EXAMPLE ONLY Positive Material Identification Procedure / Program

(Insert Supplier Name) Positive Material Identification Procedure (Insert #) (Insert Analyzer Make & Model)

Scope
1) This Procedure applies to metallic alloy materials purchased for use by (Insert Supplier Name) or our Sub suppliers, Fabricators, or Subcontractors for ExxonMobil, ExxonMobil Affiliates, or Agents on behalf of either, as it applies to ExxonMobil P 1!"1#"$1 %er &'$'$' (t includes the supply, fabrication, and erection of these materials' #) This Procedure defines the methods to ensure that the nominal chemical composition of alloy materials is in accordance )ith purchase specifications, and that such materials are properly analy*ed and mar+ed to indicate the alloy' &) ,arbon steels are not )ithin the Scope of this Procedure'

This Positive Material Identifi ation Pro edure is provided as an !"AMP#! $N#% to support omplian e &ith !''onMo(il )lo(al Pra ti e )P *+,*-,.* /er 01.1. Positive Material Identifi ation1 The intent is for the Supplier (user) to edit and 2 or modify this do ument spe ifi to the ommodity (ein3 supplied1 Additionally4 there are se tions of this pro edure ((lue te't) that re5uire spe ifi input (y the user that must (e addressed (efore the pro edure is su(mitted for revie& (y !''onMo(il or its desi3nated representative1 6is laimer7 The use of this pro edure in any form does not relieve the Supplier of omplian e &ith !''onMo(il )P *+,*-,.* /er 01.1.1 !'e ution of a su essful Positive Material Identifi ation Pro3ram remains the responsi(ility of the Supplier1
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EXAMPLE ONLY Positive Material Identification Procedure / Program

'ev!

Prepared ()

*ate

+,ec-ed ()

*ate

Approved ()

*ate

.a/le of +ontents Section 1' -e.uired -eferences 1'1 ExxonMobil lobal Practices Page & & &011 & & 2 0 2 3 1 4 1$ 11

1'# ExxonMobil /ata Sheet 1'& AP( " American Petroleum (nstitute 1'2 ASME " American Society of Mechanical Engineers 1'3 ASTM " American Society for Testing and Materials *18 (Insert Supplier Name) 9uality System :ork Pro ess (spe ifi to order) #' /efinitions &' Specific Applicability 2' eneral -e.uirements

3' Acceptance ,riteria 5' Mar+ing 1' Acceptable Methods for PM(

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EXAMPLE ONLY Positive Material Identification Procedure / Program

#!

'e2uired 'eferences

This Section lists Practices and Standards that are generically referenced and assumed to be a part of this document' 6nless other)ise specified herein, use the latest edition'

#!#! E33onMo/il Engineering Practices 4 5lo/al Practices

P 1!"$1"$1 P 1!"1#"$1 P #$"$1"$1 7elding Procedures Positi8e Material (dentification (nspection of E.uipment and Material

#!1! E33onMo/il *ata S,eets

T1!1#$1,$1 Positi8e Material (dentification " Analysis Mode /ata Sheet

#! ! API 6 American Petroleum Institute

API RP 578 Material Verification Program for New and Existing Alloy Piping Systems

#!0! ASME6American Societ) of Mec,anical Engineers

ASME SE, (( A (9T-: ASME SE, (( < (9T-: ASME SE, (( , (9T-: ASME SE, % < S/"1#4 ASME SE, % < S/"!$! Section (( A Ferrous Material Specifications ;<eginning to SA"23$) Section (( < 9onferrous Material Specifications Section (( , Specifications for 7elding -ods, Electrodes, and Filler Metals S/"1#4 Standard Test Method for Sulfur in Petroleum Products ; eneral <omb Method) S/"!$! Standard Test Method for ,hlorine in 9e) and 6sed Petroleum Products ;<omb Method)

#!7! AS.M6American Societ) for .esting and Materials

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EXAMPLE ONLY Positive Material Identification Procedure / Program

ASTM A 14&0A 14&M

Standard Specification for Alloy"Steel and Stainless Steel <olting Materials for =igh Temperature or =igh Pressure Ser8ice and :ther Special Purpose Applications Standard Test Methods, Practices, and Terminology for ,hemical Analysis of Steel Products Standard Test Methods for ,hemical Analysis of Stainless, =eat"-esisting, Maraging, and :ther Similar ,hromium"9ic+el"(ron Alloys Standard Test Methods for ,hemical Analysis of =igh"Temperature, Electrical, Magnetic, and :ther Similar (ron, 9ic+el, and ,obalt Alloys

ASTM A 131 ASTM E &3&

ASTM E &32

:ther ASTM and 9ational Standards, as applicable

*181 (Insert Supplier Name) 9uality System :ork Pro ess (spe ifi to order)
*) A do umented PMI pro3ram shall (e provided to ensure onforman e of omponents to the spe ified omposition for the items listed in Se tion 0 of this do ument1 This pro3ram may in lude se3re3ation pro edures for tested material4 markin34 and2or random samplin31 -) Approval of this pro3ram2pro edure shall (e re eived (in &ritin3) from o&ner1

1!
.erm

*efinitions
*efinition Each indi8idual component and )eld is tested' A test carried out on a +no)n standard alloy to 8erify the performance of the instrument'
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#""8 Positive Material Identification +,ec- 9instrument performance:

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EXAMPLE ONLY Positive Material Identification Procedure / Program

.erm Inspection Lot

*efinition 7ith the exception of bolting, an inspection lot is a group of components from the same heat number or heat treatment batch, from )hich a sample is dra)n' For bolting, a lot is a group of similar components in terms of alloy type and si*e' A detailed set of instructions defining the order of precedence to be follo)ed for the successful execution of a Positi8e Material (dentification ;PM() Plan' The program shall include the structure, process, and procedure to control operations, manage change, and define ho), )hen and )here Positi8e Material (dentification ;PM() is to be employed for compliance )ith the program ob>ecti8es' A procedure is defined as a specified series of actions, acts, or operations that ha8e to be implemented in a specific order to continuously obtain the same Positi8e Material (dentification ;PM() results under the same circumstances' (t shall include a se.uence of acti8ities, tas+s, steps, decisions, calculations and processes, that )hen underta+en in the se.uence prescribed )ill produce the desired PM( analysis' Mar+ings used to identify components )hich ha8e been tested and confirmed to be acceptable' A procedure used to ensure that specified metallic alloy materials are? properly identified as to alloy type, mar+ed according to :)ner@s procedures, installed as intended' PM( testing of a sample, )hich consists of one or more pieces ;components), selected at random from an inspection lot, )hich )ill be examined to determine acceptability of the inspection lot' The si*e of the representati8e sample, and the maximum number of defecti8e parts allo)ed, shall pro8ide 4$ percent confidence that not more than 3 percent of the entire lot is defecti8e, )ith the follo)ing minimum sample si*es satisfying this re.uirement if no defecti8e parts are found?
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PMI Program

PMI Procedure

PMIV 9PMI Verified: AV 9Allo) Verified: Positive Materials Identification 9PMI:

'epresentative Sampling

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EXAMPLE ONLY Positive Material Identification Procedure / Program

.erm

*efinition 1$$ percent for a lot of #! pieces or lessA #! pieces for a lot of 3$ pieces or less, &! pieces for a lot of 13$ pieces or less, and 23 pieces for a lot of &,$$$ or less'

.racea/le Mill +ertificate

A document that permits each component to be identified according to the original heat or material from )hich it )as produced'

! Specific Applica/ilit) (Supplier may edit (add 2 delete) items in this se tion as appli a(le to spe ifi s ope of supply)
1) The follo)ing metallic"alloy"material items re.uire 1$$ percent Positi8e Material (dentification ;PM()? a) All pressure"containing )elds' For double )elded >oints, both )eld caps, inside and outside, )hen accessible' :n internally clad or o8erlaid 8essels, the inside )eld cap shall be PM(@d before bac+ cladding and the result recorded on an as built and mapped 8essel dra)ing' b) All Pressure"containing piping components, including the follo)ing? c) Thermo)ells d) (nstrument manifolds e) <raided alloy"reinforced hoses in the ser8ice of ha*ardous or corrosi8e materials as designated by the :)ner@s Engineer f) Pressure"containing components of heat exchangers ;to include the plates for plate and frame heat exchangers, except components per Section &, (tem ;#)) and other pressure 8essels' g) Plate material used as Pressure"containing components' h) Pressure"containing machinery components ;e'g', pump casings, compressors, and process expansion dri8ers)' i) Pressure"containing instrument housings in alloy piping circuits that cannot be isolated from the process en8ironment, or housings )ith a design pressure abo8e 4$$ psig ;e'g', gauge glass housings, orifice meter tubes)' >) External 8al8e components ;body, flanges, bonnet, plugs, and 8ents, and associated )elds)' +) Expansion >oints and bello)s in Pressure"containing ser8ice'
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EXAMPLE ONLY Positive Material Identification Procedure / Program

l) Pressure"containing tubing )hich cannot be isolated from the process en8ironment Bexcept as excluded in Section &, (tems ;#) and ;2)C' m) Fired heater coils including all )elds on alloy tubes and air"cooled heat exchanger tubes ;air fin tubes)' n) Except for tubular products co8ered by Section &, (tem ;#a) and bolting co8ered by Section &, (tem ;#c), items designated for representati8e sampling PM( but )hich ha8e no alloy type identification ;i'e' permanent mar+ing) shall be 1$$ percent PM( 8erified' o) Any other components or materials specifically designated for PM( on the Purchase Specification' #) The follo)ing items re.uire PM( on a representati8e sampling basis, as a minimum, unless specifically exempted on the Purchase Specification? a) Tubular products used in the fabrication of e.uipment, such as heat exchangers and boilers, pro8ided that traceable mill certification is a8ailable' b) Fired heater, heat exchanger, and boiler internals ;tube hangers, tube supports, and tubesheets)' c) All ASTM A 14&0A 14&M rade <15 and alloy stud bolting, except as excluded in Section &, (tem ;2>)' d) -ing >oint flange and clamp type ;e'g', rayloc) connector flange gas+ets' e) Sheet products used in the fabrication of e.uipment, such as )elded plate and frame, pro8ided that traceable mill certification is a8ailable' &) (nternal metallic lining0cladding and )eld o8erlay used for protection against corrosi8e en8ironments shall be tested as follo)s? a) (ntegral cladding? 1$$ percent' :ne inspection for each clad component' b) 7eld o8erlay, bac+cladding, and applied linings as specified in P 1!"$1" $1 shall be tested before post)eld heat treatment' 2) The follo)ing items are exempt, unless specifically designated for PM( on the Purchase :rder? a) Alloy components, )here the alloy is installed for product purity consideration only' :)ner shall specify PM( re.uirements if special alloy re.uirements are needed for en8ironmental concerns' b) (nternal machinery parts' c) (nternal instrument parts, including orifice plates' d) Electrical components'
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EXAMPLE ONLY Positive Material Identification Procedure / Program

e) 9on"pressure"containing )elds' f) Stainless steel instrument tubing and copper tubing )ith an outside diameter of &02 in' and less, )hen properly identified by paint stencil ;exchanger tubing is not included in this exemption)' g) Stainless steel instruments installed in carbon steel piping circuits' h) ,ompression"type ferrules fittings and components ;e'g', 8al8es, filters, etc') for use )ith &02 in' outside diameter and smaller tubing' i) Steam tracing, instrument air, and hydraulic tubing' >) All ASTM A 14&0A 14&M rade <1 bolting' +) All gas+ets, except as re.uired by Section &, (tem ;#d), or :)ner@s -epresentati8e, based on criticality of ser8ice' 3) The follo)ing items re.uire PM( on a representati8e sampling basis, as a minimum, and are not exempt under any circumstance? a) (nternal non"pressure"containing parts' b) Metallic alloy components for refractory linings ;e'g', refractory anchors and hex mesh) shall be co8ered under this re.uirement'

0! 5eneral 'e2uirements
1) (Insert Supplier Name) and our subsuppliers shall pro8ide a PM( program ;including a detailed PM( procedure) to comply )ith the re.uirements of P 1!"1#"$1 and0or as specified by :)ner@s Engineer' #) :)ner@s Engineer appro8al of the PM( program0procedure shall be obtained prior to the start of fabrication' :)ner@s (nspector shall )itness tests and perform audits to ensure that PM( program re.uirements are met' :)ner@s Engineer appro8al of the PM( program shall be obtained prior to the start of fabrication' The :)ner@s (nspector shall )itness the first article and 1$ percent random sampling of all remaining PM( testing thereafter' (t is (Insert Supplier Name) responsibility to ensure that implementation of the PM( program is in accordance )ith this P 1!"1#"$1' &) -ecords of PM( results shall be pro8ided to :)ner@s Engineer as part of the As"<uilt documentation'
a

For fabricated or assembled e.uipment, these records shall include an itemi*ed list of all components and )elds on /ata Sheet T1!1#$1,$1, or its e.ui8alent'
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EXAMPLE ONLY Positive Material Identification Procedure / Program

b) Tabulation of tested items shall be +eyed to As"<uilt dra)ings through the use of reference numbers' c) Positi8ely identified materials shall be traceable to any re.uired material documentation, such as mill test reports' d) (Insert Supplier Name) report of alloy 8erification shall be submitted to :)ner@s Engineer for re8ie) upon completion of the e.uipment' 2) Materials re.uiring PM( Bper Section &, (tems 1, #, &, and 3C shall be analy*ed using an acceptable method as defined in this Practice' a) (nstruments shall be used in an analysis mode' The accuracy of the instrument shall be chec+ed by measurement against a +no)n standard of each alloy type' Measured 8alues shall meet acceptance criteria per Section 3' b) (nstruments may be used in an alloy identification or alloy matching mode, )hen appro8ed by :)ner@s Engineer' Follo)"up analysis is re.uired )hen alloy identification does not comply )ith the specified alloy' 3) 7hen 1$$ percent PM( is re.uired per Section &, (tem ;1), PM( testing shall be performed according to one of the follo)ing? (Supplier may edit items a4 (4 (elo& appli a(le to the spe ifi s ope of supply) a) :n all components and )elds, )hen the e.uipment ;e'g', pipe spool, 8essel, heat exchanger or heater) has been completely fabricated, but may be performed prior to P7=T' b) b) :n indi8idual components prior to fabrication pro8ided that they are both PM(% and alloy type mar+ed' Follo)ing fabrication, all )elds shall be PM( inspected per Section 2, (tem ;1)' Alloy type mar+ing shall meet the same re.uirements as described for PM(% mar+ing in Section 5' c) :n each indi8idual section of reinforced hose re.uiring PM( ;Section &, (tem ;1b'iii)) prior to installation' Sections )ill be mar+ed PM(% 0 A%' 5) 7here representati8e sampling is allo)ed, pieces may be tested upon receipt' Such pieces shall be mar+ed PM(% ;Positi8e Materials (dentification %erified) or A% ;or Alloy %erified)' (tems from the same lot that are not tested shall be mar+ed PM(' a' (f any piece from the representati8e sample that is unacceptable, each piece of the lot shall be examined' b' 7hen a lot is found to contain unacceptable pieces, 1$$ percent of the next t)o lots from the same Supplier 0 sub supplier shall be examined' (f
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EXAMPLE ONLY Positive Material Identification Procedure / Program

both lots are acceptable, or )hen t)o successi8e lots are acceptable, the sampling procedure defined in Section # may be resumed' 1) All )elds re.uiring PM( shall be PM( inspected, identified in the data and documentation records, and mar+ed PM(% or A%' Prior to heat treatment, painting, or insulating, Duality ,ontrol shall 8erify that materials ha8e been installed in accordance )ith the Specification' 7elds re.uiring PM( shall be inspected according to the follo)ing? a' !" c' d' Automated )elding? :ne sample from each girth or long seam' Manual )elding? T)o samples from each girth section #2 in' diameter' Manual )elding? :ne sample from each girth seam E #2 in' diameter' Autogenously )elded pipe and fittings? PM( 8erification of only the base metal is re.uired' e' 7eld repair? :ne sample PM( testing per #2 in' of length for each )eld repair' !) 7eld ,onsumables? a' Prior to use in fabrication, sample buttons shall be )elded using each heat of bare )ire and lot of co8ered or flux"cored electrodes, and PM( tested in accordance )ith this procedure' A button of bare )ire is not necessary if the PM( instrument can examine )ire' <utton si*e shall be a minimum 1'$ inch diameter ;#3'2 mm) )ith a minimum &0! inch ;'&13 inch 04'3 mm) thic+ness of deposited )eld metal' b' After successful PM( .ualification, all )elding consumables used for fabrication shall be segregated and uni.uely identified from all other )elding materials in the shop' c' A list of acceptable material heat, lot, and batch numbers shall be de8eloped and clearly identified on the documentation accompanying each 8essel in the shop' d' (f the alloy is incorrect, the entire heat or lot shall be re>ected'

7!

Acceptance +riteria

All materials re.uiring PM(, acceptance criteria shall be as follo)s?

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EXAMPLE ONLY Positive Material Identification Procedure / Program

1) Analysis Mode Examination? the measured 8alue of alloying elements shall be )ithin 1$ percent of the specified le8el or range in the applicable materials standards ;example? for 3 ,r, )here the allo)able range is 2 " 5 percent, the measured 8alue shall fall )ithin the range &'5 to 5'5 percent)' -e.uirements for minor alloying elements are defined in Table 1 notes' #) Alloy (dentification or Alloy Matching Mode Examination? the instrument shall confirm that alloys comply )ith the specified standard, )ithin the accuracy gi8en in Section 3, (tem ;1)' &) Test results shall conform to purchase documents and be properly identified to the applicable materials specifications' Materials shall be color coded in accordance )ith :)ner@s Specification, and mar+ed per Section 5, of this Practice 2) For )eld metal PM( testing, or >oints of similar base metals )ith matching filler, the acceptance criteria are based on the re.uirements of ASME Section ((, Part , ;ASME SE, (( , (9T-:)' 3) 7hen PM( test results indicate that the component is not the specified material, the item shall be re>ected' a' 7hene8er materials are identified as incorrect, Duality ,ontrol shall issue re>ection note indicating unacceptable materials ha8e been supplied' b' 6nacceptable material shall be replaced )ith the correctly specified material and PM( shall be performed on all replacement materials' c' Material re>ected by PM( shall be mar+ed by Duality ,ontrol to designate re>ection using indelible in+ or paint' The re>ected items shall be held in a designated area to prohibit their re"use' d' (f the PM( test results fall outside the acceptable range, using the standard instruments described in this Practice, a .uantitati8e chec+ analysis may be performed by an independent testing laboratory' (f no method is referenced in the applicable materials standard, an appropriate method of chemical analysis, as specified in this Practice, shall be used' -esults of this analysis shall go8ern'

%!

Mar-ing

1) Each component ;or )eld) shall be mar+ed immediately after PM( inspection and acceptance' Mar+ings shall be permanent and readily 8isible' These mar+ings shall be in addition to mar+ings re.uired by applicable ,odes' For
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EXAMPLE ONLY Positive Material Identification Procedure / Program

the purpose of this document immediatel) is defined as completion of the physical test on the component or )eld and 8erification that the component or )eld meets the specified chemistry' #) Each component or )eld analy*ed shall be mar+ed )ith the FPM(%F or FA%F code letter symbol, using a lo) stress stamp or other mar+ing appro8ed by :)ner' A permanent dye or paint may be used to mar+ bolts and tubing' The mar+ing shall be placed as follo)s? (Supplier may edit 2 delete items (elo& that are not appli a(le to the spe ifi s ope of supply) a) Pipe shall ha8e t)o mar+s, 1!$ degrees apart, 13 mm ;& in') from each end of each length on the outer surface of the pipe' b) 7eld mar+s shall be placed ad>acent to the )elder@s mar+, directly on the )eld' 7elds on tubes in heat transfer shall not be stamped, but mar+ed by either stenciling or 8ibro"etching c) 7eld o8erlay and bac+clad material )ill ha8e Positi8e Materials (dentification noted on As"<uilt dra)ings' Mar+ing of 8essel e.uipment is not re.uired' d) Fittings and forgings shall be mar+ed ad>acent to the supplier@s 0 sub supplier@s mar+ings' e) %al8es shall be mar+ed ad>acent to the supplier@s 0 sub supplier@s mar+ings on bodies and other pressure parts f) Plates shall be mar+ed ad>acent to the heat numbers' e) ,astings shall be mar+ed ad>acent to the supplier@s 0 sub supplier@s mar+ings and heat numbers' g) Tubes for =eat Transfer Ser8ice shall be stenciledGnot stampedG&$$ mm ;1# in') from each end' i) The mar+ing shall be done )ith a (Supplier to insert spe ifi produ t name) )hich is a )ater"insoluble material that contains no harmful substance, such as metallic pigments ;aluminum BAlC, lead BPbC and *inc BHnC, sulfur or chlorides), that )ould attac+ or harmfully affect austenitic or nic+el alloy steels at ambient or ele8ated temperatures'
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EXAMPLE ONLY Positive Material Identification Procedure / Program

ii) The chloride and sulfur content of )ater insoluble materials shall be limited to one percent or less as determined by ASME SE, % < S/" !$! and ASME SE, % < S/"1#4, or e.ui8alent' iii) Analysis of the mar+ing material )ill be pro8ided to the purchaser to demonstrate, by chemical analysis and history of use, that the mar+ing material meets these re.uirements' (Supplier to in lude analysis of produ t &ith su(mission of ompleted PMI pro edure)
i) Supplier shall submit an analysis of the mar+ing material to the

purchaser to demonstrate, by chemical analysis and history of use, that the mar+ing material meets the re.uirements' i) <olting shall be mar+ed on one end' >) 9uts shall be mar+ed on one flat' &) (f the material or item is too light, too small, or cannot other)ise be stamped, 8ibro"etching or color"coding shall be applied' Such shall be noted on the PM( 0 Alloy %erification -eports' 2) 7hen heat treatment is performed after material 8erification, the identification mar+ing shall be recogni*able after such heat treatments' (f the mar+ing is unrecogni*able, PM( testing shall be repeated' 3) 7hen an alloy pipe or plate is cut after PM( testing and mar+ing, the mar+ing shall be transferred onto the unmar+ed section as described in this Section'

$!

Accepta/le Met,ods for PMI

1) Positi8e Materials (dentification ;PM() shall 8erify that the alloy is as specified' Elemental analysis )ill confirm the minimum elements to be tested for each alloy type listed in Table 1' For alloys not included in Table 1, :)ner shall submit proposed elements' The instrument employed shall be used to 8erify the ma>or alloy constituents of the material'

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EXAMPLE ONLY Positive Material Identification Procedure / Program

.a/le #< Identification Elements 9#:

Materials , " 10# Mo 1 ,r " 10# Mo 1102 ,r " 10# Mo # 02 ,r I Mo 3 ,r " 0# Mo 1 ,r " 0# Mo 4 ,r " 1 Mo 1# ,r ;Type 2$3021$S) 1# ,r ;Type 21$) 11 ,r ;Type 2&$) #3 ,r ;Type 225) &$2 &$2J &$2= &$4J &$4 ,bJ &1$ &150&11 &15J0&11J &#1 &21
1 1 1

Identification Elements Mo ,r, Mo ,r, Mo ,r, Mo ,r, Mo ,r, Mo ,r, Mo ,#$ , ,r ,r ,r ,r ,r, 9i ,#$ , ,r , 9i ,#$ , ,r, 9i ,#$ , ,r, 9i ,#$ , ,r, 9i, ,b ,r, 9i ,r, 9i, Mo ,#$ , ,r, 9i, Mo ,r, 9i, Ti ,r, 9i, ,b

Materials Alloy #$,b"& <rass, Admiralty <rass, 9a8al <rass, Aluminum 4$01$ ,u09i 1$0&$ ,u09i Alloy 2$$ Titanium rades 1 and #

Identification Elements ,#$ , ,r, 9i, Mo, ,b, ,u Sn Sn Hn, Al ,u, 9i ,u, 9i 9i, ,u Ti Ti, Mo#$, 9i#$ Ti, Pd#$ Ti, -u 9i, ,r 9i, ,r 9i, ,r, Mo, ,b, Ti 9i, ,r, Al, Ti 9i, ,r, Mo, ,u, Ti ,#$ , ,r ,#$ , ,r, 9i ,r, 9i, Mo ,r, 9i, Mo 9i 9i, ,r, Mo, 7 9i, Mo

rade 1# Ti rade 15 Ti rade #5 Ti Alloy 1!# Alloy 5$$ Alloy 5#3 Alloy !$$ Alloy !#3 A(S( 212$ A(S( 2&2$ Alloy ##$3 Alloy #3$1 &'3, 3 and 4 9i =astelloy ,#15 ASTM A3&& rades <, ,, and /

Notes to .a/le #<

;1) ;#)

Acceptance criteria for (dentification Elements shall be per Section 3, (tem ;1)' :)ner@s Engineer shall specify re.uirements for minor alloying elements ;e'g', lo) carbon in Type &$2J SS or Type 21$S SS, minor alloying elements in 8arious grades of titanium) using guidance in Section 1 (tem ;2f)'

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EXAMPLE ONLY Positive Material Identification Procedure / Program

#) (nstruments or methods used for examination )hen used in either the element analysis or alloy identification mode shall include? a) Testing shall be performed according to the alloy analy*er Manufacturer@s procedures' :)ner@s Engineer shall appro8e any modification of such procedures' b) Each analy*er shall be calibrated according to (Supplier insert name of manufa turer) re.uirements' At the beginning and end of each shift, the instrument shall be chec+ed at least three times against a +no)n standard for each alloy type to be inspected during the shift, using the method to be used during the shift' This chec+ shall be performed under en8ironmental conditions similar to the test location' c) Accuracy as measured against the standard shall meet re.uirements in Section 3, (tem ;1)' 0) (Supplier to insert spe ifi details of 5ualifi ation re5uirements for the PMI te hni ians4 in ludin3 trainin3 and e'perien e1) 2) PM( shall be conducted using e.uipment appro8ed by :)ner@s engineer' The follo)ing are re.uirements to obtain appro8al' a) E.uipment shall be one of the follo)ing de8ices suitable for the elements to be determined as re.uired in Table 1' 6se of .uantitati8e, portable K"ray fluorescence analy*ers per AP( -P 31! paragraph 3'#1 ii) 6se of portable optical emission analy*ers per AP( -P 31! paragraph 3'##
i

b) E.uipment shall ha8e demonstrated as per Section 3 (tem ;1), L0" 1$M accuracy of the actual 8alue for all elements analy*ed' This shall be documented )ithin the submitted procedure )ith example data results for alloy element combinations re.uired for the proposed >ob c) (f the :)ner@s Engineer is not satisfied )ith the submitted de8ice information for appro8al' A procedure for further .ualification of instruments may be pro8ided by the :)ner@s Engineer' d) ,are shall be ta+en to not damage critical surfaces ;e'g', bearings))hen using optical emission analy*ers'

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EXAMPLE ONLY Positive Material Identification Procedure / Program

e) Analytical laboratories using K"ray fluorescence spectrometry, optical spectroscopy, or )et chemical analysis shall be used for 8erification in cases )here test results by other methods differ from Mill ,ertificate data' f) Suitable methods for identifying minor elements include? speciali*ed laboratory instrumentation, suitable optical emission analy*ers, traceable mill certificates, or a combination of traceable mill certificates and chemical analysis using lo)er measurement sensiti8ity' 3) The :)ner@s Engineer may appro8e PM( methods other than those listed in Section 1, (tem ;2) ;e'g', magnetic) for austenitic stainless steel ;e'g', &$2SS or &15SS) base metal in cryogenic ;and non"corrosi8e) ser8ice'

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E33onMo/il

EXAMPLE ONLY Positive Material Identification Procedure / Program

=AI 1"4"#4#0

.ec,nical *ata S,eet 9.#;#1"#+"#: Positive Material Identification Anal)sis Mode *ata S,eet 4 +ustomar)/Metric >nits
?a/ricator< Location< @o/ .itle< @o/ Num/er< *raBing Num/er< E33onMo/il Purc,ase Order No!< Material Specification/5rade< *ate < Inspection Agenc)< Operators< Anal)Aer Model Num/er< Anal)Aer Serial Num/er< +d4#"& Source Age< ?e477 Source Age< ALLOY +ON.EN.C D.8
Specification 'ange Standard +omponentF Min! Ma3! I!*! I!*! +r Mo Ni N/ .i Accept 'eEect

N F,omponentF refers to the specific elbo) fitting, pipe segment, plate, etc' being inspected' 'evision Log -e8 1 # & /ate Apr8l /escription e 8 2 3 /)g' 9o'? /at e A pr 8l /escription

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