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AA-6800 Series
Shimadzu
Atomic Absorption Spectrophotometers
Ta k i n g i t t o t h e p i n n a c l e . . . .
AA-6800 Series
AA-6800 Series
Shimadzu Atomic Absorption Spectrophotometers
Taking it to the pinnacle....
The demands of wide-ranging analyses now performed in various fields are pushing the
envelope of instrument functionality. Instrumentation must be capable of performing many tasks,
from routine analysis to Research and Development. Enhanced functions must provide benefits
to the customer for a user-friendly environment. In AA analysis, Shimadzu has always been at
the forefront of increasing sensitivity and precision, as well as incorporating automation and
labor-saving technology. The latest embodiment of Shimadzu's original labor-saving and multitasking functionality is included in the AA-6800 Series Atomic Absorption Spectrophotometer.
Numerous features, such as the "WizAArd" software, guide the user through a simplified
parameter setup. The unsurpassed basic performance of the AA-6800 Series, along with the
multi-tasking functionality and ease of operation provided with WizAArd, satisfies the wideranging analytical needs of demanding customers.
AA-6800 / "WizAArd" Software
Wizard functions
Supports GLP/GMP
Easy-to-read MRT worksheet
QA/QC functions incorporated
Contents
Wizard functions
Supports GLP/GMP
Easy-to-read
MRT worksheet
QA/QC functions
incorporated
P 12 - Flame Atomizer
P 18 - Specifications
P 06 - WizAArd Software
P 14 - Automated Sampling
Atomizer drive
Flame/Furnace switching
Atomizer optimum condition search function
AA-6800 Series
Computer control
Computer control
Burner height / fuel gas flow rate
Environmental
Ocean water
River and stream water
Wastewater
Sludge
Suspensions
Petroleum
Oil
Catalysts
Synthetic products
Foods
Metals
Ores
Glass
Ceramics
Blood
Biological organisms
Plants
Drugs
OIL
Standard Unit
Auto Sampler
Flame System
AA-6800F
ASC-6100
Add GFA-EX7
Add ASK-6100
Furnace System
AA-6800G
GFA-EX7
ASC-6100
ASK-6100
Add ACF-6800
Full System
(Flame and Furnace)
AA-6800F
GFA-EX7
ASC-6100
ASK-6100
fields.
Fe a t u re s
Windows fully supported " WizAArd" software
Leave it to the Wizard to set the analysis parameters. Become an expert as the Wizard guides you through the
procedure. Raw data is maintained in accordance with GLP. Measurement procedures, results, pretreatment
conditions and the measurement screen are all combined into a single MRT (Measured Results Table) worksheet,
so all information about the sample can be viewed at a glance.
QA/QC functions incorporated (flame/furnace)
With QA/QC functions like the calibration curve correlation coefficient check, spike and percent recovery of Preand Post-Digestion Spikes, and QC checks for Laboratory Control Samples (LCS), the WizAArd produces reliable
data. All QC functions have user-selectable ranges of PASS/FAIL and automatic reporting of "OUT OF CONTROL
REMARKS," with opportunities to select the appropriate action to be taken.
Newly designed flame atomization unit
The AA-6800 series is equipped with a standard titanium burner head, a ceramic impact bead and a high-density
polypropylene spray chamber. The new spray chamber has a specially processed internal surface, virtually
eliminating decomposition due to acids, organic solvents, and other chemicals. The high-sensitivity, high-precision
nebulizer is a single unit with an easy-to-maintain impact bead. In the AA-6800, the Japanese Patented dualatomizer system switches automatically at your command from flame to furnace.
Superior high-sensitivity analysis
Flame analysis: better than 0.32 Abs. for 2 ppm of Cu (Typical); furnace analysis: better than 0.20 Abs. for 20L of
1ppb Mn (Typical).
Safety features for peace of mind
Automatic safety mechanisms, such as gas leak check, flame monitoring, gas pressure monitoring, drain level
monitoring, power monitoring, use of wrong burner head, and automatic Air/N2O switching, are all incorporated
with the AA-6800. The automatic data-save function protects against important data loss in the event of sudden
power outages.
Loaded with other functions
Wi zA Ard S oft w a r e
in Windows
After the analytical conditions are set, communication
is established between the instrument and the PC.
Click the Next > button to proceed to the next
window.
Wi zA Ard S oft w a r e
The most recent 4 data sets are normally displayed; however, any saved
data set can be displayed. Overlaid display of selected data is possible.
A quick visual comparison: the current sample absorbance against the calibration curve
After setting up the measurement sequence, simply press the START button.
Find it all here: the MRT worksheet
GFA-E X 7 G r a p h i t e F u r n a c e A t o miz e r
Sensitivity
Improved !
Conventional GFA
Pb
0.12 ppb
Mn
0.02 ppb
Improvement
0 ppb
2 ppb
4 ppb adjunction
Digital temperature control: Optimal heating control achieved at all temperature regions using computer
control.
Thanks to the use of an electronic flow controller, the accurate flow rate of
the inner gas can be set in units of 0.01L/min. at each heating stage, which
means effective gas flow-rate control can be accurately performed when
background elements are being removed during ashing.
10
Prolonged tube lifespan: The tube has a more than sufficient lifespan even when used in continuous automatic
analysis of various elements and various samples.
Drying stage: The deterioration status of the graphite tube is automatically checked, and the Al function
automatically calibrates the sample drying temperature.
Heating program
1. 100C 30 sec
2. 500C 10 sec
3. 2700C 5 sec
40
30
Graphite tube
Temperature (C)
100
50
0
100
200
300
400
500
600
Heating frequency
11
Fla m e Atom i z e r
Safety measures
1. Automatic gas leak check system (Japanese Patent 1501632)
6. Momentary power failure detection system and safety measures for re-ignition
12
Automation, labor-saving
Loaded with optimum automated analysis functions for routine analysis
13
Au tom ated Sa m p l i n g
3 Random-access function
14
pretreatment functions
sample concentration in furnace
4 Automatic
(graphite furnace analysis)
15
Ba ck G round C o r r e c t i o n M o de s
Lamp current
IH spectrum
Background absorption
Background absorption
Atomic absorption
Atomic
absorption
IH
Wavelength
IL spectrum
IL
Wavelength
absorption
layer
Atomic
absorption
Background absorption
Atomic absorption
time
16
sec
0.00
True atomic
absorption
after correction
5.00
-0.300
-0.140
Background absorption
0.020
0.180
0.340
0.500
Abs
D2 lamp spectrum
Background absorption
Atomic
absorption
sec
0.00
True atomic
absorption
after correction
5.00
-0.100
0.128
0.340
Background absorption
0.560
0.780
1.000
Abs
17
Spe ci fi cati on s
Specifications
Data Processing
Lamp
Spectrophotometer
Baseline correction
Sensitivity correction
Tabular data processing
Multi-tasking
Recall of parameters
Procedure/result display
Report generation
QA/QC
Power requirements
Dimensions and weight
Ambient temperature
Ambient humidity
Burner unit
Specifications of AA-6800F
Type
Burner head
Nebulizer
Chamber
Positioning
Gas control
Safety measures
Safety features
Cooling water
Gas
Power requirements
Connection
Power Supply Unit Dimensions and weight
18
Zero-point detection
Auto rinse
Auto diagnosis
Random access
Reagent : 8 positions
Samples : 60 positions
(random access available with reagents or samples)
Sample volume
Nozzle rinse
Rinse water bottle
Power requirements
Dimensions, weight
Sample vials
: 16 mL (test tube for flame analysis), 2 mL (sample cup for furnace)
Reagent vials
: 20 mL (for furnace analysis)
Solvent container : 2000 mL
Solvent rinse discharge method (for furnace analysis)
Solvent aspiration rinse method (for flame analysis)
2L capacity
AC100 V ~ 240 V auto switching, 100 VA, 50/60 Hz
ASC-6100: 330W x 280D x 285H mm, 7.5 kg
ASC/ASK combination: 360W x 280D x 360H mm, 15 kg
Furnace Specifications
Carryover
Mixing function
Maximum number of
mixing reagents added
If the measured results exceed the range of the calibration curve, the software automatically calculates the
appropriate dilution factor and executes re-analysis, so that the measured volume is at the mid point of the calibration
curve. If dilution factor is not available, samples are diluted to 10 times.
Sampling functions
Syringe
Injection volume
Repeatability
Sensitivity Example
Typical Sensitivity (Abs.)
NOTE) The PC, monitor and printer are not included in the standard configuration.
The ASC-6100, ASK-6100 and GFA-EX7 are optional accessories.
Windows is a trademark of Microsoft Corp., U.S.A.
19
Par ts and Ac c e s s o r i e s
Quantity
1
1
1
1
Cat. No.
206-64902
206-13774
206-50733-91
200-79144-01
note) The PC, monitor, printer, hollow cathode lamps, high-temperature burner head,
pressure regulator and compressor are not included in the standard configuration.
Quantity
1
1
1
5
1
Cat. No.
206-50389-91
206-50389-92
201-79229-01
204-05899-01
202-38757-01
1
1
1
1 (0.3 m)
204-27570-02
086-11002
206-63686
200-31328-01
1
1 (2.4 m)
1 (2.4 m)
1
206-65112
016-31350-22
016-31409
206-80771-91
Quantity
1
1
1
1
Cat. No.
206-51010
206-51011
206-51014-91
206-50389-91
1
1
1
1
2
1
1
206-51028-91
206-64752
086-03016
086-03818
035-68907
206-50325-91
206-51074
NOTE) Graphite tubes, micro pipettes and pressure regulating valve for argon gas are not included in the
standard configuration.
20
Optional Accessories List (In detail, please refer to AA Series Accessories (C122-E031) brochure .)
For Flame Analysis
Part Name
ACF-6800 Furnace-to-Flame conversion unit
High-temperature burner head (titanium)
Low-noise air compressor
Air compressor
Cat. No.
206-64843-92
206-50300-92
208-91750-**
208-91742-91
206-52458-91
040-72020-01
040-72019-01
040-72019-11
040-72019-21
Required at the time of air compressor use other than the above
For C2H2*
For H2*
For N2O*
For Ar*
Remarks
Cat. No.
206-51000-00
206-50587
206-50588
206-50887-02
044-01809-03
206-84373-91
206-86147-91
Remarks
Cat. No.
200-38422200-38456-
For SR Method
Cat. No.
204-21932-01
206-17143-
(NOTE 1, 2)
(NOTE 3)
Remarks
Other Accessories
Part Name
MVU-1A Mercury Vaporizer Unit
HVG-1 Hydride Vapor Generator
Remarks
NOTE) 1. Gas flow cell (Cat. No. 201-98687), Cell holder (Cat. No. 202-35867), and Hg Hollow cathode lamp (Cat. No. 200-38422-28 ) are required.
2. Adapter, MVU-6800G (Cat. No. 206-51145-91) is required for connection with the furnace system AA-6800G.
3. Automated analysis is made possible by using ASC-6100 and Nozzle Assy, HVG (Cat. No. 206-67563).
21
Dimensions
Wall
255
150~200
80
450~550
GFA-EX7
600
about 700
450
343
360
460
282
AA-6800
53
345
1080
ASC-6100
Unit : mm
NOTE) Above dimensions do not include PC or printer.
JQA-0376