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Indian Standard
PLASTICS -
METHODS OF TESTING
PART 5
MECHANICAL
Section 4 Determination
PROPERTIES
ICS 83.080
@ BIS 1996
BUREAU
MANAK
April
1996
OF
BHAVAN,
INDIAN
STANDARDS
9 BAHADUR SHAH
NEW DELHI 110002
ZAFAR
MARG
Price Group
NATIONAL FOREWORD
This Indian Standard which is identical with IS0 180 : 1993 Plastics - Determination of izod impact
strength, issued by the International Organization for Standardization (ISO) was adopted by the
Bureau of Indian Standards on the recommendation of Methods of Test for Plastics Sectional
Committee and approval of the Petroleum, Coal and Related Products Division Council.
The text of IS0 standard has been approved as suitable for publication as Indian Standard without
deviations. Certain conventions are, however, not identical to those used in Indian Standards. Attention
is particularly drawn to the following:
a) Wherever the words International Standard appear referring to this standard, they should
be read as Indian Standard.
b) Comma (J has been used as a decimal marker while in Indian Standards, the current practice
is to use a point (.) as the decimal marker.
In this adopted standard reference appears to certain International Standards for which Indian
Standards also exist. The corresponding Indian Standards which are to be substituted intheir place
are listed below along with their degree of equivalence for the editions indicated:
International Standard
Degree of
Equivalence
Technically
equivalent
.do,
do.
Identical
NIL
NIL
180 : 1993
Indian Standard
PLASTICS -
METHODS OF TESTING
scope
1.3 The method is suitable for use with the following range of materials:
-
rigid thermoplastics moulding and extrusion materials, including filled and reinforced compounds
in addition to unfilled types; rigid thermoplastics
sheet;
fibre-reinforced
thermoset
and thermoplastics
composites incorporating unidirectional or nonunidirectional reinforcements such as mat, woven
fabrics, woven rovings, chopped strands, combination and hybrid reinforcements, rovings and
milled fibres; sheet made from pre-impregnated
materials (prepregs);
Normative references
Definitions
IS0 2602:1980,
suks interval.
of test reConfidence
3.1
. IS0 3167:-31,
Plastics -
per square
metre
3.2
in kilojoules
per square
metre
3.3 lzod impact strength of reversed-notch specimens, q,: Impact energy absorbed in breaking a
reversed-notch specimen, referred to the original
cross-sectional area of the specimen at the notch, the
pendulum striking the face opposite the notch.
It is expressed
(kJ/mz).
in kilojoules
per square
metre
3.4 parallel impact (p) (for laminar reinforced plastics): Direction of blow parallel to the laminate plane
of sheet materials. The blow direction in the lzod test
is edgewise (e) (see figure 1, edgewise paral!el).
3.5 normal impact (n) (for laminar reinforced plastics): Direction of blow normal to the laminate plane
of sheet materials (see figure 1, edgewise normal).
NOTE 1 This kind of impact is not used with the lzod
test, but is indicated only for clarifying the designation system.
4
IS0 i818:3),
Plastics mens by machining.
in kilojoules
Principle
Multipurpose
test speci-
mens.
edgewise
flatwlse f
parallel p
LOptlonal
groove
lovable vicejaw
normal
Direction of blow with respect to specimen thickness h and specimen width b: edgewise (e) and flatwise (f); with
respect to the laminate plane: parallel (p) and normal (n).
The usual lzod test is edgewise parallel. When h = b, then parallel as well as normal can be tested.
Figure 1 -
180 : 1993
Apparatus
5.1
Testing
machine
51.1
The testing machine shall be of the pendulum
type and shall be of rigid construction. It shall be capable of measuring the impact energy, W, absorbed
in breaking a test specimen The value of this energy
is defined as the .difference between the initial energy, E, of the pendulum and the energy remaining in
the pendulum after breaking the test specimen. The
energy shall be corrected for losses due to friction and
air resistance (see table 1 and 7.4).
NOTE 2
Pendulums with energies other than those given
in table1 are permitted, but it is planned to withdraw this
option at the next revision.
Energy E
Velocity at impact
(nominal)
J
,:;05
55
ll,o
22,0
Maximum permissible
frictional loss without
specimen
m/s
3.5 (* 10 %)
0,02
0.03
0.03
0,05
0,lO
0,Ol
0,Ol
0.02
0.05
0,lO
1) The permissible error shall not be exceeded over the 10 % to 80 % range of the pendulum capacity.
Dimensions en millim&tres
in contact with
Figure 2 -
Vice support, test specimen and striking edge shown at impact of notched specimen
brated torque wrench or a pneumatic or hydraulic device on the vice clamping screw.
5.2
NOTE3 The pendulum length fr+, in metres, may be determined experimentally from the period of small amplitude
oscillations of the pendulum by means of the following
equation:
Test specimens
6.1
6.1.1
Moulding
or extrusion
compounds
where
&l
Preparation
6.1.2
Sheets
Specimens shall be machined from sheets in accordance with IS0 2818. Whenever possible, specimens
of type 1 with notch A shall be used. The machined
surface of unnotched specimens shall not be tested
under tension.
6.1.3
Long-fibre-reinforced
polymers
6.1.4
Checking
NOTE 4
The fixed vice jaw may be provided with a
groove to improve positioning and handling of the test
specimen (seefigure 1).
5.1.7
Some plastics are sensitive to clamping pressure. When testing such materials, a means of
standardizing the clamping force shall be used and the
clamping force shall be recorded in the test report.
The clamping force can be controlled by using a cali-
Specimens showing measurable or observable departure from one or more of these requirements shall be
5
180 : 1993
Notching
6.1.5.1 Machined notches shall be prepared in accordance with IS0 2818. The profile of the cutting
tooth shall be such as to produce in the specimen a
notch of the centaur and depth shown in figure3, at
right angles to its principal axes.
6.2
Anisotropy
I=80f2
width:
b = 10,o f 0,2
thickness:
h = 4.0 f 0,2
The recommended thickness h is 4 mm. If thespecimen is cut from a sheet or a piece taken from a
structure, the thickness of the specimen, up to
10,2 mm, shall%be the same as the thickness of the
sheet or the structure.
Specimens taken from pieces thicker than 10,2 mm
shall be machined to 10 mm f 0,2 mm from one
surface, providing that the sheet is homo eneous in
its thickness and contains only one type o7 reinforcement regularly distributed. If unnotched specimens
are tested according to 3.1, the original surface shall
be tested under tension, in order to avoid surface effects.
Specimens are tested edgewise in the parallel direc:
tion with
the exception
of specimens
with
h = b = 10 mm, which can be tested parallel and
normal to the sheet plane (see figure 1).
Figure 3 -
Notch types
Table 2 -
Method
designationl)
IS0 180/l U 2)
Specimen type
Notch type)
3)
unnotched
Remalnlng width,
&, at notch base
-
IS0 180/l A
0,25 f 0,05
80 f 0,2
is0 180/1B
1.00 f 0.05
80 f 62
1) Attention is drawn to changes in method designations and notch type designations from those used in IS0 180:1982.
2) If specimens are taken from sheets or products, the thickness of the sheet or product shall be added to the designation
and unreinforced specimens shall not be tested with their machined surface under tension.
3) If the sheet thickness h equals the width b, the blow direction (normal n, or parallel p) should be added to the designation.
L
6.4
Number
of test specimens
6.4.1
Conditioning
7.5 Lift and support the pendulum. Place the specimen in the vice and clamp it in accordance with 5.1.6
and as shown in figure2. For the determination of
notched lzod impact strength, the notch shall be positioned on the side that is to be struck by the striking
edge of the pendulum (see figure2).
Procedure
7.6 Release the pendulum. Record the impact energy absorbed by the specimen and apply any necessary corrections for frictional losses etc. (see table 1
and 7.4).
NOTE 6
In the case of injection-moulded specimens, it is
not necessary to measure the dimensions of each specimen. It is sufficient to measure one specimen from a set
to make sure that the dimensions correspond to those in
6.3.
With multiple-cavity moulds, ensure that the dimensions of the specimens are the same for each cavity.
160: 1993
Calculation
and expression
of results
qu+x
lo=
. . . (2)
8.4
Significant figures
Precision
The precision of this test method is not known because interlaboratory data are not available. When
interlaboratory data are obtained, a precision statement will be added in the next revision.
Test report
where
8.2
Statistical parameters
10
Unnotched specimens
8.1
8.3
is the width,
specimen.
in millimetres,
Calculate the lzod impact strength of notched specimens, air.,, expressed in kilojoules per square metre,
with notches N = A or B, using the formula
aiN
J.L
h.4
lo=
...
where
is the corrected energy, in joules, ab
sorbed by breaking the test specimen;
9J
of the test
Notched specimens
IS0 180/l
j)
180 : 1993
IS
13360
l%
180:
( Part 5/Set
4 ) : 1996
1993
Annex A
(normative)
lzod impact test on specimen types 2,3 and 4 of IS0 180:1982
A.1
General
A.3
A.3.1
See 8.2.
A.2
Test specimens
(see table A. 1)
A.3.2
For sheet materials (see 6.3.21, reversed-notch specimens (see tableA.2) shall be used for specimen types
2, 3 and 4. The recommended thickness h is 3,2 mm
for type 4 if the specimen is cut from a piece or taken
from a structure. The thickness of the specimen, up
to 12,9 mm, shall be the same as the thickness of the
sheet or the structure. Specimens taken from pieces
thicker than 12,9 mm shall be machined from one
side to achieve a thickness of 12,7 mm + 0,2 mm
providing that the sheet is homogeneous in its thickness and contains only one type of reinforcement,
regularly distributed.
specimens
%I
...
lo3
where
Table A.1 -
Reversed-notch
bN
Specimen
type
2
3
4
I
Length
1
Width
b
Thickness
h
63,5 f 2
63,5 f 2
63,5 f 2
12.7 f 0,2
12,7 f 0,2
12,7 f 0,2
12,7 f 0,2
64 f 0,2
32 f 02
10
Table
A.2 -
180: 1993
_.,,,_,
l%nansinns
,.,,_
Method
designationl)
Specimen type
IS0 180/2AR
IS0 180/2BR
IS0 180/2A
IS0 180/2B
23)
A reversed
B reversed
A
B
0.25
I,00
0,25
1.00
f
f
f
f
0.05
0.05
0,05
0,05
IS0 180/3AR
IS0 180/3BR
IS0 180/3A
IS0 180/3B
A reversed
B reversed
A
B
0,25
1,oo
0,25
1.00
f
f
f
f
0,05
0,05
0.05
0,05
IS0 180/4AR
IS0 180/4BR
IS0 180/4A
IS0 180/4B
A reversed
B reversed
A
B
0,25
I,00
0,25
I,00
f
f
f
f
0,05
0,05
0,05
0,05
Notch type2)
in millimatraa
.
_..__
Remaining width,
bN, at notch base
10.2 f 0.2
1) If specimens are taken from sheets or products, the thickness of the sheet or product shall be added to the designation
and unreinforced specimens shall not be tested with their machined surface under tension,
2) For determination of the lzod impact strength of reversed-notch specimens, the pendulum strikes the face opposite that
containing the notch.
3) If the sheet thickness h equals the width b, the blow direction (normal n or parallel p) should be added to the designation.
11
Technically
equivalent
do
do
Multipur-
NIL
In the case of IS0 1268, IS0 2557-l and IS0 3167, the Technical Committee responsible for the
preparation of this standard has reviewed its contents and has decided that they are acceptable for
use in conjunction with this standard.
For tropical countries like India, the standard temperature and the relative humidity shall be taken
as 27 r 2% and 65 + 5 percent respectively.
In reporting the results of a test or analysis made in accordance with this standard, if the final value,
observed or calculated, is to be rounded off, it shall be done in accordance with IS 2 : 1960 Rules
for rounding off numerical values (revised).
BIS is a statutory institution established under the Bureau of Indian Standards Act, 1986 to promote
harmonious development of the activities of standardization, marking and quality certification of goods
and attending to connected matters in the country.
Copyright
PIS has the copyright of all its publications. No part of these publications may be reproduced in any form
without the prior permission in writing of BIS. This does not preclude the free use, in the tiourse of
implementing the standard, of necessary details, such as symbols and sizes, type or grade designations.
Enquiries relating to copyright be addressed to the Director (Publications), BIS.
Review of Indian Standards
Amendments are issued to standards as the need arises on the basis of comments. Standards are also
reviewed periodically; a standard along with amendments is reaffirmed when such review indicates that,
no changes arc needed; if the review indicates that changes are needed, it is taken up for revision. Users
of Indian Standards should ascertain that they are in possession of the latest amendments or p,dition by
referring to the latest issue of BIS Handbook and Standards Monthly Additions.
This Indian Standard has been developed from Dot : No. PCD 23 ( 1392 ).
Amendments
Amend No.
Text Affected
Date of Issue
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