New 5100 Icp-Oes

Agilent 5100
ICP-OES
Features,
performance
and capabilities
Agilent Confidential
September 9, 2014
1
Agenda
Introducing the NEW 5100 ICP-OES

Performance Proofs
Applications
Introducing the New ICP Expert V7Software
September 9, 2014
2
Agilent 5100 ICP-OES

Synchronous Vertical Dual View (SVDV) with unique Dichroic Spectral
Combiner (DSC) technology
September 9, 2014
3

Dual View ICP-OES minus the wait
Why waste time and money running your sample on a dual
view ICP instrument, which has to take 2, 3 or even 4
sequential measurements. Get accurate results on your
toughest samples in a single, simultaneous measurement,
using the Agilent 5100 SVDV with unique DSC technology
5100 SVDV has differentiated technology that delivers
the speed and performance you have been waiting for
September 9, 2014
4
How Do Traditional Dual View Instruments Work?
To detector
M
Mirror M is
movable and
provides radial
viewing (not
simultaneous)
September 9, 2014
5
What is Synchronous Vertical Dual View with unique

Dichroic Spectral Combiner technology (DSC)
Axial light from plasma
Radial light
from plasma
Dichroic
Spectral
Combiner
To detector
September 9, 2014
6
5100 SVDV model working in axial only (DV)

Mirror is moved into position for axial view only
Axial light reflected

into poly
Mirror
To detector
Radial light
reflected away
September 9, 2014
7
5100 SVDV model working in radial only (DV)

Hole is moved into the plasma light path for radial only
Axial light goes straight

through hole to photon
stop
Hole
To detector
Radial light
into poly
September 9, 2014
8
Agilent 5100 ICP-OES Project Drivers

Reduce operating costs and increase reliability
Enhance Agilent ICP-OES Performance Advantage
Improve Usability
September 9, 2014
9
Reminder of technology and industrial design

Smallest
footprint of
major ICPOES
vendors
Unique Synchronous
Vertical Dual View (SVDV)
Robust solid state RF

Smart electronics
1 orientation Vertical
Torch
Easy access to
spraychamber/nebulizer
improving usability
Corrosion
resistant sample
compartment
Easy access to
power, gas,
cooling water and
comms from RHS
Pump position close
to samples reduces
sampling times
improves throughput
Easy access to
Easy-Fit torch
September 9, 2014
10
Behind the covers
April 30, 2013

Page 11
Optimized footprint through strategic Industrial Design

Small footprint
September 9, 2014
12
Footprint Comparison
Model
Width
(mm)
Depth
(mm)
Footprint
(m2)
Height
(mm)
Weight
(kg)
Agilent 5100 (Aurora)
800
740
0.59
825
100
Agilent 700 Series
1300
750
0.98
990
203
Thermo 7000 Series
840
750
0.63
590
N/L
PE Optima 8300
1320
800
1.06
760
193
40% smaller than 700 series, 7% smaller than iCAP 7000
September 9, 2014
13
Key Agilent 5100 SVDV ICP-OES benefits

Lowest cost
of ownership
Fastest sample
throughput of difficult
samples
Low gas consumption
Enhanced
Performance
Analytical performance
System robustness and
reliability
Simple
Operation
Hardware
Software
September 9, 2014
14
1. Lowest cost of ownership

Speed = low gas costs per sample
Synchronous VDV measures axially and radially at the same time
Thermostatically stabilized optics with Vista Chip2 CCD
Reduces repeat analysis requirements
Measures wavelengths simultaneously
Hermetically sealed detector for fast warm up and low gas consumption
Low exhaust extraction (2.5m3/min, >50% lower than 700 series))

- Reduces lab air conditioning requirements saving money
Lower power consumption 2.9KVA (>40% lower than 700 series)
- Lowers power bills
September 9, 2014
15
1. Lowest cost of ownership

Reduced maintenance costs
SSRF generation
No RF power tube to replace
There are less parts and less labour for any repairs that have to be effected
Vertical Easy-fit torch
5 x longer torch life (compared to 720 torch) through vertical orientation and
strategic design
Customer maintainable
Pre optic windows and gas filter
September 9, 2014
16
2. Enhanced Performance
Analytical Performance
Elimination of EIE interference with sensitivity of axial instrument.
Long Term Stability with complex matrix
September 9, 2014
17
System Robustness
System Robustness
Improved corrosion resistance from
positive pressure design

polymer components in sample traffic area
Conformal coating of all circuit boards and SSRF
Aluminium chasis (not steel like 700)
Mains power supply and RF power supply
Located out of high volume air flow

Vertically mounted to allow dust to fall through
Enhanced diagnostics and Smart electronics
Reduce service times
September 9, 2014
18
3. Simple Operation
Easy Fit SVDV torch

Easy fit Sample Introduction System
Customer Installable Gas control module
Customer replaceable pre optic window and CCI
Customer replaceable gas filter
September 9, 2014
19
3. Simple Operation
Intuitive workflow ICP Expert V7 software
No need to pick axial or radial like conventional DV. In SVDV mode,
DSC does this automatically
PC controlled Make Up gas port
Customer replaceable dust filter
MFC on all plasma/sample gas lines
September 9, 2014
20
Performance proof EIE Immunity

5ppm K Readback
40.0
35.0
30.0
[K] ppm
25.0
Radial
20.0
Axial
SVDV
15.0
10.0
5.0
0.0
1
10
100
[Na] ppm
1000
10000
September 9, 2014
22
Performance proof EIE immunity

5ppm K Readback
40.0
35.0
30.0
[K] ppm
25.0
Radial
20.0
Axial
SVDV
15.0
Axial+1%CsCl
10.0
5.0
0.0
1
10
100
[Na] ppm
1000
10000
September 9, 2014
23
5ppm multielement LTS.

SVDV with vertical DV torch, 1.8mm injector.
19 hrs. <1%RSD.
1.2
0.8
0.6
As 188.980
Se 196.026
Zn 202.548
Zn 213.857
Cd 214.439
Pb 220.353
Ni 231.604
Mn 257.610
Cr 267.716
Cu 324.754
Cu 327.395
Al 396.152
Sr 407.771
Ba 455.403
Ba 493.408
K 766.491
LL
UL
0.4
0.2
0
12:00:00 AM
2:24:00 AM
4:48:00 AM
7:12:00 AM
9:36:00 AM
12:00:00 PM
2:24:00 PM
4:48:00 PM
7:12:00 PM
September 9, 2014
24
Performance Proof 4 hr LTS on 25% NaCl with 1ppm std.

<1.3% RSD. Axial results from VDV configuration
120%
% Readback
100%
80%
60%
40%
20%
0%
0:00:00
0:30:00
Al 167.019
Co 238.892
Ni 231.604
Sr 407.771
1:00:00
1:30:00
Al 396.152
Cr 267.716
Pb 182.143
Zn 213.857
2:00:00
Time (h:mm:ss)
As 188.980
Cu 327.395
Pb 220.353
+10% Readback
2:30:00
3:00:00
Ba 455.403
Mn 257.610
Se 185.457
-10% Readback
3:30:00
4:00:00
Cd 214.439
Mo 202.032
Se 196.026
OneNeb, Double pass glass cyclonic, Blk/Blk & Blu/Blu, AHA, demountable torch
1.8mm injector, 15rpm. (Also tried on 2.4mm injector with same results)
September 9, 2014
25
Performance Proof Interim Axial IDL (n=1

instrument)
VDV configuration.. IDLs similar to 720
VDV Axial IDL
Element nm
VDV Axial IDL
720 Axial IDL

Element nm
720 Axial IDL
Mg 279.553
ug/L
0.01
ug/L
0.01
0.1
Mn 257.610
0.03
0.03
1.79
Mo 202.032
0.37
0.5
Au 242.794
0.62
Na 589.592
0.12
0.15
B 249.772
0.2
0.1
Ni 231.604
0.6
0.3
Ba 455.403
0.02
0.03
P 177.434
1.74
1.5
Be 313.042
0.01
0.01
Pb 220.353
1.39
0.8
Bi 223.061
1.75
S 181.972
3.9
Ca 396.847
0.02
0.01
Sb 206.834
2.29
Cd 214.439
0.12
0.05
Se 196.026
2.48
Ce 418.659
0.67
Si 251.611
0.63
Co 238.892
0.38
0.2
Sn 189.925
1.56
Cr 267.716
0.2
0.15
Sr 407.771
0.004
0.01
Cu 327.395
0.12
0.3
Ti 334.941
0.05
0.1
Fe 238.204
0.17
0.1
Tl 190.794
1.76
1.5
Hg 184.887
0.79
0.8
V 292.401
0.25
0.2
K 766.491
0.28
0.3
Zn 213.857
0.11
0.2
Li 670.783
0.01
0.06
Zr 343.823
0.12
0.3
Ag 328.068
ug/L
0.16
ug/L
0.3
Al 167.019
0.14
As 188.980
Single pass S/C, Seaspray neb, semi demountable VDV torch 1.8mm injector, equivalent to 3x30 sec read
time, 15rpm, blk/blk PVC pump tubes, each element and has optimized power and neb flow.
September 9, 2014
26
Gas Use Ar/min

As per USEPA 200.7 App Note and site prep docs
5100
SVDV
Optima
8300DV
iCAP
7600
Normal + Boost
Optics purge
Detector purge
3.7
0
7
1
4
0.08
14*
0.4
Plasma flow
(coolant)
Aux flow
Neb flow
Snout
CCI/shear
total (L/min)
12
1
0.7
0
3
20.4
8
0.2
0.55
13
0.5
0.65
18
0.5
0.7
13
0.8
0.7
16.75
18.23
33.6
14.5
L/min
Spectroblue
Prodigy
EOP
Ar/min
40
35
NOTE:
8300 can use N2 for Optics and
this reduces flow to 5L/min
Boost purge chosen for all
vendors as US EPA monitors
Arsenic
SVDV mode doesnt need snout
flow for radial.
Nitrogen will additionally be
needed on the 8300 for shear
gas for US EPA 200.7 at 1823L/min.
If air is used for the 8300 shear
gas, may need a refrigerated
drier in humid environment.
30
25
20
15
10
5
0
5100 SVDV
Optima 8300DV
iCAP 7600
Prodigy
Spectroblue
EOP
September 9, 2014
27
Gas Use Ar/sample

As per US EPA 200.7 app notes
USEPA 200.7
(min)
Ar L/sample
Valve/No Valve
5100
SVDV
Optima
8300DV
iCAP
7600
1.16
23.664
2.36
39.53
2.36
43.0228
valve
Valve
Valve
Prodigy
5
168
No
Valve
Spectroblue
EOP
2.5
36.25
No Valve
Ar/sample
180
160
140
120
100
80
60
40
20
0
5100 SVDV
Optima
8300DV
iCAP 7600
Prodigy 7
Spectroblue
EOP
September 9, 2014
28
Resolution Performance Proof

PP1
PP2
September 9, 2014
29
Accuracy Performance proof

Oyster Tissue Synthetic Reference Material
Al 396.152
As 188.980
Cd 214.439
Ca 373.690
Cr 205.560
Co 228.615
Cu 324.754
Fe 259.940
Pb 220.353
Mg 279.078
Mn 257.610
Ni 231.604
P 213.618
K 769.897
Se 196.026
Si 250.690
Na 589.592
S 181.972
Zn 206.200
Target
mg/L
3
0.1
0.03
15
0.007
0.004
0.6
2
0.005
12
0.2
0.01
80
100
0.02
10
50
70
9
Axial
mg/L
3
0.1
0.03
15
0.007
0.005
0.6
2
0.004
12
0.2
0.01
79
101
0.02
9
37
70
9
%
recovery
100
100
100
100
100
125
100
100
80
100
100
100
99
101
100
90
74
100
100
Al 396.152
As 188.980
Cd 214.439
Ca 373.690
Cr 205.560
Co 228.615
Cu 324.754
Fe 259.940
Pb 220.353
Mg 279.078
Mn 257.610
Ni 231.604
P 213.618
K 769.897
Se 196.026
Si 250.690
Na 589.592
S 181.972
Zn 206.200
Target
mg/L
3
0.1
0.03
15
0.007
0.004
0.6
2
0.005
12
0.2
0.01
80
100
0.02
10
50
70
9
LP6 SVDV
%
recovery
mg/L
3
100
0.1
100
0.03
100
16
107
0.007
100
0.003
75
0.6
100
2
100
0.008
160
12
100
0.2
100
0.01
100
80
100
93
93
0.02
100
9
90
49
98
71
101
9
100
It Just Works
Agilent Restricted
June 2, 2011
30
Agilent 5100 ICP-OES market segments
Environmental
Food & Agriculture
Materials Science
Chemical & Energy
Pharmaceuticals
Drinking and natural water
Trace toxic metals in food
Mining and Metals
Petroleum refining
Heavy metals
(USP<232>/<233>)
Soil and sediment
Nutrient elements
Toys and Consumer Products
Alternative Energy (Biodiesel)
Incoming raw material testing
Waste (solids/liquids/gases)
Feed and fertilizer
Semicon, Ceramics, Batteries
Fine and Bulk Chemicals
QA/QC of Final Product
September 9, 2014
31
Why is SVDV perfect for Environmental and Food and

Agriculture segments
Performance required when measuring trace level toxic
elements and higher level nutrient elements
Speed/low gas costs (SVDV, Vista Chip2)
EIE immunity (SVDV)
LDR (Vista Chip2)
Resolution/interference minimization (Echelle optics,
FACT/IEC, Fitted Background Correction)
Usability (Software, Easy Fit Torch)
September 9, 2014
32
Why is 5100 perfect for Materials and Chemical and

Energy segments
Performance characteristics when measuring mining samples
or organic samples
Highly stable plasma system (SSRF)
Matrix tolerance and robust sample intro (Vertical torch, HF
resistant SIS)
Long term stability (MFC, Thermostatted optics)
September 9, 2014
33
Why is 5100 perfect for Pharmaceutical market

segment?
Sensitivity (USP232)
21CFR11
IQOQ classic protocol
September 9, 2014
34
Agilent 5100 ICP-OES portfolio

3 different configurations
SVDV*
Synchronous
Vertical Dual View
VDV
Vertical Dual View
RV
Radial View
*Agilent 5100 Synchronous Vertical Dual View with unique Dichroic

Spectral Combiner technology
September 9, 2014
35
Model Range
Feature
Vertically orientated plasma with dual viewing capability
Vertically orientated plasma with Synchronous Dual View
5100 VDV
5100 SVDV
O*
5100 RV
Vertically orientated with radial viewing only plasma

Robust, solid-state 27MHz RF generator
5 channel peristaltic pump
Second generation VistaChip2 CCD
Mass flow controlled nebulizer
PC controlled make-up gas for high salt solutions or hydride generator
Computer controlled oxygen accessory for organic solvents
Easy-fit torch
167 to 785 nm wavelength range
ICP Expert 7 base software
ICP Expert 7 Pro Feature Pack software
Hydride generator accessory
SVS2+ productivity accessory
Standard capacity autosampler support in software
Extended capacity autosampler support in software
21 CFR 11 compliance
Nitrogen Purge for Polychromator
April 30, 2013

Page 36
QUIZ:
What are the Key Aurora benefits?
Lowest cost
of ownership
Fastest sample
throughput of difficult
samples
Low gas consumption
Enhanced
Performance
System robustness and
reliability
Simple
Operation
Hardware
Software
September 9, 2014
37
NEW ICP Expert V7 software

Common software platform with MP-AES
MP Expert
ICP Expert
Acclaimed simplicity
Intuitive workflow
Applet mode to further simplify start up
No need to pick which wavelength uses the different view on SVDV
mode
June
2, 2011
Agilent
Restricted
38
NEW ICP Expert V7 software Method Development

MP Expert
ICP Expert
June
2, 2011
Agilent
Restricted
39
NEW ICP Expert V7 Analysis page spectrum view
June
2, 2011
Agilent
Restricted
40
NEW ICP Expert V7 Analysis Page IEC view
June
2, 2011
Agilent
Restricted
41
New ICP Expert V7 Analysis Page - Nebulizer Argon

Back pressure and Ar emission
September 9, 2014
42
Service Diagnostics Gasbox monitoring
September 9, 2014
43
Service Diagnostics Camera Control
September 9, 2014
44
SUMMARY
Agilent 5100 ICP-OES Synchronous Vertical Dual View
1. Lowest Cost of Ownership

3. Easy Operation
September 9, 2014
45
Agilent 5100 ICPOES

Technology Review
September 9, 2014
46
What patents have been granted and what are

pending?
1. Hosemans SSRF supply. Patent granted in US, China, Japan. Pending in
Europe, Australia and Canada.
2. Dichroic Spectral Combiner technology (DSC) Patent pending in US, China
and Great Britain
3. Invention disclosures submitted for work coil connection.
Carried through from 700 series:
4. Vista Chip patent
5. FACT
6. Injector taper of the High TDS torch
September 9, 2014
47
Whats not New?

1.
2.
3.
4.
Polychromator
Camera board
Peri Pump
Peri pump
CNTL board
5. PWB
6. Gas box from
TAD
7. Fan from
MPAES
8. Flue from
MPAES
9. Igniter from MP
10. Water inlet filter
from MS
1.
8.
5.
4.
3.
2.
9.
6.
7.
10.
September 9, 2014
48
Whats new:
SVDV with unique DSC technology
NOTE:
1. SVDV has assembly with dichroic
and mirror
Dichroic
Hole
2. VDV has assembly that has 2

mirrors (for balance)
3. RV does not have this assembly
Mirror
4. Early DL studies showed that the

background signal was lower on UV
lines. This is due to the DSC
filtering out stray light from red
spectrum.
September 9, 2014
49
What analysis modes can SVDV give?

1. Synchronous VDV
2. Vertical Dual View
3. Axial only
4. Radial only
4 modes in one instrument.
September 9, 2014
50
Whats new: Torch loader and pre-optics..1

Excellent registration with Torch mount
ADVANTAGE: no plasma scanning needed to optimize plasma
emission into optics.
Automatic rotating wheel to house DSC technology.
ADVANTAGE: Simplify method development for SVDV analysis
Plasma and Aux gas

lines come through
torch mount
Whats New: Torch loader and pre-optics..2
Active thermal stabilizer developed to isolate polychromator from RF

box heat. The peltier device in the thermal stabilizer does not require
additional water cooling and is not user adjustable. It sits at 35C.
ADVANTAGE: No Heat transfer from pre optics. Thermally
stability ensures LTS.
Customer replaceable CaF2 pre optic windows for radial and axial
orientation
ADVANTAGE: Reduced maintenance costs
Whats New: Sample Intro and Vertical Torch
Ground glass joint between s/c and torch

One Piece (Bonded) and semi demountable torches. (Quartz and
ceramic).
Ignites through torch (doesnt need consumeable copper strip)
Plasma can run dry, plasma sits centrally.
April 30, 2013

Page 53
RF load coil
700 series
soft and readily damaged by customers inserting torches.
Generalist FSEs often over tighten the Swagelok fitting and distort
brand new load coils

hardened copper coated in gold
Torch loader prevents customers damaging coils during loading
Collette fitting to prevent over tightening
September 9, 2014
54
Torch Range
Part Number
Description
G8010-60231
5100 HF Dual View Torch
G8010-60232
5100 High Salt Dual View Torch
G8010-60233
5100 Semi Volatile DV Torch
G8010-60234
5100 HF Radial Torch
G8010-60235
5100 Volatile Organic Rad Torch
G8010-60236
5100 Demountable DV Torch
G8010-60237
5100 Demountable Radial Torch
G8010-60238
5100 Dual View Torch
G8012-60000
5100 Radial Torch

September 9, 2014
55
Optics
All wavelengths captured in one reading
- Maximum speed and productivity
Fewer optical components
- Deliver high light throughput
- Excellent signal-to-noise
- Excellent detection limits
Thermostatted to 35oC
- Excellent long term stability
- Fast start-up, increasing sample throughput
September 9, 2014
56
Vista Chip 2 CCD
>98% wavelength coverage 167 785 nm

Use alternate wavelengths to extend Linear
dynamic range and also to confirm results
1 MHz processing speed
True simultaneous measurement
Duplex readout circuitry halves readout time
Peltier cooled to -40oC

Ensures low noise and best detection limits
September 9, 2014
57
Long term Stability

19 hrs. <1%RSD.
1.2
0.8
0.6
As 188.980
Se 196.026
Zn 202.548
Zn 213.857
Cd 214.439
Pb 220.353
Ni 231.604
Mn 257.610
Cr 267.716
Cu 324.754
Cu 327.395
Al 396.152
Sr 407.771
Ba 455.403
Ba 493.408
K 766.491
LL
UL
0.4
0.2
0
12:00:00 AM
2:24:00 AM
4:48:00 AM
7:12:00 AM
9:36:00 AM
12:00:00 PM
2:24:00 PM
4:48:00 PM
7:12:00 PM
September 9, 2014
58
Long term Stability - SSRF Generator
MgI/MgII ratio >10 @ 1kW (corrected

for Polychromator)
Efficiency of:
Oscillator: @75% above 1.2kW
Power range adjustment of 700W to
1500W in 50W increments
Tested with100% methanol &

Kerosene,
98 RON PULP (petrol), 25% NaCl for
>1 Hr.
Cycled between 5% methanol, 5%
NaCl, 1% Nitric acid for 3 hours.
New power control circuitry.
April 30, 2013

Page 59
Long Term Stability - Gas Box and Gas Control
Used the ICPMS gas box and adapted it for

5100.
Pressure sensor on nebulizer line enables neb

pressure to be monitored on analysis page
All plasma gas lines have MFC and are PC

controlled. (EPC from 7900 gasbox)
Plasma gas 0-20L/min @ 0.5L/min
Nebulizer gas 0-1.5L/min @ 0.01L/min
Auxiliary gas 0-2L/min @ 0.1L/min
Make Up gas 0-2L/min @ 0.01L/min
Polychromator has MFC on it also that was

designed in MGV SPSD.
Gas Control Module enables swap over to

modify gas usage. (1, 2 and 3 port varieties
available)
2 port gas plate shown. Default

installation on SVDV and RV
September 9, 2014
60
Mains power supply and RF power supply

Mains supply is mounted
vertically and replaces
transformer technology in
the 700 series.
Located away from blower. It
is in positive pressure
environment and at lower
voltage will attract less dust.
Has conformally coated
boards to resist dust and
acid vapor attack.
RF supply half size of mains
supply so easy to
ship/replace. Distributes
100V DC to RF oscillator.
Replaces the HVDC PS from
700 series.
September 9, 2014
61
Polychromator gas flow

MFC control of gas flow through the poly (Agilent designed)
Poly flow is used to purge the pre optics. (0.7 + 3 L/min)

Snout and CCI are separate flows to the poly
Snout and CCI are not MFC controlled
L/min
5100
SVDV
Normal + Boost
Optics purge
Detector purge
3.7
0
Plasma flow
(coolant)
Aux flow
Neb flow
Snout
CCI/shear
total (L/min)
12
1
0.7
0
3
20.4
Service engineers will have access to a super

purge (adds 6L/min into poly)
Typical plasma flow
Can have the snout gas at 0. Otherwise will be 1.4L/min when on.
September 9, 2014
62
Accessories
2 and 3 port gas control plates (separate options for VDV)
5 channel peri pump (option for VDV)
SPS3
Cetac ASX520
VGA77P
MSIS
SVS1+ and SVS2+
Isomist TBD.August 1st CPL?
September 9, 2014
63
Gas control module

VDV ships with single port gas control module
SVDV/RV 2&3 port gas control module included.
Ar= supply for plasma and optics

Option Gas= Ar/Ox mix automatically routed through Aux line for Organics (80/20 blend)
N2= Separate purge for poly
September 9, 2014
64
Additional Dust protection

Optional filter that provides a higher level of protection for components inside
the instrument than the coarse dust filter in 700 series
Customer installable.
September 9, 2014
66
External Inlet Adapter

Additional protection from corrosive vapor and dust, fresh air
from external to the laboratory can be ducted into the
instrument.
External Inlet Adapter can enable ducting to be connected to
the fresh air intake of the 5100.
September 9, 2014
67
SVS 1+/2+
SVS1+
SVS2+
Small actuator
Small actuator
ICP Expert V7 has built in

software control
Higher quality USB to QUAD

serial converter
No manual control of valve

from actuator
7 port valve assembly
Higher quality connections
Simplified assembly and

operation
Note:
Prototype
controller
September 9, 2014
68
Additional Sample Introduction kits

HF resistant sample introduction kit (Glyn/Phil show and tell)
Volatile Organics sample introduction kit
Semi volatile organics kit
NOTE: Isomist is planned to be included onto the CPL as a

chilled spray chamber.
Target is August 1st.
September 9, 2014
69
Software ICP Expert V7

Based on MP Expert
Win 7 64 Bit
Flat file data storage (apart from CFR and this has database administered through
Software Database Administrator with SQL Server 2008)
Supported in:
Japanese
Simplified Chinese
English
French
German
Italian
Spanish
Portuguese
Russian
CFR: English only at release.
September 9, 2014
70
What has been added into ICP Expert V7
Real-time correction of background, l trim, calibration fit etc.

Dynamically change sample labels, number of samples during run
Monitor nebulizer back pressure and Ar intensity during run
Fast Ethernet communications
Eliminates PCI GPIB cable and card
Access from any computer via network
Many additional pages for service diagnostics
Intelligent error messages.

Hooks for Remote Advisor
21CFR11 software SCM/SDA capability like 700 series
September 9, 2014
71
Consumables
Update for the
5100 ICP-OES
Know more,
sell better
Sell better, sell

more
Consumables for 5100 ICP-OES

PS/AE Training May 2014
Key Agilent 5100 SVDV ICP-OES benefits

Lowest cost
of ownership
Reduced maintenance
costs
Fastest sample
throughput
Low gas consumption
Enhanced
Performance
Analytical
performance
System robustness
and reliability
Simple
Operation
New sample
introduction system
Instrument hardware
design
Software

73
5100 ICP-OES Reduced Maintenance

Easy Fit Vertical torch
- 5 x longer torch life (compared to 720 torch) through vertical
orientation and strategic design
Customer replaceable components
- Pre optics window and CCI
- Argon gas filter

74
5100 ICP-OES Enhanced Performance

- Improved long term stability
- Improved performance with high TDS samples (due to vertical
orientation)

- Reduced memory effects
- Faster washout
- Improved productivity

76
5100 ICP-OES Simple Operation

Customer Installable Gas control module
Customer replaceable pre optic window and CCI
Customer replaceable gas filter

77
Enhancements with 5100 Sample Intro

U-series SeaSpray nebulizer
with Unifit sample connector
Helix nebulizer connection on
spray chamber
Unifit spray chamber drain
connector
Easyfit torch design

78
Limitations of the SeaSpray neb. with EzyFit

Many users do not seat the
EzyFit connector correctly
Small dead space between
EzyFit and nebulizer
capillary
Traps small volume of sample

Can introduce memory effects
Increases washout times slightly
Decreases sample throughput

79
Advantages of the U-Series nebulizer

Same connector (U-Series nebulizer &
UniFit connector) used with the 7900
ICP-MS
Sample connector fits directly over the
outside of the sample inlet
Eliminates any dead space between

sample connector and neb. capillary
Uniform sample channel from sample entry

to nebulizer tip reduces blockage
Reduced memory effects no trapped
sample
Faster washout
Improved productivity
Improves ease of use
Unifit connector seals directly against the

sample inlet arm

80
Advantages of the Helix spray chamber

Eliminates the O-ring seal used on nebulizer inlet
Eliminates dead volume in the nebulizer seal

No O-Rings to replace
Inert impervious to organic solvents and strong acids
Special release/lock mechanism seals the chamber
Positive stop to ensure correct nebulizer position

81
Advantages of the Unifit drain connector

PTFE connector fits directly over
the outside of the waste outlet
Improves ease of use
Remains easy to fit and remove
Doesnt bond/stick to the glass
Faster washout
Improved productivity

82
5100 Easyfit Torch
Vertical torch -
True radial analysis (25% TDS) with torch robustness

benefits from having vertical radial torch
Axial view sensitivity
Automatic torch alignment - no torch scanning required
Automatic gas connection to eliminate confusion around gas
line fitting
Longer torch lifetime

83
Torch configurations for 5100 SVDV*/VDV ICP-OES

All SVDV torches have slot for radial viewing
One piece
Permanently bonded
1.8mm ID injector
Demountable
Same as one piece torch

Torch components replaceable
Organics
demountable
Narrow 1.4mm ID injector

High Solids
demountable
Wide 2.4mm ID injector

Ceramic fully
demountable
Quartz outer & ceramic 1.8mm

ID injector (straight)
*Synchronous Vertical Dual View

(features unique Dichroic Spectral Combiner)
84
Torch configurations for 5100 RV* ICP-OES

All RV torches have shorter outer tube for radial viewing (no slot required)
One piece
Permanently bonded
1.4mm ID injector
Demountable
Same as one piece torch

Torch components
replaceable
Volatile
organics
demountable
Small 0.8mm ID injector

Torch components
replaceable
*Radial View
(Note: Can be used with SVDV for improved radial performance)
85
Some Consumables Shared with 700 Series ICP

Description
Part Number
Peristaltic pump tubing

- for sample uptake (white/white)
- for waste (blue/blue)
- for internal standard (orange/white or smaller)
3710034400
3710034600
3710046900
Y piece connector for int. standard
1610132400
Gas inlet connector (Ezylok) for nebulizer
9910127800
Clamp for ball joint
G8000-64140
Inlet cooling air filter
G8000-68002
Wavelength calibration solution

Concentrate (dilute 10x prior to use)
Ready to use solution
6610030000
6610030100

86
Consumables Unique to the 5100 ICP-OES

Description
Part Number
SeaSpray nebulizer
(features U-series sample inlet)
Sample tubing for nebulizer (0.75mm ID)
Sample tubing for nebulizer (0.5mm ID)
G8010-60255
Twister double pass spray chamber
G8010-60256
UniFit connector for spray chamber waste
TBC
Inert double pass spray chamber
G8010-68007
Torches for SVDV/VDV Instruments
TBC
G3266-80012
Part Number
Easy-fit VDV torch (one piece)
G8010-60228
Demountable version of the Easy-fit VDV

torch
G8010-60236
Organics version of the Easy-fit VDV torch

(1.4mm ID inj.; demountable)
G8010-60233
High solids version of the Easy-fit VDV

torch (2.4mm ID inj.; demountable)
G8010-60232
HF version of the Easy-fit VDV torch

(1.8mm ID inj., ceramic outer + injector;
demountable)
G8010-60231
Torches for Radial Instruments
Part Number
Easy-fit RV torch (one piece)
G8012-60000
Demountable version of the Easy-fit RV

torch
G8010-60237
Volatile organics version of the Easy-fit

VDV torch (0.8mm ID inj.; demountable)
G8010-60235

87
What Consumables to Sell with 5100 ICP-OES?

Always offer one of the ICPOES Consumables Kits with the
5100
Each kit contains all the essential and
common supplies required for routine
operation of the 5100 ICP-OES
- For SVDV/VDV models, use part #
G8010-67001 (TBC)
- For radial RV models, use part #
G8012-67001 (TBC)
Components in the Operating Supplies Kit

(Preliminary contents may change)
2 one piece torches

4 packs pump tubing (for sample + waste)
1 pack int. standard pump tubing & connectors
SeaSpray nebulizer (U series)
1 pack of Unifit connectors for nebulizer
1 pack of Ezylok gas connectors for nebulizer
Twister spray chamber with Helix fitting
1 pack of Unifit connectors for spray chamber drain
Customers can re-order regularly to

ensure they have all the essential
supplies on hand
- Minimizes downtime
- Reduces operating costs through
discounted pricing
Spare clamp for the ball joint

Spare pre-optic window
(radial kit incl. an extra window for the radial view)
Spare washer for the window assembly

Drain tubing
88

New 5100 Icp-Oes

Hochgeladen von

Dokumentinformationen

Originaltitel

Copyright

Verfügbare Formate

Dieses Dokument teilen

Dokument teilen oder einbetten

Freigabeoptionen

Stufen Sie dieses Dokument als nützlich ein?

Sind diese Inhalte unangemessen?

Copyright:

Verfügbare Formate

New 5100 Icp-Oes

Hochgeladen von

Copyright:

Verfügbare Formate

Agilent 5100

Introducing the NEW 5100 ICP-OES

Agilent 5100 ICP-OES

Agilent 5100 ICP-OES

How Do Traditional Dual View Instruments Work?

What is Synchronous Vertical Dual View with unique

Axial light from plasma

5100 SVDV model working in axial only (DV)

Axial light reflected

5100 SVDV model working in radial only (DV)

Axial light goes straight

Agilent 5100 ICP-OES Project Drivers

Reminder of technology and industrial design

Robust solid state RF

Behind the covers

April 30, 2013

Optimized footprint through strategic Industrial Design

Agilent 5100 (Aurora)

Agilent 700 Series

Thermo 7000 Series

40% smaller than 700 series, 7% smaller than iCAP 7000

Key Agilent 5100 SVDV ICP-OES benefits

1. Lowest cost of ownership

Reduces repeat analysis requirements

Measures wavelengths simultaneously

Low exhaust extraction (2.5m3/min, >50% lower than 700 series))

1. Lowest cost of ownership

No RF power tube to replace

Vertical Easy-fit torch

Pre optic windows and gas filter

positive pressure design

Mains power supply and RF power supply

Located out of high volume air flow

Enhanced diagnostics and Smart electronics

Reduce service times

Easy Fit SVDV torch

Performance proof EIE Immunity

Performance proof EIE immunity

5ppm multielement LTS.

Performance Proof 4 hr LTS on 25% NaCl with 1ppm std.

Performance Proof Interim Axial IDL (n=1

VDV Axial IDL

720 Axial IDL

720 Axial IDL

Gas Use Ar/min

Gas Use Ar/sample

Resolution Performance Proof

Accuracy Performance proof

Agilent 5100 ICP-OES market segments

Food & Agriculture

Chemical & Energy

Drinking and natural water

Trace toxic metals in food

Mining and Metals

Soil and sediment

Toys and Consumer Products

Alternative Energy (Biodiesel)

Incoming raw material testing

Feed and fertilizer

Semicon, Ceramics, Batteries

Fine and Bulk Chemicals

QA/QC of Final Product

Why is SVDV perfect for Environmental and Food and