Common test methods for concrete durability problems
are presented below. The ASTM designations for these tests (wherever applicable) have also been mentioned. Freezing and thawing 1. Tests on concrete (a) ASTM C666 Measurement of durability factor from dynamic modulus of concrete subjected to freezing and thawing cycles. (b) ASTM C671 Measurement of length change of concrete subjected to F/T cycles; not as harsh as ASTM C666. (c) ASTM C672 Visual assessment of concrete surface ponded with CaCl2 solution and subjected to F/T cycles. (d) ASTM C457 Petrographic analysis of concrete; determination of air content, spacing factor of bubbles, etc. 2. Tests on aggregate (a) Specific gravity and absorption ASTM C127 (b) ASTM C88 - Sulfate soundness test; mass loss of aggregates subjected to alternate drying and wetting in sodium sulfate solution; can be combined with F/T cycles too (c) ASTM C295 - Petrographic evaluation of aggregates Corrosion of steel 1. Mass loss of concrete due to scaling or delamination 2. ASTM C876 - Corrosion potential; determination of halfcell potential of rebar with respect to a reference electrode 3. Corrosion rate measurement (a) Polarization resistance test, where a DC current is applied, and the current response of the steel is measured, and (b) Electrochemical impedance spectroscopy, where an AC current is applied and the current response studied. 4. Cyclic polarization 5. Potentiostatic / galvanostatic measurements
6. Conductivity measurements for reinforced concrete
7. Conductivity / resistivity measurements for plain concrete: (a) Rapid chloride permeability test ASTM C1202, (b) chloride conductivity test, (c) migration test, etc. 8. Scanning electron microscopy. Sulfate Attack 1. ASTM C452 and C1012: Length change of mortar prisms immersed in sodium and/or magnesium sulfate solutions. 2. Mass, compressive strength, and dynamic modulus measurements of cement mortar and concrete immersed in sulfate solutions. 3. Thermal analysis, or X-ray diffraction to detect and quantify reaction products. 4. Scanning electron microscopy. Techniques 2, 3, and 4 are also applicable to acid attack and DEF. Length measurements on mortar prisms can also be conducted on steam cured cement mortar specimens for evaluation of DEF. Alkali silica reaction 1. ASTM C227 Cement mortar prepared with expansive aggregate (crushed to sand size) and high alkali cement, and stored at 38 oC and 100% RH. Length change is measured. 2. ASTM C1260 (P214) Cement mortars prepared with ordinary cement and reactive aggregate (crushed to sand size) stored at 80 oC in 1 N NaOH solution. The results from this test can be obtained within two weeks. 3. ASTM C289 Finely ground aggregate is immersed in 1 N NaOH solution at 80 oC for 24 hours. The amount of dissolved silica ad reduction in the OH- concentration of the solution is measured. 4. ASTM C295 Petrographic evaluation of aggregates.