Introduction Drop weight and dynamic tear tests are widely used in the steel industry to determine material characteristics such as fracture resistance, transition temperature ranges and suitability of use of a steel for a specific application. During these tests the specimens are cooled or heated over a range of temperatures in order to determine the highest temperatures at which the sample fractures. Below this Nil-Ductility Transition temperature the material will consistently fracture, but above the material does not.
The American Petroleum Institute (API) 5L test standard is used to determine the fracture ductility of metal line pipe. Specimens are cut from sections of pipe, soaked at a prescribed temperature and tested within 10 seconds. ASTM E 436, similar to API-5L, is used to establish the temperature range over which ferritic steels undergo a fracture mode transition from ductile to brittle. In both standards a determination regarding ductile to brittle behavior is based upon visual inspection of the specimens in conjunction with, at times, a calculation to determine the percentage of shear seen the materials fracture.
Dynamic tear tests, executed according to ASTM E 604, provide a measurement of the amount of energy absorbed during the fracture process of a pre-cracked specimen. The objective of the test is similar to the tests outlined above; however, the measurement of energy eliminates some of the subjectivity of the other tests. With an actual numerical output from the test, levels of acceptance specified by the end users of the steels in critical applications can be defined.
Test Configuration and Procedure An Instron
Dynatup
Model 8150 Drop Weight Impact System,
instrumented with a Model 8340, 1,000 kN tup, 1-inch radius (for ASTM E 436 and API-5L) or 0.5-inch radius (for ASTM E 604) tup insert and Impulse Data Acquisition system were used to perform tests per the standards. Fixtures designed in accordance to the test standards were used to support the specimens. See Figure 1 for an example of test setup and configuration. All specimens were tested at room temperature.
Each specimen was centered on the anvils with the point of impact being directly above the cut notch. Crosshead weight was maximized to ensure sufficient energy to break the specimens with a single impact.
Figure 1: Model 8150 Drop Weight Impact System
Drop Weight Test/Dynamic Tear Tests Application Report
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AR_DropWeightTearTests_Rev2_0907 Figure 2: ASTM E436/API-5L test setup Results* Figure 3 shows a plot of Load and Energy vs. Time for two 5/8-inch thick steel specimens tested under the same test conditions. As seen in the numerical test results and the data curves there was a significant difference in how a similar material reacted to the impact event.
Figure 3: Load and energy test results for steel specimens tested per E 436/API-5L
Figure 4 shows a comparison of test data between three -inch thick steel specimens tested per ASTM E 604. All three were tested under the same conditions and as with the specimens tested per ASTM E 436, all three specimens show different results to the same impact event.
* Contact Instron
for a detailed test report with additional results.
Figure 4: Load test results for steel specimens tested per E 604
Conclusions and Recommendations The Model 8150 impact testing system is well suited for providing both a simple uninstrumented test, as well as a fully-instrumented testing system. The impact resistance information gathered by doing instrumented testing can be used by Research and Development to evaluate the effects of metallurgical variables such as composition, processing, heat treatment can have on the dynamic fracture resistance of new or existing materials. Test results may also be used to indicate particular steels suitability for use in a specific application.
Testing System 7810-213 Frame 8150 Optional Weight Set 7900-138 Tup Model 8340 Instrumented 7910-512 Tup Insert 25.4mm (1 in.) Radius Tup Insert for ASTM E 436; ASTM E 208 & API-5L 7800-052 Fixture Dynamic Tear Fixture for ASTM E 436 & API-5L 7910-511 Tup Insert 12.7 mm (0.5 in.) Radius Tup Insert for ASTM E 604 7800-054 Fixture Dynamic Tear Test Fixture for ASTM E 604 7000-710 Data Acquisition Dynatup Impulse Data Acquisition System *Customer Supplied- Environmental Chamber Chiller large enough to handle specimens