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  • ASTM B117 - ANO 1997 - Standard Practice For Operating Salt Spray (Fog) Apparatus

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    Denise Roth
    158 Ansichten8 Seiten
    Ensaio de Salt Spray

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    ASTM B117- ANO 1997- Standard Practice for Operating Salt Spray (Fog) Apparatus

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    Ensaio de Salt Spray

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    © All Rights Reserved
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    158 Ansichten8 Seiten

    ASTM B117 - ANO 1997 - Standard Practice For Operating Salt Spray (Fog) Apparatus

    Hochgeladen von

    Denise Roth
    Ensaio de Salt Spray

    Copyright:

    © All Rights Reserved
    Als PDF herunterladen oder online auf Scribd lesen
    Markieren Sie unangemessene Inhalte
    von 8
    HD Designation: 8 117 - 87 Standard Practice for BC Cons.e An. den oR, Operating Salt Spray (Fog) Apparatus’ ‘Tis sandr issued der the red dsgauion B 19; tbe nu orginal adaption or ie the cise of rea, te yout cevson. supererit epalo (ogists ta editor changes ber immedi iy foUow 0g the devgnation indica the year of ‘A curber ia areata adicates hg yeu Ola raprohal. A ce ie ast revision or repro, ‘Peis wendard hae been approved for ne by agers of the Deparment of Defense te rps! Method 811.1 of Feder! Tet Method ‘Standard No, 1518: Consus the BeD Inde of Sreictions ‘ant Sto Departmen af Deere ° 1. Scope 1.1 This practice describes the apparatus, procedure, and conditions required to create and Maintain the salt spray (fog) test savicoament. Suitable epparatus which may be used is described ia Appendix X 1.2 This practice does not prescribe the type of test specimen or exposute periods to be used for a specific iceluct, nur the interpretation be given (o the results. 1.3 The values stated in S$] units are 10 be regarded as standard, The ineh-pound units ia parentheses are provided for information aud may be approxiasate 14 This standard does not purport 10 address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appro- priate safety and health practices and determine the applica. bility of regulatory timitations prior to use. 2. Referenced Documents 21 ASTM Standards: B 368 Method for Copper-Accelerated Acetic Acid Salt Spray (Fog) Testing (CASS Tesi)? D609 Practice for Preparation of Cold-Rolled Steet Panels for Teiting Paint, Varnish, Gonversion Coatings, and Related Coating Products? 1D 1193 Specification for Reagent Water* D16$4 Test Method for Evaluation of Painted or Coated Specie: ens Subjected to Corrosive Environaents® © 70 Test Method for pH of Aqueous Solutions with the Glass Electrode* E G91 Practice for Conducting an Interlaboratory Study to Determine ihe Precision of a Test Method® G85 Practice for Modified Salt Spray (Fog) Testing” 3. Significance and Use 3.1 ‘This practice provides a controlled corrosive envizon- ment whict has been utilized 10 produce relative corrosion resistance information for specimens of metals and coated * This peace under the jonsiaion cf ASTM Commie C1 06 Conan, of Meus andi te diet eaponsblty of Subcomanitee G01 0508 Laboratory Conosioe Tess Cores diton noyravad Aor 10, 1997. Publica November i947, Crigialy snbivbed at 117 $9 7, Las previous odhdoe B 117-93 annual Bock of STM Standards, Vol 0205 3 draal Bock of ASTM Standards, Vt 06.01 ‘ dna! Bock of ASTM Siardands, Yok 121. 2 Annual Both of AST Standard, Vet 5.05 ‘Arua dock of ASTM Standards. Vat 14.02 * Aaa Back ¢f 48TH Shanda Wat OO scart forthe spe 97 of sue hat has boon oped bythe ‘metals exposed in a given test chamber. 3.2 Prediction of performance in natura) environmen ‘has seldom been correlated with salt spray results when use as stand alone daa. 3.2.1 Correlation and extra ‘mance based om exposure to the {est eavircament provide ‘by this practice are not always predictable. 3.2.2 Cortelation and extrapolation should be considere only in cases where appropriate corroborating long-tert atmospheric exposures have been conducted, 3.3 The reprocucibility of results in the salt spray expc sure is highly dependent om the type of spec:mens tested an the eveluation criteria selected, as well a5 the control of tb operating variables. {o any testing program, sufficient repl cates should be included to establish the variability of th resuits. Variability has been observed when similar spec mens are tested in different fog chambers ven though th ‘esting conditions are nominally similar and within tb anges specified in this practice, polation of corrosion perfo 4. Apparams 4.1 The apparatus required for salt spray (fog) exposu: consists of a fog camber, a salt solution recervoit, = suppl of suitably conditioned compressed ait, one or more ator iting nozzles, specimen supports, provision for heating tk chamber, and nevessary means of control, The size an detailed construction of the apparatus are options!, provide the conditions obtained meet the zequirsments of th practice, : 4.2 Drops of solution which accumylate on the ceiling « sover of the chamber shall not be permitted to fall on tt specimens being exposed. 4.3. Drops of solution which fall (rom the specimens sha not be returned to the solution reservoir for respraying. 4.4 Material of construction shall be such that it will x affect the conrosiveness of the fog. 4.5 All water used for this practice shall cnaform to Tyg IV water in Spesification D 1193 (excep; that for th practice limite for chlorides and sodium may be ignored This does not appl: to ruhping tap water, All other water wi De referred to as reagent grade. S. Test Specimens 5.1 The type and number of test specimers to be used, ¢ ‘well as the criteria for the evaluation of the test results, she be defined is the specifications covering the uuaterial « product being exposed or shall be mutually agreed upo between the purchaser and the seller. we oa of Test Specimens 6.1 Specimets shal) be suitably cleaned. The cleanii method shall be optional =Dding rine surface and the coomationre fe dal be tate ge or careless handling. 2 Specimens for evaluation of paints and other organic Soatiues shall he mrepared in sceordaace with applicable SPecification(s) for the materials) being exposed, or se agreed upon between the purchaser and the supplier. Otherwise the lest specimens shall consist of steel meeting the requirements of Practice D 609 and shall be cleaned and preparcd for goating in accordance with the applicable procedure of Practice D 609, 6.5 Spociraens coated with paints or nonmetallic coatiugs shall not be cleaned or handfed excessively prior to test 6.4 Whenever it is desired to determine the development of corrosion from aa abraded area in the paint or orgenic coating, & scratch or scribed line shall be made through the coating with a sharp instrument $0 as to expose the under. lying metal before testing. The conditions of making the sefatch shall be 48 defined in Test Method D 1634, unless ‘otherwise agreed apon between the purchaser atid the seller, 6.5 Unless otherwise specified, the cut edges of plated, coated, or duplex materials and areas containing identifica: ‘on marks or in contact with the racks or supports shall be ‘Protected with a suitable coating stable under the conditions of the practice. Nove {—Sbould tbe desirable to cut test specimens from pens ot ‘rom preplaad pained, or otherwise conted see chet, the tut oipes shall be protected by coating them with Poist, wax, tape, oF otbct «fective media so tbat the develonmest of a galvanic fet betwecs uch eages and the adjacent pated or otherwise Coated metal surhcen is prevented. 7. Position of Specimens During Exposure 7.1 The position of the specimens in the salt spray chainber during the test shall be such that the following conditions are mei: 7.1.1 Unless otherwise specified, the specimens shall be Supported or suspended between 15 and 30° ftom the vertical and preferably pavailel to the principal direction of flow of fog through the chamber, based upon the dominant surlace being tested. 7.4.2 The specimens shall not contact each other or any ‘metallic material cr any material capable of acting as a wick. 7.1.3 Bach specimen shall be so Placed as to permit free Seltling of fog on ell specimens. 7.4.4 Salt solution from one specimen shail not drip om any other specimen, Jor Sune atrfo he sonsition cating of rata ‘and suppurts are glani, rubber, plastic, or sultably coated wood. Bare ‘itil shall bot be used. Specimens sball preferably be supported from the bottem or the side. Siotied wooden strips are suilable for Cae support ‘of Dat panele. Suspension from glass hooks or waxed scng may be Used as long asthe specified position ofthe specimens i obtained i poessary bby means of stsondary sepport atthe Sottom of the specimens. & Salt Solution 8.1 The salt solution shall be rapnred by ditoving S & 1 parts by mass of sodium chloride in 93 pans of water conforming to Type IV water in Specification D 1193 17 (except that for this practice limits for chlorides und sod may be ignored). The salt used shal be sodiiey cae Substantially the of nickel asd copper and contaiaiag sere i not more than 0.1 % of sodium iodide tod no ann eae 0.3 % of ‘otal impurities. Some salts conta: acditives that may act a corrosion inkibitors, care atten {ion should be given so the chemical content of the salt Upon agreement between the purchaser and tho sller analysis may be required and Limits established fer clement oF Compounds not specified in the chemical composition given above, 5.2 The pH of the salt solution shall be such thet when stomized ai 35°C (95°F) the collected solution will be in the BH range from 6.5 to 7.2 (Note 3). Before the solution is PH meaturement sball be made at 25°C (77°F) usiog a Suitable glass pH-sensing electrode, reference elec rode, and pH meter system in accordance with Test Methos E 70, Nore 3-—"Tesspernture aiTets the pH of a salt soluticn prepared from water eaterated with ca-boa dionide at room emperature oad pit ‘distmert may be rade by the following three methoder (1) When the pH ofa sa: solution is adjused at rooms tomperstuce, snd Momized at 35°C (95°F, the pH of the collected solu on wil 66 ‘igher than the original soivt.on due tothe lose of caiboa di2xide atthe bight tsxperature, Wheo th pH ofthe sat solution is adjusted at oom temperature, it Io therefore uecesary 19 adjust it Below 6.5 40 the ‘collected solution aftr atomniceg at 35°C (95°F) will mest tke pA fils 28.5 to 72. Take about a $0 mal sample ofthe salt solution 1s Prepared 1 oom: temperature Bol gealy for 30's, cool aad detec. ne (se pH. ‘When the DH of the alt sclstoa is adjusted 10 6.5 to Procedure, te pH of the stcrdead aad collected solution 2 will comme within this range. (2) Heating the salt solutim to boiling and cootivg to 25°C (95°F) aod “oxibtaining it at 38°C @S'F) for approximately aii h belore adjusting the pH produces solution the pH of whict doce oot ‘aterally change when atomzed at 35°C (95°F). (3) Heating the water fram which the salt solution is yrepared to 38°C SF or above, te expel carbor dioxide, aad adjusts, the DH Of he salt solution withie the Units of 6.8 to 7.2 produces a tution the DH of whieh Goer no: materi:ly change when stotalzed at 35°C (5°F). Nore 4—The freshly prenared salt solution may be Altered or ‘Searoted before it is placed ix the reservoir, o¢ the end

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