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EQUIPMENT FOR SYSTEMS

USING DOWTHERM
HEAT TRANSFER FLUIDS
Includes heat transfer system
hardware and fabrication guidelines

TABLE OF CONTENTS

I. Engineering /Consulting Firms ......................................................................... 3


II. Heaters and Vaporizers
Comparison of Steam and DOWTHERM Products ...................................... 4
Description, Operation, and Maintenance .............................................. 4
Manufacturers
Heaters and Vaporizers ............................................................... 4 5
Heat Exchangers ............................................................................. 5
Processing Equipment .................................................................... 5
Specialized Equipment .............................................................. 56
III. Pumps
Centrifugal Process Pumps ................................................................... 67
Canned Motor and Magnetically Coupled Pumps .................................. 7
Mechanical Seals ..................................................................................... 7
Packing ................................................................................................... 8
Expansion Joints ...................................................................................... 8
IV. Instruments
Instrumentation and Controls ............................................................... 10
Temperature Instruments and Controllers ............................................ 10
Flow Instruments and Controllers ......................................................... 10
Automatic Control Valves .................................................................... 10
Pressure Gauges and Controllers ........................................................... 11
Level Controllers and Switches ............................................................. 11
Level Gauges .......................................................................................... 11
V. Miscellaneous Equipment
Safety Valves .......................................................................................... 12
Traps ....................................................................................................... 12
Tanks and Jacketed Vessels ................................................................... 12
Purification Units .................................................................................. 12
Insulation ............................................................................................... 12
Filters ...................................................................................................... 13
VI. Piping Specifications
Pipe ......................................................................................................... 14
Pipe Fittings ........................................................................................... 14
Flanges and Gaskets ............................................................................... 15
Flange Bolts, Studs, and Nuts ................................................................ 15
Joint (Thread) Compounds ................................................................... 15
Bolt Lubricants ....................................................................................... 15
Pressure-Temperature Ratings for Flanges ....................................... 1617
Instrumentation Piping .......................................................................... 18
Gate Valves for Instrument Lines .......................................................... 18
Methods of Making Branch Connections ............................................. 18
Shutoff and Throttling Valves ............................................................... 18
Tight Shutoff Valves .................................................................... 18
Globe Valves ................................................................................ 19
Gate Valves .................................................................................. 19
Check Valves ................................................................................ 19
Valve Manufacturers .................................................................... 20
VII. Index to Suppliers ................................................................................. 21 23

INTRODUCTION
This brochure describes equipment
utilized in systems that employ
DOWTHERM* heat transfer fluids.
It also includes convenient lists
of equipment suppliers. These
suppliers represent a portion of
those who are capable of providing
high-temperature equipment.
Section VI of this brochure lists
piping specifications that have
been developed by The Dow
Chemical Company for use in
processes within our own production facilities.
References to a supplier or
product by name does not imply
approval or recommendation by
Dow of any supplier or product
to the exclusion of others that
may be suitable for the intended
purpose. Dow neither endorses
the suppliers or products
mentioned nor guarantees
their performance. It is the
users responsibility to select
suppliers and determine product
performance for users intended
application.

I. ENGINEERING/
CONSULTING FIRMS
The Dow Chemical Company is
not in a position to design equipment for customer use. We suggest
that you consult with competent
engineering companies, consultants, or equipment fabricators
experienced with systems utilizing
DOWTHERM fluids. A selective list
of experienced engineering firms
follows:

Sources for Engineering Services


ABB Lummus Heat Transfer
A Division of ABB Lummus Crest,
Incorporated
Bloomfield, New Jersey
American Econo-Therm Division
Petro-Chem Development
Company, Incorporated
Tulsa, Oklahoma
American Hydrotherm Corporation
New York, New York
American Schack Company,
Incorporated
Pittsburgh, Pennsylvania
Artisan Industries, Incorporated
Waltham, Massachusetts
Bechtel Group, Incorporated
San Francisco, California
John Brown E & C, Incorporated
Stamford, Connecticut
Brown & Root, Inc.
A Subsidiary of Halliburton Company
Houston, Texas
BS&B Process Systems,
Incorporated
Houston, Texas
Dow Engineering Company
Houston, Texas
First Thermal Systems, Incorporated
Chattanooga, Tennessee
Fluor Daniel, Incorporated
A Subsidiary of Fluor Corporation
Irvine, California
Foster Wheeler USA Corporation
Clinton, New Jersey

Lockwood Greene Engineers,


Incorporated
Spartanburg, South Carolina
Michigan Science &
Engineering Associates
Ann Arbor, Michigan
The Ralph M. Parsons Corporation
Pasadena, California
Petro-Chem Development
Company, Incorporated
New York, New York
PfaudlerU.S., Incorporated
Rochester, New York
Raytheon Engineers &
Constructors, Inc.
Denver, Colorado/Philadelphia,
Pennsylvania/Lexington, Massachusetts
Stone & Webster Engineering
Corporation
Boston, Massachusetts
Sverdrup Technology, Incorporated
Sverdrup Corporation
Tullahoma, Tennessee

Troubleshooting Consultants
These consultants provide services
on special problems, including
problems with mechanical seals,
heater and vaporizer scale-up, heat
exchangers, processing equipment,
and process pumps.
Michigan Science &
Engineering Associates
Ann Arbor, Michigan
Walter F. Seifert,
Consulting Engineer
Midland, Michigan

Heatec, Incorporated
An ASTEC Company
Chattanooga, Tennessee
The International Boiler
Works Company
Miami Lakes, Florida

*Trademark of The Dow Chemical Company

II. HEATERS AND VAPORIZERS


Comparison of Steam and
DOWTHERM Products
Systems designed for DOWTHERM
heat transfer fluids are, in general,
similar to systems that employ steam.
However, steam and DOWTHERM
fluids do display a number of differences that must be considered when
designing any particular system.
DOWTHERM fluids differ from steam
as follows:
1. Their vapors are heavier than air;
steam is lighter than air.
2. They are flammable or combustible.
3. They will not cause scaling, nor
are they corrosive toward standard
materials of construction.
4. They contract, rather than
expand, upon freezing.
5. They can usually be regenerated
after years of use.
6. As organic fluids, they have low
surface tension and viscosities;
therefore, systems must be tight
when these media are introduced.

Liquid heaters, in general, use forced


circulation. However, if DOWTHERM
fluid is used in the vapor state, the
hot liquid and vapor go to a separator
drum. The vapor from the separator
drum then goes to the heat user,
while the liquid is recycled.
Vaporizers should never be referred
to as boilers, since they may then be
confused with ordinary steam boilers.
Such confusion is highly undesirable
because many of the insurance and
local code restrictions under which
steam boilers operate are inapplicable
to vaporizers for DOWTHERM fluid.
Steam boilers have screwed fittings and
generally operate at much higher heat
fluxes than vaporizers for Dowtherm
fluids. Steam boilers should never be
converted to vaporizers for Dowtherm
fluids except under the guidance of the
manufacturer.
The capacities of vaporizers and
heaters range from a few thousand
Btu to over 150 million Btu per hour.
Higher-capacity units can be built;
however, multiple units may be
preferred because of their greater
operating flexibility.

liquid heaters are similarly controlled


by the exit temperature of the liquid.
The instruments which regulate fuel
flow may also be used to record the
temperature and pressure of the liquid,
or separate instruments may be
employed. It is important to measure
both temperature and pressure in
vapor systems. If the two do not correspond, it is an immediate indication
that a contaminant is present in the
system.
A temperature indicator should
be installed in the stack to give
an indication of unit efficiency and
to provide a warning of potential
operational problems.
Since heaters and vaporizers for
DOWTHERM heat transfer fluids
incorporate special design features,
they should be purchased only from
manufacturers who are experienced
in designing and constructing them.
Some manufacturers are listed in the
following section. Listed on pages 5
and 6 are manufacturers of heat
exchangers, processing equipment,
and specialized equipment.

Manufacturers of Heaters
and Vaporizers

The most important difference


between steam and DOWTHERM
heat transfer fluids is the lower vapor
pressure exhibited by the latter. For
example, while steam at 500F has a
pressure of 696 psig, DOWTHERM A
fluid operates at atmospheric pressure. Similar differences exist with
the other DOWTHERM fluids.

The thermal efficiencies of vaporizers


and heaters for DOWTHERM fluids are
between 65 and 90 percent (based
on the net heating value of the fuel).
Where high efficiencies are desired,
air preheaters must be used. In many
units, convection sections and
economizers, as well as gas-liquid
preheaters, have been employed to
increase heat efficiency.

ABB Lummus Heat Transfer


A Division of ABB Lummus Crest,
Incorporated
Bloomfield, New Jersey

Description, Operation,
and Maintenance

Vaporizers should be designed to ensure adequate circulation of medium


and to prevent stagnant liquid pockets.
A high circulation rate minimizes the
formation of higher-molecular-weight
degradation products. Heater tubes
must be tightly secured to headers and
vaporizer drums. Generally, the tubes
are both expanded and welded into
headers.

American Schack Company,


Incorporated
Pittsburgh, Pennsylvania

When a DOWTHERM heat transfer


fluid is used in the liquid state, the
unit for heating is called a heater;
when it is vaporized, the unit is
called a vaporizer.
Vaporizers use both natural and
forced circulation. Natural circulation vaporizers are subdivided into
4

liquid-tube and fire-tube types, the


latter are available as both vertical
and horizontal units.

Fuel burners on vaporizers are generally


controlled by fuel-throttling valves,
actuated either by the pressure or
temperature of the vapor. Burners on

American Econo-Therm Division


Petro-Chem Development Company,
Incorporated
Tulsa, Oklahoma
American Hydrotherm Corporation
New York, New York

Artisan Industries, Incorporated


Waltham, Massachusetts
BS&B Process Systems, Incorporated
Houston, Texas
The Bethlehem Corporation
Process Equipment Group
Easton, Pennsylvania
G. C. Broach Company
Tulsa, Oklahoma

Brown Fired Heater Division


Enercon Systems, Incorporated
Elyria, Ohio

American Schack Company,


Incorporated
Pittsburgh, Pennsylvania

Chromalox
Edwin L. Wiegand Industrial Division,
Emerson Electric Company
Pittsburgh, Pennsylvania

Brown Fired Heater Division


Enercon Systems, Incorporated
Elyria, Ohio

First Thermal Systems, Incorporated


Chattanooga, Tennessee
Foster Wheeler USA Corporation
Clinton, New Jersey
Fulton Thermal Corporation
Pulaski, New York
Heatec, Incorporated
An ASTEC Company
Chattanooga, Tennessee
Hynes Electric Heating Company
Vaporizers
Subsidiary of INDEECO
St. Louis, Missouri

Cherry-Burrell Process
Equipment Division
A United Dominion Company
Louisville, Kentucky
DEC International
Engineered Products Group
Madison, Wisconsin
First Thermal Systems, Incorporated
Chattanooga, Tennessee
Heatec, Incorporated
An ASTEC Company
Chattanooga, Tennessee

The Duriron Company, Incorporated


Pump Division
Valve Division
Dayton, Ohio
First Thermal Systems, Incorporated
Chattanooga, Tennessee
Fisher Controls International,
Incorporated
Marshalltown, Iowa
Foster Wheeler USA Corporation
Clinton, New Jersey
Heatec, Incorporated
An ASTEC Company
Chattanooga, Tennessee
INDEECO (Industrial Engineering
& Equipment Company)
St. Louis, Missouri

ITT Standard
Buffalo, New York

Invalco, Incorporated
Division of National Tank Company
Hutchinson, Kansas

INDEECO (Industrial Engineering


and Equipment Company)
St. Louis, Missouri

Manning & Lewis Engineering


Company
Union, New Jersey

Manning & Lewis Engineering


Company
Union, New Jersey

The International Boiler Works


Company
Miami Lakes, Florida

PfaudlerU.S., Incorporated
Rochester, New York

Marine & Petroleum


Manufacturing, Incorporated
Freeport, Texas

Manning & Lewis Engineering


Company
Union, New Jersey
Petro-Chem Development Company,
Incorporated
New York, New York
Riley Stoker Corporation
Worcester, Massachusetts
Struthers-Wells Corporation
Warren, Pennsylvania
SUPER-TROL Division
Enercon Systems, Incorporated
Elyria, Ohio
Thermoflux, Incorporated
Tulsa, Oklahoma
Wellman Thermal
Shelbyville, Indiana

Manufacturers of Heat Exchangers


ABB Lummus Heat Transfer
A Division of ABB Lummus Crest,
Incorporated
Bloomfield, New Jersey
American Hydrotherm Corporation
New York, New York

Struthers-Wells Corporation
Warren, Pennsylvania
SUPER-TROL Division
Enercon Systems, Incorporated
Elyria, Ohio

Manufacturers of Processing
Equipment
American Econo-Therm Division
Petro-Chem Development Company,
Incorporated
Tulsa, Oklahoma
Artisan Industries, Incorporated
Waltham, Massachusetts
Blaw Knox Food & Chemical
Equipment Company, Incorporated
Buffalo, New York
G. C. Broach Company
Tulsa, Oklahoma
Brown Fired Heater Division
Enercon Systems, Incorporated
Elyria, Ohio
BS&B Process Systems, Incorporated
Houston, Texas
Cherry-Burrell Process
Equipment Division
A United Dominion Company
Louisville, Kentucky

Petro-Chem Development
Company, Incorporated
New York, New York
PfaudlerU.S., Incorporated
Rochester, New York
SUPER-TROL Division
Enercon Systems, Incorporated
Elyria, Ohio

Manufacturers of
Specialized Equipment
ABB Lummus Heat Transfer
A Division of ABB Lummus Crest,
Incorporated
Bloomfield, New Jersey
(Pyrolysis heaters, coking heaters,
visbreaker heaters, VCM heaters, EDC
heaters)
American Hydrotherm Corporation
New York, New York
(Electric and fired heat transfer fluid
systems)
American Schack Company,
Incorporated
Pittsburgh, Pennsylvania
(Recuperators)

Ametek, Incorporated
Thermox Instruments Division
Pittsburgh, Pennsylvania
(Combustion air analyzers)

Hynes Electric Heating Company


Subsidiary of INDEECO
St. Louis, Missouri
(Vaporizers)

Artisan Industries, Incorporated


Waltham, Massachusetts
(Thin film evaporators, heat exchangers, and reactors)

INDEECO (Industrial Engineering


& Equipment Company)
St. Louis, Missouri
(Process heaters, electric heaters,
electric heat transfer fluid systems)

The Bethlehem Corporation


Process Equipment Group
Easton, Pennsylvania
(Indirect heat transfer-dryers)
Blaw Knox Food & Chemical
Equipment Company, Incorporated
Buffalo, New York
(Dryers, flakers, evaporators, reactors)
G. C. Broach Company
Tulsa, Oklahoma
(Waste heat recovery boilers)
Brown Fired Heater Division
Enercon Systems, Incorporated
Elyria, Ohio
(Gas-fired fluid heaters)
Cherry-Burrell Process
Equipment Division
A United Dominion Company
Louisville, Kentucky
(Turba-film evaporators and semicontinuous deodorizers)
Clark-Reliance Corporation
Cleveland, Ohio
(Level gauges, water columns)
Crosby Valve & Gage Company
A Moorco Company
Wrentham, Massachusetts
(JOS/JBS pressure relief valves)
DEC International
Engineered Products Group
Madison, Wisconsin
(Plate- or panel-type coils)
Dickow Pump Company
Marietta, Georgia
(Pumps that require no cooling water
to 750F)
Fisher Controls International,
Incorporated
Marshalltown, Iowa
(Cavitation and noise control trim
for control valves, rotary valves)
Heatec, Incorporated
An ASTEC Company
Chattanooga, Tennessee
(Process heaters, jacketed vessels)

Invalco, Incorporated
Division of National Tank Company
Hutchinson, Kansas
(Oil/water analyzers and monitors,
flow instruments and controllers)
The Kontro Company, Incorporated
Orange, Massachusetts
(Magnet drive centrifugal pumps for
heat transfer fluid systems)
Manning & Lewis
Engineering Company
Union, New Jersey
(Scraped-surface heat exchangers)
Masoneilan North America
Dresser Valve and Controls Division,
Dresser Industries, Incorporated
Houston, Texas
(Steam and air regulating valves)
PfaudlerU.S., Incorporated
Rochester, New York
(Corrosion-resistant glass-lined
reactors and mixing systems)
Spirax Sarco
Allentown, Pennsylvania
(Vapor-operated non-electric pumps)
Struthers-Wells Corporation
Warren, Pennsylvania
(Electric heaters, heat recovery
equipment)
SUPER-TROL Division
Enercon Systems, Incorporated
Elyria, Ohio
(Circulating fluid heat transfer
systems)
Henry Vogt Machine Company
Louisville, Kentucky
(Heat recovery steam generators)
Worcester Controls
Marlborough, Massachusetts
(Block valves, throttling and fugitive
emission valves)
Yarway Corporation
Blue Bell, Pennsylvania
(Combination valves: pressure reduction and de-superheating. Also
centrifugal pump protection valves)

III. PUMPS
Centrifugal Process Pumps
Heavy-duty, centrifugal process
pumps constructed of cast steel and
designed for operation at high
temperatures are recommended for
DOWTHERM heat transfer media.
Pumps should be equipped with a
good water-cooled stuffing box and
preferably a hard alloy or plated shaft
sleeve. In high-temperature operation (usually above 350F or 175C),
pumps should be equipped with
water-cooled bearings and have
centerline construction rather than
foot mountings. Such construction
allows expansion in all directions,
thus alleviating possible stress on the
shaft and resultant misalignment,
bearing wear, seal failure, and so on.
It is also important that no stress be
transmitted to the pump from the
piping due to change in the temperature of the system.
It is advisable to protect pumps
against freeze-ups. Pumps using
mechanical seals should be rotated by
hand before power-starting to make
sure seal parts are not frozen in the
medium.
Gear pumps with hardened steel
gears and greater-than-normal
clearances can be used with
DOWTHERM heat transfer media at
lower temperatures. Reciprocating
pumps are not recommended because
DOWTHERM fluids have limited
lubricating properties; metal-to-metal
contact may cause seizing.
Lantern rings are not normally
recommended for use with packed
pumps unless the pumps are operated
with a vacuum on the suction side.
When a lantern ring is used, it is best
connected to a source of cold
medium at atmospheric pressure.
Sufficient static liquid head to prevent cavitation should be maintained
at all times on the suction side of
centrifugal pumps.

Manufacturers of Centrifugal
Process Pumps
Pumps commonly used in systems
utilizing high-temperature
DOWTHERM fluids are manufactured by the following companies:
Buffalo Pumps
An AMPCO-Pittsburgh Company
North Tonawanda, New York
BW/IP International, Incorporated
Pump Division
(Byron Jackson/United Pumps)
Long Beach, California
Dean Pump Division
MET-PRO Corporation
Indianapolis, Indiana
The Duriron Company, Incorporated
Pump Division
Dayton, Ohio
Goulds Pumps, Incorporated
Seneca Falls, New York
Ingersoll-Dresser Pump Company
Huntington Park, California
Sundstrand Fluid Handling
Division of Milton Roy Company
Subsidiary of Sundstrand Corporation
Arvada, Colorado
Union Pump Company
Battle Creek, Michigan
Yarway Corporation
Blue Bell, Pennsylvania

Canned Motor and


Magnetically Coupled Pumps
These types of pumps are seeing
increased use in DOWTHERM fluid
applications. The rotating parts of
the pump are contained in a thin
welded can rather than using a
mechanical seal or packing. This
helps to eliminate the leak path
associated with packing and mechanical seals, and their respective
maintenance. The tradeoff in using
this equipment is that canned and
magnetically coupled pumps are less
efficient than mechanical sealed
pumps. Because of the vulnerability
of the thin can pump housing, leak

detection equipment and secondary


can containment should be considered. Many manufacturers will
provide this extra protection at
additional cost. In specifying these
pumps, care must be taken to
consider all conditions, from cold
startup to maximum operating
conditions and back down to ambient
temperature. Anticipated temperature swings and higher than normal
temperatures or pressures should also
be taken into consideration.

Manufacturers of Canned Motor


or Magnetically Coupled Pumps
Buffalo Pumps, Incorporated
An AMPCO-Pittsburgh Company
North Tonawanda, New York
BW/IP International, Incorporated
Pump Division
(Byron Jackson/United Pumps)
Long Beach, California
Chempump Division
Crane Company
Warington, Pennsylvania
Dean Pump Division
MET-PRO Corporation
Indianapolis, Indiana
Dickow Pump Company
Marietta, Georgia
The Duriron Company, Incorporated
Pump Division
Dayton, Ohio
The Kontro Company, Incorporated
Orange, Massachusetts
Sundstrand Fluid Handling
Division of Milton Roy Company
Subsidiary of Sundstrand Corporation
Arvada, Colorado
Yarway Corporation
Blue Bell, Pennsylvania

Mechanical Seals
Many pumps in service with
DOWTHERM heat transfer fluid have
mechanical seals. Mechanical seals
have wide acceptance for service
with DOWTHERM fluid because of
their superior performance over
packing. Industrial experience

indicates that the metal bellows


seal is preferred over other types.
Mechanical seals, as opposed to
packing, can ensure essentially zero
leakage. This is especially important
for liquid service in poorly ventilated
areas because of the distinctive odor
of the media. Major causes of poor
seal performance include improper
installation, excessive temperature at
the faces, face distortion, and system
contamination. When seals are
installed, strict cleanliness must be
observed. Fingerprints on the seal
face can cause temporary leaks, and
microscopic dust particles can cause
the seal to leak permanently. Ideally,
work should be done with clean
hands, clean equipment, and in a
clean area. Some seal manufacturers
will, upon request, supervise the
installation of their seals.
The design of the pump and of the
mechanical seal is important. The
pump should have a water-cooled
stuffing box, and the seal should have
the proper face surfaces and secondary seals to withstand system operating temperatures. Some seal vendors
recommend water cooling on the seal
gland itself. It is also recommended
that a small stream of fluid from the
discharge of the pump be filtered and
then put into the stuffing box at the
seal surfaces to flush any abrasive
particles away from the seal. This
side stream is often cooled to give
additional cooling at the seal face.
A mechanical seal is a precisionmachined piece of equipment and
should be handled with a great deal
of care and regard for cleanliness
while it is being installed in the pump.
After the seal is properly in place, the
pump should be installed to prevent
any strain from the piping and/or
motor alignment. The most common cause of such strain is thermal
expansion. This can be alleviated by
including expansion loops, joints, or
flexibly supported piping as long as
these items are subject to a rigorous
maintenance schedule.

A mechanically sealed pump


should be manually operated prior
to startup to ensure a flooded
stuffing box and faces that are free
to rotate. This means that both the
suction and discharge valves should
be opened and the shaft rotated by
hand. To prevent seal problems,
the valve on the discharge line
should be closed when the pump is
started. (The valve on the suction
line should be open.) The pump is
started, then the discharge valve is
opened. For complete instructions,
consult the manufacturer. Proper
maintenance of such a pump
requires that the same degree of
care be taken in its repair as was
taken in its origi-nal design and
installation.

Manufacturers of
Mechanical Seals
BW/IP International Incorporated
Seal Division
Long Beach, California
(Metal bellows seal Types BXRH,
BXH, BRC)
A. W. Chesterton Company
Stoneham, Massachusetts
(Chesterton Style 123, 153, and
155 cartridge seals)
John Crane Incorporated
Morton Grove, Illinois
(John Crane Types 8 and 9, and
Types 315 and 715 seals)
Durametallic Corporation
Kalamazoo, Michigan
(PBR metal bellows DURASEAL)
EG&G Sealol
Industrial Sealing Division
Cranston, Rhode Island
(Metal bellows seals)
Fisher Controls International,
Incorporated
Marshalltown, Iowa
(ENVIRO-SEAL bellows for
control valves)
Worcester Controls
Marlborough, Massachusetts
(TEFLON, PEEK, metal)

Packing
Aluminum packing and flexible
graphite packing are used for pump
stuffing boxes. To ensure proper
instal-lation, a good hardened shaft
or shaft sleeve with a Brinell
hardness of 600 or greater, a good
stuffing box, careful packing or
installation, and careful take-up
of the packing gland are of prime
importance.
Considerable care is required with
metallic foil packing. It is relatively
inflexible and, if handled improperly, may bind in the box. The rings
should therefore be die-cut to the
size of the stuffing box and each
one carefully tamped in place
before the next is added. Because
packing material is always being
improved, it is suggested that the
pump manufacturer be contacted
periodically regarding possible new
materials. Use flexible graphite
packing for valves.
Lubricants should never be used on
packing for stuffing boxes. Lubricants
are soluble in DOWTHERM fluid and
have much lower thermal stabilities.
As a result, they will act as contaminants and may cause difficulty by
decomposing in the system. Stuffing
box and bearing fluid cooling are
recommended.

Manufacturers of Packing
Packing made by the following
manufacturers is presently utilized
in systems using DOWTHERM fluids:
JM Clipper Corporation
Denver, Colorado
(J-M 395 aluminum)
John Crane Incorporated
Morton Grove, Illinois
(Styles 100 and 124aluminum)
Durametallic Corporation
Kalamazoo, Michigan
(D-10 aluminum)
Flexitallic, Incorporated
Pennsauken, New Jersey
(FLEXICARB flexible graphite
packing)

Fisher Controls International,


Incorporated
Marshalltown, Iowa
(ENVIRO-SEAL packing systems
for fugitive emissions control)
UCAR Carbon Company,
Incorporated
Cleveland, Ohio
(GRAFOIL flexible graphite
packing Grade GT2)
Worcester Controls
Marlborough, Massachusetts
(TEFLON, graphite)

Expansion Joints
The following measures should be
considered to relieve stress in piping
due to high-temperature expansion.
1. Steel pipe expansion loops or
steel pipe U bends
2. Bellows-type expansion joints
3. High-temperature flexible
metal hose
These items should only be used if
they are subject to a rigorous maintenance schedule. Steel pipe U bends
or loops are the most common means
of relieving stress.
There are many successful applications using stainless steel alloy
expansion joints in industrial heat
transfer systems when these items are
subject to a rigorous maintenance
schedule. However, on occasion,
austenitic stainless steel bellows joints
have failed due to contamination of
the fluid with inorganic chloride
ions. This contamination has
resulted in stress-corrosion cracking.
Failure has also occurred from
improper installation. If experience
indicates stress-corrosion cracking to
be a problem, a steel pipe loop or U
bend should be utilized. If that is not
feasible, a bellows-type expansion
joint made of an alloy such as
Inconel 600 or Monel 400 should be
used. If a bellows expansion joint is
considered, the recommendation of
the manufacturer should be obtained.
Figure 1 illustrates the piping arrangement of a pump for DOWTHERM fluid.

Figure 1 Piping of Pump for DOWTHERM Heat Transfer Fluid

1. Support discharge line to relieve pump of


thermal and mechanical strains, providing
adjustment for gasket replacement.
2. Drain or sample valve.
3. Shutoff valve.
4. Check valve.
5. Pressure gauge.

10. Needle valve.


11. Filter.
12. Cooler.
13. Flow indicator.
14. Temperature indicator. (Normal
operation, 250F, maximum.)

6. Vent and drain plugs in casing.

15. Mechanical seal coolant (DOWTHERM


medium) and flush-through stuffing box.

7. Coupling guard.

16. Bearing cooling (normally water).

8. Lubrication and vent.

17. Drain.

9. Stuffing box coolant (normally water).

18. At least two pipe diameters to


straighten out flow.

19. Flexible connection or expansion joints


to prevent thermal strains in piping
from being transmitted to pump. These
expansion bellows must be restrained to
prevent thrust from the fluid pressure on
the pump casing.
20. If reduction is necessary on the suction,
an eccentric reducer should be used with
the top side horizontal.
21. Allow space all around for servicing
gland or seal, coupling, and motor.

IV. INSTRUMENTS
Instrumentation
and Controls
In general, industrial type instruments and automatic controls are
entirely satisfactory for use with
DOWTHERM heat transfer fluid
providing the following recommendations are observed. Copper or
copper alloys should not be used
with DOWTHERM fluid in pressure
vessels operating above 400F. If
copper is required for processing
reasons, only knowledgeable
equipment vendors should be
contacted.

Temperature Instruments
and Controllers
Industrial-type temperature instruments such as bimetallic thermometers; remote bulb, capillary or
potentiometer-type temperature
indicators; recorders and/or controllers are entirely satisfactory for
measuring the temperature of a
medium in either the liquid or
vapor state. However, the instrument must have a suitable range
and the sensing element (bulb or
thermocouple) must be installed in
a suitable thermowell.

Flow Instruments
and Controllers
The flow of DOWTHERM fluid,
either liquid or vapor phase, can be
measured satisfactorily by using a
conventional orifice installed in a
suitable meter run. The differential
measuring device may be a diaphragm- or bellows-type device
that operates a conventional
indicator, recording pen, or transmitter for remote recording or
indication. The vapor phase should
be treated similarly to steam.
Variable area-type metering devices
are also satisfactory, provided they
are of all-steel construction with
ANSI flanged connections and are
suitable for the high temperatures
involved. Glass metering or indicating tubes must not be used.

Suppliers for Flow Instruments


and Controllers
Invalco, Incorporated
Division of National Tank Company
Hutchinson, Kansas

Generally, control valves should


not be depended upon for positive
shutoff. Such valves are generally
designed with line contact between
the plug and the seat and may not
exert enough pressure on the stem
to seal against scale or other solids.
Control valves are usually installed
with a bypass around them. The
bypass includes manually operated
shutoff valves that will provide
tight shutoff when necessary.
The following companies have
furnished automatic control valves
for service with DOWTHERM fluids.

Manufacturers of Automatic
Control Valves
BS&B Process Systems,
Incorporated
Houston, Texas
Conbraco Industries, Incorporated
Monroe, North Carolina
The Duriron Company,
Incorporated
Valve Division
Dayton, Ohio

Micro Motion
Boulder, Colorado

Fisher Controls International,


Incorporated
Marshalltown, Iowa

Automatic Control Valves

The Foxboro Company


Foxboro, Massachusetts

Air-operated diaphragm control


valves with steel bodies and
stainless steel trim are generally
used with DOWTHERM fluids.
Flexible graphite, mica graphite, or
aluminum can be used for packing.
The use of a valve positioner is
recommended for precise control.

Kitz Corporation of America


Subsidiary of Kitz
Corporation of Japan
Houston, Texas
Richard Klinger, Incorporated
Sidney, Ohio
Masoneilan North America
Dresser Valve & Controls Division
Dresser Industries, Incorporated
Houston, Texas
Yarway Corporation
Blue Bell, Pennsylvania

10

Pressure Gauges
and Controllers
Conventional Bourdon- or diaphragmtype pressure gauges and switches
are suitable provided that all parts
in contact with DOWTHERM fluid
are of ferrous construction. All
gauges and switches should be
equipped with a loop to seal the
Bourdon element or the diaphragm
from high-temperature liquid or
vapor.
Bourdon-type units are suitable
for indoor installations where
temperatures are sufficiently high
to prevent freezing of medium
in the tube. For outside and lowtemperature installations, the
diaphragm type is recommended
because of the ease with which the
diaphragm housing can be heated.
The freezing point of the fluid plus
the aforementioned considerations
will dictate which type of control is
necessary.

Manufacturers of
Gauges or Controllers
Ametek, Incorporated
U.S. Gauge Division
Sellersville, Pennsylvania
Dwyer Instruments, Incorporated
Michigan City, Indiana
Fisher Controls International,
Incorporated
Marshalltown, Iowa

Level Controllers
and Switches
Two general types of level controllers are used: differential pressure
(DP) cells or float-type controllers.
When DP cells are used, the vapor
leg is back-filled with the working
fluid.
Float or displacer type controllers
and switches have movement
generated by means of a torque
tube, permanent magnet, or
electrical inductance and by
operating a pneumatic pilot or
electrical contact. No packing
gland of any type should be used.
The float chamber should be of
steel with ANSI flanged connections and designed to permit
removal of the float for periodic
inspection and cleaning.
Considerable care should be used
in selecting units that are to be
operated over a wide range of
temperatures. DOWTHERM fluids
have rather high coefficients of
expansion; consequently, a float
that is buoyant at low temperatures
may sink at high temperatures. It is
suggested that the float be of such
buoyancy and shape to float high in
the liquid at low temperatures and,
as the density of the liquid decreases, to become considerably
more immersed.

Manufacturers of
Level Controllers
Clark-Reliance Corporation
Cleveland, Ohio
Dwyer Instruments, Incorporated
Michigan City, Indiana
Fisher Controls International,
Incorporated
Marshalltown, Iowa
The Foxboro Company
Foxboro, Massachusetts
Invalco, Incorporated
Division of National Tank Company
Hutchinson, Kansas
Magnetrol International
Downers Grove, Illinois
Masoneilan North America
Dresser Valve & Controls Division
Dresser Industries, Incorporated
Houston, Texas
Yarway Corporation
Blue Bell, Pennsylvania

Level Gauges
A magnetic-type level gauge with
a spiral-wound gasket of metal and
graphite, or a flexible graphite
gasket, is recommended. Gaskets
should not be made of rubber due
to the high temperatures at which
units are operated. Level gauges are
available from Clark-Reliance
Corporation, Cleveland, Ohio.

The Foxboro Company


Foxboro, Massachusetts
Masoneilan North America
Dresser Valve and Controls Division
Dresser Industries, Incorporated
Houston, Texas

11

V. MISCELLANEOUS
EQUIPMENT
Many manufacturers of miscellaneous
equipment are familiar with
DOWTHERM fluids. These manufacturers will be in a position to
recommend the product best suited
for your application, based on good
operating experience. If you have
questions regarding the use of any
equipment in a system utilizing
DOWTHERM fluids, contact your
Dow Thermal Fluids technical
representative or call 1-800-4474369 and ask for DOWTHERM heat
transfer fluids.

Safety Valves
Safety or relief valves have been
specially designed and rated for
service with DOWTHERM fluids.

Manufacturers of Safety
or Relief Valves
Conbraco Industries, Incorporated
Monroe, North Carolina
Crosby Valve & Gage Company
A Moorco Company
Wrentham, Massachusetts
Dresser Industries, Incorporated
Industrial Valve Operation
Alexandria, Louisiana
Invalco, Incorporated
Division of National Tank Company
Hutchinson, Kansas
Teledyne Farris Engineering
Palisades Park, New Jersey
When safety valves are ordered, be
certain to specify that they are for
service with DOWTHERM fluid.

12

Traps

Purification Units

Systems using DOWTHERM fluid in


vapor form may require specially
designed condensate traps. When
traps are to be used, the manufacturer should be informed that they
are for service with DOWTHERM
fluid. This is necessary because the
mechanical traps used with steam
normally operate with a pressure
difference greater than those used
in a system with DOWTHERM fluids.

Solid contaminants and highboiling materials may be removed


from DOWTHERM A, DOWTHERM J,
DOWTHERM LF, and DOWTHERM Q
heat transfer fluids by simple
vaporization. Figure 2 shows a
purification unit for manual operation; units for automatic operation
are also available.

Manufacturers of Traps

Two types of insulation, closed-cell


and open-cell, are currently used
for high-temperature applications
(up to 800F) with DOWTHERM
fluids.

Armstrong International,
Incorporated
Three Rivers, Michigan
Clark-Reliance Corporation
Cleveland, Ohio
Spirax Sarco
Allentown, Pennsylvania
Yarway Corporation
Blue Bell, Pennsylvania

Tanks and Jacketed Vessels


Tanks and jacketed vessels for
DOWTHERM fluid are of welded
construction. They should conform
to local regulatory codes and
ASME codes where applicable.
Surge (expansion) tanks should be
capable of withstanding elevated
pressures.
Storage tanks should be provided
with a fill connection so that drums
and/or bulk medium can be conveniently emptied.

Insulation

Closed-cell insulation is recommended where there is a possibility


it may come in contact with a heat
transfer fluid, especially at elevated
temperatures. When organic fluids
come into contact with open-cell
insulation, they may oxidize and
heat the insulation to above the
fluids autoignition temperature.
Open-cell insulation can be used
for long runs of pipe where there
are no fittings, make-and-break
joints, or other potential sources of
fluid leakage and insulation contamination. For covering flanges or
other connections that may leak,
the closed-cell material should be
considered. Both can be used on
the same pipe, but a metal stop ring
or collar designed to stop the flow
of any leakage to the open-cell
material should be employed. The
insulation should be covered by
weatherproof jacketing and mastic,
or a protective metal jacket.
In all cases, the insulation manufacturer should be consulted for
application and installation details.

Manufacturers of Insulation
Acceptable calcium silicate base
(asbestos-free) insulation can be
obtained from the following companies:
Owens-Corning Fiberglas
Toledo, Ohio
(KAYLO calcium silicate-base
insulation, Fiberglas SSL-II pipe
insulation with DOUBLESURE
Closure System)
Schuller International, Inc.
Mechanical Insulation Division
Denver, Colorado
(THERMO-12 Gold calcium
silicate-base insulation and
MICRO-LOK fiberglass insulation)
The only known acceptable closedcell material is FOAMGLAS
cellular glass insulation, made by
the Pittsburgh Corning Corporation, Pittsburgh, Pennsylvania.

Flexible graphite insulation is


available from UCAR Carbon
Company, Incorporated, Cleveland, Ohio (GRAFOIL Grade
GHM flexible graphite insulation).

Filters
If solid particles such as scale or
hard insoluble carbonaceous
materials are present in the
pumped fluid, they may cause:

The following filter manufacturers


can be contacted for possible
solutions to the problem. To make a
recommendation, filter manufacturers typically need to know the
operating temperature, type of
fluid, pressure, type of material to
be removed, amount of material to
be removed, and typical particle
size.

Manufacturers of Filters

1. Erosion of piping or equipment


at high velocity.

Cuno, Incorporated
Meriden, Connecticut

2. Scouring of mechanical seals


in pumps.

Memcor Power Generation Division


Memtec America Corporation
Timonium, Maryland

3. Scouring of rotating pump shafts


and/or bearings.
4. Plugging of instrument lines and
drains on piping systems.
An investigation should be made
to determine whether filtering will
remove these solid contaminants.

Pall Process Filtration Company


A Division of Pall Corporation
East Hills, New York
Parker Hannifin Corporation
Commercial Filters Division
Lebanon, Indiana

Figure 2 Typical System for Purifying DOWTHERM Heat Transfer Fluids by Vaporization

Relief
Air- or Water-Cooled
Condenser
Purified DOWTHERM Fluid
(Return to System)

DOWTHERM Fluid
to Be Purified

In
Sight Gauge
(Optional)

Hot DOWTHERM Fluid


for Heating

Drain

Drain
(Residue)

Condensate or Hot Liquid


DOWTHERM Fluid
(Return to System)

13

VI. PIPING SPECIFICATIONS


The following piping specifications
have been developed by The Dow
Chemical Company for use in
processes within our own production facilities. They are the product
of extensive Dow experience in the
design and operation of heat
transfer systems, as well as in the
development of heat transfer fluids
for a broad range of applications
and process conditions. These
specifications are suitable for most
applications. However, particular
processes may require special
hardware or fabrication. Consult
with component suppliers and
system engineers to ensure the
suitability of these specifications
for your process.
The specifications in this bulletin
are rated for service at 150 psig at
750F. This rating applies to
systems utilizing DOWTHERM A,
DOWTHERM G, DOWTHERM HT,
DOWTHERM LF, DOWTHERM J,
and DOWTHERM Q organic heat
transfer fluids. For complete
product information and engineering properties for these DOWTHERM
fluids, call 1-800-447-4369. Note:
For systems operating in a temperature range of -100F to 500F,
other types of flanges and gaskets
may be acceptable. Please consult
our liter-ature for cryogenic applications, form numbers 176-01457
and 176-01458, or call 1-800-4474369 for additional information.

General Specification
Notes and Special
Instructions
Dow recommends that the piping
in the following specifications be
welded and/or flanged. This
includes the first block valve off
the line in instrument piping, as
well as all vent and drain valves.

14

When welding, all butt welds


should be tig-root with a shielded
metal arc cover. Also, random
radiograph welds should comply
with ANSI B31.3, paragraph
341.5.1, subparagraphs (b), (c),
and (d).
The preferred flange surface finish
for use with spiral gaskets is 125 to
250 rms. As an alternative to
purchasing special flanges, machine
standard flanges to meet surface
finish requirements.
Do not use aluminum paint on
valves or fittings in the heat
transfer system.

Pipe
Standard schedule 40 seamless steel
pipe is recommended for all lines
that are welded. Where screwed
fittings are desired, pipe sizes 11/2"
or smaller in diameter should be
composed of schedule 80 pipe.
Tapered thread connections are
satisfactory for pipes 11/2" or less in
diameter, provided the threads are
cut true to gauge with a sharp,
clean die. The threads should be
washed with a good solvent, and a
pipe thread sealant should be used
in assembly.
All larger-size connections should
be welded wherever possible;
smaller lines may be bent to avoid
the use of fittings.
Under no circumstances should a
pipe joint sealant be relied upon to
make a good joint out of a poor
one.
1

/2" through 1": ASTM A-106


GR B, extra-strong seamless steel
pipe.
11/2" and larger: ASTM A-106
GR B, standard-weight seamless
steel pipe.

Pipe Fittings
Tubing 3/8" x .049" minimum:
Soft annealed seamless carbon steel
mechanical tubing, ASTM A-519
GR 1020 or GR 1025, maximum
hardness RB 72, hot finished,
pickled and oiled, suitable for
bending and flaring.
Tubing 1/2" x .065" minimum:
Soft annealed seamless carbon steel
mechanical tubing, ASTM A-519
GR 1020 or GR 1026, maximum
hardness RB 72, hot finished,
pickled and oiled, suitable for
bending and flaring.
Tubing 3/4" x .083" minimum:
Soft annealed seamless carbon steel
mechanical tubing, ASTM A-519
GR 1020 or GR 1026, maximum
hardness RB 72, hot finished,
pickled and oiled, suitable for
bending and flaring.
Tubing 1" x .095" minimum:
Soft annealed seamless carbon steel
mechanical tubing, ASTM A-519
GR 1020 or GR 1026, maximum
hardness RB 72, hot finished,
pickled and oiled, suitable for
bending and flaring.
Elbows, Tees 3/8" through 1":
Carbon steel Parker CPI, Swagelok,
or Gyrolock tube fittings and
adapters, or silver solder joints.
Elbows, Tees, Reducers 1/2"
through 1": 3,000-lb socket
welding forged steel fittings,
ASTM A-105, ANSI B16.11.
Elbows, Tees, Crosses, Reducers
11/2" and up: Standard weight
seamless steel welding fittings,
ASTM A-234 GR WPB, ANSI
B16.9

Pipe Caps 1/2" through 1":


3,000-lb socket welding forged steel
cap, ASTM A-105, ANSI B16.11.

Raised face, blind 1/2" and up:


300-lb raised face blind flange,
ASTM A-105, ANSI B16.5.

Flange Bolts, Studs,


and Nuts

Pipe Caps 11/2" and up:


Standard-weight seamless steel
welding cap, ASTM A-234 GR
WPB, ANSI B16.9.

For spiral-wound gasket with


carbon steel outer compression
gage ring, 316 stainless steel and
graphite windings and 316 stainless
steel inner ring, i.d. same as SCH
5S pipe.

ASTM A-193 GR B7 liquid


quenched and tempered alloy steel
stud bolts with ASTM A-194 GR
2H heavy hex huts.

Couplings 1/2" through 1":


3,000-lb socket welding forged steel
coupling, ASTM A-105, ANSI
B16.11.
Couplings 1/2" through 1":
3,000-lb forged steel Sockolet
fitting.
Couplings: 11/2" and up:
Standard-weight steel Weldolet
fitting, ASTM A-105.
Unions 1/2" through 1":
3,000-lb socket welding Nicholson
(Flexitallic) union, carbon steel
body, stainless steel-graphite/mica
gasket, AAR dimensions;
Nicholson 3000-SUA-W.

Flanges and Gaskets


Where make-and-break joints are
necessary, use ANSI 1/16-inch
raised-face flanges. Flanges within a
finish of 125 to 250 microinches
are generally used. Flange surfaces
must be free from nicks, dents, and
scratches, as these may cause the
joint to leak.
Spiral-wound, stainless steel and
flexible graphite gaskets are generally used with DOWTHERM fluid on
300-lb flanges. Any time a joint is
taken apart and put back together,
the gasket must be replaced with a
new one.
The temperature and pressure
ratings for ANSI flanges are given
in Tables 1 and 2, pages 16 and 17.
The rating used should match the
temperature and pressure setting of
the safety valve.
Raised face 1/2" and up: 300-lb.
raised face welding neck flange,
ASTM A-105, ANSI B16.5, bore
to match pipe.

Gasket sealants are sometimes


employed to improve the sealing
characteristics in a flanged connection. Where used, care should be
taken to avoid contaminating the
inside of the pipeline with the
sealant.

Joint (Thread) Compounds


Tubing: Solders melting at or
above 1,100F.
NPT Tube Fitting: Permatex No. 2
thread compound.

Bolt Lubricants
Manufacturers of Gaskets
John Crane Incorporated
Morton Grove, Illinois
(CRANE-FOIL gaskets)
Flexitallic, Incorporated
Pennsauken, New Jersey
(Spiral-wound stainless steel, and
FLEXICARB flexible graphite
gaskets; GRAFOIL gaskets and
gasket materials)
Furon Company
FlexSeal Division
Houston, Texas
(FlexSeal metallic and nonmetallic static seals)
Lamons Gasket Company
Houston, Texas
(SPIRALSEAL spiral-wound
gaskets)

MOLY-LIT or FEL PRO C-100

Manufacturers of Pipe Joint


Sealants/Lubricants
Permatex Industrial Corporation
Newington, Connecticut
(Pipe joint compound, thread
sealant with TEFLON, -60 to 350F)
The Swagelok Companies
Solon, Ohio
(SILVER GOOP)
UCAR Carbon Company,
Incorporated
Cleveland, Ohio
(GRAFOIL Grade GTS Thread
Sealant Paste)

Marine & Petroleum


Manufacturing, Incorporated
Freeport, Texas
(GRAPHONIC Gaskets)
PfaudlerU.S., Incorporated
Rochester, New York
(Complete line of multi-purpose
gaskets)
UCAR Carbon Company,
Incorporated
Cleveland, Ohio
(GRAFOIL Grades GHR and
GHE gasket laminate material)

15

Table 1 Pressure-Temperature Ratings for ANSI 150 Pound Flanges1,2


Pressures are in psig Class 150
Material
Group No.

1.1

1.2

1.3

1.4

1.5

1.7

1.9

Carbon Steel

Temp.
F

1.10

1.13

1.14

2.1

2.2

Alloy Steels

2.4

2.5

2.6

2.7

Austenitic Steels

1/2 Cr- 1Cr


1/2 Mo 1/2Mo
CNi- Cr- 11/4 Cr- 21/4 Cr- 5Cr1/2Mo Mo 1/2Mo 1Mo 1/2Mo

Carbon Steel

2.3

9 Cr1Mo

Type
304

Type
316

Type
304L
Type
316L

Type
321

Types
347,
348

Type
309

Type
310

-20 to 100
200
300

285
260
230

290
260
230

265
250
230

235
215
210

265
260
230

290
260
230

290
260
230

290
260
230

290
260
230

290
260
230

275
235
205

275
240
215

230
195
175

275
235
210

275
245
225

260
230
220

260
230
220

400
500
600

200
170
140

200
170
140

200
170
140

200
170
140

200
170
140

200
170
140

200
170
140

200
170
140

200
170
140

200
170
140

180
170
140

195
170
140

160
145
140

190
170
140

200
170
140

200
170
140

200
170
140

650
700
750

125
110
95

125
110
95

125
110
95

125
110
95

125
110
95

125
110
95

125
110
95

125
110
95

125
110
95

125
110
95

125
110
95

125
110
95

125
110
95

125
110
95

125
110
95

125
110
95

125
110
95

800
850
900

80
65
50

80
65
50

80
65
50

80
65
50

80
65
50

80
65
50

80
65
50

80
65
50

80
65
50

80
65
50

80
65
50

80
65
50

80
65

80
65
50

80
65
50

80
65
50

80
65
50

950
1000

35
20

35
20

35
20

35
20

35
20

35
20

35
20

35
20

35
20

35
20

35
20

35
20

35
20

35
20

35
20

35
20

1Ratings

based on all flange facings other than ring joints, with provision that gasket material and dimensions conform to ASME Unfired Pressure Vessel Code
recommendations which are generally accepted as standard in the trade.

2Table

extracted from American Standard Steel Pipe Flanges Fittings (ASME/ANSI B16.5-1988) with permission of the publisher, The American Society
of Mechanical Engineers, United Engineering Center, 345 E. 47th St., New York, New York 10017.

16

Table 2 Pressure-Temperature Ratings for ANSI 300 Pound Flanges1,2


Pressures are in psig Class 300
Material
Group No.

1.1

1.2

1.3

1.4

1.5

1.7

1.9

Carbon Steel

Temp.
F

1.10

1.13

1.14

2.1

2.2

Alloy Steels

2.4

2.5

2.6

2.7

Austenitic Steels

1/2Cr- 1Cr
1/2Mo 1/2Mo
CNi-Cr- 11/4 Cr- 21/4 Cr- 5Cr1/2Mo Mo 1/2Mo 1Mo 1/2Mo

Carbon Steel

2.3

9Cr1Mo

Type
304

Type
316

Type
304L
Type
316L

Type
321

Types
347,
348

Type
309

Type
310

-20 to 100
200
300

740
675
655

750
750
730

695
655
640

620
560
550

695
680
655

750
750
730

750
710
675

750
715
675

750
750
730

750
750
730

720
600
530

720
620
560

600
505
455

720
610
545

720
635
590

670
605
570

670
605
570

400
500
600

635
600
550

705
665
605

620
585
535

530
500
455

640
620
605

705
665
605

660
640
605

650
640
605

705
665
605

705
665
605

470
435
415

515
480
450

415
380
360

495
460
435

555
520
490

535
505
480

535
505
480

650
700
750

535
535
505

590
570
505

525
520
475

450
450
445

590
570
530

590
570
530

590
570
530

590
570
530

590
570
530

590
570
530

410
405
400

445
430
425

350
345
335

430
420
415

480
470
460

465
455
445

465
455
445

800
850
900

410
270
170

410
270
170

390
270
170

370
270
170

510
485
450

510
485
450

510
485
450

510
485
450

510
440
355

410
485
450

395
390
385

415
405
395

330
320

415
410
405

455
445
430

435
425
415

435
425
415

950
1000
1050

105
50

105
50

105
50

105
50

280
165

345
215
190

380
225
140

380
270
200

260
190
140

370
290
190

375
325
310

385
365
360

385
355
345

385
365
360

385
335
290

385
350
335

1100
1150
1200

95
50
35

115
105
55

105
70
45

115
75
50

260
195
155

325
275
205

300
235
180

325
275
170

225
170
130

290
245
205

1250
1300
1350

110
85
60

180
140
105

140
105
80

125
95
70

100
80
60

160
120
80

1400
1450
1500

50
35
25

75
60
40

60
50
40

50
40
35

45
30
25

55
40
25

1Ratings

based on all flange facings other than ring joints, with provision that gasket material and dimensions conform to ASME Unfired Pressure Vessel Code
recommendations which are generally accepted as standard in the trade.

2Table

extracted from American Standard Steel Pipe Flanges Fittings (ASME/ANSI B16.5-1988) with permission of the publisher, The American Society
of Mechanical Engineers, United Engineering Center, 345 E. 47th St., New York, New York 10017.

17

Instrumentation Piping
Instrument piping is defined as the
piping from the first block valve
off the heat transfer fluid line
(not including the valve) to the
instrument. Welded instrument
piping is preferred. Use threaded
piping only for heat transfer fluid
instrumentation in this specification. For items not listed here, the
preceding piping specifications
should be used where applicable.
Pipe fittings (elbows, tees,
crosses, reducers) 1/2" thru 1":
3000-lb threaded forged steel fittings,
ASTM A-105, ANSI B16.11
Pipe caps 1/2" thru 1": 3000-lb
threaded forged steel cap, ASTM
A-105, ANSI B16.11.

Gate Valves for


Instrument Lines
Valves 1/2" thru 1": 800-lb forged
steel screwed gate. 800-lb at 850F,
forged carbon steel body and
bonnet, 13% chrome trim, H.F.
seat rings, solid wedge, rising stem,
OS&Y, welded bonnet, conventional port.
Gate Valves for Instrument Lines
Manufacturer

Part
Number

Anvil

Fig. 825

/4" 2"

Size

Pipe caps 1/2" thru 1": Threaded


solid steel hex bull plug, ASTM
A-696 GR B or C barstock, Norris.

Smith

870-00000

/4" 2"

Vogt

2801

/4" 2"

Couplings 1/2" thru 1": 3000-lb


threaded forged steel coupling,
ASTM A-105, ANSI B16.11.

Methods of Making
Branch Connections

Couplings 1/2" thru 1": 3000-lb


threaded forged steel Threadolet
fitting, ASTM A-105.
Unions 1/2" thru 1": 3000-lb
threaded Nicholson (Flexitallic)
union, carbon steel body, stainless
steel-graphite/mica gasket, AAR
dimensions; Nicholson 3000-SUA-T.
Reducers 1/2" thru 1": Extrastrong steel swaged nipple, ASTM
A-106 or A-53 GR B, or ASTM A696 GR B or C barstock, threaded
both ends.
Pipe Nipples 1/2" thru 1": ASTM
A-106 GR B, extra-strong seamless
steel pipe nipple, threaded. Closed
nipples shall not be used.
Thread Compound: Permatex No.
2 thread compound.

18

Cleaning Procedures: Wire brush


to clean threads. Apply joint
compound. Avoid using chlorinated cleaning solvents.

/2" thru 1": For socket welding


piping, use straight size or reducing
tee. Reducer insert may be used in
place of reducing tee.

Shutoff and
Throttling Valves
Steel valves with high-temperature
flexible graphite packing are
recommended for use with
DOWTHERM fluids. Valves that
utilize metal bellows primary seals
with high-temperature secondary
packing may provide extra protection and service with DOWTHERM
fluids. Brass valves should be
avoided because of ANSI Code
temperature limitations.
All socket weld valves that terminate a line should have a threaded
nipple welded into the valve and
be capped.
Pack valves with Union Carbide
Grafoil high-temperature packing
using the following system:
Bottom One ring of John Crane
1625G braided graphite filament,
or equivalent.
Middle Union Carbide GTK dieformed Grafoil rings with passive
inhibitor, or equivalent.
Top One ring of John Crane
1625G, or equivalent.

Tight Shutoff Valves

/2" thru 1": For socket welding


branch connections for welded
piping, use Sockolet welded to
header.
11/2" and up: For welded piping,
use straight size or reducing tee.
Weldolet may be used in place of
reducing tee when branch is
smaller than header.

2" and up: 300-lb ANSI flanged


rising stem ball valve. Carbon steel
body, nickel faced ball, stainless
steel tube insert, ASTM A-193 B7
bolting.
2" and Up 300-lb ANSI Flanged
Rising Stem Ball Valve
Manufacturer

Part
Number

Orbit

1233H8
Regular Port

Size
2" 20"

Globe Valves

Gate Valves

Check Valves

1
/2" thru 1": 800-lb forged steel
socket weld globe. 800-lb at 850F,
forged carbon steel body and
bonnet, 13% chrome stainless steel
trim, loose threaded disc, OS&Y,
welded bonnet.

1
/2" thru 1": 800-lb forged steel
socket weld gate. 800-lb at 850F,
forged carbon steel body and
bonnet, 13% chrome trim, H.F.
seat rings, solid wedge, rising stem,
OS&Y, welded bonnet, conventional port.

Check valves in systems using


DOWTHERM fluid cannot be relied
upon for positive seal, and where
necessary, should be supplemented
with shutoff valves. Where check
valves are used in condensate
return lines, they should not be
spring-loaded. Satisfactory check
valves are available from the
suppliers of shutoff and throttling
valves.

/2"1": 800-lb Forged Steel


Socket Weld Globe Valves
Manufacturer
Anvil
Smith
Vogt

Part
Number
Fig. 860

Size
1

/4" 2"

G87-0000W

/4" 2"

SW2821

/4" 2"

/2"1": 800-lb Forged Steel


Socket Weld Gate Valves
Manufacturer

/2" thru 11/2": 300-lb forged


steel flanged globe. 300-lb. at
800F, 740-lb at 100F, forged steel
body and bonnet, 13% chrome
trim, H.F. seat, rising stem, OS&Y,
loose disc, bolted bonnet.

/2" 11/2": 300-lb Forged Steel


Flanged Globe Valves

Manufacturer

Part
Number

Size

G83-00060

/2" 2"

Anvil

Fig. 332

/2" 2"

Velan

F-1074-B-DZTY

/2" 2"

Smith

Anvil

Fig. 825

Smith

870-0000W

/4" 2"

SW-2801

/4" 2"

Bonney Forge WL-11-SW

/4" 2"

Velan

/4" 2"

2" and Up 300-lb Cast Carbon


Steel Flanged Globe Valves
Manufacturer

Part
Number

Size

Kitz

300 SCJB

2" 12"

Newco

23F-CB2

2" 12"

Velan

F-174B-2T

2" 12"

W-2054W-02TY

/4" 2"

/2" thru 11/2": 300-lb forged


steel flanged gate. 300-lb at 800F,
740-lb at 100F, forged steel body
and bonnet, 13% chrome trim, H.F.
seat rings, solid wedge, rising stem,
OS&Y, bolted bonnet.
1

/2" 11/2" 300-lb Forged Steel


Flanged Gate Valves

Manufacturer

Part
Number

Size

Fig. 321

/2" 2"

Smith

830

/2" 2"

Vogt

363

/2" 2"

Velan

1054B-02TY

/2" 2"

Anvil

2" and up: 300-lb cast carbon steel


flanged globe. 300-lb at 750F,
carbon steel body, 13% chrome
alloy stem and disc, nickel alloy
seat rings, rising stem, OS&Y,
bolted bonnet.

Size
1

Vogt
1

Part
Number

2" and up: 300-lb carbon steel


flanged gate. 300-lb at 800F, 600lb at 100F, carbon steel body, 13%
chrome trim, H.F. seat rings,
flexible wedge, rising stem, OS&Y,
bolted bonnet.

/2" thru 1": 800-lb F.S. socket


weld swing check. 800-lb at 825F,
2000-lb at 100F, body forged steel
ASTM A-105, 13% chrome to H.F.
seat and disc, integral cover.
1
/2"1": 800-lb F.S. Socket Weld
Swing Check Valves

Manufacturer

Part
Number

Anvil

Fig. SW847

/2" 2"

SWS74

/2" 2"

Vogt

Size

1" and up: 300-lb C.S. flanged


swing check. 300-lb at 800F, 740lb at 100F, cast carbon steel body,
13% chrome to H.F. disc and seat,
bolted cover, raised face flanges.
1" and Up 300-lb C.S. Flanged
Swing Check Valves
Manufacturer

Part
Number

Size

Kitz

300 SCOB

2" 24"

Newco

33F-CB2

2" 24"

Velan

F-101114C-02TY 2" 24"

2" and Up 300-lb Carbon Steel


Flanged Gate Valves
Manufacturer

Part
Number

Size

Kitz

K300-SCLSF

2" 24"

Newco

13F-CB2

2" 24"

Velan

F-1064C-02TY

2" 24"

19

Table 3 Manufacturers of Shutoff and Throttling Valves1


Type of Valve
Company

Ball

Bellows Butterfly

Anvil
Bonney Forge Corp.
BS&B Process Systems, Inc.
Conbraco Industries, Inc.
Crane Valves
Dresser Industries, Inc.
Duriron Co./Valve Div.
Dwyer Instruments, Inc.

Masoneilan/Dresser
Newco
Nibco, Incorporated
Orbit

1 Table

Gate

Globe

Plug

The William Powell Co.


Smith Valve Corp.
Stockham Valve & Fittings, Inc.
Vanessa Valve Corp

Velan Valve Corp.


Henry Vogt Machine Co.
Yarway Corp.

Control

EG&G Sealol Eagle Valve


Fisher Controls Intl., Inc.
Foxboro Company
Invalco, Inc.
Kerotest Mfg. Co.
Kitz Corp of America
Richard Klinger, Inc.
The Luckenheimer Co.

Check

3 is presented for reference only. This listing does not imply that a particular manufacturer and/or valve are a part of Dows piping specifications, nor does
the listing of a manufacturer imply approval or recommendation by Dow of any manufacturer to the exclusion of others that may produce a suitable product.

20

VII. INDEX TO SUPPLIERS


Company

Page(s)

ABB Lummus Heat Transfer .............................................................. 3, 4, 5


American Econo-Therm Division ..................................................... 3, 4, 5
American Hydrotherm Corporation .................................................. 3, 4, 5
American Schack Company, Incorporated ....................................... 3, 4, 5
Ametek, Incorporated, Thermox Instruments Division ........................... 6
Ametek, Incorporated, U.S. Gauge Division .......................................... 11
Anvil............................................................................................. 18, 19, 20
Armstrong International, Incorporated ................................................... 12
Artisan Industries, Incorporated .................................................... 3, 4, 5, 6
Bechtel Group, Incorporated ..................................................................... 3
The Bethlehem Corporation, Process Equipment Group ..................... 4, 6
Blaw Knox Food & Chemical Equipment Company, Incorporated ..... 5, 6
Bonney Forge Corporation................................................................. 19, 20
G. C. Broach Company ...................................................................... 4, 5, 6
John Brown E&C, Incorporated ................................................................ 3
Brown Fired Heater Division ................................................................. 5, 6
Brown & Root, Inc. .................................................................................... 3
BS&B Process Systems, Incorporated .................................... 3, 4, 5, 10, 20
Buffalo Pumps, Inc. .................................................................................... 7
BW/IP International, Incorporated, Pump Division ................................. 7
BW/IP International, Incorporated, Seal Division ................................... 8
Chempump Division, Crane Company ..................................................... 7
Cherry-Burrell Process Equipment Division .......................................... 5, 6
A. W. Chesterton Company ...................................................................... 8
Chromalox .................................................................................................. 5
Clark-Reliance Corporation .......................................................... 6, 11, 12
Conbraco Industries, Incorporated .............................................. 10, 12, 20
Crane Valves ............................................................................................ 20
John Crane Incorporated ..................................................................... 8, 15
Crosby Valve & Gage Company .......................................................... 6, 12
Cuno, Incorporated .................................................................................. 13
Dean Pump Division, MET-PRO Corporation .......................................... 7
DEC International, Engineered Products Group .................................. 5, 6
Dickow Pump Company ........................................................................ 6, 7
Dow Engineering Company ....................................................................... 3
Dresser Industries, Incorporated, Industrial Valve Operation ........... 12, 20

21

INDEX TO SUPPLIERS (CONT.)


Company

Page(s)

Durametallic Corporation .......................................................................... 8


The Duriron Company, Incorporated, Pump Division .......................... 5, 7
The Duriron Company, Incorporated, Valve Division .................. 5, 10, 20
Dwyer Instruments, Incorporated ...................................................... 11, 20
EG&G Sealol, Eagle Valve ...................................................................... 20
EG&G Sealol, Industrial Sealing Division ................................................ 8
First Thermal Systems, Incorporated ..................................................... 3, 5
Fisher Controls International, Incorporated ................... 5, 6, 8, 10, 11, 20
Flexitallic, Incorporated ....................................................................... 8, 15
Fluor Daniel, Incorporated ......................................................................... 3
Foster Wheeler USA Corporation ......................................................... 3, 5
The Foxboro Company ................................................................ 10, 11, 20
Fulton Thermal Corporation ..................................................................... 5
Furon Company, FlexSeal Division ......................................................... 15
Goulds Pumps, Incorporated ...................................................................... 7
Heatec, Incorporated ......................................................................... 3, 5, 6
Hynes Electric Heating Company ......................................................... 5, 6
INDEECO .............................................................................................. 5, 6
Ingersoll-Dresser Pump Company .............................................................. 7
The International Boiler Works Company............................................ 3, 5
Invalco, Incorporated ..................................................... 5, 6, 10, 11, 12, 20
ITT Standard .............................................................................................. 5
JM Clipper Corporation ............................................................................. 8
Kerotest Manufacturing Company .......................................................... 20
Kitz Corporation of America ....................................................... 10, 19, 20
Richard Klinger, Incorporated ........................................................... 10, 20
The Kontro Company, Incorporated ..................................................... 6, 7
Lamons Gasket Company ........................................................................ 15
Lockwood Greene Engineers, Incorporated .............................................. 3
The Luckenheimer Company .................................................................. 20
Magnetrol International .......................................................................... 11
Manning & Lewis Engineering Company ............................................. 5, 6
Marine & Petroleum Manufacturing, Incorporated ............................ 5, 15
Masoneilan North America,
Dresser Valve & Controls Division ................................. 6, 10, 11, 20
Memcor Power Generation Division, Memtec America Corporation ... 13
Michigan Science & Engineering Associates ............................................ 3

22

INDEX TO SUPPLIERS (CONT.)


Company

Page(s)

Micro Motion ........................................................................................... 10


Newco ................................................................................................. 19, 20
Nibco, Incorporated ................................................................................. 20
Orbit Valve Company ........................................................................ 18, 20
Owens-Corning Fiberglas ......................................................................... 13
Pall Process Filtration Company .............................................................. 13
Parker Hannifin Corporation, Commercial Filters Division .................. 13
The Ralph M. Parsons Corporation ........................................................... 3
Permatex Industrial Corporation ............................................................. 15
Petro-Chem Development Company, Incorporated ............................. 3, 5
PfaudlerU.S., Incorporated ...................................................... 3, 5, 6, 15
Pittsburgh Corning Corporation .............................................................. 13
The William Powell Company ................................................................ 20
Raytheon Engineers & Constructors ......................................................... 3
Riley Stoker Corporation ........................................................................... 5
Schuller International, Incorporated, Mechanical Insulation Division . 13
Walter F. Seifert, Consulting Engineer ...................................................... 3
Smith Valve Corporation ............................................................. 18, 19, 20
Spirax Sarco ......................................................................................... 6, 12
Stockham Valve & Fittings, Inc. ............................................................. 20
Stone & Webster Engineering Corporation .............................................. 3
Struthers-Wells Corporation.................................................................. 5, 6
Sundstrand Fluid Handling ........................................................................ 7
SUPER-TROL Division, Enercon Systems, Incorporated .................... 5, 6
Sverdrup Technology, Incorporated ........................................................... 3
The Swagelok Companies ........................................................................ 15
Teledyne Farris Engineering ..................................................................... 12
Thermoflux, Incorporated .......................................................................... 5
UCAR Carbon Company, Incorporated ....................................... 8, 13, 15
Union Pump Company .............................................................................. 7
Vanessa Valve Corporation ...................................................................... 20
Velan Valve Corporation ................................................................... 19, 20
Henry Vogt Machine Company ............................................... 6, 18, 19, 20
Wellman Thermal ...................................................................................... 5
Worcester Controls ................................................................................ 6, 8
Yarway Corporation ....................................................... 6, 7, 10, 11, 12, 20

23

EQUIPMENT FOR SYSTEMS


USING DOWTHERM *
HEAT TRANSFER FLUIDS
Includes heat transfer system
hardware and fabrication guidelines

For more information about DOWTHERM heat transfer fluids,


call: 1-800-447-4369

NOTICE: Dow believes the information and recommendations contained herein to be accurate and reliable as of August, 1994. However, since any assistance
furnished by Dow with reference to the proper use and disposal of its products is provided without charge, and since use conditions and disposal are not within its
control, Dow assumes no obligation or liability for such assistance and does not guarantee results from use of such products or other information contained herein.
No warranty, express or implied, is given nor is freedom from any patent owned by Dow or others to be inferred. Information contained herein concerning laws and
governmental regulations is based on U.S. federal laws and regulations except where specific reference is made to those of other jurisdictions. Since use conditions
and governmental regulations may differ from one location to another and may change with time, it is the Buyers responsibility to determine whether Dows products
are appropriate for Buyers use, and to assure Buyers workplace and disposal practices are in compliance with laws, regulations, ordinances, and other governmental
enactments applicable in the jurisdiction(s) having authority over Buyers operations.
Note: Many of the product names cited in this bulletin are trademarks of their manufacturers.

Printed in U.S.A.

*Trademark of The Dow Chemical Company

Form No. 176-01335-894AMS

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