Beruflich Dokumente
Kultur Dokumente
Characterization of Dielectric
Materials using Coupled Ring
Resonators
2.1 Introduction
Material characterization is an important field in microwave engineering and is
used in the system design from high speed circuits to satellite and telemetry
applications. [1]
Every material has a unique set of electrical characteristics that are dependent
on its dielectric properties. A measurement of these properties provides valuable
information to scientists, to properly incorporate the material into its intended
application, such as for more materials designs or to monitor a manufacturing
process for improved quality control. Several measurement techniques for
dielectric characterization have been reported in literature [1-4] and can be
classified as transmission-reflection and resonance techniques. The resonance
techniques do not have the sweep frequency capability, unlike resonance
techniques; the transmission techniques usually have the sweep frequency
ability for the measured frequency range. The transmission and/or reflection
signals are always tested to calculate the dielectric properties of the material.
However, resonance techniques are more accurate than transmission techniques,
Chapter 2
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Chapter 2
Page 35
cavity. The real and imaginary parts of materials permittivity were calculated
using the shift in the resonance frequency [11].
Luiene S. Denenicis et al. also proposed a coplanar waveguide linear resonator
technique for the characterization of dielectric properties of thin films at room
temperature. They deposited thin films of unknown dielectric constant on the
resonator using photolithography and measured the response of s parameters
[12]. For the characterization of dielectric constant, in which a microstrip line
coupled with the fork shaped feed element, to improve the coupling efficiency
were proposed by A.H. Muqaibel and his group members [13].
C.Y. Tan et.al. developed a dual resonator, for permittivity characterization. The
microstrip dual resonator consists of two half wavelength resonators, and the
gap between these two resonators was covered with the ferroelectric thin films.
The dielectric constant was calculated by measuring the resonance frequency
and the quality factor. In this method there was some inaccuracy in the
measurements due the air gap between the resonator and the ferroelectric film
[14].
Sompain Seewathanopon also developed a microstrip ring resonator for
dielectric constant measurement [15]. Victor F.M.B Melo has also proposed a
new configuration for the ring resonator to determine dielectric permittivity of
printed circuit board with high accuracy operating at higher frequency [16]. Jyh
Seen too, presented a review on transmission/reflection and resonance technique
for the characterization of dielectric constant.
Chapter 2
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Chapter 2
Page 37
This chapter deals with the dielectric constant measurements and theoretical
analysis of spirulina and ferrite, which are in, liquid and powder phase
respectively, using CRR and SRR resonators.
Chapter 2
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Where,
and
Where,
substrate thickness.
For a given characteristic impedance
, w/d ratio
(2.8)
(2.9)
Calculated mean radius of ring is 15.85 mm, feedline length is 24.9 mm, width
of the feedline is 1.77 mm, and coupling gap is 0.4108 mm as shown in Table
2.1. Inner and outer radius of the ring is calculated by subtraction and addition
of the half of width of microstrip to the mean radius respectively.
Chapter 2
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Inner radius
(2.10)
Outer radius
(2.11)
24.9 mm
1.77 mm
Coupling Gap
0.4108 mm
84.16 mm
41.08 mm
14.97 mm
Outer radius
16.74 mm
7.041mm
Outer radius
8.811 mm
Chapter 2
Inner radius
3.075 mm
Outer radius
4.845 mm
Page 40
Coupling between the feed line and the ring is taken into consideration because
its capacitive effect can change the resonance frequency significantly [8]. The
coupling gap between the feed lines represents network capacitance C and a
shunt circuit consisting of inductance (Lr) and capacitance (Cr) represents the
ring. In the split ring resonators, one more network capacitance C is added in the
shunt circuit of the ring. Fig: 2.1(a) & 2.1(b) shows the closed coupled and split
ring resonators.
(a)
(b)
Figure 2.1(a) and (b): Split and closed coupled ring resonators of the wavelength , /2 and /4
with the coupling gap 0.41 mm
Chapter 2
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In the first step, complex permittivity and loss tangent of the substrate are
calculated. Loaded quality factor QL is computed using the following relation:
(2.12)
Where f0 is the resonance frequency, f is the 3dB bandwidth. Unloaded quality
factor is estimated using:
(2.13)
Where QU is the unloaded quality factor which depends on total insertion loss
(IL) of the system. Total loss of the resonator is inverse of loaded quality factor,
which is the sum of losses due to the dielectric component, conducting
component and the losses of the resonator without any external load. QD which
is the direct measure of the loss tangent of the materials loaded to the resonator
is calculated using following expression:
(2.14)
In the present study conductor, loss is neglected due to very high conductivity of
the copper deposited on the substrate.
The loss tangent tan(substrate) is calculated using the following relation
(2.15)
where e is the energy filling factor which is the ratio of average energy stored
in the specimen to the average energy stored in resonant structure. The
Chapter 2
Page 42
following relation relates loss tangent in equation (2.15) to the real and
imaginary part of permittivity:
(2.16)
&
of substrate with sample and only substrate respectively. Values of the filling
factor are chosen empirically on the basis of transmission loss and values of
quality factor on loading the resonator with sample.
Chapter 2
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Figure 2.2: Simulated results with CRRs, ____CRR without any load, _ _ _ _ CRR loaded with
Ferrite, CRR loaded with Spirulina.
Chapter 2
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Figure 2.3: Experimental results with CRRs, ______CRR without any load _ _ _ _ CRR loaded
with Ferrite and - - - - - CRR loaded with Spirulina.
Figure 2.4: Simulated results with SRRs, _____SRR without any load, _ _ _SRR loaded
with Ferrite and SRR loaded with Spirulina.
Figure 2.5: Experimental results with SRRs, ____ SRR without any load, _ _ _ _ SRR loaded
with Ferrite and - - - - - SRR loaded with Spirulina.
Chapter 2
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Dielectric Constant of
spirulina platensisGietler
Type of ring
resonator
Dielectric constant of
Ferrite
( ' )
( )
'
Simulated
Results
Experimental
Simulated
Results
Results
Experimental
Results
CRR of length
1.9
1.92
15.1
14.6
CRR of length
and
1.93
1.84
14.76
14.05
CRR of length ,
and
1.788
14.39
14.17
SRR of length
1.74
1.75
13.8
13.68
SRR of length
and
1.76
1.76
13.6
14.01
SRR of length ,
and
2.04
1.76
14.32
13.78
Chapter 2
Page 46
(2.19)
where C is the total capacitance and, L is the total inductance and Q is quality
factor of the parallel RLC circuit.
In the ring resonators, L1 and C1 are the mutual inductance and capacitance
between the rings respectively and Lr, Lr1, Lr2 are the inductance of the rings of
length ,
and
and Q the total capacitance, total inductance, total resistance of the ring and
quality factor of the ring can be calculated as shown in figure 2.6.
Chapter 2
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(i)
(ii)
(iii)
Figure: 2.6 a (i), (ii) and (iii) Structures and the equivalent lumped circuits of the 1CRR, 2CRR,
3CRR respectively.
Chapter 2
Page 48
(i)
(ii)
(iii)
Figure: 2.6 b (i), (ii) and (iii) Structur and the equivalent lumped circuits of the 1SRR, 2SRR,
3SRR respectively.
Chapter 2
Page 49
The preceding equations and the equivalent circuit diagrams elucidate the reason
for higher sensitivity of CRR as compared to SRR. The effective capacitive
reactance of the rings increases due to additional gap capacitance resulting in
higher losses and poor sensitivity.
This could be the reason for lowest sensitivity in 3-SRR. Further, from the
theoretical model it is clear that due to the presence of split, inductance
decreases in SRR as compared to CRR, therefore the Q of the circuit also
decreases as shown in table 2.3. Thus the capacitance gap plays an important
role in deciding the sensitivity.
Reported dielectric constant of Lithium Zinc Titanium (LiZnTi) Ferrite and
Spirulina Platensis-Gietler is 15 and 1.9 respectively [6], [7]. Experimentally
measured dielectric constant of Ferrite and Spirulina Platensis-Gietler is 14.17
13.68 and 1.76-1.92 with accuracy of 5% using closed ring resonator.
Dielectric constant values using SRR are in the range of 15.1-13.6 for ferrite and
1.74-2.04 for Spirulina Platensis-Gietler respectively, with 10% accuracy as
shown in table 2.2 and 2.3.
Value of 1 for Spirulina Platensis-Gietler was 0.014, for Ferrite was 0.1 and
value of 2 for substrate were 0.04, lower value of filling factor in case of
Spirulina Platensis-Gietler is also confirmed with decrease in Q values and in
case of ferrite filling factor is greater than the value of filling factor of substrate
due to which quality factor increases. Quality factor value, which is a direct
measure of energy stored in dielectric materials, is tabulated in table 2.4.
Chapter 2
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Chapter 2
Page 51
Table 2.4 Quality factor of unloaded and loaded CRRs and SRRs
Type of ring
resonator
379
Quality Factor
With
Spirulina
370
Unloaded
With
Ferrite
471
CRR of length
CRR of length
and
377
397
479
CRR of length ,
and
377
356
485
SRR of length
408
398
423
SRR of length
and
403
399
316
SRR of length ,
and
405
398
418
Table 2.5 comparison of the achieved accuracy in the present method with
the cavity perturbation methods
Method
Chapter 2
Accuracy
5%
10%
6%
4-7%
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2.6 Conclusion
The technique elaborated in this chapter presents, the comparative study of
dielectric characterization of closed and split ring resonator. Two different kinds
of samples via ferromagnetic sample in powder form and bio sample in semi
liquid form were taken. The analysis shows that measured values of dielectric
parameters using CRR were more accurate than SRR. Experimental results were
validated by simulations of the experimental design on the CST Microwave
Studio. The method proposed herein can be used for the dielectric
characterization of liquids and solids in powder phase.
Chapter 2
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References
1.
2.
3.
4.
5.
H.K. Yong, Y. Sheung, S.C. Park, D.H. Lim, H.I. Jung, Y.J. Kim., A
Simple and Direct Bimolecules Detection Scheme Based on a Microwave
Resonator, Sensors and Actuators B Vol. 130, pp. 823-828, 2008.
6.
7.
K. Chang, Microwave Ring Circuits and Antennas, John Wiley & Sons,
1996.
8.
9.
A. Dubey, G.S. Tyagi, G.P. Srivastava, N.K. Badola , K.K. Jain, Effect of
Temperature on LiMnTi Ferrite Based Microstrip Circulator, Microwave
and Optical Technology Letters Vol. 35, No. 2, 2002.
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Chapter 2
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