Dr.

Specht Laboratorien
Summary :

FAPAS Proficiency Test 0972 Pesticide Residues in Wheat Flour

July 2011 - September 2011

Management:

FAPAS & FEPAS

Sand Hutton, York
UK York YO41 1LZ, United Kingdom

Matrix:

Wheat Flour (organic)

Used Method:

Multi residue method QuEChERS (DIN EN 15662): Extraction with Acetonitrile and dispersive SPE with PSA and final LCMS/MS and GC-MSD- or GC-FPD-measurement (accredited method)
Assigned
Value,
g/kg

Dr. Specht
results
g/kg

Z-score

Number of
Satisfactory
Z-score 2

Total Number
of Scores

Satisfactory
%

Chlorpyrifos

145

136

- 0.3

108

135

80

Fenvalerate

304

311

0.1

82

101

81

Parathion-ethyl

121

125

0.2

71

99

72

Pirimiphos-methyl

76.8

62

- 0.9

115

130

88

Analyte

(sum of all isomers)

Number and Percentage of Participants Correctly Identifying and Obtaining Satisfactory z-Scores for all
Pesticides Present 25 g/kg
Criteria
correctly identified all
1
four pesticides present
correctly identified all four pesticides
2
and obtained satisfactory z-score
correctly identified all four pesticides
and obtained satisfactory z-score and
3
used accredited methods

number of satisfactory
participants

total number participants

satisfactory
%

71

140

51

52

140

37

36

140

26

Dr. Specht Laboratorien belongs to the participants having

1
- identified ALL analytes (51% of all participants)
2
- and met ALL analytes with satisfactory z-scores (37% of all participants)
3
- and met for these pesticides satisfactory z-scores used accredited methods (26 % of all participants)
FAPAS_0972_2011

page 1 of 2

Dr. Specht Laboratorien

Scope of Pesticides to be tested for:
Acephate

Deltamethrin

Fenvalerate (sum of isomers) Metconazole

Quinoxyfen

Azinphos-methyl

Demeton-S-methyl sulfone

Fipronil

Methacrifos

Quintozene

Azoxystrobin

Diazinon

Fludioxinil

Methomyl

Spiroxamine

Bifenthrin

Dichlorvos

Fluquinconazole

Metribuzin

Tebuconazole

Captan

Difenoconazole

Flusilazole

Omethoate

Tebufenozide

Carbaryl

Diflubenzuron

Flutriafol

Oxydemeton-methyl

Thiabendazole

Carbendazim (sum)

Dimethoate

Formothion

Paclobutrazol

Thiacloprid

Carbofuran

Dimoxystrobin

alpha-HCH

Parathion (ethyl)

Thiamethoxam

3-Hydroxycarbofuran -Endosulfan

beta-HCH

Penconazole

Thiodicarb

Carboxin

-Endosulfan

gamma-HCH

Pendimethalin

Triadimefon

Chlorfenvinphos

Endosulfan sulfate

Hexaconazole

Permethrin (sum of isomers)

Triadimenol

Chlorothalonil

Epoxiconazol

Imazalil

Phosmet

Triazophos

Chlorpropham

Ethion

Imidacloprid

Phosphamidon (sum of E+Z isomers)

Tricycazole

Chlorpyrifos (ethyl)

Etrimphos

Iprodione

Pirimicarb

Trifloxystrobin

Chlorpyrifos-methyl

Fenbuconazole

Isofenphos-methyl

Desmethyl-pirimicarb

Trifluralin

Clothianidin

Fenhexamid

Isoprothiolane

Primiphos-methyl

Triticonazole

Cyfluthrin (sum)

Fenitrothion

Isoproturon

Prochloraz (sum)

Vinclozolin

Cypermethrin

Fenpropimorph

Kresoxim-methyl

Procymidone

Cyproconazole

Fenthion

Linuron

Propiconazole

Cyprodinil

Fenthion sulfone

Malaoxon

Pyraclostrobin

lambda-Cyhalothrin

Fenthion sulfoxide

Malathion

Pyrimethanil

FAPAS_0972_2011

page 2 of 2