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Scheme 1
Figure 1. Crystal structure of 46. Top: ball and cylindrical representation; bottom: Space-filling representation.
JA001411I
(10) Crystal data of 46: see Supporting Information.
(11) The equilibration 33 / 47 shifts toward 7 at low concentrations.
NMR data of 3 and 7 (from the mixture of 3 and 7): see Supporting
Information.