Beruflich Dokumente
Kultur Dokumente
KEMURNIAN
KADAR ABU
STANDARDISASI
BAHAN ALAM
KADAR AIR
1
Determination of ash
The ash remaining following ignition of herbal materials is
determined by three different methods which measure total
ash, acid-insoluble ash and water-soluble ash.
The total ash method is designed to measure the total
amount of material remaining after ignition. This include:
PRINSIP DASAR:
Pemanasan dengan suhu sangat tinggi 450 0C
(pemijaran) pada alat tanur
Yang tersisa adalah mineral oksida dan senyawa
anorganik
3/3/2014
PROCEDURE
Total ash
Kadar abu total
untuk mengukur jumlah abu total
pada simplisia setelah pembakaran
Logam fisiologis, yg berasal dari jaringan
tanaman itu sendiri (Na, Fe, K,Ca,Mg)
Logam non-fisiologis, yaitu yg merupakan residu
benda asing (pasir, tanah)
PROCEDURE (2)
Acid-insoluble ash
To the crucible containing the total ash, add 25 ml
of hydrochloric acid (~70 g/l) TS, cover with a
watch-glass and boil gently for 5 minutes. Rinse
the watch-glass with 5 ml of hot water and add
this liquid to the crucible. Collect the insoluble
matter on an ashless filter-paper and wash with
hot water until the filtrate is neutral. Transfer the
filter-paper containing the insoluble matter to the
original crucible, dry on a hotplate and ignite to
constant weight. Allow the residue to cool in a
suitable desiccator for 30 minutes, then weigh
without delay. Calculate the content of acidinsoluble ash in mg per g of air-dried material.
3/3/2014
PROCEDURE (3)
Akar Kelembak:
SIMPLISIA:
Abu Total: Tidak lebih dari 11,6%
Abu Tidak Larut Asam: Tidak
lebih dari 0,5%
EKSTRAK:
EKSTRAK:
Abu Total: Tidak lebih dari 3,4% Abu Total: Tidak lebih dari 2,3%
Abu Tidak Larut Asam: Tidak
Abu Tidak Larut Asam: Tidak
lebih dari 0,5%
lebih dari 0,2%
Water-soluble ash
To the crucible containing the total ash, add
25 ml of water and boil for 5 minutes.
Collect the insoluble matter in a sinteredglass crucible or on an ashless filterpaper.
Wash with hot water and ignite in a crucible
for 15 minutes at a temperature not
exceeding 450 C. Subtract the weight of
this residue in mg from the weight of total
ash. Calculate the content of water-soluble
ash in mg per g of air-dried material.
KEMURNIAN
KADAR ABU
CEMARAN LOGAM BERAT
CEMARAN MIKROBA
KADAR AIR
3/3/2014
Determination of microorganisms
KEMURNIAN
KADAR ABU
CEMARAN LOGAM BERAT
CEMARAN MIKROBA
KADAR AIR
3/3/2014
KEMURNIAN
Berdasarkan WHO:
Penggunaan Mikroba
Patogen
Bakteri
/gram
Jamur
/gram
Oral
105
103
Topikal
107
104
KADAR ABU
CEMARAN LOGAM BERAT
CEMARAN MIKROBA
KADAR AIR
Determination of water
and volatile matter
Destillation
Gravimetry
3/3/2014
Gravimetri
24