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Paten US1944444 - Production of copper sulphate in solution from metallic or scrap copper and ... - Google Paten
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US1944444 A
Pemberian
23 Jan 1934
1 Jul 1931
1 Jul 1931
Penemu
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Paten US1944444 - Production of copper sulphate in solution from metallic or scrap copper and ... - Google Paten
allow the escape oi excess air or steam when such pressure is attained. Air under pressure, supplied from an air tank or
compressor or blower is introduced through valves 5 and 7 together with the steam. The solution is maintained at 90 degrees
to 100 degrees centigrade and the pressure which is maintained Within the oxidizing tank A during this reaction is above
atmospheric pressure, preferably in the neighborhood of 25 to 30 pounds per `square inch. A certain amount of air is
continually escaping through relief valve 9 and the more rapidly the air is forced through the liquid, the more rapid Will be the
conversion of the metallic copper to copper sulphate in solution.
When the reaction is complete, the steam is discontinued and the copper sulphate solution is forced through lter 11 and into
crystallizing tank 13 Where it is allowed to cool and crystallize. 'Ihe uncrystallized portion is returned to tank A through pump
14 and pipe 15 for further concentration.
`While We have shown one form of apparatus suitable for carrying out our process, various other forms of apparatus may be
employed for g5 this purpose, the essential feature or" our process being the conversion of metallic copper to copper
sulphate solution While in a closed reaction vessel by introducing an oxidizing agent such as air or air and steam, the
conversion or reaction taking .100 place under pressure greater than atmospheric pressure and at an elevated temperature.
Having thus described our invention, what we claim and desire to secure by Letters Patent is:
1. The process which consists of heating a 105 dilute solution of sulphuric acid in a closed reaction vessel containing
metallic copper immersed therein, passing air into the vessel and through said solution while maintaining Within the reaction
vessel, a pressure above atmospheric 110 above pressure andan elevated temperature so as to convert metallic copper into
copper sulphate solution.
2. The process which comprises passing air through a hot solution of dilute sulphuric acid containing metallic copper
immersed therein, passing air into the vessel, under a pressure greater than atmospheric while heating the solution to an
elevated temperature.
3. The method of producing copper sulphate in solution by immersing metallic copper in a dilute solution of sulphuric acid
while in a closed vessel, passing air and steam into the vessel under a pressure greater than atmospheric pressure and at
an elevated temperature and allowing the solution to run into crystallizing tank,V cool and crystallize.
4. The process which comprises subjecting metallic copper to the oxidizing action of air and steam while immersed in a hoi'
solution of dilute sulphuric acid within a closed reaction vessel wherein the pressure is greater than atmospheric pressure.
5. The process which comprises subjecting metallic copper to the oxidizing action of air and steam While immersed in a
solution of copper sulphate within a closed reaction vessel wherein the pressure is greater than atmospheric pressure.
6. The method of producing copper sulphate in solution by immersing metallic copper in a dilute solution of sulphuric acid
while in a closed vessel and passing air and steam into the vessel under a pressure greater than atmospheric pressure.
'7. In a process of dissolving metallic copper in sulphuric acid which comprises suspending metallic copper in dilute
sulphuric acid, and acting upon said reaction mixture with an oxygen containing gas, Vthe step of maintaining the reaction
mixture at super-atmospheric pressure and at an elevated temperature.
DANIEL W. MARSH. BENJAMIN H. MARSH.
DIRUJUK OLEH
Merujuk Paten
Tanggal pengajuan
Tanggal publikasi
Pemohon
Judul
US2533245 *
24 Feb 1948
12 Des 1950
Tennessee Copper
Company
US2726929 *
31 Jan 1951
13 Des 1955
US3632308 *
5 Des 1969
4 Jan 1972
US6294146 *
9 Ags 1999
25 Sep 2001
Gabriel Benet
KLASIFIKASI
Klasifikasi AS
423/557
Klasifikasi Internasional
C01G3/10
Klasifikasi Gabungan
C01G3/10
Klasifikasi Eropa
C01G3/10
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