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1. Scope
1.1 This specification covers mineral-colloid-stabilized,
emulsified coal-tar pitch suitable for use as a weatherprotective and aliphatic-solvent resistant coating over bituminous pavements of airports, parking areas, and driveways.
1.2 The values stated in SI (metric) units are to be regarded
as the standard.
1.3 The following precautionary caveat pertains only to the
test method portion, Section 6, of this specification: This
standard does not purport to address all of the safety concerns,
if any, associated with its use. It is the responsibility of the user
of this standard to establish appropriate safety and health
practices and determine the applicability of regulatory limitations prior to use.
2. Referenced Documents
2.1 ASTM Standards:
D 140 Practice for Sampling Bituminous Materials2
D 466 Test Methods for Films Deposited from Bituminous
Emulsions2
D 490 Specification for Road Tar3
D 529 Test Method for Accelerated Weathering Test Conditions and Procedures for Bituminous Materials (CarbonArc Method)2
D 2939 Test Methods for Emulsified Bitumens Used as
Protective Coatings2
2.2 Federal Specification:
VV-K-211 Kerosene4
6. Test Methods
6.1 Wet Film ContinuityUsing a spatula, spread the wet
emulsion to a thin film on a sheet of standard 67.7-g/m2(18-lb)
mimeograph paper. As the emulsion is drawn out to a smear, it
shall show a uniformly smooth nongranular consistency, free
of coarse particles.
6.2 Resistance to Freezing (when specified)Expose a
representative specimen of the emulsion to a temperature
of 18C (0F) for 24 h; then warm the specimen to 25C
(77F) in an environment not exceeding 38C (100F) and stir
thoroughly.
5. Sampling
5.1 Sample in accordance with Practice D 140 and Test
Methods D 2939.
1
This specification is under the jurisdiction of ASTM Committee D08 on
Roofing, Waterproofing, and Bituminous Materials and is the direct responsibility of
Subcommittee D08.09 on Bituminous Emulsions.
Current edition approved June 10, 2000. Published August 2000. Originally
published as D 3320 74 T. Last previous edition D 3320 90(1998).
2
Annual Book of ASTM Standards, Vol 04.04.
3
Annual Book of ASTM Standards, Vol 04.03.
4
Available from Standardization Documents Order Desk, Bldg. 4 Section D, 700
Robbins Ave. Philadelphia, PA 19111-5094, Attn: NPODS.
NOTE 3In any test utilizing an oven, the oven to be used shall be a
gravity convection type. The internal dimensions of the oven shall be not
less than 305 by 305 by 305 mm (12 by 12 by 12 in.).
Copyright ASTM, 100 Barr Harbor Drive, West Conshohocken, PA 19428-2959, United States.
D 3320
TABLE 1 Physical Properties of Emulsified Coal-Tar Pitch (Mineral Colloid Type)
Characteristics
Property
Min
Wet film continuity
Resistance to freezing (when specified)
Density at 25C (77F), kg/m3
Volatiles, %
Residue by evaporation, %
Resistance to volatilization, residue weight loss, %
Solubility of residue in CS2, %
Ash content of residue, %
Flammability
Drying time, firm set, h
Resistance to heat
Resistance to kerosine
Resistance to water
Resistance to impact before and after accelerated weathering
Max
...
63
...
15
...
40
8
Degrease the metal with a suitable solvent such as trichloroethylene; then polish with steel wool. Protect the reverse side of
the panel against corrosion.
6.14.2 Apply the emulsion with a doctor blade set at a
thickness of 1.6 mm (464 in.) to the prepared surface and allow
to dry as described in 6.12.2.
6.14.3 Then place each specimen, coating uppermost, on a
solid horizontal base, and subject it to the impact of a 0.9-kg
(2-lb) steel ball dropped from a height of 2.4 m (8 ft). Conduct
the test at 25 6 1C (77 6 2F). Examine the coating
immediately for evidence of chipping, cracking, or loss of
adhesion to the metal.
6.15 Resistance to Impact after Accelerated Weathering:
6.15.1 Prepare the specimens used in this test in accordance
with 6.14; then subject them to 25 cycles of cycle B as
described in Test Method D 529.
6.15.2 At the completion of the accelerated weathering
period, subject each specimen to the impact test as described in
6.14.3.
D 3320
from normal hazards of handling and shipping.
10.2 Each package shall be plainly marked with the name
and brand of the manufacturer or distributor as well as the type
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