28

30.93
35.20
52.28
61. 92
65.92
81. 02
83.89
92.50
111.92
116.02
160.66
185.07
239.86
277.00
302.88
307.05
333.86
338.44
356.12
383.83
386.86
391.35
414.72
418.07
437.30
467.92
510.56
526.73

2118
513
61
253
111
818
18
42
193
39
17
37
14
59
150
21
88
23
546
127
154
48
60
25
81
20
32
6

103
93
100
65
69
54
43
102
70
50
97
54
43
52
18
24
15
16
54
31
46
16
10
8
16
6
7
0

3
3
0
5
5
1
1
0
1
1
0
0
0
0
1
1
3
3
0
4
4
0
1
1
0
0
0
0

7-AUG-2013 08:09:45.44

Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian

FWHM Channel
1.43
1. 51
1.79
1. 72
2.15
1. 50
1.37
1. 78
1. 55
1. 56
1.42
1. 39
1.45
1. 82
1.46
1. 79
1. 70
2.20
1. 37
2.05
1.49
1. 70
1. 88
1. 89
1. 69
1. 33
3.73
1. 98

31. 04
35.32
52.40
62.03
66.04
81.14
84.00
92.61
112.03
116.14
160.77
185.18
239.97
277.11
302.99
307.16
333.96
338.55
356.23
383.94
386.97
391.45
414.83
418.17
437.40
468.03
510.67
526.83

7-AUG-2013 07:54:29.
1.00000E+OO filter
0
BAFIL
0 00:15:00.30 0.0%
4096
10.00000

Left

Pw

Cts/Sec %Err

26
26
49
58
58
77
77
88
108
108
158
182
235
272
299
299
328
328
352
380
380
390
411
411
433
465
506
524

15
15
8
16
16
11
11
10
15
15
9
6
7
11
12
12
18
18
8
10
10
6
14
14
9
6
12
6

2.35E+OO 2.3
5.70E-01 5.4
6.82E-02 30.8
2.81E-01 7.8
1.23E-01 16.7
9.09E-01 3.8
1.97E-02103.2
4.64E-02 47.9
2.15E-01 9.7
4.32E-02 35.4
1.84E-02110.6
4.09E-02 36.1
1.56E-02 82.4
6.60E-02 26.5
1.67E-01 8.9
2.29E-02 47.5
9.75E-02 12.1
2.59E-02 40.6
6.06E-01 4.9
1.41E-01 11. 2
1.71E-01 9.9
5.38E-02 20.4
6.69E-02 14.5
2.75E-02 37.7
9.00E-02 14.2
2.22E-02 29.6
3.58E-02 23.4
6.67E-03 40.8

Fit
7.79E+OO
1.83E+OO
3.78E+OO
1.68E+OO

2.06E+OO
1. 68E+OO
1. 40E+Ol
4.23E+OO

Summary of Nuclide Activity


Sample ID : 1307149-02

Acquisition date

Total number of lines in spectrum


Number of unidentified lines
Number of lines tentatively identified by NID

28
24
4

Page :
2
7-AUG-2013 07:54:29

14.29%

Nuclide Type : FISSION


Nuclide
BA-133

Hlif e
10.50Y

Wtd Mean
Uncorrected
Decay pCi/filter
1. 00 4.141E+02

Total Activity

--------

4.141E+02

Wtd Mean
Decay Corr
pCi/filter
4.141E+02

--------

Decay Corr
2-Sigma
2-Sigma Error %Error Flags
0.789E+02
19.05

4.141E+02

Nuclide Type : NATURAL


Nuclide
Hlif e
TH-234 4.47E+09Y

Wtd Mean
Uncorrected
Decay pCi/filter
1. 00 8.687E+02

Total Activity
Grand Total Activity :

--------

Wtd Mean
Decay Corr
pCi/filter
8.687E+02

--------

8.687E+02

8.687E+02

l.283E+03

l.283E+03

Flags: "K" = Keyline not found


"E" = Manually edited

Decay Corr
2-Sigma
2-Sigma Error %Error Flags
1.577E+02
18.15

"M" = Manually accepted


"A" = Nuclide specific abn. limit

:8383

Nuclide Line Activity Report


Sample ID : 1307149-02

Acquisition date

Page :
3
7-AUG-2013 07:54:29

Nuclide Type: FISSION


Nuclide
BA-133

Energy
81. 00
302.84
356.01

%Abn
33.00*
17.80
60.00

Final Mean for

Uncorrected Decay Corr 2-Sigma


%Ef f
pCi/filter pCi/filter %Error
l.799E+Ol 4.141E+02
4.141E+02 19.05
7.560E+OO 3.348E+02
3.348E+02 34.84
7.170E+OO 3.809E+02
3.809E+02 18.02

3 Valid Peaks

Status
OK
OK
OK

4.141E+02+/- 7.888E+Ol ( 19.05%)

Nuclide Type: NATURAL


Nuclide
TH-234

Energy
63.29

%Abn
3.80*

Final Mean for


Flag: "*"

Uncorrected Decay Corr 2-Sigma


%Eff
pCi/filter pCi/filter %Error
2.305E+Ol 8.687E+02
8.687E+02 18.15

1 Valid Peaks

Status
OK

8.687E+02+/- 1.577E+02 ( 18.15%)

Keyline

G384

Combined Activity-MDA Report


Sample ID : 1307149-02

Acquisition date

4
Page :
7-AUG-2013 07:54:29

Identified Nuclides
Nuclide
BA-133
TH-234

Activity
(pCi/ filter)
4.141E+02
8.687E+02

Act error

MDA

(pCi/ filter)

MDA error

Act/MDA

7.888E+Ol
l.577E+02

l.998E+Ol

l.297E+02

3.402E+OO
l.072E+Ol

20.727
6.695

Act error

MDA

(pCi/filter)

MDA error

Act/MDA

6.159E+OO
l.146E+02
3.961E+OO
l.854E+OO
3.322E+Ol
9.943E+OO

8.903E+OO
l.732E+02
7.943E+OO
3.422E+OO
5.020E+Ol
1.887E+Ol

l.367E+OO
l.989E+Ol
l.513E-01
7.058E-02
5.668E+OO
1.461E+OO

-0.536
0.199
3.264
1. 244
0.196
1. 302

Non-Identified Nuclides

Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241

Key-Line
Activity K.L.
(pCi/filter)Ided
-4.776E+OO
3.444E+Ol
2.592E+Ol
4.257E+OO
9.829E+OO
2.456E+Ol

fii385

VAX/VMS Peak Search Report Generated


Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level

c-
rar7~

DK.AlOO: [GAMMA.SCUSR.ARCHIVE]SMP_130714903 GE2 BAFIL 194404.CN


PEAK Vl6.9 PEAKEFF V2.2
D-81 TOT
7-AUG-2013 00:00:00.
1307149-03
FILTER
GE2
0 00:15:00.00
25
3.00000
No

Pk It

Energy

Area

Bkgnd

1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34

28.10
30.98
35.05
52.64
61. 58
66.11
81. 07
84.60
92.67
111. 87
116.75
120.03
161.62
186.40
239.09
272.89
276.73
302.87
306.80
333.75
338.24
351.98
355.99
383.79
387.01
391.45
411.76
414.94
437.09
467.88
473.07
510.40
603.34
609.27

32
2081
498
73
244
78
818
27
39
206
34
15
26
46
51
10
46
141
27
67
31
21
525
156
201
51
7
45
89
23
9
18
7
12

147
101
97
95
124
86
54
35
86
47
49
50
84
75
22
10
21
11
12
5
10
3
11
13
11
7
12
19
12
4
2
12
4
2

3
3
3
0
0
0
3
3
0
1
1
1
0
0
0
1
1
2
2
2
2
1
1
3
3
3
1
1
0
1
1
0
0
0

7-AUG-2013 08:35:46.01

Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian

FWHM Channel
1. 66
1. 36
1. 68
2.69
1.45
1. 32
1. 40
1. 82
1. 66
1.55
1. 56
1. 56
1. 23
2.80
4.12
1.59
1. 76
1. 56
1. 97
1. 78
2.00
1. 83
1. 55
1. 82
1. 92
2.02
1. 88
1. 88
1. 31
1. 93
1. 93
1. 20
2.45
1. 50

28.22
31.10
35.17
52.75
61.70
66.22
81.19
84.72
92.78
111. 99
116.86
120.14
161. 73
186.51
239.20
273.00
276.84
302.98
306.91
333.86
338.35
352.09
356.10
383.89
387.11
391.56
411.86
415.04
437.19
467.98
473.18
510.50
603.44
609.37

7-AUG-2013 08:20:31.
1.00000E+OO filter
0
BAFIL
0 00:15:00.29 0.0%
4096
10.00000

Left

Pw

Cts/Sec %Err

26
26
26
49
58
65
76
76
89
107
107
107
158
182
235
272
272
299
299
328
328
350
350
380
380
380
409
409
433
465
465
507
601
607

15
15
15
9
7
5
12
12
7
17
17
17
7
8
8
8
8
11
11
18
18
14
14
15
15
15
12
12
8
15
15
8
6
6

3.56E-02 72.3
2.31E+OO 2.3
5.53E-01 5.6
8.lOE-02 26.7
2.71E-01 9.9
8.62E-02 21.8
9.09E-01 3.7
3.0lE-02 71. 6
4.33E-02 42.6
2.29E-01 8.8
3.82E-02 37.0
1.67E-02 74.1
2.89E-02 61. 7
5.17E-02 35.5
5.66E-02 21. 6
1. 06E-02 53.1
5.07E-02 21. 0
1.57E-01 9.1
2.99E-02 33.2
7.43E-02 14.l
3.49E-02 24.9
2.31E-02 22.8
5.83E-01 4.5
1.74E-01 8.2
2.23E-01 9.2
5.62E-02 18.3
8.02E-03106.6
5.03E-02 21. 8
9.89E-02 12.6
2.54E-02 23.7
9.77E-03 50.2
2.00E-02 40.8
8.18E-03 53.5
1. 32E-02 36.3

Fit
9.30E+OO

1.50E+OO
3.03E+OO

1.14E+Ol
2.87E+OO
l.80E+OO
1.03E+OO
6.98E+OO
5.91E+OO
8.99E-01

Summary of Nuclide Activity


Sample ID : 1307149-03

Acquisition date

Total number of lines in spectrum


Number of unidentified lines
Number of lines tentatively identified by NID

34
29
5

Page :
2
7-AUG-2013 08:20:31

14.71%

Nuclide Type : FISSION


Nuclide
Hlif e
BA-133
10.SOY
NP-237 2.14E+06Y

Wtd Mean
Uncorrected
Decay pCi/filter
1. 00 4.138E+02
1. 00 3.812E+Ol

Total Activity

4.520E+02

Wtd Mean
Decay Corr
pCi/filter
4.139E+02
3.812E+Ol

Decay Corr
2-Sigma
2-Sigma Error %Error Flags
0.786E+02
19.00
5.479E+Ol
143.72

4.520E+02

Nuclide Type : NATURAL


Nuclide
Hlif e
TH-234 4.47E+09Y

Wtd Mean
Uncorrected
Decay pCi/filter
1.00 8.374E+02

Total Activity
Grand Total Activity :
Flags: "K"
"E"

Wtd Mean
Decay Corr
pCi/filter
8.374E+02

8.374E+02

8.374E+02

l.289E+03

1.289E+03

Keyline not found


Manually edited

"M"
"A"

=
=

Decay Corr
2-Sigma
2-Sigma Error %Error Flags
1.833E+02
21. 89

Manually accepted
Nuclide specific abn. limit

ii3S7

Nuclide Line Activity Report


Sample ID : 1307149-03

Acquisition date

Page :
3
7-AUG-2013 08:20:31

Nuclide Type: FISSION


Nuclide
BA-133

Energy
81.00
302.84
356.01

%Abn
33.00*
17.80
60.00

Final Mean for


NP-237

86.50

3 Valid Peaks

12.60*

Final Mean for

Uncorrected Decay Corr 2-Sigma


%Ef f
pCi/filter pCi/filter %Error
l.799E+Ol 4.138E+02
4.139E+02 19.00
7.560E+OO 3.152E+02
3.152E+02 35.00
7.170E+OO 3.663E+02
3.663E+02 17.59

l.691E+Ol

1 Valid Peaks

= 4.139E+02+/- 7.863E+Ol
3.812E+Ol

Status
OK
OK
OK

19.00%)

3.812E+Ol 143.72

OK

= 3.812E+Ol+/- 5.479E+Ol (143.72%)

Nuclide Type: NATURAL


Nuclide
TH-234

Energy
63.29

%Abn
3.80*

Final Mean for


Flag:

11

* 11

Keyline

Uncorrected Decay Corr 2-Sigma


%Ef f
pCi/f ilter pCi/filter %Error
2.305E+Ol 8.374E+02
8.374E+02 21.89

1 Valid Peaks

Status
OK

8.374E+02+/- l.833E+02 ( 21.89%)

Combined Activity-MDA Report


Sample ID : 1307149-03

Acquisition date

Page :
4
7-AUG-2013 08:20:31

Identified Nuclides
Nuclide
BA-133
TH-234
NP-237

Activity
(pCi/filter)
4.139E+02
8.374E+02
3.812E+Ol

Act error
7.863E+Ol
l.833E+02
5.479E+Ol

MDA
(pCi/filter)
l.978E+Ol
l.684E+02
3.895E+Ol

MDA error

Act/MDA

3.367E+OO
l.391E+Ol
4.398E+OO

20.928
4.973
0.979

MDA error

Act/MDA

l.464E+OO
l.867E+Ol
l.439E-01
6.916E-02
l.533E+OO

-0.148
0.450
3.199
1. 238
1. 431

Non-Identified Nuclides

Nuclide
C0-57
CD-109
PA-231
PA-234
AM-241

Key-Line
Activity K.L.
(pCi/filter)Ided
-l.412E+OO
7.316E+Ol
2.418E+Ol
4.151E+OO
2.835E+Ol

Act error
6.073E+OO
9.900E+Ol
3.732E+OO
l.810E+OO
l.125E+Ol

MDA
(pCi/filter)
9.536E+OO
l.626E+02
7.558E+OO
3.353E+OO
l.981E+Ol

8389

VAX/VMS Peak Search Report Generated


Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level

7-AUG-2013 09:04:21.09

DK.AlOO: [GAMMA.SCUSR.ARCHIVE]SMP_130714904 GE2 BAFIL 194406.CN


PEAK V16.9 PEAKEFF V2.2
PZ-302-AS TOT
7-AUG-2013 00:00:00.
1307149-04
FILTER
GE2
0 00:15:00.00
25
3.00000
No

Pk It

Energy

Area

Bkgnd

1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33

28.05
30.98
35.05
52.67
61.82
65.80
81.05
93.08
111.75
115.75
276.23
284.82
295.55
302.81
306.85
325.52
333.55
337.84
356.11
368.91
377.33
383.79
386.84
391.46
414.91
418.08
437.06
467.94
472.15
511.87
523.57
596.61
610.30

54
1777
433
65
189
72
731
35
140
29
43
16
10
135
25
14
57
23
482
25
14
95
195
40
30
22
94
18
6
31
4
10
8

133
94
97
78
59
78
115
72
54
63
13
14
15
13
25
14
7
4
36
28
11
20
19
18
6
9
10
7
10
2
4
2
9

3
3
3
0
4
4
0
0
1
1
2
2
2
3
3
0
2
2
0
0
0
1
1
0
2
2
0
3
3
0
0
0
0

c~(f?/O

Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian

FWHM Channel
1. 66
1. 39
1. 68
2.37
1. 94
1. 95
1. 44
1. 29
1. 55
1. 56
1.93
1.94
1. 95
1.47
2.16
3.40
1. 99
2.00
1.48
7.53
1. 88
1. 86
1. 64
1. 82
2.07
2.08
1. 70
2.33
2.34
6.76
2.66
2.75
2.63

28.16
31.10
35.17
52.78
61.94
65.92
81.17
93.19
111.86
115.86
276.34
284.92
295.66
302.92
306.96
325.63
333.65
337.95
356.22
369.02
377.43
383.89
386.95
391.56
415.02
418.18
437.16
468.04
472.26
511.97
523.67
596.71
610.40

Left

Pw

26
26
26
48
57
57
76
89
108
108
272
272
272
299
299
322
329
329
352
362
375
381
381
390
411
411
433
463
463
507
521
593
606

15
15
15
9
13
13
10
7
11
11
27
27
27
12
12
8
15
15
8
13
6
9
9
6
12
12
7
13
13
11
5
7
8

7-AUG-2013 08:48:54.
l.OOOOOE+OO filter
0
BAFIL
0 00:15:00.28 0.0%
4096
10.00000
Cts/Sec %Err

5.98E-02
1.97E+OO
4.81E-01
7.27E-02
2.lOE-01
7.98E-02
8.12E-01
3.87E-02
1. 56E-01
3.20E-02
4.77E-02
1.79E-02
1. 06E-02
1.50E-01
2.72E-02
1.51E-02
6.30E-02
2.57E-02
5.35E-01
2.79E-02
1.51E-02
1.05E-01
2.17E-01
4.41E-02
3.34E-02
2.44E-02
1. 05E-01
2.00E-02
7.22E-03
3.40E-02
4.44E-03
l.14E-02
9.25E-03

42.2
2.5
6.0
27.4
10.1
23.5
4.6
44.3
12.2
43.5
21. 5
43.5
75.9
9.2
39.5
55.1
16.0
29.0
5.0
50.1
46.9
14.9
9.1
23.9
24.8
37.4
11. 6
35.8
86.0
20.8
89.0
37.7
73.1

Fit
6.42E+OO

3.25E+OO

3.68E+OO
2.14E+OO
1.78E+OO
l.72E+OO

8.51E-01
6.69E-01
7.68E-01

Summary of Nuclide Activity


Sample ID : 1307149-04

Acquisition date

Total number of lines in spectrum


Number of unidentified lines
Number of lines tentatively identified by NID

33
28
5

Page :
2
7-AUG-2013 08:48:54

15.15%

Nuclide Type : FISSION


Nuclide
BA-133

Hlif e
10.50Y

Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
3.698E+02

Total Activity

---------

3.698E+02

Wtd Mean
Decay Corr
pCi/filter
3.698E+02

Decay Corr
2-Sigma
2-Sigma Error %Error Flags
0.731E+02
19.77

---------

3.698E+02

Nuclide Type : NATURAL


Nuclide
Hlife
PA-231 3.28E+04Y
TH-234 4.47E+09Y

Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
2.337E+03
1. 00
6.483E+02

Total Activity
Grand Total Activity :

---------

Wtd Mean
Decay Corr
pCi/filter
2.337E+03
6.483E+02

---------

2.985E+03

2.985E+03

3.355E+03

3.355E+03

Flags: "K" = Keyline not found


"E" = Manually edited

Decay Corr
2-Sigma
2-Sigma Error %Error Flags
0.786E+03
33.65
l.435E+02
22.14

"M" = Manually accepted


"A" = Nuclide specific abn. limit

Nuclide Line Activity Report


Sample ID : 1307149-04

Acquisition date

Page :
3
7-AUG-2013 08:48:54

Nuclide Type: FISSION


Nuclide
BA-133

Energy
81. 00
302.84
356.01

%Abn
33.00*
17.80
60.00

Final Mean for

Uncorrected Decay Corr 2-Sigma


%Ef f
pCi/filter pCi/filter %Error
1.799E+Ol 3.698E+02
3.698E+02 19.77
7.560E+OO 3.020E+02
3.021E+02 35.14
7.170E+OO 3.363E+02
3.363E+02 18.20

3 Valid Peaks

Status
OK
OK
OK

3.698E+02+/- 7.311E+Ol ( 19.77%)

Nuclide Type: NATURAL


Nuclide
PA-231

Energy
9.28
10.11
283.67
302.67

%Abn
42.00*
20.20
1. 60
2.30

Final Mean for


TH-234

63.29

Flag: "*"

2 Valid Peaks

3.80*

Final Mean for

Uncorrected
%Ef f
pCi/filter
l.OOOE+02 - - - - - Line
l.OOOE+02 - - - - - Line
7.750E+OO 3.910E+02
7.562E+OO 2.337E+03

2.305E+Ol

1 Valid Peaks

Status
Absent
Absent
OK
OK

2.337E+03+/- 7.863E+02 ( 33.65%)

6.483E+02

Decay Corr 2-Sigma


pCi/filter %Error
Out Of Range - - - Out Of Range - - - 3.910E+02 91.11
2.337E+03 33.65

6.483E+02

22.14

OK

6.483E+02+/- 1.435E+02 ( 22.14%)

Keyline

8392

Combined Activity-MDA Report


Sample ID : 1307149-04

Acquisition date

Page :
4
7-AUG-2013 08:48:54

Identified Nuclides
Nuclide
BA-133
PA-231
TH-234

Activity
(pCi/ filter)
3.698E+02
2.337E+03
6.483E+02

Act error
7.311E+Ol
7.863E+02
l.435E+02

MDA
(pCi/filter)
1.867E+Ol
7.985E+OO
1.418E+02

MDA error

Act/MDA

3.179E+OO
l.521E-01
l.171E+Ol

19.811
292.663
4.573

Non-Identified Nuclides

Nuclide
C0-57
CD-109
PA-234
NP-237
AM-241

Key-Line
Activity K.L.
(pCi/filter)Ided
3.255E+OO
3.799E+Ol
3.825E+OO
-4.332E+OO
1.606E+Ol

Act error

MDA
(pCi/filter)

MDA error

Act/MDA

5.991E+OO
1.123E+02
l.829E+OO
3.350E+Ol
9.870E+OO

l.029E+Ol
1.711E+02
3.350E+OO
4.736E+Ol
1.793E+Ol

1.580E+OO
1.964E+Ol
6.910E-02
5.348E+OO
1.388E+OO

0.316
0.222
1.142
-0.091
0.895

-1393

c_
VAX/VMS Peak Search Report Generated
Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level

~fflr?

DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP_130714905 GE2 BAFIL 194409.CN


PEAK V16.9 PEAKEFF V2.2
PZ-302-AS DIS
7-AUG-2013 00:00:00.
1307149-05
FILTER
GE2
0 00:15:00.00
25
3.00000
No

Pk It

Energy

Area

Bkgnd

1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24

30.94
35.01
61.75
65.90
81. 01
111.78
115.96
204.74
276.80
302.88
307.79
333.73
351.73
356.03
384.11
387.03
391.26
414.11
418.37
421.65
424.50
437.05
468.26
511.14

1495
371
167
48
586
135
46
27
39
148
11
61
9
430
64
141
30
26
21
9
10
71
14
24

86
75
54
65
126
36
34
44
27
22
30
21
6
15
21
14
12
10
8
6
5
4
5
2

1
1
1
1
0
2
2
0
0
1
1
0
1
1
9
9
9
4
4
4
4
0
0
0

7-AUG-2013 09:27:48.36

Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian

FWHM Channel
1. 38
1. 39
1.46
1.47
1. 31
1. 71
1. 71
4.42
1. 69
1. 51
1.79
2.12
1.83
1.52
2.35
1. 96
2.39
2.51
2.51
2.52
2.52
1. 77
2.07
1.66

31.06
35.13
61. 87
66.02
81.12
111.89
116.07
204.85
276.91
302.98
307.89
333.84
351.83
356.14
384.22
387.14
391. 36
414.22
418.48
421.76
424.60
437.16
468.37
511. 25

Left

Pw

26
26
58
58
77
109
109
201
272
298
298
330
350
350
380
380
380
410
410
410
410
434
464
508

13
13
12
12
8
16
16
8
7
14
14
7
24
24
18
18
18
19
19
19
19
7
7
8

7-AUG-2013 09:12:32.
1.00000E+OO filter
0
BAFIL
0 00:15:00.27 0.0%
4096
10.00000
Cts/Sec %Err

1.66E+OO
4.12E-01
1.85E-01
5.29E-02
6.51E-01
l.50E-01
5.lOE-02
2.98E-02
4.37E-02
1. 64E-01
1.27E-02
6.79E-02
9.60E-03
4.78E-01
7.lOE-02
1.57E-01
3.29E-02
2.88E-02
2.34E-02
1.03E-02
1.06E-02
7.91E-02
l.52E-02
2.63E-02

2.8
6.4
10.1
27.9
5.3
11.1
24.4
47.6
26.9
9.4
68.4
17.8
50.1
5.0
24.6
11. 5
35.3
27.0
38.2
83.2
68.7
12.7
38.8
23.2

Fit
6.70E+OO
4.15E+OO
1.18E+OO

2.21E+OO
1.83E+OO
4.83E+OO
4.24E+OO

Summary of Nuclide Activity


Sample ID : 1307149-05

Acquisition date

Total number of lines in spectrum


Number of unidentified lines
Number of lines tentatively identified by NID

24
20
4

Page :
2
7-AUG-2013 09:12:32

16.67%

Nuclide Type : FISSION


Nuclide
BA-133

Hlif e
10.50Y

Wtd Mean
Uncorrected
Decay pCi/filter
1.00 2.965E+02

Total Activity

2.965E+02

Wtd Mean
Decay Corr
pCi/filter
2.965E+02

2-Sigma
Decay Corr
2-Sigma Error %Error Flags
0.606E+02
20.45

2.965E+02

Nuclide Type : NATURAL


Nuclide
Hlif e
TH-234 4.47E+09Y

Wtd Mean
Uncorrected
Decay pCi/filter
1.00 5.721E+02

Total Activity
Grand Total Activity :
Flags: "K"
"E"

=
=

Wtd Mean
Decay Corr
pCi/filter
5.721E+02

5.721E+02

5.721E+02

8.686E+02

8.686E+02

Keyline not found


Manually edited

"M"
"A"

=
=

Decay Corr
2-Sigma
2-Sigma Error %Error Flags
1.273E+02
22.26

Manually accepted
Nuclide specific abn. limit

Q395

Nuclide Line Activity Report


Sample ID : 1307149-05

Acquisition date

Page :
3
7-AUG-2013 09:12:32

Nuclide Type: FISSION


Nuclide
BA-133

Energy
81. 00
302.84
356.01

%Abn
33.00*
17.80
60.00

Final Mean for

Uncorrected Decay Corr 2-Sigma


%Ef f
pCi/filter pCi/filter %Error
l.799E+Ol 2.965E+02
2.965E+02 20.45
7.560E+OO 3.303E+02
3.303E+02 35.29
7.170E+OO 3.004E+02
3.004E+02 18.17

3 Valid Peaks

Status
OK
OK
OK

2.965E+02+/- 6.064E+Ol ( 20.45%)

Nuclide Type: NATURAL


Nuclide
TH-234

Energy
63.29

%Abn
3.80*

Final Mean for


Flag:

11

* 11

Uncorrected Decay Corr 2-Sigma


%Eff
pCi/filter pCi/filter %Error
2.305E+Ol 5.721E+02
5.721E+02 22.26

1 Valid Peaks

Status
OK

5.721E+02+/- l.273E+02 ( 22.26%)

Keyline

1396

Combined Activity-MDA Report


Sample ID : 1307149-05
----

Acquisition date

Page :
4
7-AUG-2013 09:12:32

Identified Nuclides

Nuclide
BA-133
TH-234

Activity
(pCi/filter)
2.965E+02
5.721E+02

Act error
6.064E+Ol
1.273E+02

MDA
(pCi/filter)
1.947E+Ol
l.489E+02

MDA error

Act/MDA

3.314E+OO
1.230E+Ol

15.233
3.842

Non-Identified Nuclides

Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241

Key-Line
Activity K.L.
(pCi/filter)Ided
1.lOOE+OO
6.847E+OO
2.690E+Ol
2.474E+OO
-2.505E+Ol
1.357E+Ol

Act error

MDA
(pCi/filter)

MDA error

Act/MDA

4.877E+OO
1.042E+02
3.953E+OO
1.652E+OO
3.324E+Ol
9.486E+OO

8.845E+OO
1.718E+02
7.958E+OO
2.976E+OO
4.919E+Ol
l.796E+Ol

1.358E+OO
1.972E+Ol
1.516E-01
6.139E-02
5.554E+OO
1.390E+OO

0.124
0.040
3.380
0.831
-0.509
0.756

&397

<:..
VAX/VMS Peak Search Report Generated
Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
.
Sensitivity
Critical level

DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP_130714906 GE2 BAFIL 194413.CN


PEAK V16.9 PEAKEFF V2.2
LR-100 TOT
7-AUG-2013 00:00:00.
1307149-06
FILTER
GE2
0 00:15:00.00
25
3.00000
No

Pk It

Energy

Area

Bkgnd

1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28

30.91
35.25
52.90
61. 83
65.80
81. 06
108.03
111.92
115.89
160.70
185.02
276.49
299.11
302.88
333.73
337.91
356.08
383.84
386.87
390.92
414.72
418.07
422.07
437.00
464.04
467.92
508.07
511. 08

1885
436
44
212
101
766
14
159
38
38
35
47
8
135
71
31
480
135
158
37
30
31
12
82
7
28
6
15

111
101
79
82
81
120
19
37
34
66
66
35
6
18
7
7
30
19
13
17
3
3
3
7
0
2
2
6

4
4
0
3
3
0
1
1
1
0
0
0
2
2
3
3
0
6
6
6
1
1
1
0
4
4
1
1

<t;(~

7-AUG-2013 09:46:00.13

Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian

FWHM Channel
1. 38
1. 64
2.55
1. 76
1. 77
1. 32
1. 54
1.55
1.41
2.90
1.29
1.80
1. 96
1. 56
2.19
2.20
1.39
2.04
1. 56
2.83
1. 88
1.89
1. 89
1.48
1.92
2.57
1. 96
1. 96

31. 02
35.36
53.01
61. 95
65.91
81.17
108.14
112.03
116.00
160.81
185.13
276.60
299.22
302.99
333.84
338.02
356.18
383.95
386.98
3 91. 03
414.83
418.17
422.17
437.10
464.15
468.03
508.18
511.18

Left

Pw

26
26
49
57
57
77
107
107
107
158
181
273
298
298
330
330
352
380
380
380
411
411
411
433
463
463
507
507

14
14
7
13
13
8
15
15
15
8
7
8
8
8
13
13
8
17
17
17
17
17
17
9
12
12
8
8

7-AUG-2013 09:30:41.
l.OOOOOE+OO filter
0
BAFIL
0 00:15:00.28 0.0%
4096
10.00000
Cts/Sec %Err

2.09E+OO
4.84E-01
4.92E-02
2.36E-01
1.12E-01
8.51E-01
1.56E-02
1.76E-01
4.25E-02
4.18E-02
3.86E-02
5.24E-02
9.22E-03
1.50E-01
7.91E-02
3.46E-02
5.33E-01
1.50E-01
1.76E-01
4.llE-02
3.29E-02
3.50E-02
1.30E-02
9.12E-02
8.05E-03
3.07E-02
6.22E-03
1.66E-02

2.4
6.0
36.5
9.5
17.8
4.4
50.7
10.4
27.2
40.5
42.4
26.7
44.3
9.7
14.8
26.9
5.0
10.5
9.3
41. 2
23.5
23.7
43.9
12.4
28.4
23.2
43.8
38.4

Fit
4.llE+OO
2.28E+OO
2.08E+OO

2.21E+OO
1. 73E+OO
5.17E+OO
2.26E+OO

8.50E-01
1.94E+OO

Summary of Nuclide Activity


Sample ID : 1307149-06

Acquisition date

Total number of lines in spectrum


Number of unidentified lines
Number of lines tentatively identified by NID

28
24
4

Page :
2
7-AUG-2013 09:30:41

14.29%

Nuclide Type : FISSION


Nuclide
BA-133

Hlife
10.SOY

Wtd Mean
Uncorrected
Decay pCi/filter
1.00 3.875E+02

Total Activity

3.875E+02

Wtd Mean
Decay Corr
pCi/filter
3.875E+02

2-Sigma
Decay Corr
2-Sigma Error %Error Flags
19.56
0.758E+02

3.875E+02

Nuclide Type : NATURAL


Nuclide
Hlife
TH-234 4.47E+09Y

Wtd Mean
Uncorrected
Decay pCi/filter
1.00 7.285E+02

Total Activity
Grand Total Activity :
Flags: "K"
"E"

Wtd Mean
Decay Corr
pCi/filter
7.285E+02

7.285E+02

7.285E+02

l.116E+03

l.116E+03

Keyline not found

= Manually edited

"M"
"A"

Decay Corr
2-Sigma
2-Sigma Error %Error Flags
1.539E+02
21.13

= Manually accepted
= Nuclide specific abn. limit

1!239S

Nuclide Line Activity Report


Sample ID : 1307149-06

Acquisition date

Page :
3
7-AUG-2013 09:30:41

Nuclide Type: FISSION


Nuclide
BA-133

Energy
81.00
302.84
356.01

%Abn
33.00*
17.80
60.00

Final Mean for

Uncorrected Decay Corr 2-Sigma


%Ef f
pCi/filter pCi/filter %Error
l.799E+Ol 3.875E+02
3.875E+02 19.56
7.560E+OO 3.021E+02
3.022E+02 35.69
7.170E+OO 3.349E+02
3.349E+02 18.12

3 Valid Peaks

Status
OK
OK
OK

3.875E+02+/- 7.581E+Ol ( 19.56%)

Nuclide Type: NATURAL


Nuclide
TH-234

Energy
63.29

%Abn
3.80*

Final Mean for


Flag: "*"

Keyline

Uncorrected Decay Corr 2-Sigma


%Ef f
pCi/filter pCi/f ilter %Error
2.305E+Ol 7.285E+02
7.285E+02 21.13

1 Valid Peaks

Status
OK

7.285E+02+/- 1.539E+02 ( 21.13%)

Combined Activity-MDA Report


Sample ID : 1307149-06

Acquisition date

Page :
4
7-AUG-2013 09:30:41

Identified Nuclides
Nuclide
BA-133
TH-234

Activity
(pCi/filter)

Act error

MDA
(pCi/filter)

MDA error

Act/MDA

3.875E+02
7.285E+02

7.581E+Ol
1.539E+02

l.695E+Ol
1.528E+02

2.886E+OO
1.262E+Ol

22.860
4.769

Non-Identified Nuclides

Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241

Key-Line
Activity K.L.
(pCi/filter)Ided
1.459E+OO
6.970E+Ol
2.554E+Ol
2.723E+OO
-9.894E+OO
2.350E+Ol

Act error

MDA
(pCi/filter)

MDA error

Act/MDA

5.223E+OO
1.016E+02
3.976E+OO
l.779E+OO
3.042E+Ol
l.107E+Ol

8.868E+OO
1.792E+02
7.955E+OO
3.181E+OO
4.778E+Ol
2.026E+Ol

1.362E+OO
2.057E+Ol
1.515E-01
6.560E-02
5.395E+OO
1.568E+OO

0.164
0.389
3.211
0.856
-0.207
1.160

c--
VAX/VMS Peak Search Report Generated
Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
Pk It
1
2
3
4
5
6

7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28

3
3
0
4
4
2
2
2
2
2
0
0
0
3
3
3
0
3
3
3
3
0
2
2
0
0
0
0

7-AUG-2013 08:10:18.51

ftrA-

DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP_130714907 GE3 BAFIL 194402.CN


PEAK V16.9 PEAKEFF V2.2
LR-100 DIS
7-AUG-2013 00:00:00.
1307149-07
FILTER
GE3
0 00:15:00.00
25
3.00000
No

Energy

Area

Bkgnd

30.82
35.11
52.36
61. 89
65.74
80.98
83.68
92.98
111.93
114.83
160.57
191. 50
277.13
303.11
307.03
311.24
334.09
356.26
364.71
384.06
387.18
391.61
415.06
418.53
437.37
459.44
468.87
511.49

1969
490
46
254
137
771
29
26
204
29
28
15
57
141
37
21
81
465
21
86
189
24
40
24
92
7
18
17

87
70
122
75
74
73
49
58
42
33
74
90
44
12
11
9
18
13
27
21
34
32
17
20
9
4
16
9

Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian

FWHM Channel
1.59
1. 64
2.64
1.66
2.02
1.70
1.41
1. 72
1. 75
1. 60
1. 24
1. 55
1. 98
1. 73
2.19
2.19
1.95
1.63
2.24
2.26
1. 74
1. 59
2.08
2.09
2.02
1.18
1. 80
1. 83

31.14
35.43
52.68
62.21
66.06
81. 29
84.00
93.30
112.24
115.15
160.88
191.81
277.43
303.41
307.34
311.54
334.40
356.56
365.01
384.36
387.48
391.91
415.36
418.84
437.67
459.74
469.17
511.79

7-AUG-2013 07:54:58.
1.00000E+OO filter
0
BAFIL
0 00:15:05.60 0.6%
4096
10.00000

Left

Pw

Cts/Sec %Err

26
26
48
58
58
76
76
76
107
107
158
190
274
300
300
300
332
351
351
381
381
391
411
411
432
456
465
506

15
15
8
12
12
26
26
26
16
16
7
8
10
22
22
22
5
19
19
10
10
6
11
11
10
8
9
12

2.19E+OO 2.3
5.44E-01 5.3
5.lOE-02 44.2
2.82E-01 8.0
1.53E-01 14.8
8.56E-01 4.0
3.27E-02 74.3
2.86E-02 51. 3
2.26E-01 8.9
3.23E-02 51. 8
3.llE-02 54.2
1.71E-02109.7
6.31E-02 25.4
1.57E-01 9.0
4.14E-02 32.0
2.32E-02 42.2
9.02E-02 13.5
5.17E-01 4.8
2.32E-02 40.5
9.54E-02 19.5
2.lOE-01 8.9
2.70E-02 44.4
4.39E-02 22.5
2.70E-02 36.1
1.02E-01 12.3
7.37E-03 65.7
2.00E-02 46.3
l.89E-02 42.9

Fit
1.06E+Ol
1.65E+OO
7.13E+OO
5.99E+OO

2.17E+OO

2.15E+OO
1.91E+Ol
5.69E+OO

Summary of Nuclide Activity


Sample ID : 1307149-07

Acquisition date

Total number of lines in spectrum


Number of unidentified lines
Number of lines tentatively identified by NID
Nuclide Type
Nuclide
BA-133

Wtd Mean
Uncorrected
Decay pCi/f ilter
1. 00
3.694E+02

Total Activity
:

14.29%

FISSION

Hlife
10.50Y

Nuclide Type

28
24
4

Page :
2
7-AUG-2013 07:54:58

--------

3.694E+02

Wtd Mean
Decay Corr
pCi/filter
3.694E+02

--------

Decay Corr
2-Sigma
2-Sigma Error %Error Flags
0.653E+02
17.68

3.694E+02

NATURAL

Nuclide
Hlif e
TH-234 4.47E+09Y

Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
7.580E+02

Total Activity
Grand Total Activity :

--------

Wtd Mean
Decay Corr
pCi/filter
7.580E+02

--------

7.580E+02

7.580E+02

l.127E+03

1.127E+03

Flags: "K" = Keyline not found


"E" = Manually edited

Decay Corr
2-Sigma
2-Sigma Error %Error Flags
1.319E+02
17.40

"M" = Manually accepted


"A" = Nuclide specific abn. limit

Nuclide Line Activity Report


Sample ID : 1307149-07

Acquisition date

Page :
3
7-AUG-2013 07:54:58

Nuclide Type: FISSION


Nuclide
BA-133

Energy
81. 00
302.84
356.01

%Abn
33.00*
17.80
60.00

Final Mean for

Uncorrected Decay Corr 2-Sigma


%Ef f
pCi/filter pCi/filter %Error
1.899E+Ol 3.694E+02
3.694E+02 17.68
6.222E+OO 3.823E+02
3.823E+02 27.30
5.860E+OO 3.971E+02
3.972E+02 16.66

3 Valid Peaks

Status
OK
OK
OK

3.694E+02+/- 6.531E+Ol ( 17.68%)

Nuclide Type: NATURAL


Nuclide
TH-234

Energy
63.29

%Abn
3.80*

Final Mean for


Flag:

11

* 11

Keyline

Uncorrected Decay Corr 2-Sigma


%Eff
pCi/filter pCi/filter %Error
2.648E+Ol 7.580E+02
7.580E+02 17.40

1 Valid Peaks

Status
OK

7.580E+02+/- 1.319E+02 ( 17.40%)

Combined Activity-MDA Report


Sample ID : 1307149-07

Acquisition date

Page :
4
7-AUG-2013 07:54:58

Identified Nuclides
Nuclide
BA-133
TH-234

Activity
(pCi/ filter)
3.694E+02
7.580E+02

Act error
6.531E+Ol
1.319E+02

MDA
(pCi/filter)
2.069E+Ol
1.251E+02

MDA error

Act/MDA

3.165E+OO
6.717E+OO

17.853
6.061

Non-Identified Nuclides

Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241

Key-Line
Activity K.L.
(pCi/filter)Ided
-6.017E-01
-1.145E+02
7.952E-01
4.077E+OO
-3.425E+Ol
2.322E+Ol

Act error

MDA
(pCi/filter)

MDA error

Act/MDA

5.861E+OO
1.093E+02
1.579E+OO
1.528E+OO
3.143E+Ol
8.771E+OO

9.352E+OO
1.710E+02
2.947E+OO
2.910E+OO
4.896E+Ol
1.731E+Ol

1.068E+OO
1.410E+Ol
4.191E-02
4.139E-02
3.958E+OO
8.509E-01

-0.064
-0.669
0.270
1.401
-0.700
1. 342

<:::..--

VAX/VMS Peak Search Report Generated


Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level

DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP_130714908 GE3


PEAK Vl6.9 PEAKEFF V2.2
D-81 TOT
7-AUG-2013 00:00:00.
1307149-08
FILTER
GE3
0 00:15:00.00
25
3.00000
No

Pk It

Energy

Area

Bkgnd

1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26

30.83
35.10
51.80
61.85
66.05
76.98
80.98
84.68
92.23
111.87
116.78
277.41
294.74
303.16
307.53
334.02
356.30
383.79
386.97
391.57
415.10
418.41
437.73
468.28
511.54
610.28

2045
494
60
217
81
18
887
21
23
252
45
48
17
153
24
67
478
59
173
50
50
38
95
21
10
11

95
98
120
144
112
39
56
39
81
49
52
39
16
13
15
29
35
33
70
27
20
19
20
14
7
3

4
4
0
0
0
2
2
2
0
3
3
0
0
4
4
0
0
7
7
0
4
4
0
0
0
0

7-AUG-2013 08:36:30.11

Acquisition date :
Sample Ql.,.lantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian

FWHM Channel
1.49
1. 64
3.06
1. 30
1.71
1. 69
1. 70
1.41
1. 88
1. 82
1. 93
1. 23
1. 75
1. 81
2.03
1. 53
1. 93
1. 88
1.87
2.57
2.52
2.07
1. 74
1. 67
1. 41
2.02

31.15
35.42
52.11
62.17
66.36
77.29
81. 29
85.00
92.55
112.18
117.10
277.71
295.05
303.46
307.84
334.33
356.61
384.09
387.27
391.87
415.40
418.71
438.03
468.58
511.84
610.57

Left

Pw

26
26
50
59
65
76
76
76
90
107
107
274
292
299
299
330
352
381
381
391
412
412
433
464
508
607

15
15
8
6
5
14
14
14
8
19
19
7
7
16
16
7
10
10
10
6
11
11
9
8
7
7

fdrr--
BAFIL 194405.CN

7-AUG-2013 08:21:10.
1.00000E+OO filter
0
BAFIL
0 00:15:05.99 0.7%
4096
10.00000
Cts/Sec %Err

2.27E+OO
5.49E-01
6.67E-02
2.41E-01
9.00E-02
1.95E-02
9.86E-01
2.38E-02
2.59E-02
2.80E-01
4.99E-02
5.29E-02
1. 89E-02
1.70E-01
2.62E-02
7.49E-02
5.32E-01
6.50E-02
l.92E-01
5.53E-02
5.53E-02
4.26E-02
l.05E-01
2.35E-02
1. lOE-02
1.21E-02

2.3
5.5
33.8
11.1
22.9
49 .4
3.5
51. 8
69.6
7.5
32.5
26.1
45.7
8.7
35.1
17.9
5.1
26.0
11.6
25.6
24.2
27.2
13.4
37.5
54.4
41. 0

Fit
7.93E+OO

1.71E+Ol

2.57E+OO

1.78E+OO

9.03E+Ol
2.57E+OO

Summary of Nuclide Activity


Sample ID : 1307149-08

Acquisition date

Total number of lines in spectrum


Number of unidentified lines
Number of lines tentatively identified by NID

26
21
5

Page :
2
7-AUG-2013 08:21:10

19.23%

Nuclide Type : FISSION


Nuclide
Hlif e
BA-133
10.50Y
NP-237 2.14E+06Y

Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
4.253E+02
1. 00
2.915E+Ol

Total Activity

---------

4.545E+02

Wtd Mean
Decay Corr
pCi/filter
4.253E+02
2.915E+Ol

Decay Corr
2-Sigma
2-Sigma Error %Error Flags
0.736E+02
17.32
104.06
3.034E+Ol

---------

4.545E+02

Nuclide Type : NATURAL


Nuclide
Hlif e
TH-234 4.47E+09Y

Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
6.483E+02

Total Activity
Grand Total Activity :
Flags: "K"
"E"

---------

Wtd Mean
Decay Corr
pCi/filter
6.483E+02

---------

6.483E+02

6.483E+02

l.103E+03

l.103E+03

= Keyline not found


= Manually edited

Decay Corr
2-Sigma
2-Sigma Error %Error Flags
1.498E+02
23.11

"M"
"A"

= Manually accepted
= Nuclide specific abn. limit

Nuclide Line Activity Report


Sample ID : 1307149-08

Acquisition date

Page :
3
7-AUG-2013 08:21:10

Nuclide Type: FISSION


Nuclide
BA-133

Energy
81.00
302.84
356.01

%Abn
33.00*
17.80
60.00

Final Mean for


NP-237

86.50

3 Valid Peaks =

12.60*

Final Mean for

Uncorrected Decay Corr 2-Sigma


%Ef f
pCi/filter pCi/filter %Error
l.899E+Ol 4.253E+02
4.253E+02 17.32
6.222E+OO 4.139E+02
4.139E+02 26.97
5.860E+OO 4.086E+02
4.086E+02 17.06

1.749E+Ol

4.253E+02+/- 7.365E+Ol ( 17.32%)

2.915E+Ol

1 Valid Peaks =

Status
OK
OK
OK

2.915E+Ol 104.06

OK

2.915E+Ol+/- 3.034E+Ol (104.06%)

Nuclide Type: NATURAL


Nuclide
TH-234

Energy
63.29

%Abn
3.80*

Final Mean for


Flag:

11

* 11

Keyline

Uncorrected Decay Corr 2-Sigma


%Eff
pCi/filter pCi/filter %Error
2.648E+Ol 6.483E+02
6.483E+02 23.11

1 Valid Peaks

Status
OK

6.483E+02+/- l.498E+02 ( 23.11%)

Combined Activity-MDA Report


Sample ID : 1307149-08

Acquisition date

4
Page :
7-AUG-2013 08:21:10

Identified Nuclides
Nuclide
BA-133
TH-234
NP-237

Activity
(pCi/filter)
4.253E+02
6.483E+02
2.915E+Ol

Act error
7.365E+Ol
1. 498E+02

3.034E+Ol

MDA
(pCi/filter)
1.778E+Ol
1.611E+02
5.069E+Ol

MDA error

Act/MDA

2.719E+OO
8.651E+OO
4.098E+OO

23.922
4.025
0.575

MDA error

Act/MDA

1.309E+OO
1.415E+Ol
4.018E-02
4.080E-02
8.999E-01

0.341
0.334
0.366
1.300
1.581

Non-Identified Nuclides

Nuclide
C0-57
CD-109
PA-231
PA-234
AM-241

Key-Line
Activity K.L.
(pCi/filter)Ided
3.910E+OO
5.733E+Ol
l.035E+OO
3.729E+OO
2.894E+Ol

Act error
6.263E+OO
1.109E+02
1.482E+OO
1.522E+OO
l.039E+Ol

MDA
(pCi/filter)
1.146E+Ol
l.716E+02
2.825E+OO
2.868E+OO
1.830E+Ol

VAX/VMS Peak Search Report Generated


Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
Pk It
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30

6
6
6
0
1
1
0
0
0
0
0
0
1
1
3
3
0
0
1
1
0
6
6
0
0
0
0
0
0
0

7-AUG-2013 09:04:47.22

~~(~

DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP_l30714909 - GE3 BAFIL 194407.CN


PEAK Vl6.9 PEAKEFF V2.2
D-81 DIS
7-AUG-2013 00:00:00.
1307149-09
FILTER
GE3
0 00:15:00.00
25
3.00000
No

Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian

Energy

Area

Bkgnd

FWHM Channel

Left

Pw

27.95
30.84
34.96
53.01
61. 75
65.82
81. 03
92.79
111. 71
159.85
170.35
276.49
302.86
307.53
333.68
338.38
356.26
365.45
383.71
386.87
391.62
415.15
418.34
437.17
467.87
498.50
511.08
532.29
609.26
1016.15

53
2062
629
70
252
101
890
51
238
34
23
61
137
28
90
22
474
29
121
185
38
47
23
107
33
4
21
6
10
7

60
73
94
114
74
78
147
67
95
74
46
23
15
15
22
15
30
12
26
49
17
18
14
0
7
3
2
2
2
0

1. 57
28.27
1. 49
31.16
2.07
35.28
3.12
53.33
1. 51
62.07
1. 52
66.14
1. 81
81. 35
1. 39
93.11
1. 95 112.03
1. 99 160.17
2.31 170.66
1. 61 276.79
1. 80 303.16
1.81 307.84
1. 87 333.99
2.22 338.68
1. 98 356.57
2.46 365.75
1. 87 384.02
1. 87 387.17
2.65 391.92
2.52 415.45
2.11 418.64
2.00 437.47
1. 22 468.17
2.66 498.79
3.66 511.38
1.37 532.58
1. 53 609.55
1.12 1016.43

27
27
27
50
58
58
76
90
108
158
168
273
299
299
329
329
351
362
381
381
391
410
410
435
465
495
508
529
607
1013

14
14
14
8
12
12
11
7
7
8
6
7
15
15
17
17
12
7
10
10
6
12
12
6
7
6
8
6
6
7

7-AUG-2013 08:49:28.
l.OOOOOE+OO filter
0
BAFIL
0 00:15:05.21 0.6%
4096
10.00000
Cts/Sec %Err

5.84E-02
2.29E+OO
6.99E-01
7.81E-02
2.80E-01
l.12E-01
9.89E-01
5.68E-02
2.64E-01
3.82E-02
2.53E-02
6.83E-02
1. 52E-01
3.06E-02
9.96E-02
2.49E-02
5.27E-01
3.25E-02
l.35E-01
2.05E-01
4.28E-02
5.26E-02
2.55E-02
l.19E-01
3.63E-02
4.60E-03
2.30E-02
7.15E-03
l.14E-02
7.78E-03

Fit

23.8 3.54E+Ol
2.3
5.8
28.9
8.4 5.52E+OO
17.4
4.3
30.0
9.4
45.8

51.8

18.1

9.8 3.38E+OO

29.6

13.8 2.lOE+OO

46.7

5.1

27.0

12.2 2.17E+Ol

10.7

27.4

22.9 8.08E-01

41. 8

9.7

22.1

81. 9

25.l

49.7

36.8

37.8

Summary of Nuclide Activity


Sample ID : 1307149-09

Acquisition date

Total number of lines in spectrum


Number of unidentified lines
Number of lines tentatively identified by NID

30
26
4

Page :
2
7-AUG-2013 08:49:28

13.33%

Nuclide Type : FISSION


Nuclide
BA-133

Hlif e
10.SOY

Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
4.265E+02

Total Activity

---------

4.265E+02

Wtd Mean
Decay Corr
pCi/filter
4.265E+02

Decay Corr
2-Sigma
2-Sigma Error %Error Flags
0.766E+02
17.97

---------

4.265E+02

Nuclide Type : NATURAL


Nuclide
Hlife
TH-234 4.47E+09Y

Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
7.512E+02

Total Activity
Grand Total Activity :
Flags: "K"
"E"

=
=

---------

Wtd Mean
Decay Corr
pCi/filter
7.512E+02

---------

7.512E+02

7.512E+02

l.178E+03

1.178E+03

Keyline not found


Manually edited

"M"
"A"

=
=

Decay Corr
2-Sigma
2-Sigma Error %Error Flags
l.358E+02
18.08

Manually accepted
Nuclide specific abn. limit

l~411

Nuclide Line Activity Report


Sample ID : 1307149-09

Acquisition date

Page :
3
7-AUG-2013 08:49:28

Nuclide Type: FISSION


Nuclide
BA-133

Energy
81. 00
302.84
356.01

%Abn
33.00*
17.80
60.00

Final Mean for

uncorrected Decay Corr 2-Sigma


%Ef f
pCi/filter pCi/filter %Error
1.899E+Ol 4.265E+02
4.265E+02 17.97
6.222E+OO 3.715E+02
3.715E+02 28.45
5.860E+OO 4.052E+02
4.053E+02 17.08

3 Valid Peaks

Status
OK
OK
OK

4.265E+02+/- 7.664E+Ol ( 17.97%)

Nuclide Type: NATURAL


Nuclide
TH-234

Energy
63.29

%Abn
3.80*

Final Mean for


Flag:

11

* 11

Uncorrected Decay Corr 2-Sigma


%Eff
pCi/filter pCi/filter %Error
2.648E+Ol 7.512E+02
7.512E+02 18.08

1 Valid Peaks

Status
OK

7.512E+02+/- 1.358E+02 ( 18.08%)

Keyline

i412

Combined Activity-MDA Report


Sample ID : 1307149-09

Acquisition date

Page :
4
7-AUG-2013 08:49:28

Identified Nuclides
Nuclide
BA-133
TH-234

Activity
(pCi/filter)

Act error

4.265E+02
7.512E+02

7.664E+Ol
1.358E+02

MDA
(pCi/filter)
1.840E+Ol
l.480E+02

MDA error

Act/MDA

2.814E+OO
7.948E+OO

23.176
5.077

Non-Identified Nuclides

Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241

Key-Line
Activity K.L.
(pCi/filter)Ided
-4.659E+OO
-2.444E+Ol
1.349E+OO
2.966E+OO
-6.651E+OO
2.051E+Ol

Act error

MDA
(pCi/filter)

MDA error

Act/MDA

6.419E+OO
l.144E+02
1.673E+OO
l.368E+OO
3.448E+Ol
1.027E+Ol

l.028E+Ol
1.576E+02
3.168E+OO
2.688E+OO
4.760E+Ol
1.842E+Ol

1.175E+OO
1.299E+Ol
4.505E-02
3.823E-02
3.848E+OO
9.056E-01

-0.453
-0.155
0.426
1.103
-0.140
1.113

8413

<:...-

VAX/VMS Peak Search Report Generated


Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level

'B(1t-

DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP_l30714910 GE3 BAFIL 194410.CN


PEAK V16.9 PEAKEFF V2.2
PZ-204-SS TOT
7-AUG-2013 00:00:00.
1307149-10
FILTER
GE3
0 00:15:00.00
25
3.00000
No

Pk It

Energy

Area

Bkgnd

1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27

30.84
35.07
52.28
61. 78
65.81
80.98
83.68
112.80
142.96
276.65
286.85
303.08
307.49
333.64
338.14
356.21
384.01
387.05
391. 34
414.92
418.27
422.04
437.08
467.28
511. 20
610.51
660.38

2082
567
52
250
154
727
22
315
17
58
12
138
27
75
18
456
131
222
58
51
31
18
108
25
21
7
6

88
75
86
73
74
54
33
91
74
21
14
27
30
17
24
27
5
3
0
11
7
5
2
8
2
3
0

3
3
0
4
4
2
2
0
0
1
1
6
6
3
3
0
2
2
2
3
3
3
0
0
0
0
0

7-AUG-2013 09:28:25.86

Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian

FWHM Channel
1.48
1. 71
1. 51
1. 68
1. 95
1. 70
1.41
1. 98
2.03
1.78
1. 79
1. 70
1. 95
1. 91
2.22
1. 96
2.06
2.06
2.06
2.29
2.07
2.30
2.05
2.28
3.90
2.40
1. 00

31.16
35.39
52.60
62.10
66.13
81. 29
84.00
113.12
143.27
276.96
287.16
303.38
307.80
333.95
338.45
356.52
384.31
387.36
391. 64
415.23
418.57
422.34
437.38
467.58
511. 50
610.80
660.67

Left

Pw

27
27
50
57
57
76
76
108
141
273
273
300
300
329
329
352
381
381
381
412
412
412
433
463
507
606
658

13
13
6
16
16
12
12
11
7
19
19
12
12
13
13
10
18
18
18
17
17
17
8
10
9
7
6

7-AUG-2013 09:13:05.
l.OOOOOE+OO filter
0
BAFIL
0 00:15:05.69 0.6%
4096
10.00000
Cts/Sec %Err

2.31E+OO
6.30E-01
5.72E-02
2.78E-01
1.71E-01
8.08E-01
2.45E-02
3.50E-01
l.93E-02
6.47E-02
l.38E-02
1.53E-Ol
3.0lE-02
8.36E-02
2.0lE-02
5.07E-01
1.46E-01
2.46E-01
6.48E-02
5.63E-02
3.39E-02
2.00E-02
l.20E-01
2.82E-02
2.32E-02
7.33E-03
6.67E-03

2.3
4.9
31. 7
8.1
13.2
4.1
92.0
8.2
84.6
16.2
53.8
9.9
38.6
15.5
56.4
5.1
9.8
8.4
16.3
17.9
30.8
42.1
9.9
28.3
25.4
60.8
40.8

Fit
6.28E+OO
2.58E+OO
1.15E+Ol

4.19E+OO
4.73E+OO
4.26E+OO
5.09E+OO
3.82E+OO

Summary of Nuclide Activity


Sample ID : 1307149-10

Acquisition date

Total number of lines in spectrum


Number of unidentified lines
Number of lines tentatively identified by NID

27
23
4

Page :
2
7-AUG-2013 09:13:05

14.81%

Nuclide Type : FISSION


Nuclide
BA-133

Hlife
10.50Y

Wtd Mean
Uncorrected
Decay pCi/filter
1.00 3.486E+02

Total Activity

3.486E+02

Wtd Mean
Decay Corr
pCi/filter
3.486E+02

Decay Corr
2-Sigma
2-Sigma Error %Error Flags
0.620E+02
17.77

3.486E+02

Nuclide Type : NATURAL


Nuclide
Hlife
TH-234 4.47E+09Y

Wtd Mean
Uncorrected
Decay pCi/filter
1.00 7.466E+02

Total Activity
Grand Total Activity :
Flags: "K"
"E"

=
=

Wtd Mean
Decay Corr
pCi/filter
7.466E+02

7.466E+02

7.466E+02

l.095E+03

1.095E+03

Keyline not found


Manually edited

"M"
"A"

=
=

Decay Corr
2-Sigma
2-Sigma Error %Error Flags
1.309E+02
17.54

Manually accepted
Nuclide specific abn. limit

ti415

Nuclide Line Activity Report


Sample ID : 1307149-10

Acquisition date

Page :
3
7-AUG-2013 09:13:05

Nuclide Type: FISSION


Nuclide
BA-133

Energy
81. 00
302.84
356.01

%Abn
33.00*
17.80
60.00

Final Mean for

uncorrected Decay Corr 2-Sigma


%Ef f
pCi/filter pCi/filter %Error
l.899E+Ol 3.486E+02
3.486E+02 17.77
6.222E+OO 3.730E+02
3.730E+02 28.58
5.860E+OO 3.897E+02
3.897E+02 17.09

3 Valid Peaks

Status
OK
OK
OK

3.486E+02+/- 6.195E+Ol ( 17.77%)

Nuclide Type: NATURAL


Nuclide
TH-234

Energy
63.29

%Abn
3.80*

Final Mean for


Flag:

11

* 11

uncorrected Decay Corr 2-Sigma


%Ef f
pCi/f ilter pCi/f ilter %Error
2.648E+Ol 7.466E+02
7.466E+02 17.54

1 Valid Peaks

Status
OK

7.466E+02+/- l.309E+02 ( 17.54%)

Keyline

1415

Combined Activity-MDA Report


Sample ID : 1307149-10
- - - -

Acquisition date

4
Page :
7-AUG-2013 09:13:05

Identified Nuclides

Nuclide
BA-133
TH-234

Activity
(pCi/filter)

Act error

MDA

(pCi/ filter)

MDA error

Act/MDA

3.486E+02
7.466E+02

6.195E+Ol
1.309E+02

1.855E+Ol

1.231E+02

2.838E+OO
6.610E+OO

18.789
6.066

Act error

MDA

(pCi/filter)

MDA error

Act/MDA

5.732E+OO
1.023E+02
l.607E+OO
1.460E+OO
2.859E+Ol
9.509E+OO

9.980E+OO
l.609E+02
3.262E+OO
2.754E+OO
4.680E+Ol
l.816E+Ol

l.140E+OO
l.327E+Ol
4.640E-02
3.917E-02
3.783E+OO
8.931E-01

0.330
-0.155
0.913
0.782
0.033
1. 573

Non-Identified Nuclides

Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241

Key-Line
Activity K.L.
(pCi/filter)Ided
3.294E+OO
-2.488E+Ol
2.978E+OO
2.153E+OO
l.556E+OO
2.856E+Ol

C-
VAX/VMS Peak Search Report Generated
Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level

81~

DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP_130714911 - GE3 BAFIL- 194414.CN


PEAK V16.9 PEAKEFF V2.2
PZ-204-SS DIS
7-AUG-2013 00:00:00.
1307149-11
FILTER
GE3
0 00:15:00.00
25
3.00000
No

Pk It

Energy

Area

Bkgnd

1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25

30.83
35.06
53.03
61.83
65.86
81.05
111.96
225.35
277.03
295.98
302.94
307.65
333.78
337.84
352.51
356.19
383.79
387.03
391.74
414.53
417.87
421.53
437.36
468.55
511. 54

1995
492
49
261
126
859
237
34
57
9
136
30
79
33
15
480
76
194
50
37
29
11
105
22
18

92
82
68
68
81
130
112
56
39
65
21
22
14
9
6
10
40
39
16
8
7
6
9
13
6

3
3
3
3
3
0
0
0
0
0
2
2
3
3
3
3
3
3
0
1
1
1
0
0
0

7-AUG-2013 09:46:53.64

Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian

FWHM Channel
1.48
1.72
1.80
1. 82
1. 83
1. 87
1.74
3.97
1. 97
5.61
1. 69
1. 99
1. 98
2.22
2.23
1.61
2.17
1. 81
1.17
1. 89
1.90
1. 90
1. 84
1. 62
1. 96

31.15
35.38
53.35
62.15
66.18
81. 37
112.27
225.66
277.34
296.28
303.25
307.96
334.09
338.15
352.82
356.49
384.09
387.33
392.04
414.83
418.17
421. 83
437.66
468.84
511.84

7-AUG-2013 09:31:32.
1.00000E+OO filter
0
BAFIL
0 00:15:05.65 0.6%
4096
10.00000

Left

Pw

Cts/Sec %Err

26
26
50
50
50
76
108
221
273
282
299
299
330
330
351
351
381
381
391
410
410
410
434
464
507

14
14
20
20
20
11
7
9
9
17
19
19
12
12
12
12
10
10
5
15
15
15
8
10
8

2.22E+OO 2.3
5.47E-01 5.5
5.42E-02 30.2
2.90E-01 7.6
l.39E-01 16.1
9.55E-01 4.3
2.63E-01 9.9
3.83E-02 43.2
6.37E-02 23.9
1.0lE-02205.1
l.51E-01 9.8
3.29E-02 31. 7
8.80E-02 13.7
3.67E-02 31.2
1. 72E-02 32.0
5.34E-01 4.7
8.46E-02 23.1
2.16E-01 8.7
5.58E-02 19.9
4.15E-02 19.7
3.19E-02 29.9
l.20E-02 56.3
1. 17E-01 11. 0
2.49E-02 36.4
2.02E-02 33.0

Fit
5.50E+OO
3.31E+OO

1.22E+OO
2.49E+OO
1.34E+OO
1. 40E+Ol
9.48E-01

Summary of Nuclide Activity


Sample ID : 1307149-11

Acquisition date

Total number of lines in spectrum


Number of unidentified lines
Number of lines tentatively identified by NID

25
21
4

Page :
2
7-AUG-2013 09:31:32

16.00%

Nuclide Type : FISSION


Nuclide
BA-133

Hlif e
10.SOY

Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
4.119E+02

Total Activity
Nuclide Type

Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
7.790E+02

Total Activity
Grand Total Activity :

=
=

Decay Corr
2-Sigma
2-Sigma Error %Error Flags
0.740E+02
17.96

---------

4.119E+02

NATURAL

Nuclide
Hlife
TH-234 4.47E+09Y

Flags: "K"
"E"

---------

4.119E+02

Wtd Mean
Decay Corr
pCi/filter
4.119E+02

---------

Wtd Mean
Decay Corr
pCi/filter
7.790E+02

---------

7.790E+02

7.790E+02

l.191E+03

1.191E+03

Keyline not found


Manually edited

"M"
"A"

=
=

Decay Corr
2-Sigma
2-Sigma Error %Error Flags
1.298E+02
16.66

Manually accepted
Nuclide specific abn. limit

Nuclide Line Activity Report


Sample ID : 1307149-11

Acquisition date

Page :
3
7-AUG-2013 09:31:32

Nuclide Type: FISSION


Nuclide
BA-133

Energy
81. 00
302.84
356.01

%Abn
33.00*
17.80
60.00

Final Mean for

Uncorrected Decay Corr 2-Sigma


%Ef f
pCi/filter pCi/filter %Error
1.899E+Ol 4.119E+02
4.119E+02 17.96
6.222E+OO 3.692E+02
3.693E+02 28.39
5.860E+OO 4.103E+02
4.104E+02 16.53

3 Valid Peaks

Status
OK
OK
OK

4.119E+02+/- 7.399E+Ol ( 17.96%)

Nuclide Type: NATURAL


Nuclide
TH-234

Energy
63.29

%Abn
3.80*

Final Mean for


Flag:

11

* 11

Keyline

Uncorrected Decay Corr 2-Sigma


%Eff
pCi/filter pCi/filter %Error
2.648E+Ol 7.790E+02
7.790E+02 16.66

1 Valid Peaks

Status
OK

7.790E+02+/- 1.298E+02 ( 16.66%)

Combined Activity-MDA Report


Sample ID : 1307149-11

Acquisition date

Page :
4
7-AUG-2013 09:31:32

Identified Nuclides
Nuclide
BA-133
TH-234

Activity
(pCi/filter)

Act error

4.119E+02
7.790E+02

7.399E+Ol
l.298E+02

MDA
(pCi/filter)
1.646E+Ol
1.172E+02

MDA error

Act/MDA

2.517E+OO
6.293E+OO

25.026
6.649

Non-Identified Nuclides

Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241

Key-Line
Activity K.L.
(pCi/filter)Ided
l.056E+OO
-4.659E+Ol
4.497E+OO
3.202E+OO
1.620E+Ol
2.832E+Ol

Act error

MDA
(pCi/filter)

MDA error

Act/MDA

5.335E+OO
1.004E+02
1.679E+OO
1.436E+OO
2.913E+Ol
8.811E+OO

9.567E+OO
1.532E+02
3.533E+OO
2.703E+OO
5.034E+Ol
1.776E+Ol

1.093E+OO
1.263E+Ol
5.025E-02
3.844E-02
4.069E+OO
8.732E-01

0.110
-0.304
1. 273
1.185
0.322
1.594

Sd21

VAX/VMS Peak Search Report Generated


Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level

0(~

DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP_130714912 GE3 BAFIL 194416.CN


PEAK V16.9 PEAKEFF V2.2
LR-103 TOT
7-AUG-2013 00:00:00.
1307149-12
FILTER
GE3
0 00:15:00.00
25
3.00000
No

Pk It

Energy

Area

Bkgnd

1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32

28.00
30.85
34.98
44.78
52.29
61. 87
65.79
81.11
92.48
111. 83
116.09
160.27
186.50
276.30
302.95
307.35
311.35
314.56
333.56
338.14
356.25
383.93
387.04
391.06
414.92
417.92
421. 86
437.16
445.23
468.33
473.31
511. 41

47
2047
533
25
76
285
118
801
27
227
57
32
24
69
148
25
12
10
78
28
493
130
222
53
47
29
10
96
7
16
13
15

96
71
57
55
97
49
52
135
76
55
71
74
62
28
12
9
7
6
21
20
33
16
8
5
8
9
7
5
7
10
2
2

4
4
4
0
0
2
2
0
0
5
5
0
0
0
2
2
2
2
3
3
0
2
2
2
3
3
3
3
3
0
0
0

C-

7-AUG-2013 10:07:17.63

Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian

FWHM Channel
1. 90
1. 40
1. 93
2.93
3.54
1. 66
1. 67
1. 88
1.14
1.91
2.34
1.67
1. 22
1.54
1. 60
1. 99
1. 99
1. 99
1.88
2.22
1.93
2.06
1. 74
2.06
2.29
2.29
2.30
1. 96
2.32
1. 82
1. 95
3.18

28.32
31.17
35.30
45.10
52.61
62.19
66.11
81. 42
92.80
112.14
116.41
160.59
186.81
276.61
303.26
307.66
311.66
314.86
333.86
338.45
356.56
384.23
387.35
391.36
415.23
418.23
422.16
437.46
445.53
468.63
473.61
511.71

Left

Pw

26
26
26
44
49
58
58
78
90
108
108
158
183
273
298
298
298
298
330
330
351
381
381
381
411
411
411
434
434
465
472
507

18
18
18
5
9
16
16
9
6
15
15
7
7
9
20
20
20
20
17
17
11
18
18
18
14
14
14
20
20
7
6
8

7-AUG-2013 09:51:55.
1.00000E+OO filter
0
BAFIL
0 00:15:05.21 0.6%
4096
10.00000
Cts/Sec %Err

5.26E-02
2.27E+OO
5.92E-01
2.76E-02
8.40E-02
3.17E-01
l.31E-01
8.90E-01
3.00E-02
2.53E-01
6.35E-02
3.50E-02
2.66E-02
7.63E-02
1. 64E-01
2.78E-02
1. 30E-02
1.14E-02
8.65E-02
3.15E-02
5.48E-01
l.45E-01
2.46E-01
5.84E-02
5.22E-02
3.28E-02
1.09E-02
l.06E-01
8.02E-03
1. 78E-02
1. 39E-02
1.65E-02

29.0
2.3
6.6
48.3
26.5
7.1
13.8
4.4
54.3
8.4
30.8
48.5
58.9
18.3
8.7
31. 3
57.5
64.1
14.6
36.4
5.0
10.0
7.7
25.2
19.9
32.8
49.8
11. 8
68.2
41.5
34.4
30.9

Fit
1.22E+Ol

2.00E+OO

8.70E-01

3.0lE+OO

1.37E+OO
4.87E+OO
3.50E+OO
1. 49E+OO

Summary of Nuclide Activity


Sample ID : 1307149-12

Acquisition date

Total number of lines in spectrum


Number of unidentified lines
Number of lines tentatively identified by NID

32
28
4

Page :
2
7-AUG-2013 09:51:55

12.50%

Nuclide Type : FISSION


Nuclide
BA-133

Hlife
10.50Y

Wtd Mean
Uncorrected
Decay pCi/filter
1.00 3.840E+02

Total Activity

3.840E+02

Wtd Mean
Decay Corr
pCi/filter
3.841E+02

Decay Corr
2-Sigma
2-Sigma Error %Error Flags
0.695E+02
18.10

3.841E+02

Nuclide Type : NATURAL


Nuclide
Hlife
TH-234 4.47E+09Y

Wtd Mean
Uncorrected
Decay pCi/filter
1.00 8.511E+02

Total Activity
Grand Total Activity :
Flags: "K"
"E"

=
=

Wtd Mean
Decay Corr
pCi/filter
8.511E+02

8.511E+02

8.511E+02

l.235E+03

l.235E+03

Keyline not found


Manually edited

"M"
"A"

Decay Corr
2-Sigma
2-Sigma Error %Error Flags
15.74
1.340E+02

= Manually accepted
= Nuclide specific abn. limit

~423

Nuclide Line Activity Report


Sample ID : 1307149-12

Acquisition date

Page :
3
7-AUG-2013 09:51:55

Nuclide Type: FISSION


Nuclide
BA-133

Energy
81.00
302.84
356.01

%Abn
33.00*
17.80
60.00

Final Mean for

Uncorrected Decay Corr 2-Sigma


%Ef f
pCi/filter pCi/filter %Error
l.899E+Ol 3.840E+02
3.841E+02 18.10
6.222E+OO 4.000E+02
4.001E+02 26.97
5.860E+OO 4.212E+02
4.212E+02 16.96

3 Valid Peaks

Status
OK
OK
OK

3.841E+02+/- 6.950E+Ol ( 18 .10%)

Nuclide Type: NATURAL


Nuclide
TH-234

Energy
63.29

%Abn
3.80*

Final Mean for


Flag:

11

* 11

Keyline

Uncorrected Decay Corr 2-Sigma


%Eff
pCi/filter pCi/filter %Error
2.648E+Ol 8.511E+02
8.511E+02 15.74

1 Valid Peaks

Status
OK

8.511E+02+/- 1.340E+02 ( 15.74%)

Combined Activity-MDA Report


Sample ID : 1307149-12

Acquisition date

Page :
4
7-AUG-2013 09:51:55

Identified Nuclides
Nuclide
BA-133
TH-234

Activity
(pCi/filter)

Act error

3.841E+02
8.511E+02

6.950E+Ol
1.340E+02

MDA
(pCi/filter)
1.958E+Ol
8.938E+Ol

MDA error

Act/MDA

2.995E+OO
4.801E+OO

19.611
9.522

MDA error

Act/MDA

l.206E+OO
1.387E+Ol
4.273E-02
4.015E-02
4.276E+OO
8.416E-01

0.310
-0.138
0.819
1. 233
0.136
1.916

Non-Identified Nuclides

Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241

Key-Line
Activity K.L.
(pCi/filter)Ided
3.269E+OO
-2.328E+Ol
2.461E+OO
3.482E+OO
7.216E+OO
3.279E+Ol

Act error
6.151E+OO
l.220E+02
1.475E+OO
l.506E+OO
3.624E+Ol
8.325E+OO

MDA
(pCi/filter)
1.055E+Ol
1.682E+02
3.004E+OO
2.823E+OO
5.290E+Ol
l.712E+Ol

VAX/VMS Peak Search Report Generated


Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
Pk It
1
2
3

1
1
0

1
1
1

7
8
9

0
1

10

11

0
0
3
3
3
0
0

12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32

1
1
1
1
1
0
1
1

0
1
1
1

33

2
1
1

34
35

0
0

7-AUG-2013 10:06:34.44

DKAlOO: [GA,MMA.SCUSR.ARCHIVE]SMP_130714913 GE2 BAFIL 194415.CN


PEAK Vl6.9 PEAKEFF V2.2
LR-103 DIS
7-AUG-2013 00:00:00.
1307149-13
FILTER
GE2
0 00:15:00.00
25
3.00000
No

Energy

Area

Bkgnd

30.89
35.01
52.68
61. 76
66.02
71.02
81. 03
93.02
111. 81
116.03
135.00
143.11
161.40
164.40
170.88
186.09
276.71
302.85
307.05
331.06
334.01
337.73
356.05
383.72
386.83
391.00
411.89
414.89
418.07
432.68
437.05
464.97
467.84
511.05
608.41

1798
394
46
189
95
17
716
44
195
42
48
32
29
12
17
24
69
157
27
10
72
27
512
100
170

115
93
72
47
52
54
145
77
65
55
62
39
45
42
37
82
42
9
6
1
8
12
26
18
27
18
2
10

32

: .0

$1
24

87
7

17
25
14

Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian

7-AUG-2013 09:51:15.
1.00000E+OO filter
0

BAFIL
0 00:15:00.28
4096
10.00000

FWHM Channel

Left

Pw

Cts/Sec %Err

1. 38
31. 00
1.39
35.13
1.41
52.79
1.46
61. 87
1. 47
66.13
1. 48
71.13
1. 44
81.15
1. 71
93.13
1. 55 111.92
1. 56 116.14
2.75 135.11
2.56 143.22
1. 96 161.51
1. 97 164.51
1. 98 170.99
1. 22 186.20
2.01 276.82
1. 51 302.95
1.79 307.16
1. 81 331.16
1. 81 334.11
1. 82 337.83
1.37 356.16
1.86 383.83
1. 52 386.94
1. 34 .39+.11
1,71 412.00
1,88 414.99
11 1. 89
418.17
1 2.09 1~2.79
1 1. 88 '. 437.15
6 1.92 465.08
6 . i. 93
467.94
6 2.46 511.16
2 4.63 608.51

26
26
49
59
59
59
76
89
107
107
130
140
157
157
157
182
273
299
299
330
330
330
352
381
381
390
4'.J.l
4l;l.

15
15
7
17
17
17
10
8
18
18
10
7
20
20
20
8
10
11
11
16
16
16

2.5
6.5
33.9
9.1
15.1
62.6
4.9
37.7
9.3
32.9
33.9
37.2
42.6
95.8
66.6
67.9
21.4
8.5
30.8
15.6
13.7
28.3
4.7
13.5
8.8
27.3
14.8
16.3
37.6
28.2
11. 2
70.8
37.3
26.3
30.4

411
432
432

462

462

507
605

2.00E+OO
4.38E-01
5.llE-02
2.lOE-01
1.05E-01
1.94E-02
7.96E-01
4.91E-02
2.17E-01
4.63E-02
5.34E-02
3.50E-02
3.25E-02
1.38E-02
1. 85E-02
2.69E-02
7.67E-02
1.74E-01
3.0lE-02
1.13E-02
8.05E-02
2.95E-02
8 .. 5 , 6 9 E - 01
9/1.llE-01
9,1.89E-01
53.60E-02
l~ 8,98E-03
15 S.64E-02
15 2.63E-02
>9 9;Q2E-03
9, 9,,EiSE-02
9 .. 8.l6E-03
. 9 'i.: B4E-02
8 2.77E-02
7 1.59E-02

0.0%

Fit
6.89E+OO
7.38E-01

2.95E+OO

1.56E+OO

1.19E+OO
5.28E+OO

7.97E+OO
1.37E+Ol
2.66E+OO
l.07E+OO

Summary of Nuclide Activity


Sample ID : 1307149-13

Acquisition date

Total number of lines in spectrum


Number of unidentified lines
Number of lines tentatively identified by NID

35
30
5

Page :
2
7-AUG-2013 09:51:15

14.29%

Nuclide Type : FISSION


Nuclide
BA-133

Hlif e
10.50Y

Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
3.623E+02

Total Activity

---------

3.623E+02

Wtd Mean
Decay Corr
pCi/filter
3.623E+02

Decay Corr
2-Sigma
2-Sigma Error %Error Flags
0.726E+02
20.03

---------

3.623E+02

Nuclide Type : NATURAL


Nuclide
Hlif e
TH-234 4.47E+09Y

Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
6.479E+02

Total Activity
Grand Total Activity :
Flags: "K"
"E"

=
=

---------

Wtd Mean
Decay Corr
pCi/filter
6.479E+02

---------

6.479E+02

6.479E+02

1.0lOE+03

1.010E+03

Keyline not found


Manually edited

"M"
"A"

=
=

Decay Corr
2-Sigma
2-Sigma Error %Error Flags
l.325E+02
20.45

Manually accepted
Nuclide specific abn. limit

E1127

Nuclide Line Activity Report


Sample ID : 1307149-13

Acquisition date

Page :
3
7-AUG-2013 09:51:15

Nuclide Type: FISSION


Nuclide
BA-133

Energy
81. 00
302.84
356.01

%Abn
33.00*
17.80
60.00

Final Mean for

Uncorrected Decay Corr 2-Sigma


%Ef f
pCi/filter pCi/filter %Error
1.799E+Ol 3.623E+02
3.623E+02 20.03
7.560E+OO 3.498E+02
3.498E+02 34.36
7.170E+OO 3.575E+02
3.575E+02 17.87

3 Valid Peaks

Status
OK
OK
OK

3.623E+02+/- 7.259E+Ol ( 20.03%)

Nuclide Type: NATURAL


Nuclide
TH-234

Energy
63.29

%Abn
3.80*

Final Mean for


Flag:

11

* 11

Keyline

Uncorrected Decay Corr 2-Sigma


%Ef f
pCi/f ilter pCi/f ilter %Error
2.305E+Ol 6.479E+02
6.479E+02 20.45

1 Valid Peaks

Status
OK

6.479E+02+/- 1.325E+02 ( 20.45%)

Combined Activity-MDA Report


Sample ID : 1307149-13

Acquisition date

Page :
4
09:51:15
7-AUG-2013

Identified Nuclides
Nuclide
BA-133
TH-234

Activity
(pCi/filter)
3.623E+02
6.479E+02

Act error
7.259E+Ol
1.325E+02

MDA
(pCi/filter)
1.978E+Ol
l.297E+02

MDA error

Act/MDA

3.367E+OO
l.072E+Ol

18.322
4.993

MDA error

Act/MDA

l.508E+OO
l.936E+Ol
l.520E-01
6.665E-02
5.835E+OO
1.374E+OO

-0.180
0.123
3.353
1. 046
-0.169
1.187

Non-Identified Nuclides

Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241

Key-Line
Activity K.L.
(pCi/filter)Ided
-l.767E+OO
2.071E+Ol
2.677E+Ol
3.379E+OO
-8.749E+OO
2.109E+Ol

Act error
5.798E+OO
l.134E+02
3.972E+OO
1.772E+OO
3.738E+Ol
9.342E+OO

MDA
(pCi/filter)
9.818E+OO
1.686E+02
7.983E+OO
3.231E+OO
5.168E+Ol
l.776E+Ol

VAX/VMS Peak Search Report Generated


Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level

DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP_130714914 GE2


PEAK V16.9 PEAKEFF V2.2
PZ-111-KS TOT
7-AUG-2013 00:00:00.
1307149-14
FILTER
GE2
0 00:15:00.00
25
3.00000
No

Pk It

Energy

Area

Bkgnd

3
3
0
2
2
0
0
1
1
0
0
0
0
0
0
0
0
2
2
2
1
1
0
4
4
0

30.92
35.18
52.24
61.78
65.90
81. 08
92.75
108.03
111.77
163.30
237.74
277.05
302.86
307.56
333.96
338.16
356.05
383.70
387.02
391.24
414.72
418.07
436.89
509.72
512.90
595.99

2008
486
83
228
97
811
17
13
170
28
21
64
154
29
70
23
566
101
186
43
45
14
100
32
10
11

115
108
65
70
74
126
80
28
97
86
36
36
27
17
28
16
22
13
8
4
18
33
13
1
2
0

1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26

7-AUG-2013 10:25:12.94

Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian

FWHM Channel
1.43
1.68
1.62
1.60
1. 61
1. 38
1. 30
1. 54
1. 55
4.33
1. 93
1.86
1. 23
1. 55
1. 43
2.45
1. 42
1. 89
1. 87
2.05
1. 88
1. 89
1. 48
2.61
1. 78
3.94

31. 03
35.29
52.36
61.89
66.02
81. 20
92.87
108.14
111.88
163.41
237.85
277.16
302.97
307.66
334.07
338.27
356.16
383.81
387.13
391.35
414.83
418.17
437.00
509.83
513.00
596.09

Left

Pw

26
26
49
57
57
77
90
107
107
158
232
271
300
306
330
337
352
380
380
380
411
411
432
507
507
593

14
14
7
13
13
8
7
9
9
8
9
12
6
4
7
6
8
19
19
19
11
11
8
9
9
7

c:::---

BAFI~~CN

7-AUG-2013 10:09:53.
l.OOOOOE+OO filter
0
BAFIL
0 00:15:00.30 0.0%
4096
10.00000
Cts/Sec %Err

2.23E+OO
5.40E-01
9.17E-02
2.54E-01
1.07E-01
9.0lE-01
1.89E-02
1.42E-02
1.89E-01
3.14E-02
2.36E-02
7.14E-02
1.71E-01
3.25E-02
7.78E-02
2.59E-02
6.29E-01
1.12E-Ol
2.07E-01
4.75E-02
4.98E-02
1. 60E-02
1.llE-01
3.55E-02
1.16E-02
l.22E-02

2.3
5.8
19.6
8.7
17.0
4.3
90.1
69.5
11. 3
60.6
55.3
22.4
9.7
27.1
17.3
35.4
4.4
12.6
9.0
24.5
21. 8
71. 7
11. 7
19.6
57.9
30.2

Fit
7.81E+OO
2.25E+OO

5.27E+OO

3.92E+OO
8.97E+OO
7.28E+OO

Summary of Nuclide Activity


Sample ID : 1307149-14

Acquisition date

Total number of lines in spectrum


Number of unidentified lines
Number of lines tentatively identified by NID

26
22
4

Page :
2
7-AUG-2013 10:09:53

15.38%

Nuclide Type : FISSION


Nuclide
BA-133

Hlif e
10.50Y

Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
4.104E+02

Total Activity

--------

4.104E+02

Wtd Mean
Decay Corr
pCi/filter
4.104E+02

2-Sigma
Decay Corr
2-Sigma Error %Error Flags
19.45
0.798E+02

--------

4.104E+02

Nuclide Type : NATURAL


Nuclide
Hlife
TH-234 4.47E+09Y

Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
7.826E+02

Total Activity
Grand Total Activity :
Flags: "K"
"E"

=
=

--------

Wtd Mean
Decay Corr
pCi/filter
7.826E+02

--------

7.826E+02

7.826E+02

l.193E+03

1.193E+03

Keyline not found


Manually edited

2-Sigma
Decay Corr
2-Sigma Error %Error Flags
19.71
1.542E+02

"M"
"A"

=
=

Manually accepted
Nuclide specific abn. limit

i431

Nuclide Line Activity Report


Sample ID : 1307149-14

Acquisition date

Page :
3
7-AUG-2013 10:09:53

Nuclide Type: FISSION


Nuclide
BA-133

Energy
81. 00
302.84
356.01

%Abn
33.00*
17.80
60.00

Final Mean for

Uncorrected Decay Corr 2-Sigma


%Ef f
pCi/filter pCi/f ilter %Error
1.799E+Ol 4.104E+02
4.104E+02 19.45
7.560E+OO 3.436E+02
3.437E+02 35.60
7.170E+OO 3.949E+02
3.949E+02 17.56

3 Valid Peaks

Status
OK
OK
OK

4.104E+02+/- 7.981E+Ol ( 19.45%)

Nuclide Type: NATURAL


Nuclide
TH-234

Energy
63.29

%Abh
3.80*

Final Mean for


Flag:

11

* 11

Uncorrected Decay Corr 2-Sigma


%Eff
pCi/filter pCi/filter %Error
2.305E+Ol 7.826E+02
7.826E+02 19.71

1 Valid Peaks

Status
OK

7.826E+02+/- 1.542E+02 ( 19.71%)

Keyline

5432

Combined Activity-MDA Report


Sample ID : 1307149-14

Acquisition date

4
Page :
7-AUG-2013 10:09:53

Identified Nuclides
Nuclide
BA-133
TH-234

Activity
(pCi/filter)

Act error

4.104E+02
7.826E+02

7.981E+Ol
l.542E+02

MDA
(pCi/filter)
2.008E+Ol
l.379E+02

MDA error

Act/MDA

3.419E+OO
1.139E+Ol

20.438
5.676

MDA error

Act/MDA

1.363E+OO
1.835E+Ol
1.544E-01
6.696E-02
5.662E+OO
1.520E+OO

-0.168
-0.280
3.194
0.708
-0.096
1. 307

Non-Identified Nuclides

Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241

Key-Line
Activity K.L.
(pCi/filter)Ided
-l.488E+OO
-4.469E+Ol
2.590E+Ol
2.299E+OO
-4.798E+OO
2.567E+Ol

Act error
5.204E+OO
l.183E+02
4.073E+OO
1.852E+OO
3.563E+Ol
l.045E+Ol

MDA
(pCi/filter)
8.877E+OO
1.598E+02
8.108E+OO
3.246E+OO
5.015E+Ol
1.963E+Ol

C-

VAX/VMS Peak Search Report Generated


Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level

~~

DKAlOO: [GA,MMA.SCUSR.ARCHIVE]SMP_130714915 GE3 BAFIL 194419.CN


PEAK V16.9 PEAKEFF V2.2
PZ-111-KS DIS
7-AUG-2013 00:00:00.
1307149-15
FILTER
GE3
0 00:15:00.00
25
3.00000
No

Pk It

Energy

Area

Bkgnd

1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27

30.83
35.07
52.55
61. 86
65.89
80.98
83.68
92.38
111.87
116.41
237.21
242.16
276.49
303.10
312.26
334.91
351.70
356.26
383.83
387.05
391.15
415.04
418.25
421.77
437.30
469.22
511. 52

1928
439
58
182
73
897
16
16
293
52
15
18
58
141
10
55
15
512
91
224
31
52
21
13
104
24
28

89
82
132
151
110
58
50
64
47
39
37
26
23
29
22
44
2
9
8
4
1
9
7
5
5
7
0

4
4
0
0
0
2
2
2
5
5
3
3
0
0
0
0
3
3
4
4
4
4
4
4
0
0
0

7-AUG-2013 10:25:52.62

Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian

FWHM Channel
1. 37
1. 66
1. 51
1. 23
1. 79
1. 59
1.41
1. 72
2.16
2.34
2.11
2.11
1. 28
1. 83
1.43
1. 97
1. 68
1. 54
1. 99
2.04
2.50
2.52
2.52
2.53
1. 97
4.34
3.33

31.15
35.39
52.86
62.18
66.21
81. 29
84.00
92.70
112.18
116.73
237.52
242.47
276.80
303.40
312.56
335.21
352.00
356.56
384.13
387.35
391.45
415.34
418.55
422.08
437.60
469.52
511.82

7-AUG-2013 10:10:29.
1.00000E+OO filter
0
BAFIL
0 00:15:05.66 0.6%
4096
10.00000

Left

Pw

Cts/Sec %Err

26
26
49
59
65
78
78
78
107
107
234
234
274
300
311
329
351
351
381
381
381
411
411
411
435
465
509

16
16
9
6
5
21
21
21
18
18
14
14
6
7
7
9
9
9
18
18
18
18
18
18
9
9
7

2.14E+OO 2.4
4.88E-01 5.8
6.45E-02 37.9
2.02E-01 13.0
8.16E-02 25.0
9.97E-01 3.5
l.73E-02136.8
l.83E-02 77.1
3.26E-01 6.9
5.75E-02 33.5
1.62E-02 66.7
2.04E-02 56.1
6.45E-02 18.5
l.57E-01 10.5
1.09E-02 86.2
6.06E-02 25.9
1.68E-02 7.9
5.69E-01 4.5
1.0lE-01 12.6
2.49E-01 7.9
3.45E-02 39.6
5.77E-02 19.4
2.37E-02 48.3
l.45E-02 62.5
l.15E-01 10.5
2.68E-02 28.1
3.llE-02 18.9

Fit
3.26E+OO

1.07E+Ol
2.60E+OO
2.88E+OO

7.57E+OO
6.19E+OO
2.74E+OO

Summary of Nuclide Activity


Sample ID : 1307149-15

Acquisition date

Total number of lines in spectrum


Number of unidentified lines
Number of lines tentatively identified by NID

27
23
4

Page :
2

7-AUG-2013 10:10:29

14.81%

Nuclide Type : FISSION


Nuclide
BA-133

Hlif e
10.SOY

Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
4.299E+02

Total Activity

---------

4.299E+02

Wtd Mean
Decay Corr
pCi/filter
4.299E+02

2-Sigma
Decay Corr
2-Sigma Error %Error Flags
0.744E+02
17.30

---------

4.299E+02

Nuclide Type : NATURAL


Nuclide
Hlife
TH-234 4.47E+09Y

Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
5.428E+02

Total Activity
Grand Total Activity :
Flags: "K"
"E"

---------

Wtd Mean
Decay Corr
pCi/filter
5.428E+02

---------

5.428E+02

5.428E+02

9.726E+02

9.726E+02

Keyline not found


Manually edited

2-Sigma
Decay Corr
2-Sigma Error %Error Flags
1.459E+02
26.88

"M"
"A"

Manually accepted
Nuclide specific abn. limit

f!.1435

Nuclide Line Activity Report


Sample ID : 1307149-15

Acquisition date

Page :
3
.7-AUG-2013 10:10:29

Nuclide Type: FISSION


Nuclide
BA-133

Energy
81.00
302.84
356.01

%Abn
33.00*
17.80
60.00

Final Mean for

Uncorrected Decay Corr 2-Sigma


%Ef f
pCi/filter pCi/filter %Error
l.899E+Ol 4.299E+02
4.299E+02 17.30
6.222E+OO 3.828E+02
3.829E+02 29.39
5.860E+OO 4.372E+02
4.372E+02 16.34

3 Valid Peaks

Status
OK
OK
OK

4.299E+02+/- 7.438E+Ol ( 17.30%)

Nuclide Type: NATURAL


Nuclide
TH-234

Energy
63.29

%Abn
3.80*

Final Mean for


Flag:

11

* 11

Keyline

Uncorrected Decay Corr 2-Sigma


%Eff
pCi/filter pCi/filter %Error
2.648E+Ol 5.428E+02
5.428E+02 26.88

1 Valid Peaks

Status
OK

5.428E+02+/- l.459E+02 ( 26.88%)

Combined Activity-MDA Report


Sample ID : 1307149-15

Acquisition date

4
Page :
7-AUG-2013 10:10:29

Identified Nuclides
Nuclide
BA-133
TH-234

Activity
(pCi/filter)

Act error

MDA

(pCi/ filter)

MDA error

Act/MDA

4.299E+02
5.428E+02

7.438E+Ol
l.459E+02

1.663E+Ol

1.674E+02

2.543E+OO
8.992E+OO

25.849
3.242

Act error

MDA

(pCi/filter)

MDA error

Act/MDA

5.463E+OO
9.691E+Ol
l.561E+OO
l.517E+OO
2.758E+Ol
l.013E+Ol

9.095E+OO
1.752E+02
3.150E+OO
2.925E+OO
4.936E+Ol
1.776E+Ol

1.039E+OO
1.444E+Ol
4.480E-02
4.160E-02
3.990E+OO
8.732E-01

0.096
0.191
0.827
1. 503
0.120
1.494

Non-Identified Nuclides

Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241

Key-Line
Activity K.L.
(pCi/filter)Ided
8.698E-01
3.349E+Ol
2.606E+OO
4.397E+OO
5.921E+OO
2.653E+Ol

Das könnte Ihnen auch gefallen