Aim : To determine the empirical formula of magnesium oxide
Problem Statement : What is the empirical formula of magnesium oxide?
Hypothesis : The empirical formula of magnesium oxide can be determined by combustion of magnesium in fixed quantity of oxygen to produce fixed quantity of magnesiumoxide Material : Magnesium Ribbon , oxygen Apparatus : Crucible with lid , Bunsen Burner , Tongs , pipeclay triangle, eletronics balance , Tripod stand,!andpaper Procedure : "# $mpty crucible without lid is weighed %# &bout %'cm of magnesium ribbon is cleaned with sandpaper (# The magnesium ribbon is rolled and inserted into crucible )# The crucible is heated strongly until magnesium lights up *# &s magnesium starts to burn, crucible is closed using its lid +# The crucible continue to heat ,# Crucible lid is opened and shut once rapidly -# .id is remo/ed when magnesium ribbon is no longer glowing 0# Crucible is heated strongly to ensure the complete burning of magnesium "'# The crucible and contents are left to cool at room temperature and weighed again ""# The heating, cooling , and weighing steps are repeated to obtain constant mass Precaution Steps : The lid of crucible is opened and closed at inter/als to pre/ent white smo1e of magnesium oxide released to the surrounding Magnesium is cleaned with sand paper to remo/e layer of oxide on surface Tabulation of data Mass of crucible 2 lid3 a 4g5 Mass of crucible 2 lid 2 magnesium3 b 4g5 Mass of crucible 2 lid 2 Magnesium oxide3 c 4g5 Calculation $lement Magnesium 6xygen Mass 7 g b 8 a c b 9o# of moles b 8 a c 8b %) "+
!implest ratio m n Arrangement of apparatus : Aim : To determine the empirical formula of copper oxide Problem Statement : What is the empirical formula of copper oxide? Hypothesis : The empirical formula of copper oxide can be determined by using a fixed mass of copper oxide to produce fixed mass of copper Materials : Copper oxide powder, ,htdrogen gas :inc pieces , ;ilute <ydrochloric &cid , &nhydrous Calcium Chloride Procedure : 1. combustion tube with porcelain dish are weighed using electronics balance,the weight is recorded %# a spatula of copper powder is placed in porcelain dish#the combustiontube with its contain is weighed again#the weight is recorded# (# ;ry hydrogen gas is flow through the apparatus se/eral times to expell the air )# The copper oxide is heated strongly *# <ydrogen gas exit at the end of tube is lit +# The blac1 copper oxide is reduced by hydrogen into brown copper metal ,# <ydrogen continue flow through to cool the apparatus -# When cooled, the combustion tube with its contain is weighed again# The weight is recorded 0# The heating, cooling, and weighing process are repeated to obtain constant mass Precaution Steps : "# &ll connections are ensure to be tight %# <ydrogen gas is flow through the apparatus for se/eral minutes to expell the air as the air will cause explosion (# the flow of hydrogen must continued throughout heating to ensure the air do not enter# )# <ot copper metal allowed to cool in stream og h% to ensure it does not oxidise by the air *# heating, cooling, weighing process is repeated until a constant weight is obtained to ensure all copper has been reduced Tabulation of data Mass of combustion tube 2 $mpty asbestos crucible 3 x 4g5 Mass of combustion tube 2 asbestos crucible 2 copper oxide 3 y 4g5 Mass of combustion tube 2 asbestos crucible 2 copper 3 = 4g5 Calculation $lement Copper 6xygen Mass 7 g = x y = 9o# of moles = 8 x +) y 8 = "+ !implest ratio p q >>The empirical formula of############## is ?######### Arrangement of apparatus : Aim : To prepare !odium 9itrate salt through reaction between 9itric &cid and !odium <ydroxide solution Material : " mol dm@A 9itric &cid, " mol dm !odium <ydroxide solution, phenolphthalein indicator Apparatus : %*' cmA conical flas1, %* cmA pipette, burette, white tile, e/aporating dish, filter paper, filter funnel, glass rod, bea1er, retort stand, tripod stand, wire gau=e, Bunsen burner, asbestos sheet Procedure : "# Measured %* cmA of " mol dm@A !odium <ydroxide solution into conical flas1 by using pipette %# & few drops of phenolphthalein indicator is added into !odium <ydroxide solution (# " mol dm@A of 9itric &cid is put into the burette# The initial reading of the burette is recorded )# 9itric &cid is added slowly into !odium <ydroxide while sha1ing the conical flas1, until the pin1 solution turns colourless *# The final reading of burette is recorded +# Bolume of 9itric &cid added to the !odium <ydroxide is recorded ,# !teps (+ is repeated to obtain the a/erage /olume of acid used -# The experiment is repeated without the use of phenolphthalein indicator, using the a/erage /olume of acid obtained 0# The mixture in the conical flas1 is poured into e/aporating dish "'# The mixture is heated until "7( of its solution is left ""# !aturated solution produced is left to cool in room temperature "%# White salt crystals formed are filtered and rinsed with cool distilled water "(# White salt crystals are dried with filter paper Tabulation of data Titration Rough " % ( Cinal Reading of burette 7 cmA Dnitial Reading of burette 7 cmA Bolume of &cid used 7 cmA &/erage /olume of &cid 7 cmA Arrangement of apparatus Aim : To prepare Magnesium !ulphate salts through reaction between sulphuric acid and magnesium oxide Material : " mol dm@A suphuric acid, magnesium oxide Apparatus : %*' cmA conical flas1, "'' cmA bea1er, measuring cylinder, burette, white tile, e/aporating dish, filter paper, filter funnel, glass rod, retort stand, tripod stand, wire gau=e, Bunsen burner, spatula, asbestos sheet Procedure : "# *' cmA of " mol dm@A !ulphuric &cid is measured using measuring cylinder and poured into bea1er %# !ulphuric &cid is heated slowly (# Magnesium oxide powder is added using spatula a little at a time while stirring the mixture with glass rod )# &ddition of Magnesium 6xide stopped when substances no longer soluble *# <ot solution is filtered into e/aporating dish to extract excess magnesium oxide +# The mixture is heated until saturated ,# The saturated solution is cooled to room temperature -# The salt crystal formed is filtered and rinsed with cold distilled water 0# !alt crystal are dried using filtered paper Aim : To prepare .ead 4 5 Dodide salt through double decomposition method Material : " mol dm .ead 4 5 9itrate solution, " mol dm Eotassium Dodide solution Apparatus : %*' cm bea1er, glass rod, filter funnel, filter paper Procedure : "# *' cm of " mol dm Eotassium Dodide solution is added to *' cm of " mol .ead 4 5 9itrate solution in a bea1er %# The mixture is stirred (# !alt crystal has formed as yellow precipitate )# The salt crystal formed are filtered and rinsed with distilled water *# The salt crystal are dried using filter paper Arrangement of apparatus Carbonate ion "# &bout % cmA of of !odium Carbonate is poured into a test tube %# ;ilute <ydrochloric &cid is added (# Fas produced is passed through lime water )# .ime water turns cloudy Sulphate ion "# &bout % cmA of !odium !ulphate is poured into a test tube %# ;ilute <ydrochloric &cid is added (# Barium Chloride or .ead 4 5 9itrate is added )# White precipitate formed Chloride ion "# &bout % cmA of !odium Chloride is poured into a test tube %# ;ilute 9itric &cid is added (# !il/er 9itrate or .ead 4 5 9itrate is added )# White precipitate formed Df .ead 4 5 9itrate is choosed, white precipitate formed is dissol/e when heated up Nitrate ion "# &bout % cmA of !odium 9itrate is poured into a test tube %# ;ilute !ulphuric &cid is added (# Dron 4 DD5 sulphate is added, the mixture is sha1en )# !e/eral drops of concentrated suphuric acid is added slowly along the wall of test tube *# Brown ring formed Aim :To determine the characteristic of /ulcanised and un/ulcanised rubber Problem Statement :What is the difference between /ulcani=ed and un/ulcanised rubber Hypothesis : Bulcanised rubber is tougher, stronger, and more elastic than natural rubber Variables :Manipulated G Type of rubber strips Responding G The stretching of rubber strip Cixed G The width and thic1ness of rubber strip Material : Hn/ulcanised rubber strip, Bulcanised rubber strip Apparatus :Retort !tand, Weight, Ruler , Clip Procedure : "# Bulcanised and un/ulcanised rubber are cut into equal length %# Both strips are hung using the clip (# The distance between the clip for both rubber are same )# The original length of both rubber are measured *# Weights with the same mass are hung on both rubber strip +# The length of both rubber strip are measured ,# The weights are ta1en away and the length of both strips are measured again Obseration Type of !ubber Strip Hn/ulcanised Rubber Bulcanised Rubber Original "ength #cm "ength $ith $eight #cm %&tension #cm 'inal "ength #cm Conclusion :Bulcanised rubber is tougher and more elastic Arrangement of apparatus : Aim : To prepare ethyl ethanoate 4ester5 in laboratory Material : pure $thanol, glacial $thanoic &cid, concentrated !ulphuric &cid Apparatus : .iebig condenser, Roundbottomed flas1, oil bath,porcelain chips Procedure : "# (' cmA of pure ethanol and %* cmA of glacial ethanoic acid is added into the round bottomed flas1# %# * cmA of concentrated !ulphuric &cid is added drop by drop and sha1en gently (# & few pieces of porcelain are added into the flas1 to pre/ent bumping and ensure e/en boiling process )# The mixture is heated under reflux for (' minutes *# $thyl $thanoate is distilled out from the mixture of the product at temperature of ,,-' Precaution steps : "# The mixture need to be heat under reflux because ethanol and ester that produced are /olatile %# The mixture is heat in water bath to ensure heating temperature is e/en (# The concentrated sulphuric acid function as catalyst and dying agent Aim : To study the relationship between the si=e of reactant and he rate of reaction Problem Statement : <ow does the si=e of reactant affect the rate of reaction? Hypothesis : The smaller the si=e of reactant, the higher the rate of reaction Variables : Manipulated G The si=e of marble chips Responding G The rate of reaction Cixed G Bolume and Concentration of !ulphuric &cid Material : !mall and large marble chips, '#" mol dm@A <ydrochloric &cid Apparatus : "'' cmA of conical flas1, rubber stopper with deli/ery tube, basin, measuring cylinder, stopwatch, retort stand with clamp, electrical balance Procedure : "# The basin and burette are filled with water %# The burette is in/erted in the basin and the meniscus is mar1ed at *' cmA (# + g of large marble chips is weighed and put into the conical flas1 )# *' cmA of '#" mol dm@A <ydrochloric &cid is measured with measuring cylinder and pour into conical flas1 *# The conical flas1 is co/er with rubber stopper immediately and sha1en +# The stopwatch started ,# The /olume of gas collected in burette is recorded e/ery (' seconds for * minutes -# The experiment is repeated with + g of small marble chips Tabulation of data (sing "arge Marble Chips Time 7s Burette Reading 7cmA Bolume of gas 7cmA (sing Small Marble Chips Time 7s Burette Reading 7cmA Bolume of gas 7cmA Aim :To study the relationship between the concentration of reactant and the rate of reaction Problem Statement :<ow does the concentration of reactant effect the rate of reaction? Hypothesis :The higher the concentration of reactant, the higher the rate of reaction Variables : Manipulated G The concentration of !odium Thiosulphate Responding G The rate of reacion Cixed G Bolume and Concentration of !ulphuric &cid Materials :" mol dm@A !ulphuric &cid, '#% mol dm@A !odium Thiosulphate solution, white paper Apparatus :"'' cmA conical flas1, "' cmA and *' cmA measuring cylinder, stopwatch Procedure : "# The white paper is mar1ed with %# *' cmA of !odium Thiosulphate solution is measured using *' cmA of measuring cylinder and pour into conical flas1 (# The flas1 is placed on tha white paper mar1ed with IxJ )# * cmA of " mol dm@A !ulphuric &cid is measured using "' cmA measuring cylinder *# The !ulphuric &cid is pour into conical flas1 containing of !odium Thiosulphate solution immediately and sha1en +# !topwatch is started ,# & yellow precipitate of !ulphur is obser/ed at the op part of conical flas1 -# Time is recorde when the IxJ mar1 on he white paper is no longer /isible 0# The experiment is repeated using different solution of '#% mol dm@A !odium Thiosulphate which is diluted with distilled water Tabulation of data $xperiment 9o# ) * + , - Bolume of !ulphuric &cid 7cmA Bolume of !odium Thiosulphate !olution, B7cmA Bolume of distilled water 7cmA Concentration of !odium Thiosulphate, BK'#% *' Time ta1en, t7s "7time, "7t7s@L