Beruflich Dokumente
Kultur Dokumente
Minerals Engineering
journal homepage: www.elsevier.com/locate/mineng
a r t i c l e
i n f o
Article history:
Available online 26 October 2013
Keywords:
Hydrocyclone
Partition curve
Classication
Fish-hook
Fine particle separation
a b s t r a c t
In many cases, the hydrocyclone partition curve exhibits a non-monotonic course in the ne particle
range. The so-called sh-hook effect indicates an increased separation of the ne fraction, which is of
practical interest and has a positive effect on solid/liquid separation. However, for classication purposes,
the separation is less distinct. In this contribution an equation of a partition curve containing a sh-hook
is derived considering the laws of disturbed settling in dense, polydisperse suspensions. The following
effects are considered: the entrainment of ne particles in the boundary layer of the coarse settling particles, the hindered settling due to the increased effective density and viscosity of the uid, and the counter ow of the displaced uid caused by the settling particles. The calculations indicate that the sh-hook
effect is primarily caused by ne particle entrainment, which is inuenced by the feed solid content and
the feed particle size distribution. An approximated analytical solution for the partition curve is presented for aRosinRammlerSperlingBennet (RRSB)-distributed feed. Experiments using 25-mm hydrocyclone conrm the calculations.
2013 Elsevier Ltd. All rights reserved.
1. Introduction
The fundamental scheme for the hydrocyclone is shown in
Fig. 1a.
The partition curve (Fig. 1b) used to characterize the separation
efciency of the hydrocyclones involves the mass fraction T(d) for
each particle size d, which is discharged in the coarse product
(underow). Schubert and Neesse (1980) demonstrated that the
typical S-shaped partition curve derives from the superposition
of the settling ow and a turbulent diffusion ow in the rotating
uid.
The so-called tapping model (Neesse et al. (1991), Schubert
(2010)), which neglects the distribution of the hydrodynamic characteristics in the processing zone of the apparatus, describes the
inuence of various factors on the separation characteristics. The
theoretical partition curve calculated using the free settling velocity according to the Stokes formula, increases monotonically with d
(see the dashed curve in Fig. 1b).
However, in many cases in the ne particle range, an increased
particle removal can be observed (see the continuous curve in
Fig. 1b). This so-called sh-hook effect is subject of many investigations and discussions.
Corresponding author at: Friedrich-Alexander-Universitt, Erlangen-Nuremberg, Germany. Tel.: +49 9131 85 23 200.
E-mail address: johann.dueck@mbt.uni-erlangen.de (J. Dueck).
0892-6875/$ - see front matter 2013 Elsevier Ltd. All rights reserved.
http://dx.doi.org/10.1016/j.mineng.2013.10.004
26
Nomenclature
a
cV
d
dm
Dc
Do
Din
Dt
D(d)
E(d)
fe(d)
g(cV)
q(d)
H
centrifugal acceleration ()
entrainment constant ()
total volume solid concentration ()
particle size (lm)
characteristic particle size (lm)
diameter of the cylindrical portion of the hydrocyclone
(mm)
overow diameter (mm)
diameter of the inlet (mm)
coefcient of turbulent diffusion (m/s2)
deceleration function for the disturbed settling ()
acceleration function ()
entrainment function ()
function of solids content ()
density of the particle size distribution (lm1)
depth of the sh-hook ()
n
uin
Dp
s
S
T(d)
Vh(d)
VS(d)
VSt,j
wtan
_o
W
_u
W
qf
qp
lf
C
Td
1
h
i:
Dc
V s d
1 Sexp 2D
t
Overflow
Do
Din
Vortex finder
Dc
Inlet
Partition function
0.75
Partition function
(after Stokes)
0.5
H
0.25
0
0
Du
10
15
Particle size d, m
Underflow
(a)
(b)
Fig. 1. (a) Principal scheme for the hydrocyclone and (b) partition curve of the hydrocyclone.
20
27
As demonstrated by Eq. (2), the predicted sedimentation velocity of a particle depends not only on its size, the medium properties, and the solid-phase concentration in the suspension but also
on the particle size distribution.
4. Approximation for the RRSB size distribution
In the present work, specic equations are derived for a typical
case when the two-parameter RRSB (RosenRammlerBennet
Sperling) function for the particle size distribution is used:
qd
n1
n
n d
d
exp
dm dm
dm
0
11=3
2
2
B
C
V S d
dm
6=n 1C 6=n 1
C
gcV B
1
@ 6n
A
V h d
d
n
bd
6=n
1
C
6=n
1
dm
2
dm
2
cV C
1
n
d
V S d
2
2
1 d gcV fe bd d cV
V h d
s2 gcV fe bsqsds
ad2j qp qf
18lf
V S d
1ED
V h d
E
dm
d
D
2
dm
d
0
@
0:9c0:46
V
6n
n
2 (
6:8 )
2
3
2:6 10 cV
n
11=3
A
The rst term on the right side of Eq. (2) corresponds to the hindered sedimentation velocity of a particle (the Stokes velocity accounts for the impact of solid content). The second term, the
2
acceleration function E d gcV fe bd, reects the increase in
the particle velocity due to its entrainment by larger particles.
R1
2
The third term, the deceleration function D d cV 0
s2 gcV fe bsqsds, determines how the ow of the liquid displaced by the settling solid phase inuences the particle settling
velocity.
In Eq. (2) the following designations are used: a centrifugal
acceleration, entrainment constant, cV total solid volume concentration, g(cV) function of the intensity of the entrainment on
the solid concentration, fe(d) entrainment function, q(d) density
of the particle size distribution, VSt(d) Stokes settling velocity,
Vh(d) hindered settling velocity, qf uid density, qp solid
density, lf uid viscosity in kg/ms.
28
1.0E+05
Sedimentation functions,-
1.0E+03
1.0E-01
1.0E-03
1.0E-05
0.01
0.1
10
a w2tan =Dc
wtan 3:7
Din
uin
Dc
Dof
uin 0:52
Din
!0:5
Dp
qf
10
Dt 16 104 wtan Dc :
11
Table 1
Parameters of hydrocyclone experiments.
Hydrocyclone diameter
Inlet diameter
Overow diameter
Feed pressure
Particle density
Particle size distribution of ne material (Mf)
Particle size distribution of coarse material (Mc)
Dc = 25 103 m
Din = 10.5 103 m
Dof = 1 102 m
Dp = 105 Pa
qp = 2.6 g/cm3
dm = 6 lm, n = 1.2
dm = 11 lm, n = 1.3
29
1.0E+08
1.0E+06
0.75
Settling velocity
1.0E+04
0.5
Partition function
(Stokes velocity)
1.0E+02
0.25
Partition function, -
Stokes velocity
Partition function
(disturbed settling)
1.0E+00
0
0.1
10
100
Relative particle size d/dm, Fig. 3. Calculated partition curves and settling velocities for a 25-mm hydrocyclone using a ne particle suspension and solid content cV = 0.04. The parameters are listed in
Table 1.
1
Mf (calc)
Mc (calc)
Mf (exp)
Mc (exp)
Partition function, -
Partition function, -
1
0.8
0.6
0.4
0.8
dm=6 m
0.6
dm=7 m
dm=8 m
0.4
dm=9 m
0.2
0.2
T(d) after
Stokes
0
0
0.1
0.1
10
100
0.8
0.6
Mc (calc)
0.4
T(0), -
Mc (exp)
0.6
Mf (exp)
0.4
Mf (calc)
0.2
T(0) for Mc
0.2
T(0) for Mf
0
0
0.1
0.2
0.3
0.4
Solid volume concentration cV,Fig. 5. Comparison of calculated and measured sh-hook depths as a function of
the solid concentration.
4:5 2:26
V S 0 7:07V St dm c0:46
n
V 1 cV
12
10
100
The maximum value of VS(0) in Fig. 5 occurs at the concentration cV = 0.09, which is higher than the experimental value of
approximately 0.04.
In addition, VS(0) explicitly depends on the parameters dm and n
2
from the size distribution in Eq. (12): V S 0 / dm and VS(0) / n2.26.
Given VS(0), T0 can be easily estimated based on Eq. (1).
The calculated and experimental curves of H are qualitatively
similar, but quantitative differences can arise for various reasonsthe simplications included in Eq. (5), for example. Specically, these variations may be caused by the difference between
the inlet solid concentration used for the calculations and the actual cV values inside the hydrocyclone.
The physically reasonable model appears to adequately describe some of the effects observed in the experiments. A parametric study using the particle size distribution Eq. (3) was performed
to clarify the effect of the constants in the equation on the value of
the sh-hook.
In Fig. 6, each curve is drawn by changing one variable only (dm)
with all other parameters held constant. The increase in dm causes
a marked increase in T0 and smooth increases in the Tmin values,
leading to an increased depth of the sh-hook effect (H), which
can be interpreted as follows: the coarser the particles, the greater
the chance for small particles to enter the boundary layer of a large
particle and be captured by it.
This phenomenon is conrmed by the experiments of Gerhart
(2001) in which small and coarse materials were mixed in various
proportions. In these experiments, the value of H increased steadily
with the proportion of the coarse material.
30
Partition function, -
n=1.1
0.8
n=1.2
0.6
n=1.3
0.4
n=1.4
0.2
T(d) after
Stokes
0
0.1
10
100
Fig. 7 illustrates that the growth of parameter n leads to a weakening of the sh-hook effect.
Thus, the theory predicts that the effect should be particularly
signicant for a suspension with at distribution functions and
more coarse fractions.
7. Conclusions
The presented separation model rst enables the rst approximated calculation of the non-monotonous course of the hydrocyclone partition curve. The model indicates the importance of the
disturbed settling of the particles. Even given the excessive simplications of the complicated three-dimensional turbulent ow inside the cyclone, the separation can be satisfactorily simulated by
considering the particle interactions.
The entrainment of the ne particles by the settling of the
coarse particles is primarily responsible for the sh-hook effect.
Consequently, the parameters of the feed size distribution and
the feed solid content were introduced into the equation for the
partition curve, providing a new element in the separation model.
Although the experimental database remains relatively small, the
experiments with a 25-mm cyclone largely conrm the calculations. One can conclude that the hydrocyclone separation in the
ne particle range is primarily limited by the sh-hook effect,
which can be explained physically. The approximated partition
function also indicates the factors inuencing the sh-hook effect.
These factors can be controlled using known methods: dilution of
the feed and/or changing the feed size distribution using a multistage separation. The opposite is true for thickening and successfully removing the nest fractions in which high sh-hook
fractions would be advantageous, and the addition of coarse
particles for that purpose is less practicable.
References
Bourgeois, F., Majumder, A.K., 2013. Is the sh-hook effect in hydrocyclones a real
phenomenon? Powder Technology 237, 367375.