Steven Knapp sknap054@uottawa.ca Graduate Student Mechanical Engineering Dr. Arnaud Weck aweck@uottawa.ca Outline Introduction Objectives Results Conclusion Future Work 2 Importance to Industry Dissimilar Metal Welds are used to connect to different metals together Used where an object (pipe) is subjected to multiple environments in one application Advantage Each section of the pipe can be optimized for its specific application Disadvantage Weld consists of a mixture of materials which have unknown material properties when combined with unevenly distributed heating 3 4 Heavy Water Nuclear Reactor 120 mm Right to Left: Inconel 600 Inconel 82 Carbon Steel Gr. 106 B Tungsten Inert Gas (TIG) Welding (also called GTAW) Transporting Heavy Water at 310C CANDU Nuclear Reactor CANDU: CANada Deuterium Uranium Fuel Rods 5 Background Why this weld? Primary Water Stress Corrosion Cracking (PWSCC) was observed in an Inconel Nozzle welded to Stainless Steel Researching areas in the reactor with similar composition Specific Weld Information: High values of hoop residual stress 800 MPa peaking at start/stop welding point (Neutron Diffraction) Inconel-Weld fusion susceptible to PWSCC 6 Objectives To determine the mechanical properties and fracture mechanics of the Inconel 600 / Inconel 82 Filler/ Grade 106 B Carbon Steel Welded Pipe used in CANDU nuclear reactors Specific Test Goals To reveal the microstructure and grain size of each section To observe the evolution of strain and the amount of strain in each section Extract Local Material properties for use in FEA modeling Observe through thickness crack growth and failure 7 Inconel 600 Carbon Steel Grade 106B Weld Spatial Variations Inconel 82 Weld Filler Carbon Steel Grade 106B Inconel 600 Defining the Regions: Outer (Diameter) Middle Inner (Diameter) Weld Region: Very Large Grains 7 Weld Sections 4 mm 8 Inconel HAZ-Inconel (big grains) Weld (very large grains) Weld Ctd. Carbon Steel HAZ (small grains) Carbon Steel (larger grains) Before testing 9 After testing Inconel HAZ-Inconel (big grains) Weld (very large grains) Weld Ctd. Carbon Steel HAZ (small grains) Carbon Steel (larger grains)10 Indentation of Inconel Weld Hardness Tests with varying spacing Small Spacing (Large amount of data in small area) Large Spacing (Large area tested) Hardness Tests 11 OD MID ID Inconel hardness far from the weld 150 190 230 270 310 0 1000 2000 3000 4000 5000 6000 7000 8000 V i c k e r s
H a r d n e s s
( H V ) Distance From Inner Diameter (m) Inconel Through Thickness Hardness Hardness Tests +/- 6 HV 12 160 200 240 280 320 0 5000 10000 15000 20000 V i c k e r s
H a r d n e s s
( H V ) Distance (m) Weld Inconel 600 13 Inconel hardness along weld 0.3mm from OD 160 180 200 220 0 5000 10000 15000 20000 V i c k e r s
H a r d n e s s
( H V ) Distance (m) Across Weld Hardness (3.3 mm from OD) Weld Inconel 600 HAZ 14 Inconel hardness along weld 3.3mm from OD 160 170 180 190 200 210 220 0 5000 10000 15000 20000 25000 V i c k e r s
H a r d n e s s
( H V ) Distance (m) Weld Carbon Steel Inconel 600 HAZ 15 Inconel hardness along weld 3.3mm from OD 16 0 100 200 300 400 500 600 0 0.05 0.1 0.15 0.2 S t r e s s
[ M P a ] Strain OD - Sample 1B ID - Sample 2A MID - Sample 3A Tensile test on 1 mm thick samples Digital Image Correlation 17 Carbon Steel Inconel 17 Mirror polish for video Speckle patter for DIC Set-up for testing large samples 18 Testing (Movie) Until Failure - Polished surface Carbon Steel Inconel Carbon Steel Inconel Carbon Steel Inconel Outer Diameter Sample Inner Diameter Sample Middle Sample 19 9.76mm 8.16mm 7.36mm 6.88mm 5.60mm Weld width 20 Steel Inconel Weld Digital Image Correlation Early stages of deformation - Formation of a Lders Band in the C-steel Eng. 413 MPa 421MPa 446MPa 457MPa 464MPa 477MPa Stress 21 Sample deforms first in Inconel/Weld region Deformation is spatially inhomogeneous Deformation then localizes in C-Steel Deformation more homogeneous Eng. 413 MPa 536MPa 583MPa 524MPa Stress 22 0 100 200 300 400 500 600 0 0.1 0.2 0.3 0.4 0.5 S t r e s s
[ M P a ] Strain Inconel - DIC Weld - DIC Carbon Steel - DIC 300 320 340 360 380 400 0 0.02 0.04 23 Stress strain curves extracted from DIC 0 100 200 300 400 500 600 700 800 900 1000 0 0.1 0.2 0.3 0.4 0.5 T r u e
S t r e s s
[ M P a ] True Strain Inconel - DIC Inconel - Small Sample Carbon Steel - DIC Carbon Steel - Small Sample Miniature Tensile Tests vs. DIC 24 3mm Conclusions to Date Microstructure: Inconel Small Grains, Weld Big Grains Hardness: Inconel decreases from OD to ID residual stresses Hardness varies across sample, through the weld Large Tensile Tests: ID fails first, Middle second, OD last Trends: Amount of strain at failure directly related to weld width DIC: Obtain local material properties (stress vs. strain curve) Miniature Tensile Tests: Confirms material properties seen in DIC Expands stress vs. strain curve for Inconel 25 Future Work EDS Compositional Changes EDS results obtained across the weld Variations still to be analyzed Blue: Iron Purple: Nickel Green: Chromium Future Work Fracture Crack Propagation in 4-Point Bending Crack Growth Path Crack Interactions Deformation Field at Crack Tip with DIC Model Deformation and Fracture using FEA
Sexton's Pocket-Book for Boiler-Makers and Steam Users: Comprising a Variety of Useful Information for Employer and Workmen, Government Inspectors, Board of Trade Surveyors, Engineers in Charge of Works and Ships, Foreman of Manufactories, and the General Steam-Using Public