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Introduction
The bursting strength of paper or paperboard is a composite strength
property that is affected by various other properties of the sheet, principally
tensile strength and stretch. Generally, bursting strength depends upon the
kind, proportion, and amount of fibers present in the sheet, their method of
preparation, their degree of beating and refining, upon sheet formation, and
the use of additives.
Bursting strength is measured by means of a Mullen tester. The test
specimen, held between annular clamps, is subjected to an increasing
pressure by a rubber diaphragm, which is expanded by hydraulic pressure at
a controlled rate, until the test specimen ruptures. The pressure reading at
the instant of rupture is recorded as the bursting strength. The units of
expression are pounds per square inch or "points".
The measurement is
variously termed the "Mullen", "pop test", or simply the "burst". The burst
test for paperboard differs from that of lighter papers in that a heavier
Mullen tester is used with a larger diaphragm opening.
Significance
Bursting strength is used widely as a measure of strength in many
kinds of papers, primarily as an indication of the suitability of certain fibers
and the extent of beating and refining. Its main reason for existence is that
it is one of the oldest of the strength tests, it is easy to run, it appears to
correlate with some use requirements, and everyone has the equipment.
While interpretation is empirical, the bursting strength serves as a quick
check on the utility of some papers which do not have an absolute tensile
requirement.
The
Note that 1 kPa = 1 kN/m2, where kPa stands for kilopascal and kN for
kilonewton. Grammage is the basis weight in units of gf/m2.
The Mullen Burst Testers
Two quite different Mullen testers are available commercially and are
both used in the Paper Testing Laboratory:
The Model A Mullen tester; this is a much heavier instrument for the
testing of paperboard.
The light Model C instrument for testing paper has two gages, one
ranging from 0 to 30 psi, the other from 0 to 120 psi. Never exceed the
range of a gage, because serious damage to the gage may result.
Obviously, this instrument is intended for testing papers of bursting strength
less than 120 psi. The circular specimen area tested has diameter 30.50
0.05 mm.
The heavy Model A tester for paperboard also has two gages, with
ranges 0 - 200 psi and 0 - 800 psi, respectively. The specimen area tested
has diameter 31.50 0.03 mm, different from the light instrument.
The
Model A tester also has a much heavier molded rubber diaphragm, whereas
the Model C tester has a fairly thin and pliable rubber diaphragm.
Because of these differences between the two instruments, they do
not have a common scale. This means that a paper sample would have a
totally different value of bursting strength when tested on the Model A
tester. It is therefore a serious mistake to measure the bursting strength of
paper on the Model A tester, as the test value obtained is meaningless.
In both instruments, the specimen is firmly clamped between two
concentric platens, each having a circular opening in the center. The
specimen exposed
Place the handle with the red knob, which operates the clamp, in the
central or vertical position.
Turn on the motor switch, which is located at the bottom of the front
side.
Lower the clamping plate by turning the the handle with the red knob
clockwise to "CLOSE".
The first test on a new sample should always be done with the gauge
of greater range (0 to 800 psi). Make sure the valve to this range is
OPEN, and the valve to the other gauge (0 to 200 psi) is CLOSED.
Make sure the red maximum hand on the gauge you want to use is at
zero;
To burst the sample, proceed as follows. Find the operating lever with
the black knob, located at the far right of the instrument. Move the
operating lever to the LEFT and hold it there, all the while keeping
your eyes on the gauge. If either the sample bursts or the pressure
indicator needle comes too close to the maximum pressure of the
gauge,
the
knurled
of
the gauge
counterclockwise.
Open
the
clamp
by
turning
the
handle
with
the
red
knob
between tests.
Model C Mullen Tester for Paper
Make sure that the valve to the pressurized air supply line is OPEN.
This valve is located to the left and above the nearest Lorentzen &
Wettre tensile tester.
Push the brass ring located at the top of the clamp assembly upward
to raise the clamping plate.
The first test on a new sample should always be done with the gauge
of greater range (0 to 120 psi). Make sure that the valve to this gauge
is OPEN, and the valve to the other gauge (0 to 30 psi) is CLOSED.
Make sure the red maximum hand on the gauge you want to use is at
zero;
To burst the sample, proceed as follows. Find the operating lever with
the black knob, located at the far right of the instrument. Move the
operating lever to the LEFT and hold it there, all the while keeping
your eyes on the gauge. If either the sample bursts or the pressure
indicator needle comes too close to the maximum pressure of the
gauge, it is extremely important that you quickly move the
operating lever to the RIGHT as far as it will go and release it
immediately; failure to move the operating lever to the right
immediately the sample bursts may result in a ruptured
diaphragm. The instrument will automatically return to the starting
position.
Push the brass ring upward and remove the old sample.
instrument is ready for the next test.
The
Report
Report the mean bursting strength in points (lb/in 2) as the arithmetical
mean of all ten tests on a sample, the burst factor, and the burst index. Also
report 95% confidence intervals.
References
ASTM D 774
TAPPI T 403, "Bursting Strength of Paper"
TAPPI T 807, "Bursting Strength of Paperboard and Linerboard"
TAPPI T 810, "Bursting Strength of Corrugated and Solid Fiberboard"
5
Mechanical Properties