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ABSTRACT
Despite the economic success in the Woodford Shale
play, variability in petrophysical parameters controlling
reservoir quality is poorly understood and hence,
exploration activities rely heavily on history matching.
This limits the identication of new sweetspots and also
expansion of exploration activities outside the proven area.
Here we present a set of laboratory-measured petrophysical
properties collected on 300 samples of the Woodford Shale
from six wells. This dataset provided an opportunity to
cluster the Woodford Shale in three different petrotypes
(good, intermediate and poor). Good correlations between
different petrotypes with geological core descriptions,
along with the good conformance between different
petrotypes with production data ascertain the practical
applicability of such petrotyping. It was possible to upscale
such petrotypes through calibration of well logs with
core measurements. Porosity, bulk density, grain density,
mineralogy, acoustic velocities (Vp-fast, Vs-fast and Vsslow), mercury-injection capillary pressure along with
INTRODUCTION
The Woodford Shale, which has long been known as
the source of most of Oklahomas hydrocarbon reserves,
emerged as resource play in its own right following the huge
success of the Barnett Shale play in 2005. Geographically,
the Woodford Shale play can be grouped into three regions:
Woodford, Cana-Woodford (Midwest) and Barnett Woodford
(Southwest), with estimated technically recoverable resource
as 22.21 Tcf, 5.72 Tcf and 32.15 Tcf, respectively (EIA,
2011). This study focuses on an area in the Midwest where
the shale is reported to produce dry gas, condensate as well
and oil and has an average thickness of 200 ft.
The Woodford Shale is not only characterized by highly
heterogeneous nature but also acts as the source, seal, and
reservoir, which make it difcult to identify or rather, dene
the reservoir unit within this rock. Appropriate petrophysical
characterization leads to identication of different petrotypes
Manuscript received by the Editor April 11, 2013; revised manuscript received June 10, 2013.
1
Originally presented at the 53rd Annual Logging Symposium, Cartagena, Colombia, June 16-20, Paper LLL
2
Mewbourne School of Petroleum and Geological Engineering, University of Oklahoma, SEC-1210, Sarkeys Energy Center, 100
E. Boyd St., Norman, OK 73019-1003, USA; Email: nabanitag@gmail.com; crai@ou.edu; csondergeld@ou.edu
3
Now at Shell Oil Company, 25519 Somerset Meadows Ct., Katy, Tx 77494, USA; Email: Nabanita.gupta@shell.com
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LABORATORY MEASUREMENTS
A set of petrophysical properties impacting two critical
reservoir-assessment categories, i.e., storage capacity and
ow capacity, were measured: crushed rock porosity (I),
(bulk density (b), grain density (g) (Karastathis, 2007;
Kale, 2009), mineralogy through Fourier Transform InfraRed transmission spectroscopy (FTIR) (Ballard, 2007;
Matteson and Herron, 1993; Sondergeld and Rai, 1993),
acoustic velocities (Vp-fast, Vs-fast and Vs-slow) (Birch,
1960; Schreiber et al., 1973; Raina, 2010), total organic
carbon (TOC) content, Rock-Eval analyses, and mercuryinjection capillary pressure (MICP) (Kale, 2009). In
addition, microscopic and submicroscopic inspections of
samples were conducted through petrographic analyses of
thin sections and scanning electron microscopic (SEM)
analyses of focused ion beam (FIB) milled samples. Nuclear
magnetic resonance (NMR) measurements were performed
on a few samples to gain knowledge of shale wettability.
Most of these measurements were made at the Integrated
Core Characterization Center (IC3) at the University of
Oklahoma. The organic content (TOC) and Rock-Eval
measurements were made at a commercial laboratory.
Dynamic elastic moduli calculated from ultrasonic acoustic
velocities provide indirect estimates for rock-mechanical
characteristics.
Crushed rock porosity (I) represents the total porosity
of shales and includes the free and capillary-bound pore
spaces but excludes the spaces occupied by clay-bound
water. The FTIR mineralogy system was setup to identify 16
common rock-forming minerals, which were grouped into
ve mineral groups (Table 1).
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r=
2kcos
Pcap
(1)
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Porosity
Porosity (I) ranges between 0 and 10% and shows a
normal distribution, especially when wells with high organic
maturity are considered. The porosity of samples from wells
with low thermal maturity fall into a different distribution.
In wells with high thermal maturity (Wells 1, 2, 3, and 6),
porosity ranges from 2 to 10% and averages 6%. For wells
within the oil window (Wells 4 and 5) porosity ranges from
0 to 5% and averages 2.7%.
Density
Bulk density ranges from 2.2 to 2.9 g/cm3, averaging 2.4
g/cm3; grain density ranges from 2.4 to 3 g/cm3, averaging
2.6 g/cm3.
Mineralogy
Figures 4 through 6 summarize the mineralogy listed
in Table 1. Individual mineral weight percentages for
Wells 1 through 6, located in different parts of the basin,
show an overall narrow spread while quartz and illite
show comparatively wider spread (Fig. 4a). Fig. 4b shows
distributions of ve group of minerals mentioned in Table 1.
Despite the narrow range in mineralogy, plots of mineral wt%
vs. depth for Wells 1, 2 and 3 (Fig. 5) show strong variations.
For example, Well 3 has a higher clay concentration
compared to Wells 1 and 2, and there is a signicant decease
in clay concentration with shallower depths in Well 2.
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Fig. 7Crossplot of quartz vs. clays, the two dominant minerals in the
Wells 1 through 6, indicates that these two parameters are inversely
related.
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Fig. 12Crossplot of core porosity (IHe) vs. total clays. Data are colored
with quartz content (wt%). Data bounded by the two ellipses indicate
two clusters of rocks. The cluster with higher clay concentration is
characterized by low quartz concentration and the other cluster with
lower clay concentration is characterized by higher quartz concentration.
Points marked by 1 indicate carbonate-rich samples characterized by
both low clays and low quartz concentrations.
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Fig. 13Crossplot of core porosity (I) vs. quartz. The crossplot exhibits
two clusters of rocks as shown by the two ellipses. IHe increases with
increasing quartz for quartz concentration <40%, and decreases with
increasing quartz for quartz concentrations >40%.
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Fig. 14Crossplots of TOC vs clays (a) and TOC vs. quartz (b). Data
are colored with quartz and clay content in (a) and (b), respectively.
Crossplots indicate more than one cluster of data as bounded by the
ellipses.
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Fig. 15Crossplots of (a) Vp-fast vs. TOC; (b) Vs-fast vs. TOC; (c)
shear-wave anisotropy vs. clay; and (d) Youngs modulus vs. TOC. Black
circles indicate possible different rock types holding unique a correlation
between different petrophysical parameters. Data are colored with IHe,
as indicated on the color bar.
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Fig. 18Crossplots of (a) clay vs. quartz, (b) porosity vs. quartz,; (c)
clay vs. TOC, and (d) quartz vs. TOC. These crossplots indicate three
petrotypes identied through cluster analyses. In (a), Petrotypes 1
through 3 are colored pink, green and red, respectively. Figure 18a
indicates that each petrotype is characterized by unique range of clay
and quartz concentrations.
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a high Poissons ratio, and high Vp/Vs ratio and thus dened as
ductile (Fig. 19). In order to initiate hydraulic fracturing and
produce hydrocarbons from these otherwise impermeable
resource shales, the ductile hydrocarbon/TOC-enriched
intervals require intervening brittle layers. Consequently,
the vertical juxtaposition of petrotypes with contrasting
mechanical properties (brittle versus ductile) will improve
the reservoir quality of resource shales. Among the studied
wells, the best producing well, Well 2, is characterized by
broadest distribution of petrophysical parameters, thus
indicating the presence of different petrotypes within the
producing Woodford Shale interval. On the other hand,
despite the presence of good reservoir storage capacity
(based on the concentration of TOC and porosity) Well 3
is nonproductive. The lack of contrasting petrotypes in the
vertical Woodford section combined with high clay content
limited the effectiveness of hydraulic fracturing in this well.
This is an ideal example of a well with good storage capacity
and zero hydrocarbon production due to inability to initiate
hydraulic fracturing. Petrotyping was not performed on Well
6, located between Wells 2 and 3 (Fig. 2), due to limited
sample availability.
WELL-LOG ANALYSIS
Fig. 19Crossplots of (a) Youngs modulus vs. Poissons ratio, and (b)
Youngs modulus vs Vp-fast/Vs-fast ratio. Circle size is proportional to
TOC concentration.
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ACKNOWLEDGEMENT
We would like to thank Cimarex Energy for providing the
funding and some cores used in this study. We acknowledge
the help and guidance provided by the people at the
University of Oklahomas Integrated Core Characterization
(IC3) Laboratory.
REFERENCES
PR
NOMENCLATURE
FIB = focused-ion beam
FTIR = Fourier transform infra-red transmission
spectroscopy
Hg = mercury
IC3 = integrated core characterization center
MICP = mercury-injection capillary pressure
NMR = nuclear magnetic resonance
SEM = scanning electron microscope
Tcf = trillion cubic feet
TOC = total organic carbon
k = constant used in Washburn equation
Pcap = capillary pressure, psi
r = pore-throat radius, m
Ro = vitrinite reectance, %
S1 = amount free hydrocarbons, mg/g
S2 = amount of remaining hydrocarbons that could be
S3 generated, mg/g
Tmax = temperature at maximum release of hydrocarbons,
C
Vp = compressional-wave velocity, km/s
Vs = shear-wave velocity, km/s
= interfacial tension, dyne/cm
= contact angle between mercury and air
b = bulk density, density, g/cm3
g = grain density, density, g/cm3
I = porosity, %
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