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CB&I

500 Penn Center Blvd.


Suite 1000
Pittsburgh, PA 15235
Tel: 412.372.7701
Fax: 412.380.4091
www.CBI.com

March7,2016
ProjectNo.156319

Mr.GeoffreyBrown
EmergencyResponseProgram
OregonDepartmentofEnvironmentalQuality
WesternRegionEugene
165E7thAve,Suite100
Eugene,OR974013049

Re:
PathtoClosureWorkPlan

AT&THallRidgeCellTower

NationalResponseCenterReportNo.1140291

OregonEmergencyResponseSystemReportNo.20160374

Detroit,MarionCounty,Oregon

DearMr.Brown:

CB&IonthebehalfofAT&T,ispleasedtopresentthisPathtoClosureWorkPlanforthepostexcavation
and characterization activities at the AT&Ts Hall Ridge, Detroit, Oregon, cell tower (Site). The
emergencyresponseteam,whichconsistedofCB&I,NRC,NWFF,andSMAF,havecompletedtheinitial
phase of the emergency response including the removal of impacted soil in the release area,
containmentofthedownslopemigrationoffuel,characterizationoftheimpactedsoil,snowremoval,
andinitialroadrepairs.
OnFebruary11,2016,BarryWilliams(AT&T)receivednotificationofareleaseofdieselatthesubject
site.Theinitialinvestigationestimatedtheamountoffuelreleasedfromthetanksystemat550gallons.
It appeared the fuel was pumped from the 800gallon main tank to the 220gallon day tank, which
discharged from the vent located on the roof. Mr. Williams notified the National Response Center to
reportthespillat1740EasternStandardTime(EST).TheNationalResponseCenterassignedReportNo.
1140291tothespill.Mr.WilliamsalsonotifiedtheOregonEmergencyResponseSystemat1750ESTto
reportthespillandwasassignedReportNo.20160374.
ThisWorkPlanwasdevelopedtoprovideguidancefortheimplementationofbiostimulationtreatment
activitiesandpostexcavationandcharacterizationmonitoring.

Mr.GeoffreyBrown

March7,2016

Background

The site and surrounding area are located on the U.S. Geological Survey 7.5minute Detroit, Oregon,
topographic quadrangle map. The site is located at approximately 444309.7 north latitude,
1221303.6 west longitude. A review of the quadrangle map shows the site at an elevation of
approximately 4,400 feet above mean sea level (msl). The nearest surface water to the site is an
unnamed tributary, which is approximately 600 feet northeast of the site. A site vicinity map is
presentedasFigure1.
AccordingtotheUnitedStatesGeologicalSurveysNationalGeologicMapDatabase,thesiteislocated
ontheeasternflankoftheSardineSynclineandtheBreitenbushAnticlineislocatedtotheeast.Bedrock
dips at a shallow angle to the west. Bedrock listed is the Sardine Series, which consists of series of
Miocene age rhyolite, andesite, basalt, tuff, and breccia exposed on Sardine Mountain northwest of
Detroit.
EmergencyResponseTasksCompleted

Thefollowingtaskshavebeencompletedunderthisemergencyresponse:

OnFebruary12,2016,crewsweremobilizedtoinspectthesite.Theimpactedareawas
assessedandabsorbentboomsandpadsplacedinstrategicareastocapturethefreephase
diesel.

FromFebruary13throughFebruary19,2016Roadclearingcontinuedwithadditionalsnow
fall.Severalimpactedareaswerehandexcavated.Absorbentpadsinspectedandreplaced.
Wastewascontainerizedandstagedfordisposal.

OnFebruary22,2016,theORDEQandUSFSprovisionallyapprovedtheSamplingandAnalysis
Plan.

OnFebruary23,2016,theUSFSlocatedandauthorizedNRCtocollectwaterfromasourcenear
thesiteforthepercolationtest.

OnFebruary2425,2016,thepercolationtestcommencedoveratwodayperiodusing
fluorescentdye(BrightDyesFLTYellowGreenPowder)torecreatetheflowpathsofdieselfuel
throughbedrock.

OnFebruary26,2016,soilsampleswerecollectedona20footgridtodelineatetheextentof
thedieselintheshallowsoildownslopefromtherelease.

OnFridayFebruary19,2016,SundayFebruary21,2016,andSundayFebruary28,2016,four
surfacewatersampleswerecollectedfromtheunnamedtributaries(SW01,SW02,SW03,and
SW04)andSW05onThursdayFebruary25,2016.Dailyinspectionsoccuratthefivesurface
waterlocations.

Mr.GeoffreyBrown

March7,2016

DiscussionofSoilSampleResults

On February 26, 2016, soil samples were taken from 21 locations at the release area excavation and
downslope areas. Sample locations were identified using an established downslope grid and biased
wheredieselfuelwasvisuallyobserved(Figure3).Soilsampleswereanalyzedfordieselrangeorganics
byNWTPHDx,RBDMVOCsbyEPA8260B,andPAHsbyEPA8270DSIM.Thelaboratoryanalyticalresults
havebeentabulatedandpresentedinTable1.
The soil sample results were compared against ORDEQ riskbased concentrations (RBCs) for two
exposure pathways: soil ingestion, dermal contact, and inhalation (RBCSS), and soil leaching to
groundwater(RBCSW).ThreesamplelocationsshowedNWTPHDxconcentrationsthatexceedRBCsvia
eitherexposurepathway.Thesethreehotspotlocations(0C,1C,and2C)followthecenterlineofthe
downslopegrid,adjacenttothereleaseareaexcavation.
At sample location 0C, laboratory results show RBC exceedances for NWTPHDx (9,430 milligrams per
kilogram[mg/kg]),Benzene(0.161mg/kg),Ethylbenzene(3.70mg/kg),Naphthalene(2.15mg/kg),and
1,2,4Trimethylbenzene(19.9mg/kg).Atsamplelocation1C,resultsshowRBCexceedanceforNWTPH
Dx(66,400mg/kg).Atsamplelocation2C,resultsshowRBCexceedanceforNWTPHDx(96,800mg/kg).
NWTPHDx concentrations were also observed at sample locations EWSIDEWALLE (184 mg/kg), 0B
(1,090 mg/kg), 1B (44.6 mg/kg), 2B (70.2 mg/kg), and 3A (29.1 mg/kg). These locations are directly
adjacent to the hot spot locations, with the exception of 3A. The NWTPHDx concentrations at all
othersamplelocationswerenondetect.ThelaboratoryanalyticalresultsarepresentedinAppendixA.
OutcropSourceRemoval

Dieselhasaccumulatedontopofabedrockoutcroplocatedapproximately40feetdownslopefromthe
releaseareaasindicatedbysoilanalyticaldata,PIDreadingsandsiteobservation.Impactedsoilontop
of the rock outcrop will be excavated to provide mass removal and eliminate known potential source
areasforfutureleachingofdiesel.Thelimitsoftheexcavationwillextendapproximately4feetupslope
from the rock outcrop, approximately 10 feet across the width of the rock outcrop, and extend
approximately1footdeeptobedrock.Thelimitsoftheexcavationwillbedeterminedinthefieldusing
aPIDandfieldobservations.Duetotheextremesiteconditions,theimpactedsoilwillbeexcavatedby
hand.
Confirmationsoilsampleswillbecollectedonthesidewallsoftheexcavation,estimatedattwosamples
alongthetopwallandonesampleoneachsidewallsoftheexcavation.Theflooranddownslopewall
of the excavation are anticipated to be bedrock; therefore, soil samples are not anticipated at these
locations. Soil samples will be analyzed for diesel range organics by NWTPHDx, RBDM VOCs by EPA
8260B,andPAHsbyEPA8270DSIM.

Mr.GeoffreyBrown

March7,2016

Biostimulation

AT&T proposes to use a combination of two biostimulation products to naturally degrade residual
dieselattheSite.TheseproductsincludeOilSpillEatersInternationalCorporationsproprietaryOSEII
and MicroBlaze NonFormulated. MicroBlaze NonFormulated is a consortium of hydrocarbon
degrading bacteria that will be applied to the individual release areas in a 10% solution following the
application of OSE II. MicroBlaze NonFormulated contains no surfactants or nutrients, just a
consortiumofknownhydrocarbondegradingbacteria.
AT&T proposes to use Oil Spill Eaters International Corporations proprietary OSE II amendment to
breakdown residual diesel LNAPL in the subsurface. OSE II is a biocatalyst that contains enzymes and
nutrients designed to enhance the emulsification of LNAPL and stimulate hydrocarbon consuming
bacteriatodegradehydrocarbonsreleasedintheenvironment.NutrientswithinOSEIIwillincreasethe
rate of biodegradation of the dieselconsuming bacteria present beneath the Site to remove the
dissolveddiesel.OSEIIhasbeenevaluatedbytheEnvironmentalProtectionAgencyandislistedasan
accepted remedial response technology for hydrocarbon releases (Environmental Protection Agency,
2009).TheCaliforniaDepartmentofWildlife(formerlyDepartmentofFishandGame)haslicensedOSE
IIforoilspilltreatmentinCalifornia.DocumentationoftheOSEIIisprovidedinAppendixB.
The application of the OSE II and MicroBlaze NonFormulated is proposed in three areas. The first
application will be applied to a small trench excavated on the upgradient side of the AT&T
communicationbuilding.Thiswillbeconductedtotreatresidualdieselinthebasecoursebeneaththe
building foundation. The second application will be in the release area excavation to introduce these
solutionsintothesubsurfacefollowingasimilarpathwayastheoriginalrelease.Thethirdapplication
willbeasurfaceapplicationofthesesolutionswithinthelimitsofthedownslopeexcavationfollowing
theremovalofimpactedsoilontopoftherockoutcropandthesurfaceapplicationofthesoilbetween
the release area and rock outcrop. Documentation of MicroBlaze NonFormulated is provided in
AppendixB.Eachoftheseapplicationsisdiscussedbelow.
BuildingFoundationApplication
OSE II/MicroBlaze NonFormulated will be applied hydraulically upgradient of the AT&T
Communicationbuildinginanattempttotreatresidualdieselresidinginthebasecoursebeneaththe
building foundation. A small trench will be excavated along the north footing of the building for the
application of the OSE II. The trench will be approximately 1 foot wide and 6 inches deep. Excavated
materialwillbeplacedalongtheoutsideextentofthetrenchtoformaberm.Alicensedarcheologist
willbeonsiteduringallgrounddisturbanceactivities.Approximately300gallonsoftheOSEIIsolution
will be gravity fed into the trench at such a rate as to not overflow the trench, while maintaining a
constantheadinthetrench.Absorbentpadswillbeplacedadjacenttotheexposedbasecoursealong
thesouthsideofthebuildingtocapturedieselthatmaybedisplacedduringthisprocedure.

Mr.GeoffreyBrown
5
March7,2016

ReleaseAreaApplication
OSEIIwillbeappliedwithinthelimitsofthereleaseareainanefforttofollowthesamepathwayasthe
dieselduringtheoriginalrelease.Approximately900gallonsofOSEIIsolutionwillbeappliedontopof
theexposedbedrockinthereleaseareaexcavation.Theapplicationratewillbeconsistentwiththedye
test conducted on February 23, 2016 to evaluate flow pathways and maintained at a rate as to not
overflow the excavation. Absorbent pads located downslope of the excavation will be monitored and
replacedasnecessaryduringthistask.
OutcropExcavationOSEIIApplication
OSEIIwillbeappliedtothesurfaceofthedownslopeoutcropexcavationadjacenttotherockoutcrop
andsurroundingsoil.Approximately100gallonsofOSEIIsolutionwillbeappliedontopofthesoilinthe
areaextendingfromthereleaseareatotherockoutcropusingahose.Thesoilinthisareaispotentially
impactedbasedonsoilanalyticaldataandsiteobservations.Theapplicationrateshouldbemonitored
to prevent surface runoff, but sufficient to promote infiltration and near saturation. If the soil in the
treatment area becomes saturated to the point surface runoff occurs, the application rate will be
reduced. If surface water runoff continues to occur, the remaining volume of OSE II solution will be
applied to the release area. Absorbent pads located downslope of the impacted soil area will be
monitoredandreplacedasnecessaryduringthistask.
MixingProcedure
MicroBlaze NonFormulated will be mixed to a 10% solution using 5 gallons of MicroBlaze to 50
gallonsofwater.Thewaterwillbecollectedfromthesamplesourceusedinthedyetest,pendingUSFS
approval.
The OSE II application system will consist of a bulk mixing tank, one 55 gallon drum of OSE II, a
circulationpump,andassociatedhoses,valves,andfittings.Theapplicationsystemwillbepoweredby
anexistingonsitegenerator.SurfacewaterfromanearbystreamwillbeusedtoblendwiththeOSEIIto
makethe25:1solutionofwatertoOSEII,pendingUSFSapproval.Approximately1,375gallonsofthe
OSE II/surface water solution will be applied in and around the release area. It is anticipated that the
OSE II/surface water solution will be prepared in 300gallon batches for application; therefore, 12
gallonsofOSEIIwillbemixedwith300gallonsofwatertopreparethe25:1solution.
SurfaceWaterSampling

Currently, CB&I performs a daily visual inspection of five unnamed tributaries (SW01, SW02, SW03,
SW04,andSW05)andcollectsweeklysurfacewatersamplesfromtheselocationsonaweeklybasis.
These surface water samples are analyzed for RBDM VOCs by EPA Method 8260B and PAHs by EPA
Method8270DSIM.NoVOCsorPAHshavebeendetectedinanyofthesurfacewatersamplescollected
from the identified streams. The laboratory analytical results have been tabulated and presented in
Table2.SurfacewatersamplelocationsarepresentedinFigure4.

Mr.GeoffreyBrown
6
March7,2016

Surfacewatersampleswillbecollected30days,90days,and180daysfollowingtheapplicationofOSE
II to monitor potential impact to the adjacent surface water streams. Surface water sampling will be
discontinued following the 180 day sampling event if the analytical results remain below laboratory
detectionlimits.ApprovalwillberequestedfromORDEQandUSFStodiscontinuethesamplingprogram
if no VOCs or PAHs have been detected in the surface water following the 180 days of post bio
stimulationsampling.
In the event that any RBDM VOCs and PAHs are detected in the surface water samples above the
applicablestandards,thenthesurfacewatersamplingplanwillbeamendedtocollectsamplesfurther
downstream and/or at the reservoir discharge locations. The new surface water locations and the
numberofcollectedsampleswillbeapprovedbyORDEQandUSFS.
DatafromthesamplingwillbesubmittedtotheORDEQandUSFSinstatusreports.Thestatusreports
willprovideabriefsummaryoftheanalyticalresultsandconfirmthefuturesamplingfrequency.
AbsorbentandWeirMaintenance

Afterexcavationofthesourcearea,crewsestablishedadownslopecatchmentsystemincludingaweir
and trenches containing absorbent booms, and absorbent pads interweaved across the exposed
bedrock seepage areas. Crews are monitoring the absorbents daily and replacing them as needed.
SaturatedabsorbentsarecontainerizedinSuperSacsandremovedoffsitetoalandfill.
FollowingapplicationoftheOSEIItreatment,crewswillcontinuetochangeoutabsorbentpadsand/or
booms along the downslope hillside on a weekly basis. In the event that no color change in the
absorbents is observed for 30 days, then crews will remove absorbents and booms from the site and
backfill the weir, trenches, and potholes. Crews will restore the site as close as possible to pre
disturbancedrainageconditions.
SiteRestoration

Releasearea
The release area excavation and adjacent area will be restored to preexcavation conditions following
thebiostimulationapplication.Approximately4inchlayerofpeatmosswillbeappliedadjacenttothe
exposed building footing and over the exposed bedrock with previously observed contact with diesel.
The diesel readily binds with peat moss until it naturally biodegrades, preventing any residual diesel
frommigratingoffsite.Sufficientgravelwillbeplacedoverthepeatmosstorestorethesitetonearpre
excavation grade. Clean gravel that was excavated during the initial response and temporarily
stockpiled adjacent to the excavation will be used as fill material. Additional gravel from an offsite
sourceconsistingof3/4inchminuswillbeappliedtotheexcavationtorestoretheareatotheoriginal
grade.Fillmaterialwillbeappliedin6inchliftsandcompactedbydrivingoverthefillmaterialwiththe
equipment.Theareawillbegradedtopromotepositivedrainageawayfromthebuilding.

Mr.GeoffreyBrown
7
March7,2016

OutcropExcavation
The outcrop excavation and adjacent area will be restored to preexcavation conditions following the
biostimulation application. Approximately 4inch layer of peat moss will be applied adjacent to the
exposed bedrock with previously observed contact with diesel. Top soil will be applied on top of the
peatmossin6inchliftsandhandcompacteduntiltheelevationofthefillmaterialisconsistentwiththe
surroundingtopography.Grassmattingwillbeappliedoverthetopsoiltominimizeerosion.
Recommendation

Please provide your written approval if this Work Plan is acceptable or let us know if you have any
questions,comments,orrevisions.Ifnecessary,theWorkPlanwillberevisedandresubmittedforyour
approval.Thankyouforyourtimeduringouronsitemeetingsandforyourresponsivenessinworking
withustodevelopthisPlan.
Pleasecontacteitheroftheundersignedifyouhaveanyquestionsconcerningthisreport.

Sincerely:

RonaldMalec,P.G.
IncidentCommander,UnitChief
4123804484

Ron.Malec@CBI.com

MF:KR:RM:lmk
Attachments

cc:LaurenPlunk(AT&T)
BrynThoms(ORDEQ)
GregAitken(ORDEQ)
GradyMcMahan(USFS)
DarrinNeff(USFS)
JamieSheahanAlonso(USFS)
PennyKeen(USFS)
MarkFinney(CB&I)
BryanHolmes(CB&I)

KentRoberts
SeniorOperationsManager
3215431194

Kent.Roberts@cbi.com

Tables

Table1
SoilSampleAnalyticalResults
AT&THallRidge
OregonEmergencyResponseSystemReportNo.20160374
WillametteNationalForest
Detroit,Oregon
SoilSampleAnalyticalResults

RBCsw
Contaminant
PIDReading(ppm)
NWTPHDx:Diesel
NWTPHDx:Oil
Benzene
Toluene
Ethylbenzene
Xylenes
Naphthalene
MTBE
Isopropylbenzene
nPropylbenzene
1,2,4Trimethylbenzene
1,3,5Trimethylbenzene
1,2Dibromoethane(EDB)
1,2Dichloroethane(EDC)

RBCss

(mg/kg) (mg/kg)

9,500
4,600
>Max
11,000
0.10
300
310
28,000
0.94
1,700
49
20,000
0.37
580
0.50
12,000
280
27,000
NoStd. NoStd.
5.6
2,000
110
3,500
0.00056
9
0.013
200

1A
(mg/kg)
5.4
ND
123
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

1B
(mg/kg)
6.4
44.6
159
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

Page1of7

1C
(mg/kg)
397
66,400
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

2A
(mg/kg)
2.7
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

2B
(mg/kg)
1.9
70.2
312
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

2C
(mg/kg)
183
96,800
ND
0.0449
0.887
0.832
4.74
ND
ND
ND
0.642
3.53
1.04
ND
ND

2D
(mg/kg)
33.8
ND
606
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

Table1
SoilSampleAnalyticalResults
AT&THallRidge
OregonEmergencyResponseSystemReportNo.20160374
WillametteNationalForest
Detroit,Oregon
SoilSampleAnalyticalResults

RBCsw
Contaminant
Acenaphthene
Acenaphthylene
Anthracene
Benz(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(g,h,i)perylene
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
Fluoranthene
Fluorene
Indeno(1,2,3cd)pyrene
1Methylnaphthalene
2Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene

RBCss

(mg/kg) (mg/kg)

21,000
NoStd. NoStd.

110,000
2.3
24
1.9
2.4

24

240
NoStd. NoStd.

2,400

2.4
NoStd. NoStd.

10,000

14,000

24
NoStd. NoStd.
NoStd. NoStd.
0.37
580
NoStd. NoStd.

7,500

1A
(mg/kg)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

1B
(mg/kg)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

Page2of7

1C
(mg/kg)
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA

2A
(mg/kg)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

2B
(mg/kg)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

2C
(mg/kg)
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA

2D
(mg/kg)
ND
ND
ND
ND
ND
0.0249
ND
ND
ND
ND
ND
ND
0.0229
ND
0.0284
0.0433
0.0502
0.0229
ND

Table1
SoilSampleAnalyticalResults
AT&THallRidge
OregonEmergencyResponseSystemReportNo.20160374
WillametteNationalForest
Detroit,Oregon
SoilSampleAnalyticalResults

RBCsw
Contaminant
PIDReading(ppm)
NWTPHDx:Diesel
NWTPHDx:Oil
Benzene
Toluene
Ethylbenzene
Xylenes
Naphthalene
MTBE
Isopropylbenzene
nPropylbenzene
1,2,4Trimethylbenzene
1,3,5Trimethylbenzene
1,2Dibromoethane(EDB)
1,2Dichloroethane(EDC)

RBCss

(mg/kg) (mg/kg)

9,500
4,600
>Max
11,000
0.10
300
310
28,000
0.94
1,700
49
20,000
0.37
580
0.50
12,000
280
27,000
NoStd. NoStd.
5.6
2,000
110
3,500
0.00056
9
0.013
200

3A
(mg/kg)
3.3
29.1
116
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

3B
(mg/kg)
2.0
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

Page3of7

3C
(mg/kg)
3.3
ND
98.7
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

3D
(mg/kg)
1.7
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

4A
(mg/kg)
3.4
ND
117
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

4B
(mg/kg)
4.8
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

4C
(mg/kg)
1.1
ND
87.2
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

Table1
SoilSampleAnalyticalResults
AT&THallRidge
OregonEmergencyResponseSystemReportNo.20160374
WillametteNationalForest
Detroit,Oregon
SoilSampleAnalyticalResults

RBCsw
Contaminant
Acenaphthene
Acenaphthylene
Anthracene
Benz(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(g,h,i)perylene
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
Fluoranthene
Fluorene
Indeno(1,2,3cd)pyrene
1Methylnaphthalene
2Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene

RBCss

(mg/kg) (mg/kg)

21,000
NoStd. NoStd.

110,000
2.3
24
1.9
2.4

24

240
NoStd. NoStd.

2,400

2.4
NoStd. NoStd.

10,000

14,000

24
NoStd. NoStd.
NoStd. NoStd.
0.37
580
NoStd. NoStd.

7,500

3A
(mg/kg)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

3B
(mg/kg)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

Page4of7

3C
(mg/kg)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

3D
(mg/kg)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

4A
(mg/kg)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

4B
(mg/kg)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

4C
(mg/kg)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

Table1
SoilSampleAnalyticalResults
AT&THallRidge
OregonEmergencyResponseSystemReportNo.20160374
WillametteNationalForest
Detroit,Oregon
SoilSampleAnalyticalResults

RBCsw
Contaminant
PIDReading(ppm)
NWTPHDx:Diesel
NWTPHDx:Oil
Benzene
Toluene
Ethylbenzene
Xylenes
Naphthalene
MTBE
Isopropylbenzene
nPropylbenzene
1,2,4Trimethylbenzene
1,3,5Trimethylbenzene
1,2Dibromoethane(EDB)
1,2Dichloroethane(EDC)

RBCss

(mg/kg) (mg/kg)

9,500
4,600
>Max
11,000
0.10
300
310
28,000
0.94
1,700
49
20,000
0.37
580
0.50
12,000
280
27,000
NoStd. NoStd.
5.6
2,000
110
3,500
0.00056
9
0.013
200

4D
(mg/kg)
1.2
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

0A
(mg/kg)
0.9
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

Page5of7

0B
(mg/kg)
10.5
1,090
ND
ND
0.224
0.200
1.04
ND
ND
ND
0.162
0.755
0.264
ND
ND

0C
(mg/kg)
36.8
9,430
ND
0.161
2.93
3.70
20.6
2.15
ND
1.03
3.82
19.9
6.59
ND
ND

ExSidewall
S
(mg/kg)
5.0
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

ExSidewall
W
(mg/kg)
1.8
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

ExSidewall
E
(mg/kg)
6.0
184
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

Table1
SoilSampleAnalyticalResults
AT&THallRidge
OregonEmergencyResponseSystemReportNo.20160374
WillametteNationalForest
Detroit,Oregon
SoilSampleAnalyticalResults

RBCsw
Contaminant
Acenaphthene
Acenaphthylene
Anthracene
Benz(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(g,h,i)perylene
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
Fluoranthene
Fluorene
Indeno(1,2,3cd)pyrene
1Methylnaphthalene
2Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene

RBCss

(mg/kg) (mg/kg)

21,000
NoStd. NoStd.

110,000
2.3
24
1.9
2.4

24

240
NoStd. NoStd.

2,400

2.4
NoStd. NoStd.

10,000

14,000

24
NoStd. NoStd.
NoStd. NoStd.
0.37
580
NoStd. NoStd.

7,500

4D
(mg/kg)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

0A
(mg/kg)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

Page6of7

0B
(mg/kg)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.0620
ND
ND
ND
0.114
0.155
ND
0.0489
0.0411

0C
(mg/kg)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.376
ND
0.454
ND
3.29
5.58
2.08
0.740
0.389

ExSidewall
S
(mg/kg)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

ExSidewall
W
(mg/kg)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

ExSidewall
E
(mg/kg)
ND
0.0181
0.0526
0.635
0.219
0.603
0.206
0.0799
0.947
0.0306
ND
1.86
ND
0.116
ND
0.0135
ND
0.0119
1.60

Table1
SoilSampleAnalyticalResults
AT&THallRidge
OregonEmergencyResponseSystemReportNo.20160374
WillametteNationalForest
Detroit,Oregon

Notes:
1

RiskBasedConcentrationsForIndividualChemicals(StateofOregonDepartmentofEnvironmentalQuality),SoilsLeachingtoGroundwater(RBCsw),UrbanResidential
datedNovember1,2015.
2
RiskBasedConcentrationsForIndividualChemicals(StateofOregonDepartmentofEnvironmentalQuality),SoilsLeachingtoSoilIngestion,DermalContact,and
Inhalation(RBCss),ConstructionWorkerdatedNovember1,2015.
Bold=SoilSampleanalyticalresultsexceededapplicablestandard.
AnalyticalResultswerecomparedtotheOregonstandardsfortheSoilsLeachingtoGroundwater(RCBsw)UrbanResidentialandtheSoilLeachingtoSoilIngestion,
DermalContactandInhulation(RCBss)ConstructionWorker.Thelowereofthetwovalueswasselectedforcomparisontotheanalyticresultsforsoils.
mg/kg=milligramsperkilogram.
>Max=TheconstituentRBCforthispathwayiscalculatedasgreaterthan1,000,000mg/kgor1,000,000mg/L.Therefore,thissubstanceisdeemednottoposerisksin
thisscenario.
MTBE=Methyltertbutylether
NoStd.=NostandardlistedinRiskBasedConcentrationsforIndividualChemicalsStateofOregonDepartmentofEnvironmentalQualitydatedNovember1,2015.
PID=Photoionizationdetectorreadingsarereportedinpartspermillion(ppm).
SoilsampleswerecollectedonFebruary26,2016.
ND=Concentrationnotdetectedatthelaboratorymethoddetectionlimit.
NA=NotAnalyzed
=AllRBCvaluesforindirectpathwaysthatexceedalimit(Csat,S,orPv)areremovedfromtheRiskBasedConcentrationsForIndividualChemicalsTable.

Page7of7

Table2
WaterSampleAnalyticalResults
AT&THallRidge
OregonEmergencyResponseSystemReportNo.20160374
WillametteNationalForest
Detroit,Oregon
SW01
UnnamedTributary
Contaminant
NWTPHDx:Diesel
NWTPHDx:Oil
Benzene
Toluene
Ethylbenzene
Xylenes
Naphthalene
MTBE
Isopropylbenzene
nPropylbenzene
1,2,4Trimethylbenzene
1,3,5Trimethylbenzene
1,2Dibromoethane(EDB)
1,2Dichloroethane(EDC)

WaterSampleAnalyticalResults
1

RBCtw

(g/L)
100
300
2.0
4,400
6.7
710
0.78
64
1,800
NoStd.
54
500
0.034
0.78

SW01
02/19/16
(g/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

SW01
02/21/16
(g/L)
NA
NA
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

SW01
02/28/16
(g/L)
NA
NA
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

Page1of11

SW01

SW01

SW01

SW01

(g/L)

(g/L)

(g/L)

(g/L)

Table2
WaterSampleAnalyticalResults
AT&THallRidge
OregonEmergencyResponseSystemReportNo.20160374
WillametteNationalForest
Detroit,Oregon
SW01
UnnamedTributary
Contaminant
Acenaphthene
Acenaphthylene
Anthracene
Benz(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(g,h,i)perylene
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
Fluoranthene
Fluorene
Indeno(1,2,3cd)pyrene
1Methylnaphthalene
2Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene

WaterSampleAnalyticalResults

RBCtw
(g/L)
2,400
NoStd.

0.043
0.011
0.11

NoStd.

0.011
NoStd.

1,400
0.11
NoStd.
NoStd.
0.78
NoStd.

SW01
02/19/16
(g/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

SW01
02/21/16
(g/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

SW01
02/28/16
(g/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

Page2of11

SW01

SW01

SW01

SW01

(g/L)

(g/L)

(g/L)

(g/L)

Table2
WaterSampleAnalyticalResults
AT&THallRidge
OregonEmergencyResponseSystemReportNo.20160374
WillametteNationalForest
Detroit,Oregon
SW02
UnnamedTributary
Contaminant
NWTPHDx:Diesel
NWTPHDx:Oil
Benzene
Toluene
Ethylbenzene
Xylenes
Naphthalene
MTBE
Isopropylbenzene
nPropylbenzene
1,2,4Trimethylbenzene
1,3,5Trimethylbenzene
1,2Dibromoethane(EDB)
1,2Dichloroethane(EDC)

WaterSampleAnalyticalResults

RBCtw
(g/L)
100
300
2.0
4,400
6.7
710
0.78
64
1,800
NoStd.
54
500
0.034
0.78

SW02
02/19/16
(g/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

SW02
02/21/16
(g/L)
NA
NA
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

SW02
02/28/16
(g/L)
NA
NA
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

Page3of11

SW02

SW02

SW02

SW02

(g/L)

(g/L)

(g/L)

(g/L)

Table2
WaterSampleAnalyticalResults
AT&THallRidge
OregonEmergencyResponseSystemReportNo.20160374
WillametteNationalForest
Detroit,Oregon
SW02
UnnamedTributary
Contaminant
Acenaphthene
Acenaphthylene
Anthracene
Benz(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(g,h,i)perylene
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
Fluoranthene
Fluorene
Indeno(1,2,3cd)pyrene
1Methylnaphthalene
2Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene

WaterSampleAnalyticalResults

RBCtw
(g/L)
2,400
NoStd.

0.043
0.011
0.11

NoStd.

0.011
NoStd.

1,400
0.11
NoStd.
NoStd.
0.78
NoStd.

SW02
02/19/16
(g/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

SW02
02/21/16
(g/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

SW02
02/28/16
(g/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

Page4of11

SW02

SW02

SW02

SW02

(g/L)

(g/L)

(g/L)

(g/L)

Table2
WaterSampleAnalyticalResults
AT&THallRidge
OregonEmergencyResponseSystemReportNo.20160374
WillametteNationalForest
Detroit,Oregon
SW03
UnnamedTributary
Contaminant
NWTPHDx:Diesel
NWTPHDx:Oil
Benzene
Toluene
Ethylbenzene
Xylenes
Naphthalene
MTBE
Isopropylbenzene
nPropylbenzene
1,2,4Trimethylbenzene
1,3,5Trimethylbenzene
1,2Dibromoethane(EDB)
1,2Dichloroethane(EDC)

WaterSampleAnalyticalResults

RBCtw
(g/L)
100
300
2.0
4,400
6.7
710
0.78
64
1,800
NoStd.
54
500
0.034
0.78

SW03
02/19/16
(g/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

SW03
02/21/16
(g/L)
NA
NA
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

SW03
02/28/16
(g/L)
NA
NA
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

Page5of11

SW03

SW03

SW03

SW03

(g/L)

(g/L)

(g/L)

(g/L)

Table2
WaterSampleAnalyticalResults
AT&THallRidge
OregonEmergencyResponseSystemReportNo.20160374
WillametteNationalForest
Detroit,Oregon
SW03
UnnamedTributary
Contaminant
Acenaphthene
Acenaphthylene
Anthracene
Benz(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(g,h,i)perylene
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
Fluoranthene
Fluorene
Indeno(1,2,3cd)pyrene
1Methylnaphthalene
2Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene

WaterSampleAnalyticalResults

RBCtw
(g/L)
2,400
NoStd.

0.043
0.011
0.11

NoStd.

0.011
NoStd.

1,400
0.11
NoStd.
NoStd.
0.78
NoStd.

SW03
02/19/16
(g/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

SW03
02/21/16
(g/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

SW03
02/28/16
(g/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

Page6of11

SW03

SW03

SW03

SW03

(g/L)

(g/L)

(g/L)

(g/L)

Table2
WaterSampleAnalyticalResults
AT&THallRidge
OregonEmergencyResponseSystemReportNo.20160374
WillametteNationalForest
Detroit,Oregon
SW04
UnnamedTributary
Contaminant
NWTPHDx:Diesel
NWTPHDx:Oil
Benzene
Toluene
Ethylbenzene
Xylenes
Naphthalene
MTBE
Isopropylbenzene
nPropylbenzene
1,2,4Trimethylbenzene
1,3,5Trimethylbenzene
1,2Dibromoethane(EDB)
1,2Dichloroethane(EDC)

WaterSampleAnalyticalResults

RBCtw
(g/L)
100
300
2.0
4,400
6.7
710
0.78
64
1,800
NoStd.
54
500
0.034
0.78

SW04
02/19/16
(g/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

SW04
02/21/16
(g/L)
NA
NA
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

SW04
02/28/16
(g/L)
NA
NA
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

Page7of11

SW04

SW04

SW04

SW04

(g/L)

(g/L)

(g/L)

(g/L)

Table2
WaterSampleAnalyticalResults
AT&THallRidge
OregonEmergencyResponseSystemReportNo.20160374
WillametteNationalForest
Detroit,Oregon
SW04
UnnamedTributary
Contaminant
Acenaphthene
Acenaphthylene
Anthracene
Benz(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(g,h,i)perylene
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
Fluoranthene
Fluorene
Indeno(1,2,3cd)pyrene
1Methylnaphthalene
2Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene

WaterSampleAnalyticalResults

RBCtw
(g/L)
2,400
NoStd.

0.043
0.011
0.11

NoStd.

0.011
NoStd.

1,400
0.11
NoStd.
NoStd.
0.78
NoStd.

SW04
02/19/16
(g/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

SW04
02/21/16
(g/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

SW04
02/28/16
(g/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

Page8of11

SW04

SW04

SW04

SW04

(g/L)

(g/L)

(g/L)

(g/L)

Table2
WaterSampleAnalyticalResults
AT&THallRidge
OregonEmergencyResponseSystemReportNo.20160374
WillametteNationalForest
Detroit,Oregon
SW05
UnnamedTributary
Contaminant
Benzene
Toluene
Ethylbenzene
Xylenes
Naphthalene
MTBE
Isopropylbenzene
nPropylbenzene
1,2,4Trimethylbenzene
1,3,5Trimethylbenzene
1,2Dibromoethane(EDB)
1,2Dichloroethane(EDC)

WaterSampleAnalyticalResults

RBCtw
(g/L)
2.0
4,400
6.7
710
0.78
64
1,800
NoStd.
54
500
0.034
0.78

SW05
02/25/16
(g/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

SW05
02/28/16
(g/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

SW05

SW05

SW05

SW05

SW05

(g/L)

(g/L)

(g/L)

(g/L)

(g/L)

Page9of11

Table2
WaterSampleAnalyticalResults
AT&THallRidge
OregonEmergencyResponseSystemReportNo.20160374
WillametteNationalForest
Detroit,Oregon
SW05
UnnamedTributary
Contaminant
Acenaphthene
Acenaphthylene
Anthracene
Benz(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(g,h,i)perylene
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
Fluoranthene
Fluorene
Indeno(1,2,3cd)pyrene
1Methylnaphthalene
2Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene

WaterSampleAnalyticalResults

RBCtw
(g/L)
2,400
NoStd.

0.043
0.011
0.11

NoStd.

0.011
NoStd.

1,400
0.11
NoStd.
NoStd.
0.78
NoStd.

SW05
02/25/16
(g/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

SW05
02/28/16
(g/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

SW05

SW05

SW05

SW05

SW05

(g/L)

(g/L)

(g/L)

(g/L)

(g/L)

Page10of11

Table2
WaterSampleAnalyticalResults
AT&THallRidge
OregonEmergencyResponseSystemReportNo.20160374
WillametteNationalForest
Detroit,Oregon

Notes:
1

RiskBasedConcentrationsForIndividualChemicals(StateofOregonDepartmentofEnvironmentalQuality),GroundwaterIngestion&InhalationfromTapwater
(RBCtw),UrbanResidentialdatedNovember1,2015.
(g/L)=microgramsperliter.
MTBE=Methyltertbutylether
NoStd.=NoStandardListed
ND=Concentrationnotdetectedatthelaboratoryreportinglimit.
NA=NotAnalyzed
=AllRBCvaluesforindirectpathwaysthatexceedalimit(Csat,S,orPv)areremovedfromtheRiskBasedConcentrationsForIndividualChemicalsTable.

Page11of11

Figures

AppendixA
DraftLaboratoryAnalyticalResults

Apex Labs

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Sunday, February 28, 2016


Ron Malec
NRC-CB&I
6211 N Ensign St
Portland, OR 97217

RE: AT&T Hall Ridge / 156319


Enclosed are the results of analyses for work order A6B0900, which was received by the laboratory on
2/27/2016 at 9:15:00AM.
Thank you for using Apex Labs. We appreciate your business and strive to provide the highest quality
services to the environmental industry.
If you have any questions concerning this report or the services we offer , please feel free to contact me by
email at: dthomas@apex-labs.com, or by phone at 503-718-2323.

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 1 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL REPORT FOR SAMPLES


SAMPLE INFORMATION
Sample ID

Laboratory ID

Matrix

1A

A6B0900-01
A6B0900-02
A6B0900-03
A6B0900-04
A6B0900-05
A6B0900-06
A6B0900-07
A6B0900-08
A6B0900-09
A6B0900-10
A6B0900-11
A6B0900-12
A6B0900-13
A6B0900-14
A6B0900-15
A6B0900-16
A6B0900-17
A6B0900-18
A6B0900-19
A6B0900-20
A6B0900-21

Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil

1B
1C
2A
2B
2C
2D
3A
3B
3C
3D
4A
4B
4C
4D
0A
0B
0C
Ex Sidewall S
Ex Sidewall W
Ex Sidewall E

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Date Sampled

Date Received

02/26/16 09:40
02/26/16 09:50
02/26/16 10:00
02/26/16 10:55
02/26/16 11:00
02/26/16 10:10
02/26/16 10:05
02/26/16 10:40
02/26/16 10:45
02/26/16 10:50
02/26/16 10:15
02/26/16 10:35
02/26/16 10:30
02/26/16 10:25
02/26/16 10:20
02/26/16 12:00
02/26/16 12:05
02/26/16 12:10
02/26/16 12:20
02/26/16 12:30
02/26/16 12:40

02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15
02/27/16 09:15

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 2 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


Diesel and/or Oil Hydrocarbons by NWTPH-Dx
Analyte

Result

MDL

1A (A6B0900-01)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Diesel

ND

---

28.6

mg/kg dry

02/27/16 13:53

NWTPH-Dx

Oil

123

---

57.2

"

"

"

"

"

"

"

Surrogate: o-Terphenyl (Surr)

Recovery: 88 %

1B (A6B0900-02)

Notes

Batch: 6020836

Limits: 50-150 %

Matrix: Soil

F-17

Batch: 6020836

Diesel

44.6

---

32.2

mg/kg dry

02/27/16 14:33

NWTPH-Dx

F-17

Oil

159

---

64.3

"

"

"

"

F-17

"

"

"

Surrogate: o-Terphenyl (Surr)

Recovery: 90 %

1C (A6B0900-03)

Diesel

Oil

Limits: 50-150 %

Matrix: Soil

Batch: 6020835

66400

---

2040

mg/kg dry

50

02/27/16 13:53

NWTPH-Dx

ND

---

4080

"

"

"

"

"

"

"

Surrogate: o-Terphenyl (Surr)

Recovery: %

2A (A6B0900-04)

Limits: 50-150 %

Matrix: Soil

Batch: 6020836

Diesel

ND

---

26.1

mg/kg dry

02/27/16 15:12

NWTPH-Dx

Oil

ND

---

52.2

"

"

"

"

"

"

"

Surrogate: o-Terphenyl (Surr)

Recovery: 90 %

2B (A6B0900-05)

S-01

Limits: 50-150 %

Matrix: Soil

Batch: 6020836

Diesel

70.2

---

35.9

mg/kg dry

02/27/16 15:32

NWTPH-Dx

F-17

Oil

312

---

71.8

"

"

"

"

F-17

"

"

"

Surrogate: o-Terphenyl (Surr)

Recovery: 83 %

2C (A6B0900-06)

Diesel

Oil

Limits: 50-150 %

Matrix: Soil

Batch: 6020835

96800

---

2490

mg/kg dry

50

02/27/16 14:33

NWTPH-Dx

ND

---

4970

"

"

"

"

"

"

"

Surrogate: o-Terphenyl (Surr)

Recovery: %

2D (A6B0900-07)

Limits: 50-150 %

Matrix: Soil

Batch: 6020836

Diesel

ND

---

180

mg/kg dry

02/27/16 16:12

NWTPH-Dx

Oil

606

---

360

"

"

"

"

"

"

"

Surrogate: o-Terphenyl (Surr)

Recovery: 84 %

3A (A6B0900-08)

S-01

Limits: 50-150 %

Matrix: Soil

F-17

Batch: 6020836

Diesel

29.1

---

27.2

mg/kg dry

02/27/16 16:32

NWTPH-Dx

F-17

Oil

116

---

54.4

"

"

"

"

F-17

"

"

"

Surrogate: o-Terphenyl (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Recovery: 90 %

Limits: 50-150 %

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 3 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


Diesel and/or Oil Hydrocarbons by NWTPH-Dx
Analyte

Result

MDL

3B (A6B0900-09)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Diesel

ND

---

25.7

mg/kg dry

02/27/16 17:12

NWTPH-Dx

Oil

ND

---

51.5

"

"

"

"

"

"

"

Surrogate: o-Terphenyl (Surr)

Recovery: 92 %

3C (A6B0900-10)

Limits: 50-150 %

Matrix: Soil

Batch: 6020836

Diesel

ND

---

27.0

mg/kg dry

02/27/16 17:31

NWTPH-Dx

Oil

98.7

---

54.0

"

"

"

"

"

"

"

Surrogate: o-Terphenyl (Surr)

Recovery: 90 %

3D (A6B0900-11)

Limits: 50-150 %

Matrix: Soil

ND

---

27.6

mg/kg dry

02/27/16 17:12

NWTPH-Dx

Oil

ND

---

55.3

"

"

"

"

"

"

"

Recovery: 90 %

4A (A6B0900-12)

Limits: 50-150 %

Matrix: Soil

Batch: 6020836

Diesel

ND

---

29.8

mg/kg dry

02/27/16 17:31

NWTPH-Dx

Oil

117

---

59.6

"

"

"

"

"

"

"

Surrogate: o-Terphenyl (Surr)

Recovery: 91 %

4B (A6B0900-13)

Limits: 50-150 %

Matrix: Soil

ND

---

25.0

mg/kg dry

02/27/16 14:52

NWTPH-Dx

Oil

ND

---

50.0

"

"

"

"

"

"

"

Recovery: 94 %

4C (A6B0900-14RE1)

Diesel
Oil

Limits: 50-150 %

Matrix: Soil

Batch: 6020836

ND

---

28.9

mg/kg dry

02/27/16 15:12

NWTPH-Dx

87.2

---

57.7

"

"

"

"

"

"

"

Surrogate: o-Terphenyl (Surr)

Recovery: 95 %

4D (A6B0900-15)

Limits: 50-150 %

Matrix: Soil

ND

---

25.0

mg/kg dry

02/27/16 15:32

NWTPH-Dx

Oil

ND

---

50.0

"

"

"

"

"

"

"

Recovery: 94 %

0A (A6B0900-16)

Limits: 50-150 %

Matrix: Soil

Batch: 6020836

Diesel

ND

---

34.5

mg/kg dry

02/27/16 12:29

NWTPH-Dx

Oil

ND

---

69.1

"

"

"

"

"

"

"

Surrogate: o-Terphenyl (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Recovery: 90 %

F-17

Batch: 6020836

Diesel

Surrogate: o-Terphenyl (Surr)

F-17

Batch: 6020836

Diesel

Surrogate: o-Terphenyl (Surr)

F-17

Batch: 6020836

Diesel

Surrogate: o-Terphenyl (Surr)

Notes

Batch: 6020836

Limits: 50-150 %

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 4 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


Diesel and/or Oil Hydrocarbons by NWTPH-Dx
Analyte

Result

MDL

0B (A6B0900-17)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Diesel

1090

---

33.4

mg/kg dry

02/27/16 15:52

NWTPH-Dx

Oil

ND

---

66.8

"

"

"

"

"

"

"

Surrogate: o-Terphenyl (Surr)

Recovery: 99 %

0C (A6B0900-18)

Limits: 50-150 %

Matrix: Soil

Batch: 6020836

Diesel

9430

---

186

mg/kg dry

02/27/16 16:32

NWTPH-Dx

Oil

ND

---

372

"

"

"

"

"

"

"

Surrogate: o-Terphenyl (Surr)

Recovery: 137 %

Ex Sidewall S (A6B0900-19)

Limits: 50-150 %

Matrix: Soil

ND

---

25.0

mg/kg dry

02/27/16 12:49

NWTPH-Dx

Oil

ND

---

50.0

"

"

"

"

"

"

"

Recovery: 95 %

Ex Sidewall W (A6B0900-20)

Limits: 50-150 %

Matrix: Soil

Batch: 6020836

Diesel

ND

---

26.7

mg/kg dry

02/27/16 12:49

NWTPH-Dx

Oil

ND

---

53.5

"

"

"

"

"

"

"

Surrogate: o-Terphenyl (Surr)

Recovery: 95 %

Ex Sidewall E (A6B0900-21)

Limits: 50-150 %

Matrix: Soil

Batch: 6020836

Diesel

184

---

25.0

mg/kg dry

02/27/16 16:52

NWTPH-Dx

Oil

ND

---

50.0

"

"

"

"

"

"

"

Surrogate: o-Terphenyl (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Recovery: 94 %

S-05

Batch: 6020836

Diesel

Surrogate: o-Terphenyl (Surr)

Notes

Batch: 6020836

Limits: 50-150 %

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 5 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Result

Analyte

MDL

1A (A6B0900-01)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Benzene

ND

---

0.0217

mg/kg dry

50

02/27/16 13:54

5035/8260B

Toluene

ND

---

0.108

"

"

"

"

Ethylbenzene

ND

---

0.0542

"

"

"

"

Xylenes, total

ND

---

0.163

"

"

"

"

Naphthalene

ND

---

0.217

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

0.108

"

"

"

"

Isopropylbenzene

ND

---

0.108

"

"

"

"

n-Propylbenzene

ND

---

0.0542

"

"

"

"

1,2,4-Trimethylbenzene

ND

---

0.108

"

"

"

"

1,3,5-Trimethylbenzene

ND

---

0.108

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.0542

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.0542

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 106 %

Limits: 70-130 %

"

"

1,4-Difluorobenzene (Surr)

103 %

Limits: 70-130 %

"

"

"

Toluene-d8 (Surr)

100 %

Limits: 70-130 %

"

"

"

97 %

Limits: 70-130 %

"

"

"

4-Bromofluorobenzene (Surr)

1B (A6B0900-02)

Matrix: Soil

Batch: 6020833

Benzene

ND

---

0.0272

mg/kg dry

50

02/27/16 14:51

5035/8260B

Toluene

ND

---

0.136

"

"

"

"

Ethylbenzene

ND

---

0.0680

"

"

"

"

Xylenes, total

ND

---

0.204

"

"

"

"

Naphthalene

ND

---

0.272

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

0.136

"

"

"

"

Isopropylbenzene

ND

---

0.136

"

"

"

"

n-Propylbenzene

ND

---

0.0680

"

"

"

"

1,2,4-Trimethylbenzene

ND

---

0.136

"

"

"

"

1,3,5-Trimethylbenzene

ND

---

0.136

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.0680

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.0680

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 104 %

Limits: 70-130 %

"

"

1,4-Difluorobenzene (Surr)

102 %

Limits: 70-130 %

"

"

"

Toluene-d8 (Surr)

100 %

Limits: 70-130 %

"

"

"

98 %

Limits: 70-130 %

"

"

"

02/27/16 15:20

5035/8260B

4-Bromofluorobenzene (Surr)

2A (A6B0900-04)

Benzene

Matrix: Soil

ND

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

---

0.0162

Notes

Batch: 6020833

Batch: 6020833

mg/kg dry

50

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 6 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Result

Analyte

MDL

2A (A6B0900-04)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Toluene

ND

---

0.0812

mg/kg dry

50

"

5035/8260B

Ethylbenzene

ND

---

0.0406

"

"

"

"

Xylenes, total

ND

---

0.122

"

"

"

"

Naphthalene

ND

---

0.162

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

0.0812

"

"

"

"

Isopropylbenzene

ND

---

0.0812

"

"

"

"

n-Propylbenzene

ND

---

0.0406

"

"

"

"

1,2,4-Trimethylbenzene

ND

---

0.0812

"

"

"

"

1,3,5-Trimethylbenzene

ND

---

0.0812

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.0406

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.0406

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 109 %

Limits: 70-130 %

"

"

104 %

Limits: 70-130 %

"

"

"

Toluene-d8 (Surr)

99 %

Limits: 70-130 %

"

"

"

4-Bromofluorobenzene (Surr)

96 %

Limits: 70-130 %

"

"

"

1,4-Difluorobenzene (Surr)

2B (A6B0900-05)

Matrix: Soil

Batch: 6020833

Benzene

ND

---

0.0353

mg/kg dry

50

02/27/16 15:48

5035/8260B

Toluene

ND

---

0.177

"

"

"

"

Ethylbenzene

ND

---

0.0883

"

"

"

"

Xylenes, total

ND

---

0.265

"

"

"

"

Naphthalene

ND

---

0.353

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

0.177

"

"

"

"

Isopropylbenzene

ND

---

0.177

"

"

"

"

n-Propylbenzene

ND

---

0.0883

"

"

"

"

1,2,4-Trimethylbenzene

ND

---

0.177

"

"

"

"

1,3,5-Trimethylbenzene

ND

---

0.177

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.0883

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.0883

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 105 %

Limits: 70-130 %

"

"

102 %

Limits: 70-130 %

"

"

"

Toluene-d8 (Surr)

99 %

Limits: 70-130 %

"

"

"

4-Bromofluorobenzene (Surr)

95 %

Limits: 70-130 %

"

"

"

1,4-Difluorobenzene (Surr)

2D (A6B0900-07)

Matrix: Soil

Batch: 6020833

Benzene

0.0449

---

0.0391

mg/kg dry

50

02/27/16 16:16

5035/8260B

Toluene

0.887

---

0.195

"

"

"

"

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020833

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 7 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Result

Analyte

MDL

2D (A6B0900-07)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Ethylbenzene

0.832

---

0.0976

mg/kg dry

50

"

Xylenes, total

4.74

---

0.293

"

"

"

"

Naphthalene

ND

---

0.391

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

0.195

"

"

"

"

Isopropylbenzene

ND

---

0.195

"

"

"

"

n-Propylbenzene

0.642

---

0.0976

"

"

"

"

1,2,4-Trimethylbenzene

3.53

---

0.195

"

"

"

"

5035/8260B

1,3,5-Trimethylbenzene

1.04

---

0.195

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.0976

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.0976

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 108 %

Limits: 70-130 %

"

"

103 %

Limits: 70-130 %

"

"

"

Toluene-d8 (Surr)

93 %

Limits: 70-130 %

"

"

"

4-Bromofluorobenzene (Surr)

96 %

Limits: 70-130 %

"

"

"

1,4-Difluorobenzene (Surr)

3A (A6B0900-08)

Matrix: Soil

Batch: 6020833

Benzene

ND

---

0.0216

mg/kg dry

50

02/27/16 16:45

5035/8260B

Toluene

ND

---

0.108

"

"

"

"

Ethylbenzene

ND

---

0.0539

"

"

"

"

Xylenes, total

ND

---

0.162

"

"

"

"

Naphthalene

ND

---

0.216

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

0.108

"

"

"

"

Isopropylbenzene

ND

---

0.108

"

"

"

"

n-Propylbenzene

ND

---

0.0539

"

"

"

"

1,2,4-Trimethylbenzene

ND

---

0.108

"

"

"

"

1,3,5-Trimethylbenzene

ND

---

0.108

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.0539

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.0539

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 105 %

Limits: 70-130 %

"

"

1,4-Difluorobenzene (Surr)

102 %

Limits: 70-130 %

"

"

"

Toluene-d8 (Surr)

100 %

Limits: 70-130 %

"

"

"

97 %

Limits: 70-130 %

"

"

"

4-Bromofluorobenzene (Surr)

3B (A6B0900-09)

Matrix: Soil

Batch: 6020833

Benzene

ND

---

0.0160

mg/kg dry

50

02/27/16 17:13

5035/8260B

Toluene

ND

---

0.0801

"

"

"

"

Ethylbenzene

ND

---

0.0400

"

"

"

"

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020833

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 8 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Result

Analyte

MDL

3B (A6B0900-09)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Xylenes, total

ND

---

0.120

mg/kg dry

50

"

5035/8260B

Naphthalene

ND

---

0.160

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

0.0801

"

"

"

"

Isopropylbenzene

ND

---

0.0801

"

"

"

"

n-Propylbenzene

ND

---

0.0400

"

"

"

"

1,2,4-Trimethylbenzene

ND

---

0.0801

"

"

"

"

1,3,5-Trimethylbenzene

ND

---

0.0801

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.0400

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

"

"

"

Recovery: 108 %

Limits: 70-130 %

"

"

1,4-Difluorobenzene (Surr)

103 %

Limits: 70-130 %

"

"

"

Toluene-d8 (Surr)

100 %

Limits: 70-130 %

"

"

"

93 %

Limits: 70-130 %

"

"

"

Surrogate: Dibromofluoromethane (Surr)

4-Bromofluorobenzene (Surr)

3C (A6B0900-10)

0.0400

"

Matrix: Soil

Batch: 6020833

Benzene

ND

---

0.0156

mg/kg dry

50

02/27/16 17:41

5035/8260B

Toluene

ND

---

0.0782

"

"

"

"

Ethylbenzene

ND

---

0.0391

"

"

"

"

Xylenes, total

ND

---

0.117

"

"

"

"

Naphthalene

ND

---

0.156

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

0.0782

"

"

"

"

Isopropylbenzene

ND

---

0.0782

"

"

"

"

n-Propylbenzene

ND

---

0.0391

"

"

"

"

1,2,4-Trimethylbenzene

ND

---

0.0782

"

"

"

"

1,3,5-Trimethylbenzene

ND

---

0.0782

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.0391

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.0391

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 106 %

Limits: 70-130 %

"

"

1,4-Difluorobenzene (Surr)

103 %

Limits: 70-130 %

"

"

"

Toluene-d8 (Surr)

101 %

Limits: 70-130 %

"

"

"

93 %

Limits: 70-130 %

"

"

"

4-Bromofluorobenzene (Surr)

3D (A6B0900-11)

Matrix: Soil

Batch: 6020833

Benzene

ND

---

0.0199

mg/kg dry

50

02/27/16 18:10

5035/8260B

Toluene

ND

---

0.0994

"

"

"

"

Ethylbenzene

ND

---

0.0497

"

"

"

"

Xylenes, total

ND

---

0.149

"

"

"

"

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020833

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 9 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Result

Analyte

MDL

3D (A6B0900-11)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Naphthalene

ND

---

0.199

mg/kg dry

50

"

5035/8260B

Methyl tert-butyl ether (MTBE)

ND

---

0.0994

"

"

"

"

Isopropylbenzene

ND

---

0.0994

"

"

"

"

n-Propylbenzene

ND

---

0.0497

"

"

"

"

1,2,4-Trimethylbenzene

ND

---

0.0994

"

"

"

"

1,3,5-Trimethylbenzene

ND

---

0.0994

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.0497

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.0497

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 104 %

Limits: 70-130 %

"

"

102 %

Limits: 70-130 %

"

"

"

Toluene-d8 (Surr)

99 %

Limits: 70-130 %

"

"

"

4-Bromofluorobenzene (Surr)

95 %

Limits: 70-130 %

"

"

"

1,4-Difluorobenzene (Surr)

4A (A6B0900-12)

Matrix: Soil

Benzene

ND

---

Toluene

ND

Ethylbenzene

ND

Xylenes, total

Batch: 6020833

0.0205

mg/kg dry

50

02/27/16 18:38

5035/8260B

---

0.103

"

"

"

"

---

0.0513

"

"

"

"

ND

---

0.154

"

"

"

"

Naphthalene

ND

---

0.205

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

0.103

"

"

"

"

Isopropylbenzene

ND

---

0.103

"

"

"

"

n-Propylbenzene

ND

---

0.0513

"

"

"

"

1,2,4-Trimethylbenzene

ND

---

0.103

"

"

"

"

1,3,5-Trimethylbenzene

ND

---

0.103

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.0513

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.0513

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 105 %

Limits: 70-130 %

"

"

1,4-Difluorobenzene (Surr)

102 %

Limits: 70-130 %

"

"

"

Toluene-d8 (Surr)

101 %

Limits: 70-130 %

"

"

"

96 %

Limits: 70-130 %

"

"

"

4-Bromofluorobenzene (Surr)

4B (A6B0900-13)

Matrix: Soil

Batch: 6020833

Benzene

ND

---

0.0162

mg/kg dry

50

02/27/16 19:07

5035/8260B

Toluene

ND

---

0.0809

"

"

"

"

Ethylbenzene

ND

---

0.0404

"

"

"

"

Xylenes, total

ND

---

0.121

"

"

"

"

Naphthalene

ND

---

0.162

"

"

"

"

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020833

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 10 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Result

Analyte

MDL

4B (A6B0900-13)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Methyl tert-butyl ether (MTBE)

ND

---

0.0809

mg/kg dry

50

"

5035/8260B

Isopropylbenzene

ND

---

0.0809

"

"

"

"

n-Propylbenzene

ND

---

0.0404

"

"

"

"

1,2,4-Trimethylbenzene

ND

---

0.0809

"

"

"

"

1,3,5-Trimethylbenzene

ND

---

0.0809

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.0404

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.0404

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 107 %

Limits: 70-130 %

"

"

1,4-Difluorobenzene (Surr)

102 %

Limits: 70-130 %

"

"

"

Toluene-d8 (Surr)

100 %

Limits: 70-130 %

"

"

"

98 %

Limits: 70-130 %

"

"

"

4-Bromofluorobenzene (Surr)

4C (A6B0900-14)

Matrix: Soil

Batch: 6020834

Benzene

ND

---

0.0140

mg/kg dry

50

02/27/16 14:15

5035/8260B

Toluene

ND

---

0.0702

"

"

"

"

Ethylbenzene

ND

---

0.0351

"

"

"

"

Xylenes, total

ND

---

0.105

"

"

"

"

Naphthalene

ND

---

0.140

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

0.0702

"

"

"

"

Isopropylbenzene

ND

---

0.0702

"

"

"

"

n-Propylbenzene

ND

---

0.0351

"

"

"

"

1,2,4-Trimethylbenzene

ND

---

0.0702

"

"

"

"

1,3,5-Trimethylbenzene

ND

---

0.0702

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.0351

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

"

"

"

Recovery: 97 %

Limits: 70-130 %

"

"

1,4-Difluorobenzene (Surr)

93 %

Limits: 70-130 %

"

"

"

Toluene-d8 (Surr)

97 %

Limits: 70-130 %

"

"

"

4-Bromofluorobenzene (Surr)

97 %

Limits: 70-130 %

"

"

"

Surrogate: Dibromofluoromethane (Surr)

4D (A6B0900-15)

0.0351

"

Matrix: Soil

Batch: 6020834

Benzene

ND

---

0.00983

mg/kg dry

50

02/27/16 14:41

5035/8260B

Toluene

ND

---

0.0491

"

"

"

"

Ethylbenzene

ND

---

0.0246

"

"

"

"

Xylenes, total

ND

---

0.0737

"

"

"

"

Naphthalene

ND

---

0.0983

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

0.0491

"

"

"

"

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020833

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 11 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Result

Analyte

MDL

4D (A6B0900-15)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Isopropylbenzene

ND

---

0.0491

mg/kg dry

50

"

5035/8260B

n-Propylbenzene

ND

---

0.0246

"

"

"

"

1,2,4-Trimethylbenzene

ND

---

0.0491

"

"

"

"

1,3,5-Trimethylbenzene

ND

---

0.0491

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.0246

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.0246

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 96 %

Limits: 70-130 %

"

"

1,4-Difluorobenzene (Surr)

92 %

Limits: 70-130 %

"

"

"

Toluene-d8 (Surr)

97 %

Limits: 70-130 %

"

"

"

4-Bromofluorobenzene (Surr)

97 %

Limits: 70-130 %

"

"

"

0A (A6B0900-16)

Matrix: Soil

Batch: 6020834

Benzene

ND

---

0.0324

mg/kg dry

50

02/27/16 15:08

5035/8260B

Toluene

ND

---

0.162

"

"

"

"

Ethylbenzene

ND

---

0.0810

"

"

"

"

Xylenes, total

ND

---

0.243

"

"

"

"

Naphthalene

ND

---

0.324

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

0.162

"

"

"

"

Isopropylbenzene

ND

---

0.162

"

"

"

"

n-Propylbenzene

ND

---

0.0810

"

"

"

"

1,2,4-Trimethylbenzene

ND

---

0.162

"

"

"

"

1,3,5-Trimethylbenzene

ND

---

0.162

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.0810

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.0810

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 97 %

Limits: 70-130 %

"

"

1,4-Difluorobenzene (Surr)

92 %

Limits: 70-130 %

"

"

"

Toluene-d8 (Surr)

96 %

Limits: 70-130 %

"

"

"

4-Bromofluorobenzene (Surr)

98 %

Limits: 70-130 %

"

"

"

02/27/16 15:35

5035/8260B

0B (A6B0900-17)

Benzene

Matrix: Soil

ND

---

0.0272

Batch: 6020834

mg/kg dry

50

Toluene

0.224

---

0.136

"

"

"

"

Ethylbenzene

0.200

---

0.0680

"

"

"

"

Xylenes, total

1.04

---

0.204

"

"

"

"

Naphthalene

ND

---

0.272

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

0.136

"

"

"

"

Isopropylbenzene

ND

---

0.136

"

"

"

"

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020834

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 12 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Result

Analyte

MDL

0B (A6B0900-17)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

n-Propylbenzene

0.162

---

0.0680

mg/kg dry

50

"

1,2,4-Trimethylbenzene

0.755

---

0.136

"

"

"

"

1,3,5-Trimethylbenzene

0.264

---

0.136

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.0680

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.0680

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

5035/8260B

Recovery: 94 %

Limits: 70-130 %

"

"

1,4-Difluorobenzene (Surr)

91 %

Limits: 70-130 %

"

"

"

Toluene-d8 (Surr)

96 %

Limits: 70-130 %

"

"

"

4-Bromofluorobenzene (Surr)

98 %

Limits: 70-130 %

"

"

"

5035/8260B

0C (A6B0900-18)

Matrix: Soil

Batch: 6020834

Benzene

0.161

---

0.0336

mg/kg dry

50

02/27/16 16:29

Toluene

2.93

---

0.168

"

"

"

"

Ethylbenzene

3.70

---

0.0840

"

"

"

"

Xylenes, total

20.6

---

0.252

"

"

"

"

Naphthalene

2.15

---

0.336

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

0.168

"

"

"

"

Isopropylbenzene

1.03

---

0.168

"

"

"

"

n-Propylbenzene

3.82

---

0.0840

"

"

"

"

1,2,4-Trimethylbenzene

19.9

---

0.168

"

"

"

"

1,3,5-Trimethylbenzene

6.59

---

0.168

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.0840

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.0840

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)


1,4-Difluorobenzene (Surr)
Toluene-d8 (Surr)
4-Bromofluorobenzene (Surr)

Ex Sidewall S (A6B0900-19)

Recovery: 97 %

Limits: 70-130 %

"

"

93 %

Limits: 70-130 %

"

"

"

101 %

Limits: 70-130 %

"

"

"

98 %

Limits: 70-130 %

"

"

"

Matrix: Soil

ND

---

0.00773

mg/kg dry

50

02/27/16 16:56

5035/8260B

Toluene

ND

---

0.0386

"

"

"

"

Ethylbenzene

ND

---

0.0193

"

"

"

"

Xylenes, total

ND

---

0.0580

"

"

"

"

Naphthalene

ND

---

0.0773

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

0.0386

"

"

"

"

Isopropylbenzene

ND

---

0.0386

"

"

"

"

n-Propylbenzene

ND

---

0.0193

"

"

"

"

DRAFT REPORT, DATA SUBJECT TO CHANGE

M-04

Batch: 6020834

Benzene

DRAFT REPORT

Notes

Batch: 6020834

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 13 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Result

Analyte

MDL

Ex Sidewall S (A6B0900-19)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

1,2,4-Trimethylbenzene

ND

---

0.0386

mg/kg dry

50

"

5035/8260B

1,3,5-Trimethylbenzene

ND

---

0.0386

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.0193

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.0193

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 94 %

Limits: 70-130 %

"

"

1,4-Difluorobenzene (Surr)

91 %

Limits: 70-130 %

"

"

"

Toluene-d8 (Surr)

96 %

Limits: 70-130 %

"

"

"

4-Bromofluorobenzene (Surr)

97 %

Limits: 70-130 %

"

"

"

Ex Sidewall W (A6B0900-20)

Matrix: Soil

Batch: 6020834

Benzene

ND

---

0.0119

mg/kg dry

50

02/27/16 17:22

5035/8260B

Toluene

ND

---

0.0594

"

"

"

"

Ethylbenzene

ND

---

0.0297

"

"

"

"

Xylenes, total

ND

---

0.0890

"

"

"

"

Naphthalene

ND

---

0.119

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

0.0594

"

"

"

"

Isopropylbenzene

ND

---

0.0594

"

"

"

"

n-Propylbenzene

ND

---

0.0297

"

"

"

"

1,2,4-Trimethylbenzene

ND

---

0.0594

"

"

"

"

1,3,5-Trimethylbenzene

ND

---

0.0594

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.0297

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.0297

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 94 %

Limits: 70-130 %

"

"

1,4-Difluorobenzene (Surr)

92 %

Limits: 70-130 %

"

"

"

Toluene-d8 (Surr)

96 %

Limits: 70-130 %

"

"

"

4-Bromofluorobenzene (Surr)

98 %

Limits: 70-130 %

"

"

"

Ex Sidewall E (A6B0900-21)

Matrix: Soil

Batch: 6020834

Benzene

ND

---

0.00717

mg/kg dry

50

02/27/16 17:49

5035/8260B

Toluene

ND

---

0.0358

"

"

"

"

Ethylbenzene

ND

---

0.0179

"

"

"

"

Xylenes, total

ND

---

0.0538

"

"

"

"

Naphthalene

ND

---

0.0717

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

0.0358

"

"

"

"

Isopropylbenzene

ND

---

0.0358

"

"

"

"

n-Propylbenzene

ND

---

0.0179

"

"

"

"

1,2,4-Trimethylbenzene

ND

---

0.0358

"

"

"

"

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020834

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 14 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Result

Analyte

MDL

Ex Sidewall E (A6B0900-21)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

1,3,5-Trimethylbenzene

ND

---

0.0358

mg/kg dry

50

"

5035/8260B

1,2-Dibromoethane (EDB)

ND

---

0.0179

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.0179

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 93 %

Limits: 70-130 %

"

"

1,4-Difluorobenzene (Surr)

91 %

Limits: 70-130 %

"

"

"

Toluene-d8 (Surr)

97 %

Limits: 70-130 %

"

"

"

4-Bromofluorobenzene (Surr)

98 %

Limits: 70-130 %

"

"

"

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020834

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 15 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

1A (A6B0900-01)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Acenaphthene

ND

---

0.0143

mg/kg dry

02/27/16 14:05

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0143

"

"

"

"

Anthracene

ND

---

0.0143

"

"

"

"

Benz(a)anthracene

ND

---

0.0143

"

"

"

"

Benzo(a)pyrene

ND

---

0.0143

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0143

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0143

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0143

"

"

"

"

Chrysene

ND

---

0.0143

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0143

"

"

"

"

Dibenzofuran

ND

---

0.0143

"

"

"

"

Fluoranthene

ND

---

0.0143

"

"

"

"

Fluorene

ND

---

0.0143

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0143

"

"

"

"

1-Methylnaphthalene

ND

---

0.0143

"

"

"

"

2-Methylnaphthalene

ND

---

0.0143

"

"

"

"

Naphthalene

ND

---

0.0143

"

"

"

"

Phenanthrene

ND

---

0.0143

"

"

"

"

Pyrene

ND

---

0.0143

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020836

Recovery: 87 %

Limits: 44-115 %

"

"

"

105 %

Limits: 54-127 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 16 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

1B (A6B0900-02)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Acenaphthene

ND

---

0.0161

mg/kg dry

02/27/16 14:59

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0161

"

"

"

"

Anthracene

ND

---

0.0161

"

"

"

"

Benz(a)anthracene

ND

---

0.0161

"

"

"

"

Benzo(a)pyrene

ND

---

0.0161

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0161

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0161

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0161

"

"

"

"

Chrysene

ND

---

0.0161

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0161

"

"

"

"

Dibenzofuran

ND

---

0.0161

"

"

"

"

Fluoranthene

ND

---

0.0161

"

"

"

"

Fluorene

ND

---

0.0161

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0161

"

"

"

"

1-Methylnaphthalene

ND

---

0.0161

"

"

"

"

2-Methylnaphthalene

ND

---

0.0161

"

"

"

"

Naphthalene

ND

---

0.0161

"

"

"

"

Phenanthrene

ND

---

0.0161

"

"

"

"

Pyrene

ND

---

0.0161

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020836

Recovery: 89 %

Limits: 44-115 %

"

"

"

107 %

Limits: 54-127 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 17 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

2A (A6B0900-04)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Acenaphthene

ND

---

0.0130

mg/kg dry

02/27/16 15:27

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0130

"

"

"

"

Anthracene

ND

---

0.0130

"

"

"

"

Benz(a)anthracene

ND

---

0.0130

"

"

"

"

Benzo(a)pyrene

ND

---

0.0130

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0130

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0130

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0130

"

"

"

"

Chrysene

ND

---

0.0130

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0130

"

"

"

"

Dibenzofuran

ND

---

0.0130

"

"

"

"

Fluoranthene

ND

---

0.0130

"

"

"

"

Fluorene

ND

---

0.0130

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0130

"

"

"

"

1-Methylnaphthalene

ND

---

0.0130

"

"

"

"

2-Methylnaphthalene

ND

---

0.0130

"

"

"

"

Naphthalene

ND

---

0.0130

"

"

"

"

Phenanthrene

ND

---

0.0130

"

"

"

"

Pyrene

ND

---

0.0130

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020836

Recovery: 86 %

Limits: 44-115 %

"

"

"

102 %

Limits: 54-127 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 18 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

2B (A6B0900-05)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Acenaphthene

ND

---

0.0180

mg/kg dry

02/27/16 15:54

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0180

"

"

"

"

Anthracene

ND

---

0.0180

"

"

"

"

Benz(a)anthracene

ND

---

0.0180

"

"

"

"

Benzo(a)pyrene

ND

---

0.0180

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0180

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0180

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0180

"

"

"

"

Chrysene

ND

---

0.0180

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0180

"

"

"

"

Dibenzofuran

ND

---

0.0180

"

"

"

"

Fluoranthene

ND

---

0.0180

"

"

"

"

Fluorene

ND

---

0.0180

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0180

"

"

"

"

1-Methylnaphthalene

ND

---

0.0180

"

"

"

"

2-Methylnaphthalene

ND

---

0.0180

"

"

"

"

Naphthalene

ND

---

0.0180

"

"

"

"

Phenanthrene

ND

---

0.0180

"

"

"

"

Pyrene

ND

---

0.0180

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020836

Recovery: 80 %

Limits: 44-115 %

"

"

"

98 %

Limits: 54-127 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 19 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

2D (A6B0900-07)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Acenaphthene

ND

---

0.0180

mg/kg dry

02/27/16 13:37

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0180

"

"

"

"

Anthracene

ND

---

0.0180

"

"

"

"

Benz(a)anthracene

ND

---

0.0198

"

"

"

"

Benzo(a)pyrene

ND

---

0.0180

"

"

"

"

Benzo(b)fluoranthene

0.0249

---

0.0180

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0180

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0180

"

"

"

"

Chrysene

ND

---

0.0207

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0180

"

"

"

"

Dibenzofuran

ND

---

0.0180

"

"

"

"

Fluoranthene

ND

---

0.0180

"

"

"

"

0.0229

---

0.0180

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0180

"

"

"

"

1-Methylnaphthalene

0.0284

---

0.0180

"

"

"

"

2-Methylnaphthalene

0.0433

---

0.0180

"

"

"

"

Naphthalene

0.0502

---

0.0180

"

"

"

"

Phenanthrene

0.0229

---

0.0180

"

"

"

"

ND

---

0.0180

"

"

"

"

Fluorene

Pyrene
Surrogate: 2-Fluorobiphenyl (Surr)
p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020836

Recovery: 84 %

Limits: 44-115 %

"

"

"

102 %

Limits: 54-127 %

"

"

"

R-02
M-02

R-02

M-02

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 20 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

3A (A6B0900-08)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Acenaphthene

ND

---

0.0136

mg/kg dry

02/27/16 16:21

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0136

"

"

"

"

Anthracene

ND

---

0.0136

"

"

"

"

Benz(a)anthracene

ND

---

0.0136

"

"

"

"

Benzo(a)pyrene

ND

---

0.0136

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0136

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0136

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0136

"

"

"

"

Chrysene

ND

---

0.0136

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0136

"

"

"

"

Dibenzofuran

ND

---

0.0136

"

"

"

"

Fluoranthene

ND

---

0.0136

"

"

"

"

Fluorene

ND

---

0.0136

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0136

"

"

"

"

1-Methylnaphthalene

ND

---

0.0136

"

"

"

"

2-Methylnaphthalene

ND

---

0.0136

"

"

"

"

Naphthalene

ND

---

0.0136

"

"

"

"

Phenanthrene

ND

---

0.0136

"

"

"

"

Pyrene

ND

---

0.0136

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020836

Recovery: 87 %

Limits: 44-115 %

"

"

"

107 %

Limits: 54-127 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 21 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

3B (A6B0900-09)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Acenaphthene

ND

---

0.0129

mg/kg dry

02/27/16 16:48

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0129

"

"

"

"

Anthracene

ND

---

0.0129

"

"

"

"

Benz(a)anthracene

ND

---

0.0129

"

"

"

"

Benzo(a)pyrene

ND

---

0.0129

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0129

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0129

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0129

"

"

"

"

Chrysene

ND

---

0.0129

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0129

"

"

"

"

Dibenzofuran

ND

---

0.0129

"

"

"

"

Fluoranthene

ND

---

0.0129

"

"

"

"

Fluorene

ND

---

0.0129

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0129

"

"

"

"

1-Methylnaphthalene

ND

---

0.0129

"

"

"

"

2-Methylnaphthalene

ND

---

0.0129

"

"

"

"

Naphthalene

ND

---

0.0129

"

"

"

"

Phenanthrene

ND

---

0.0129

"

"

"

"

Pyrene

ND

---

0.0129

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020836

Recovery: 92 %

Limits: 44-115 %

"

"

"

109 %

Limits: 54-127 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 22 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

3C (A6B0900-10)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Acenaphthene

ND

---

0.0135

mg/kg dry

02/27/16 17:15

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0135

"

"

"

"

Anthracene

ND

---

0.0135

"

"

"

"

Benz(a)anthracene

ND

---

0.0135

"

"

"

"

Benzo(a)pyrene

ND

---

0.0135

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0135

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0135

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0135

"

"

"

"

Chrysene

ND

---

0.0135

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0135

"

"

"

"

Dibenzofuran

ND

---

0.0135

"

"

"

"

Fluoranthene

ND

---

0.0135

"

"

"

"

Fluorene

ND

---

0.0135

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0135

"

"

"

"

1-Methylnaphthalene

ND

---

0.0135

"

"

"

"

2-Methylnaphthalene

ND

---

0.0135

"

"

"

"

Naphthalene

ND

---

0.0135

"

"

"

"

Phenanthrene

ND

---

0.0135

"

"

"

"

Pyrene

ND

---

0.0135

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020836

Recovery: 89 %

Limits: 44-115 %

"

"

"

109 %

Limits: 54-127 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 23 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

3D (A6B0900-11)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Acenaphthene

ND

---

0.0138

mg/kg dry

02/27/16 18:09

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0138

"

"

"

"

Anthracene

ND

---

0.0138

"

"

"

"

Benz(a)anthracene

ND

---

0.0138

"

"

"

"

Benzo(a)pyrene

ND

---

0.0138

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0138

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0138

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0138

"

"

"

"

Chrysene

ND

---

0.0138

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0138

"

"

"

"

Dibenzofuran

ND

---

0.0138

"

"

"

"

Fluoranthene

ND

---

0.0138

"

"

"

"

Fluorene

ND

---

0.0138

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0138

"

"

"

"

1-Methylnaphthalene

ND

---

0.0138

"

"

"

"

2-Methylnaphthalene

ND

---

0.0138

"

"

"

"

Naphthalene

ND

---

0.0138

"

"

"

"

Phenanthrene

ND

---

0.0138

"

"

"

"

Pyrene

ND

---

0.0138

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020836

Recovery: 86 %

Limits: 44-115 %

"

"

"

100 %

Limits: 54-127 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 24 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

4A (A6B0900-12)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Acenaphthene

ND

---

0.0149

mg/kg dry

02/27/16 18:36

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0149

"

"

"

"

Anthracene

ND

---

0.0149

"

"

"

"

Benz(a)anthracene

ND

---

0.0149

"

"

"

"

Benzo(a)pyrene

ND

---

0.0149

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0149

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0149

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0149

"

"

"

"

Chrysene

ND

---

0.0149

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0149

"

"

"

"

Dibenzofuran

ND

---

0.0149

"

"

"

"

Fluoranthene

ND

---

0.0149

"

"

"

"

Fluorene

ND

---

0.0149

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0149

"

"

"

"

1-Methylnaphthalene

ND

---

0.0149

"

"

"

"

2-Methylnaphthalene

ND

---

0.0149

"

"

"

"

Naphthalene

ND

---

0.0149

"

"

"

"

Phenanthrene

ND

---

0.0149

"

"

"

"

Pyrene

ND

---

0.0149

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020836

Recovery: 86 %

Limits: 44-115 %

"

"

"

102 %

Limits: 54-127 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 25 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

4B (A6B0900-13)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Acenaphthene

ND

---

0.0123

mg/kg dry

02/27/16 19:02

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0123

"

"

"

"

Anthracene

ND

---

0.0123

"

"

"

"

Benz(a)anthracene

ND

---

0.0123

"

"

"

"

Benzo(a)pyrene

ND

---

0.0123

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0123

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0123

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0123

"

"

"

"

Chrysene

ND

---

0.0123

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0123

"

"

"

"

Dibenzofuran

ND

---

0.0123

"

"

"

"

Fluoranthene

ND

---

0.0123

"

"

"

"

Fluorene

ND

---

0.0123

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0123

"

"

"

"

1-Methylnaphthalene

ND

---

0.0123

"

"

"

"

2-Methylnaphthalene

ND

---

0.0123

"

"

"

"

Naphthalene

ND

---

0.0123

"

"

"

"

Phenanthrene

ND

---

0.0123

"

"

"

"

Pyrene

ND

---

0.0123

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020836

Recovery: 95 %

Limits: 44-115 %

"

"

"

119 %

Limits: 54-127 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 26 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

4C (A6B0900-14)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Acenaphthene

ND

---

0.0144

mg/kg dry

02/27/16 19:29

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0144

"

"

"

"

Anthracene

ND

---

0.0144

"

"

"

"

Benz(a)anthracene

ND

---

0.0144

"

"

"

"

Benzo(a)pyrene

ND

---

0.0144

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0144

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0144

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0144

"

"

"

"

Chrysene

ND

---

0.0144

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0144

"

"

"

"

Dibenzofuran

ND

---

0.0144

"

"

"

"

Fluoranthene

ND

---

0.0144

"

"

"

"

Fluorene

ND

---

0.0144

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0144

"

"

"

"

1-Methylnaphthalene

ND

---

0.0144

"

"

"

"

2-Methylnaphthalene

ND

---

0.0144

"

"

"

"

Naphthalene

ND

---

0.0144

"

"

"

"

Phenanthrene

ND

---

0.0144

"

"

"

"

Pyrene

ND

---

0.0144

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020836

Recovery: 91 %

Limits: 44-115 %

"

"

"

115 %

Limits: 54-127 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 27 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

4D (A6B0900-15)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Acenaphthene

ND

---

0.0120

mg/kg dry

02/27/16 19:56

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0120

"

"

"

"

Anthracene

ND

---

0.0120

"

"

"

"

Benz(a)anthracene

ND

---

0.0120

"

"

"

"

Benzo(a)pyrene

ND

---

0.0120

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0120

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0120

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0120

"

"

"

"

Chrysene

ND

---

0.0120

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0120

"

"

"

"

Dibenzofuran

ND

---

0.0120

"

"

"

"

Fluoranthene

ND

---

0.0120

"

"

"

"

Fluorene

ND

---

0.0120

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0120

"

"

"

"

1-Methylnaphthalene

ND

---

0.0120

"

"

"

"

2-Methylnaphthalene

ND

---

0.0120

"

"

"

"

Naphthalene

ND

---

0.0120

"

"

"

"

Phenanthrene

ND

---

0.0120

"

"

"

"

Pyrene

ND

---

0.0120

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020836

Recovery: 92 %

Limits: 44-115 %

"

"

"

115 %

Limits: 54-127 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 28 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

0A (A6B0900-16)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Acenaphthene

ND

---

0.0173

mg/kg dry

02/27/16 20:23

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0173

"

"

"

"

Anthracene

ND

---

0.0173

"

"

"

"

Benz(a)anthracene

ND

---

0.0173

"

"

"

"

Benzo(a)pyrene

ND

---

0.0173

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0173

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0173

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0173

"

"

"

"

Chrysene

ND

---

0.0173

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0173

"

"

"

"

Dibenzofuran

ND

---

0.0173

"

"

"

"

Fluoranthene

ND

---

0.0173

"

"

"

"

Fluorene

ND

---

0.0173

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0173

"

"

"

"

1-Methylnaphthalene

ND

---

0.0173

"

"

"

"

2-Methylnaphthalene

ND

---

0.0173

"

"

"

"

Naphthalene

ND

---

0.0173

"

"

"

"

Phenanthrene

ND

---

0.0173

"

"

"

"

Pyrene

ND

---

0.0173

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020836

Recovery: 91 %

Limits: 44-115 %

"

"

"

111 %

Limits: 54-127 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 29 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

0B (A6B0900-17)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Acenaphthene

ND

---

0.0167

mg/kg dry

02/27/16 20:49

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0167

"

"

"

"

Anthracene

ND

---

0.0167

"

"

"

"

Benz(a)anthracene

ND

---

0.0167

"

"

"

"

Benzo(a)pyrene

ND

---

0.0167

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0167

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0167

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0167

"

"

"

"

Chrysene

ND

---

0.0167

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0167

"

"

"

"

Dibenzofuran

0.0620

---

0.0167

"

"

"

"

Fluoranthene

ND

---

0.0167

"

"

"

"

Fluorene

ND

---

0.0401

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0167

"

"

"

"

1-Methylnaphthalene

0.114

---

0.0167

"

"

"

"

2-Methylnaphthalene

0.155

---

0.0167

"

"

"

"

ND

---

0.0301

"

"

"

"

Phenanthrene

0.0489

---

0.0167

"

"

"

"

Pyrene

0.0411

---

0.0167

"

"

"

"

Naphthalene

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020836

Recovery: 100 %

Limits: 44-115 %

"

"

"

118 %

Limits: 54-127 %

"

"

"

R-02

R-02

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 30 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

0C (A6B0900-18)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Notes

Batch: 6020836

Acenaphthene

ND

---

0.208

mg/kg dry

02/27/16 21:16

EPA 8270D (SIM)

R-02

Acenaphthylene

ND

---

0.0763

"

"

"

"

R-02

Anthracene

ND

---

0.104

"

"

"

"

R-02

Benz(a)anthracene

ND

---

0.0242

"

"

"

"

R-02

Benzo(a)pyrene

ND

---

0.0186

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0186

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0186

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0186

"

"

"

"

Chrysene

ND

---

0.0260

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0186

"

"

"

"

Dibenzofuran

0.376

---

0.0186

"

"

"

"

Fluoranthene

ND

---

0.0186

"

"

"

"

0.454

---

0.0186

"

"

"

"

ND

---

0.0186

"

"

"

"

Fluorene

Indeno(1,2,3-cd)pyrene
1-Methylnaphthalene

3.29

---

0.0186

"

"

"

"

2-Methylnaphthalene

5.58

---

0.0186

"

"

"

"

Naphthalene

2.08

---

0.0186

"

"

"

"

Phenanthrene

0.740

---

0.0186

"

"

"

"

Pyrene

0.389

---

0.0186

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Recovery: 78 %

Limits: 44-115 %

"

"

"

112 %

Limits: 54-127 %

"

"

"

R-02

M-04

M-02

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 31 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

Ex Sidewall S (A6B0900-19)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Acenaphthene

ND

---

0.0107

mg/kg dry

02/27/16 21:43

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0107

"

"

"

"

Anthracene

ND

---

0.0107

"

"

"

"

Benz(a)anthracene

ND

---

0.0107

"

"

"

"

Benzo(a)pyrene

ND

---

0.0107

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0107

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0107

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0107

"

"

"

"

Chrysene

ND

---

0.0107

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0107

"

"

"

"

Dibenzofuran

ND

---

0.0107

"

"

"

"

Fluoranthene

ND

---

0.0107

"

"

"

"

Fluorene

ND

---

0.0107

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0107

"

"

"

"

1-Methylnaphthalene

ND

---

0.0107

"

"

"

"

2-Methylnaphthalene

ND

---

0.0107

"

"

"

"

Naphthalene

ND

---

0.0107

"

"

"

"

Phenanthrene

ND

---

0.0107

"

"

"

"

Pyrene

ND

---

0.0107

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020836

Recovery: 97 %

Limits: 44-115 %

"

"

"

123 %

Limits: 54-127 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 32 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

Ex Sidewall W (A6B0900-20)

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Acenaphthene

ND

---

0.0134

mg/kg dry

02/27/16 22:10

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0134

"

"

"

"

Anthracene

ND

---

0.0134

"

"

"

"

Benz(a)anthracene

ND

---

0.0134

"

"

"

"

Benzo(a)pyrene

ND

---

0.0134

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0134

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0134

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0134

"

"

"

"

Chrysene

ND

---

0.0134

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0134

"

"

"

"

Dibenzofuran

ND

---

0.0134

"

"

"

"

Fluoranthene

ND

---

0.0134

"

"

"

"

Fluorene

ND

---

0.0134

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0134

"

"

"

"

1-Methylnaphthalene

ND

---

0.0134

"

"

"

"

2-Methylnaphthalene

ND

---

0.0134

"

"

"

"

Naphthalene

ND

---

0.0134

"

"

"

"

Phenanthrene

ND

---

0.0134

"

"

"

"

Pyrene

ND

---

0.0134

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020836

Recovery: 93 %

Limits: 44-115 %

"

"

"

114 %

Limits: 54-127 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 33 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

Ex Sidewall E (A6B0900-21)

Acenaphthene

Reporting
Limit

Dilution

Units

Matrix: Soil

Date Analyzed

Method

Notes

Batch: 6020836

ND

---

0.0105

mg/kg dry

02/27/16 22:36

EPA 8270D (SIM)

Acenaphthylene

0.0181

---

0.0105

"

"

"

"

Anthracene

0.0526

---

0.0105

"

"

"

"

Benz(a)anthracene

0.635

---

0.0105

"

"

"

"

Benzo(a)pyrene

0.219

---

0.0105

"

"

"

"

Benzo(b)fluoranthene

0.603

---

0.0105

"

"

"

"

M-02, Q-42

Benzo(k)fluoranthene

0.206

---

0.0105

"

"

"

"

M-02

Benzo(g,h,i)perylene

0.0799

---

0.0105

"

"

"

"

Chrysene

0.947

---

0.0105

"

"

"

"

Dibenz(a,h)anthracene

0.0306

---

0.0105

"

"

"

"

Dibenzofuran

ND

---

0.0105

"

"

"

"

Fluoranthene

1.86

---

0.0105

"

"

"

"

Fluorene

ND

---

0.0105

"

"

"

"

0.116

---

0.0105

"

"

"

"

Indeno(1,2,3-cd)pyrene

1-Methylnaphthalene

ND

---

0.0105

"

"

"

"

2-Methylnaphthalene

0.0135

---

0.0105

"

"

"

"

ND

---

0.0105

"

"

"

"

0.0119

---

0.0105

"

"

"

"

1.60

---

0.0105

"

"

"

"

Naphthalene
Phenanthrene
Pyrene
Surrogate: 2-Fluorobiphenyl (Surr)
p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Recovery: 95 %

Limits: 44-115 %

"

"

"

121 %

Limits: 54-127 %

"

"

"

Q-42

Q-42

Q-42

Q-42

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 34 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


Percent Dry Weight
Analyte

Result

MDL

1A (A6B0900-01)

% Solids

Matrix: Soil

65.4

---

57.4

---

44.8

---

72.9

---

1B (A6B0900-02)

% Solids

49.6

---

36.0

---

53.9

---

68.4

---

75.0

---

67.6

---

63.3

---

64.6

---

74.8

---

67.9

---

76.7

---

49.2

---

1.00
Matrix: Soil

0A (A6B0900-16)

% Solids

1.00
Matrix: Soil

4D (A6B0900-15)

% Solids

1.00
Matrix: Soil

4C (A6B0900-14)

% Solids

1.00
Matrix: Soil

4B (A6B0900-13)

% Solids

1.00
Matrix: Soil

4A (A6B0900-12)

% Solids

1.00
Matrix: Soil

3D (A6B0900-11)

% Solids

1.00
Matrix: Soil

3C (A6B0900-10)

% Solids

1.00
Matrix: Soil

3B (A6B0900-09)

% Solids

1.00
Matrix: Soil

3A (A6B0900-08)

% Solids

1.00
Matrix: Soil

2D (A6B0900-07)

% Solids

1.00
Matrix: Soil

2C (A6B0900-06)

% Solids

1.00
Matrix: Soil

2B (A6B0900-05)

% Solids

1.00
Matrix: Soil

2A (A6B0900-04)

% Solids

1.00
Matrix: Soil

1C (A6B0900-03)

% Solids

Reporting
Limit

1.00
Matrix: Soil

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

1.00

Dilution

Units

Date Analyzed

Method

02/27/16 13:34

EPA 8000C

02/27/16 13:34

EPA 8000C

02/27/16 13:34

EPA 8000C

02/27/16 13:34

EPA 8000C

02/27/16 13:34

EPA 8000C

02/27/16 13:34

EPA 8000C

02/27/16 13:34

EPA 8000C

02/27/16 13:34

EPA 8000C

02/27/16 13:34

EPA 8000C

02/27/16 13:34

EPA 8000C

02/27/16 13:34

EPA 8000C

02/27/16 13:34

EPA 8000C

02/27/16 13:34

EPA 8000C

02/27/16 13:34

EPA 8000C

02/27/16 13:34

EPA 8000C

02/27/16 13:34

EPA 8000C

Notes

Batch: 6020837

% by Weight

Batch: 6020837

% by Weight

Batch: 6020837

% by Weight

Batch: 6020837

% by Weight

Batch: 6020837

% by Weight

Batch: 6020837

% by Weight

Batch: 6020837

% by Weight

Batch: 6020837

% by Weight

Batch: 6020837

% by Weight

Batch: 6020837

% by Weight

Batch: 6020837

% by Weight

Batch: 6020837

% by Weight

Batch: 6020837

% by Weight

Batch: 6020837

% by Weight

Batch: 6020837

% by Weight

Batch: 6020837

% by Weight

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 35 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

ANALYTICAL SAMPLE RESULTS


Percent Dry Weight
Analyte

Result

MDL

55.4

---

0B (A6B0900-17)

% Solids

Matrix: Soil

0C (A6B0900-18)

% Solids

51.2

---

91.7

---

71.1

---

82.9

---

1.00
Matrix: Soil

Ex Sidewall E (A6B0900-21)

% Solids

1.00
Matrix: Soil

Ex Sidewall W (A6B0900-20)

% Solids

1.00
Matrix: Soil

Ex Sidewall S (A6B0900-19)

% Solids

Reporting
Limit

1.00
Matrix: Soil

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

1.00

Dilution

Units

Date Analyzed

Method

02/27/16 13:34

EPA 8000C

02/27/16 13:34

EPA 8000C

02/27/16 13:34

EPA 8000C

02/27/16 13:34

EPA 8000C

02/27/16 13:34

EPA 8000C

Notes

Batch: 6020837

% by Weight

Batch: 6020837

% by Weight

Batch: 6020837

% by Weight

Batch: 6020837

% by Weight

Batch: 6020837

% by Weight

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 36 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

QUALITY CONTROL (QC) SAMPLE RESULTS


Diesel and/or Oil Hydrocarbons by NWTPH-Dx
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

RPD
Limit

Notes

Soil

Batch 6020835 - EPA 3546 (Fuels)

Prepared: 02/27/16 10:01 Analyzed: 02/27/16 13:13

Blank (6020835-BLK1)
NWTPH-Dx

Diesel

ND

---

25.0

mg/kg wet

---

---

---

---

---

---

Oil

ND

---

50.0

"

"

---

---

---

---

---

---

---

---

Surr: o-Terphenyl (Surr)

Recovery: 97 %

Limits: 50-150 %

Dilution: 1x

Prepared: 02/27/16 10:01 Analyzed: 02/27/16 13:33

LCS (6020835-BS1)
NWTPH-Dx

Diesel

119

---

Surr: o-Terphenyl (Surr)

25.0
Recovery: 98 %

mg/kg wet

125

Limits: 50-150 %

---

95

76-115%

Dilution: 1x

Prepared: 02/27/16 10:01 Analyzed: 02/27/16 14:13

Duplicate (6020835-DUP1)
QC Source Sample: 1C (A6B0900-03)
NWTPH-Dx

Diesel
Oil

54200

---

2010

mg/kg dry

50

---

66400

---

---

20

30%

ND

---

4030

"

"

---

ND

---

---

---

30%

Surr: o-Terphenyl (Surr)

Recovery: %

Limits: 50-150 %

Dilution: 50x

S-01

Soil

Batch 6020836 - EPA 3546 (Fuels)

Prepared: 02/27/16 10:02 Analyzed: 02/27/16 13:13

Blank (6020836-BLK1)
NWTPH-Dx

Diesel

ND

---

25.0

mg/kg wet

---

---

---

---

---

---

Oil

ND

---

50.0

"

"

---

---

---

---

---

---

---

---

34

30%

Surr: o-Terphenyl (Surr)

Recovery: 92 %

Limits: 50-150 %

Dilution: 1x

Prepared: 02/27/16 10:02 Analyzed: 02/27/16 13:33

LCS (6020836-BS1)
NWTPH-Dx

Diesel

120

---

Surr: o-Terphenyl (Surr)

25.0
Recovery: 88 %

mg/kg wet

125

Limits: 50-150 %

---

96

76-115%

Dilution: 1x

Prepared: 02/27/16 10:02 Analyzed: 02/27/16 14:13

Duplicate (6020836-DUP1)
QC Source Sample: 1A (A6B0900-01)
NWTPH-Dx

Diesel

33.9

---

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

26.9

mg/kg dry

---

24.2

---

---

F-17, Q-05

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 37 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

QUALITY CONTROL (QC) SAMPLE RESULTS


Diesel and/or Oil Hydrocarbons by NWTPH-Dx
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

RPD
Limit

Notes

42

30%

F-17, Q-05

Soil

Batch 6020836 - EPA 3546 (Fuels)

Prepared: 02/27/16 10:02 Analyzed: 02/27/16 14:13

Duplicate (6020836-DUP1)
QC Source Sample: 1A (A6B0900-01)

Oil

188

---

Surr: o-Terphenyl (Surr)

53.7
Recovery: 89 %

mg/kg dry

"

---

Limits: 50-150 %

123

---

---

Dilution: 1x

Prepared: 02/27/16 10:02 Analyzed: 02/27/16 17:52

Duplicate (6020836-DUP2)
QC Source Sample: 3C (A6B0900-10)
NWTPH-Dx

Diesel

34.3

---

27.3

mg/kg dry

---

23.7

---

---

36

30%

F-17, Q-05

Oil

122

---

54.6

"

"

---

98.7

---

---

21

30%

F-17

Surr: o-Terphenyl (Surr)

Recovery: 88 %

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Limits: 50-150 %

Dilution: 1x

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 38 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

QUALITY CONTROL (QC) SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Analyte

Result

MDL

Reporting
Limit

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

RPD
Limit

Notes

Soil

Batch 6020833 - EPA 5035A

Prepared: 02/27/16 10:00 Analyzed: 02/27/16 13:26

Blank (6020833-BLK1)
5035/8260B

Benzene

ND

---

0.00667

mg/kg wet

50

---

---

---

---

---

---

Toluene

ND

---

0.0333

"

"

---

---

---

---

---

---

Ethylbenzene

ND

---

0.0167

"

"

---

---

---

---

---

---

Xylenes, total

ND

---

0.0500

"

"

---

---

---

---

---

---

Naphthalene

ND

---

0.0667

"

"

---

---

---

---

---

---

Methyl tert-butyl ether


(MTBE)
Isopropylbenzene

ND

---

0.0333

"

"

---

---

---

---

---

---

ND

---

0.0333

"

"

---

---

---

---

---

---

n-Propylbenzene

ND

---

0.0167

"

"

---

---

---

---

---

---

1,2,4-Trimethylbenzene

ND

---

0.0333

"

"

---

---

---

---

---

---

1,3,5-Trimethylbenzene

ND

---

0.0333

"

"

---

---

---

---

---

---

1,2-Dibromoethane (EDB)

ND

---

0.0167

"

"

---

---

---

---

---

---

1,2-Dichloroethane (EDC)

ND

---

0.0167

"

"

---

---

---

---

---

---

---

---

Surr: Dibromofluoromethane (Surr)

Recovery: 107 %

Limits: 70-130 %

Dilution: 1x

103 %

70-130 %

"

Toluene-d8 (Surr)

98 %

70-130 %

"

4-Bromofluorobenzene (Surr)

97 %

70-130 %

"

1,4-Difluorobenzene (Surr)

Prepared: 02/27/16 10:00 Analyzed: 02/27/16 12:01

LCS (6020833-BS1)
5035/8260B

Benzene

1.08

---

0.0100

mg/kg wet

50

1.00

---

108

65-135%

Toluene

1.02

---

0.0500

"

"

"

---

102

"

---

---

Ethylbenzene

0.979

---

0.0250

"

"

"

---

98

"

---

---

Xylenes, total

2.85

---

0.0750

"

"

3.00

---

95

"

---

---

Naphthalene

0.948

---

0.100

"

"

1.00

---

95

"

---

---

Methyl tert-butyl ether


(MTBE)
Isopropylbenzene

1.01

---

0.0500

"

"

"

---

101

"

---

---

0.982

---

0.0500

"

"

"

---

98

"

---

---

n-Propylbenzene

0.991

---

0.0250

"

"

"

---

99

"

---

---

1,2,4-Trimethylbenzene

0.983

---

0.0500

"

"

"

---

98

"

---

---

1,3,5-Trimethylbenzene

0.996

---

0.0500

"

"

"

---

100

"

---

---

1,2-Dibromoethane (EDB)

1.08

---

0.0250

"

"

"

---

108

"

---

---

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 39 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

QUALITY CONTROL (QC) SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Analyte

Result

MDL

Reporting
Limit

Units

Dil.

Spike
Amount

%REC

%REC
Limits RPD

RPD
Limit

Notes

Soil

Batch 6020833 - EPA 5035A

Prepared: 02/27/16 10:00 Analyzed: 02/27/16 12:01

LCS (6020833-BS1)

1,2-Dichloroethane (EDC)

Source
Result

0.986

Surr: Dibromofluoromethane (Surr)

---

0.0250

mg/kg wet

"

"

---

Recovery: 102 %

Limits: 70-130 %

Dilution: 1x

102 %

70-130 %

"

Toluene-d8 (Surr)

97 %

70-130 %

"

4-Bromofluorobenzene (Surr)

97 %

70-130 %

"

1,4-Difluorobenzene (Surr)

99

"

---

---

Prepared: 02/26/16 09:40 Analyzed: 02/27/16 14:23

Duplicate (6020833-DUP1)
QC Source Sample: 1A (A6B0900-01)
5035/8260B

Benzene

ND

---

0.0198

mg/kg dry

50

---

ND

---

---

---

30%

Toluene

ND

---

0.0988

"

"

---

ND

---

---

---

30%

Ethylbenzene

ND

---

0.0494

"

"

---

ND

---

---

---

30%

Xylenes, total

ND

---

0.148

"

"

---

ND

---

---

---

30%

Naphthalene

ND

---

0.198

"

"

---

ND

---

---

---

30%

Methyl tert-butyl ether


(MTBE)
Isopropylbenzene

ND

---

0.0988

"

"

---

ND

---

---

---

30%

ND

---

0.0988

"

"

---

ND

---

---

---

30%

n-Propylbenzene

ND

---

0.0494

"

"

---

ND

---

---

---

30%

1,2,4-Trimethylbenzene

ND

---

0.0988

"

"

---

ND

---

---

---

30%

1,3,5-Trimethylbenzene

ND

---

0.0988

"

"

---

ND

---

---

---

30%

1,2-Dibromoethane (EDB)

ND

---

0.0494

"

"

---

ND

---

---

---

30%

1,2-Dichloroethane (EDC)

ND

---

0.0494

"

"

---

ND

---

---

---

30%

Surr: Dibromofluoromethane (Surr)

Recovery: 104 %

Limits: 70-130 %

Dilution: 1x

101 %

70-130 %

"

Toluene-d8 (Surr)

99 %

70-130 %

"

4-Bromofluorobenzene (Surr)

93 %

70-130 %

"

1,4-Difluorobenzene (Surr)

Prepared: 02/26/16 10:30 Analyzed: 02/27/16 19:35

Matrix Spike (6020833-MS1)


QC Source Sample: 4B (A6B0900-13)
5035/8260B

Benzene

1.75

---

0.0162

mg/kg dry

50

1.62

ND

108

65-135%

---

---

Toluene

1.64

---

0.0809

"

"

"

ND

101

"

---

---

Ethylbenzene

1.59

---

0.0404

"

"

"

ND

98

"

---

---

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 40 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

QUALITY CONTROL (QC) SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Analyte

Result

MDL

Reporting
Limit

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

RPD
Limit

Notes

Soil

Batch 6020833 - EPA 5035A

Prepared: 02/26/16 10:30 Analyzed: 02/27/16 19:35

Matrix Spike (6020833-MS1)


QC Source Sample: 4B (A6B0900-13)

Xylenes, total

4.58

---

0.121

mg/kg dry

"

4.86

ND

94

"

---

---

Naphthalene

1.39

---

0.162

"

"

1.62

ND

86

"

---

---

Methyl tert-butyl ether


(MTBE)
Isopropylbenzene

1.63

---

0.0809

"

"

"

ND

101

"

---

---

1.57

---

0.0809

"

"

"

ND

97

"

---

---

n-Propylbenzene

1.55

---

0.0404

"

"

"

ND

96

"

---

---

1,2,4-Trimethylbenzene

1.51

---

0.0809

"

"

"

ND

93

"

---

---

1,3,5-Trimethylbenzene

1.55

---

0.0809

"

"

"

ND

96

"

---

---

1,2-Dibromoethane (EDB)

1.67

---

0.0404

"

"

"

ND

103

"

---

---

1,2-Dichloroethane (EDC)

1.67

---

0.0404

"

"

"

ND

103

"

---

---

Surr: Dibromofluoromethane (Surr)

Recovery: 103 %

Limits: 70-130 %

Dilution: 1x

1,4-Difluorobenzene (Surr)

99 %

70-130 %

"

Toluene-d8 (Surr)

98 %

70-130 %

"

4-Bromofluorobenzene (Surr)

93 %

70-130 %

"

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 41 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

QUALITY CONTROL (QC) SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

RPD
Limit

Notes

Soil

Batch 6020834 - EPA 5035A

Prepared: 02/27/16 10:00 Analyzed: 02/27/16 13:48

Blank (6020834-BLK1)
5035/8260B

Benzene

ND

---

0.00667

mg/kg wet

50

---

---

---

---

---

---

Toluene

ND

---

0.0333

"

"

---

---

---

---

---

---

Ethylbenzene

ND

---

0.0167

"

"

---

---

---

---

---

---

Xylenes, total

ND

---

0.0500

"

"

---

---

---

---

---

---

Naphthalene

ND

---

0.0667

"

"

---

---

---

---

---

---

Methyl tert-butyl ether


(MTBE)
Isopropylbenzene

ND

---

0.0333

"

"

---

---

---

---

---

---

ND

---

0.0333

"

"

---

---

---

---

---

---

n-Propylbenzene

ND

---

0.0167

"

"

---

---

---

---

---

---

1,2,4-Trimethylbenzene

ND

---

0.0333

"

"

---

---

---

---

---

---

1,3,5-Trimethylbenzene

ND

---

0.0333

"

"

---

---

---

---

---

---

1,2-Dibromoethane (EDB)

ND

---

0.0167

"

"

---

---

---

---

---

---

1,2-Dichloroethane (EDC)

ND

---

0.0167

"

"

---

---

---

---

---

---

---

---

Surr: Dibromofluoromethane (Surr)

Recovery: 96 %

Limits: 70-130 %

Dilution: 1x

1,4-Difluorobenzene (Surr)

92 %

70-130 %

"

Toluene-d8 (Surr)

97 %

70-130 %

"

4-Bromofluorobenzene (Surr)

98 %

70-130 %

"

Prepared: 02/27/16 10:00 Analyzed: 02/27/16 12:54

LCS (6020834-BS1)
5035/8260B

Benzene

0.878

---

0.0100

mg/kg wet

50

1.00

---

88

65-135%

Toluene

0.924

---

0.0500

"

"

"

---

92

"

---

---

Ethylbenzene

0.981

---

0.0250

"

"

"

---

98

"

---

---

Xylenes, total

2.96

---

0.0750

"

"

3.00

---

99

"

---

---

Naphthalene

0.940

---

0.100

"

"

1.00

---

94

"

---

---

Methyl tert-butyl ether


(MTBE)
Isopropylbenzene

0.876

---

0.0500

"

"

"

---

88

"

---

---

1.05

---

0.0500

"

"

"

---

105

"

---

---

n-Propylbenzene

0.898

---

0.0250

"

"

"

---

90

"

---

---

1,2,4-Trimethylbenzene

0.988

---

0.0500

"

"

"

---

99

"

---

---

1,3,5-Trimethylbenzene

0.998

---

0.0500

"

"

"

---

100

"

---

---

1,2-Dibromoethane (EDB)

1.00

---

0.0250

"

"

"

---

100

"

---

---

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 42 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

QUALITY CONTROL (QC) SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

%REC

%REC
Limits RPD

RPD
Limit

Notes

Soil

Batch 6020834 - EPA 5035A

Prepared: 02/27/16 10:00 Analyzed: 02/27/16 12:54

LCS (6020834-BS1)

1,2-Dichloroethane (EDC)

Source
Result

0.848

---

Surr: Dibromofluoromethane (Surr)

0.0250

mg/kg wet

"

"

---

Recovery: 97 %

Limits: 70-130 %

Dilution: 1x

1,4-Difluorobenzene (Surr)

92 %

70-130 %

"

Toluene-d8 (Surr)

95 %

70-130 %

"

4-Bromofluorobenzene (Surr)

99 %

70-130 %

"

85

"

---

---

Prepared: 02/26/16 12:05 Analyzed: 02/27/16 16:02

Duplicate (6020834-DUP1)
QC Source Sample: 0B (A6B0900-17)
5035/8260B

Benzene

ND

---

0.0288

mg/kg dry

50

---

0.0177

---

---

***

30%

Toluene

0.247

Ethylbenzene

0.220

---

0.144

"

"

---

0.224

---

---

10

30%

---

0.0719

"

"

---

0.200

---

---

10

30%

Xylenes, total
Naphthalene

1.16

---

0.216

"

"

---

1.04

---

---

11

30%

ND

---

0.288

"

"

---

ND

---

---

---

30%

Methyl tert-butyl ether


(MTBE)
Isopropylbenzene

ND

---

0.144

"

"

---

ND

---

---

---

30%

ND

---

0.144

"

"

---

ND

---

---

---

30%

n-Propylbenzene

0.167

---

0.0719

"

"

---

0.162

---

---

30%

1,2,4-Trimethylbenzene

0.698

---

0.144

"

"

---

0.755

---

---

30%

1,3,5-Trimethylbenzene

0.262

---

0.144

"

"

---

0.264

---

---

0.7

30%

1,2-Dibromoethane (EDB)

ND

---

0.0719

"

"

---

ND

---

---

---

30%

1,2-Dichloroethane (EDC)

ND

---

0.0719

"

"

---

ND

---

---

---

30%

Surr: Dibromofluoromethane (Surr)

Recovery: 93 %

Limits: 70-130 %

Dilution: 1x

1,4-Difluorobenzene (Surr)

91 %

70-130 %

"

Toluene-d8 (Surr)

95 %

70-130 %

"

100 %

70-130 %

"

4-Bromofluorobenzene (Surr)

Prepared: 02/26/16 12:40 Analyzed: 02/27/16 18:16

Matrix Spike (6020834-MS1)


QC Source Sample: Ex Sidewall E (A6B0900-21)
5035/8260B

Benzene

0.642

---

0.00717

mg/kg dry

50

0.710

ND

90

65-135%

---

---

Toluene

0.680

---

0.0358

"

"

"

ND

96

"

---

---

Ethylbenzene

0.718

---

0.0179

"

"

"

ND

101

"

---

---

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 43 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

QUALITY CONTROL (QC) SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

RPD
Limit

Notes

Soil

Batch 6020834 - EPA 5035A

Prepared: 02/26/16 12:40 Analyzed: 02/27/16 18:16

Matrix Spike (6020834-MS1)


QC Source Sample: Ex Sidewall E (A6B0900-21)

Xylenes, total

2.16

---

0.0538

mg/kg dry

"

2.13

ND

102

"

---

---

Naphthalene

0.697

---

0.0717

"

"

0.710

ND

98

"

---

---

Methyl tert-butyl ether


(MTBE)
Isopropylbenzene

0.644

---

0.0358

"

"

"

ND

91

"

---

---

0.775

---

0.0358

"

"

"

ND

109

"

---

---

n-Propylbenzene

0.652

---

0.0179

"

"

"

ND

92

"

---

---

1,2,4-Trimethylbenzene

0.721

---

0.0358

"

"

"

ND

102

"

---

---

1,3,5-Trimethylbenzene

0.738

---

0.0358

"

"

"

ND

104

"

---

---

1,2-Dibromoethane (EDB)

0.746

---

0.0179

"

"

"

ND

105

"

---

---

1,2-Dichloroethane (EDC)

0.616

---

0.0179

"

"

"

ND

87

"

---

---

Surr: Dibromofluoromethane (Surr)

Recovery: 96 %

Limits: 70-130 %

Dilution: 1x

1,4-Difluorobenzene (Surr)

91 %

70-130 %

"

Toluene-d8 (Surr)

96 %

70-130 %

"

4-Bromofluorobenzene (Surr)

99 %

70-130 %

"

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 44 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

QUALITY CONTROL (QC) SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

RPD
Limit

Notes

Soil

Batch 6020836 - EPA 3546 (Fuels)

Prepared: 02/27/16 10:02 Analyzed: 02/27/16 12:43

Blank (6020836-BLK2)
EPA 8270D (SIM)

Acenaphthene

ND

---

0.00833

mg/kg wet

---

---

---

---

---

---

Acenaphthylene

ND

---

0.00833

"

"

---

---

---

---

---

---

Anthracene

ND

---

0.00833

"

"

---

---

---

---

---

---

Benz(a)anthracene

ND

---

0.00833

"

"

---

---

---

---

---

---

Benzo(a)pyrene

ND

---

0.00833

"

"

---

---

---

---

---

---

Benzo(b)fluoranthene

ND

---

0.00833

"

"

---

---

---

---

---

---

Benzo(k)fluoranthene

ND

---

0.00833

"

"

---

---

---

---

---

---

Benzo(g,h,i)perylene

ND

---

0.00833

"

"

---

---

---

---

---

---

Chrysene

ND

---

0.00833

"

"

---

---

---

---

---

---

Dibenz(a,h)anthracene

ND

---

0.00833

"

"

---

---

---

---

---

---

Dibenzofuran

ND

---

0.00833

"

"

---

---

---

---

---

---

Fluoranthene

ND

---

0.00833

"

"

---

---

---

---

---

---

Fluorene

ND

---

0.00833

"

"

---

---

---

---

---

---

Indeno(1,2,3-cd)pyrene

ND

---

0.00833

"

"

---

---

---

---

---

---

1-Methylnaphthalene

ND

---

0.00833

"

"

---

---

---

---

---

---

2-Methylnaphthalene

ND

---

0.00833

"

"

---

---

---

---

---

---

Naphthalene

ND

---

0.00833

"

"

---

---

---

---

---

---

Phenanthrene

ND

---

0.00833

"

"

---

---

---

---

---

---

Pyrene

ND

---

0.00833

"

"

---

---

---

---

---

---

Surr: 2-Fluorobiphenyl (Surr)

Recovery: 91 %

Limits: 44-115 %

Dilution: 1x

104 %

54-127 %

"

p-Terphenyl-d14 (Surr)

Prepared: 02/27/16 10:02 Analyzed: 02/27/16 13:10

LCS (6020836-BS2)
EPA 8270D (SIM)

Acenaphthene

0.718

---

0.0100

mg/kg wet

0.800

---

90

40-122%

---

---

Acenaphthylene

0.709

---

0.0100

"

"

"

---

89

32-132%

---

---

Anthracene

0.771

---

0.0100

"

"

"

---

96

47-123%

---

---

Benz(a)anthracene

0.701

---

0.0100

"

"

"

---

88

49-126%

---

---

Benzo(a)pyrene

0.727

---

0.0100

"

"

"

---

91

45-129%

---

---

Benzo(b)fluoranthene

0.729

---

0.0100

"

"

"

---

91

45-132%

---

---

Benzo(k)fluoranthene

0.731

---

0.0100

"

"

"

---

91

47-132%

---

---

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 45 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

QUALITY CONTROL (QC) SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

%REC

%REC
Limits RPD

RPD
Limit

Notes

Soil

Batch 6020836 - EPA 3546 (Fuels)

Prepared: 02/27/16 10:02 Analyzed: 02/27/16 13:10

LCS (6020836-BS2)

Benzo(g,h,i)perylene

Source
Result

0.657

---

0.0100

"

"

"

---

82

43-134%

---

---

Chrysene

0.698

---

0.0100

"

"

"

---

87

50-124%

---

---

Dibenz(a,h)anthracene

0.691

---

0.0100

"

"

"

---

86

45-134%

---

---

Dibenzofuran

0.721

---

0.0100

"

"

"

---

90

44-120%

---

---

Fluoranthene

0.708

---

0.0100

"

"

"

---

89

50-127%

---

---

Fluorene

0.719

---

0.0100

"

"

"

---

90

43-125%

---

---

Indeno(1,2,3-cd)pyrene

0.653

---

0.0100

"

"

"

---

82

45-133%

---

---

1-Methylnaphthalene

0.677

---

0.0100

"

"

"

---

85

40-120%

---

---

2-Methylnaphthalene

0.715

---

0.0100

"

"

"

---

89

38-122%

---

---

Naphthalene

0.697

---

0.0100

"

"

"

---

87

35-123%

---

---

Phenanthrene

0.722

---

0.0100

"

"

"

---

90

50-121%

---

---

Pyrene

0.719

---

0.0100

"

"

"

---

90

47-127%

---

---

Surr: 2-Fluorobiphenyl (Surr)

Recovery: 92 %

Limits: 44-115 %

Dilution: 1x

101 %

54-127 %

"

p-Terphenyl-d14 (Surr)

Prepared: 02/27/16 10:02 Analyzed: 02/27/16 14:32

Duplicate (6020836-DUP3)
QC Source Sample: 1A (A6B0900-01)
EPA 8270D (SIM)

Acenaphthene

ND

---

0.0134

mg/kg dry

---

ND

---

---

---

30%

Acenaphthylene

ND

---

0.0134

"

"

---

ND

---

---

---

30%

Anthracene

ND

---

0.0134

"

"

---

ND

---

---

---

30%

Benz(a)anthracene

ND

---

0.0134

"

"

---

ND

---

---

---

30%

Benzo(a)pyrene

ND

---

0.0134

"

"

---

ND

---

---

---

30%

Benzo(b)fluoranthene

ND

---

0.0134

"

"

---

ND

---

---

---

30%

Benzo(k)fluoranthene

ND

---

0.0134

"

"

---

ND

---

---

---

30%

Benzo(g,h,i)perylene

ND

---

0.0134

"

"

---

ND

---

---

---

30%

Chrysene

ND

---

0.0134

"

"

---

ND

---

---

---

30%

Dibenz(a,h)anthracene

ND

---

0.0134

"

"

---

ND

---

---

---

30%

Dibenzofuran

ND

---

0.0134

"

"

---

ND

---

---

---

30%

Fluoranthene

ND

---

0.0134

"

"

---

ND

---

---

---

30%

Fluorene

ND

---

0.0134

"

"

---

ND

---

---

---

30%

Indeno(1,2,3-cd)pyrene

ND

---

0.0134

"

"

---

ND

---

---

---

30%

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 46 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

QUALITY CONTROL (QC) SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

RPD
Limit

Notes

Soil

Batch 6020836 - EPA 3546 (Fuels)

Prepared: 02/27/16 10:02 Analyzed: 02/27/16 14:32

Duplicate (6020836-DUP3)
QC Source Sample: 1A (A6B0900-01)

1-Methylnaphthalene

ND

---

0.0134

"

"

---

ND

---

---

---

30%

2-Methylnaphthalene

ND

---

0.0134

"

"

---

ND

---

---

---

30%

Naphthalene

ND

---

0.0134

"

"

---

ND

---

---

---

30%

Phenanthrene

ND

---

0.0134

"

"

---

ND

---

---

---

30%

Pyrene

ND

---

"

"

---

ND

---

---

---

30%

Surr: 2-Fluorobiphenyl (Surr)

0.0134
Recovery: 88 %

Limits: 44-115 %

Dilution: 1x

106 %

54-127 %

"

p-Terphenyl-d14 (Surr)

Prepared: 02/27/16 10:02 Analyzed: 02/27/16 17:43

Duplicate (6020836-DUP4)
QC Source Sample: 3C (A6B0900-10)
EPA 8270D (SIM)

Acenaphthene

ND

---

0.0137

mg/kg dry

---

ND

---

---

---

30%

Acenaphthylene

ND

---

0.0137

"

"

---

ND

---

---

---

30%

Anthracene

ND

---

0.0137

"

"

---

ND

---

---

---

30%

Benz(a)anthracene

ND

---

0.0137

"

"

---

ND

---

---

---

30%

Benzo(a)pyrene

ND

---

0.0137

"

"

---

ND

---

---

---

30%

Benzo(b)fluoranthene

ND

---

0.0137

"

"

---

ND

---

---

---

30%

Benzo(k)fluoranthene

ND

---

0.0137

"

"

---

ND

---

---

---

30%

Benzo(g,h,i)perylene

ND

---

0.0137

"

"

---

ND

---

---

---

30%

Chrysene

ND

---

0.0137

"

"

---

ND

---

---

---

30%

Dibenz(a,h)anthracene

ND

---

0.0137

"

"

---

ND

---

---

---

30%

Dibenzofuran

ND

---

0.0137

"

"

---

ND

---

---

---

30%

Fluoranthene

ND

---

0.0137

"

"

---

ND

---

---

---

30%

Fluorene

ND

---

0.0137

"

"

---

ND

---

---

---

30%

Indeno(1,2,3-cd)pyrene

ND

---

0.0137

"

"

---

ND

---

---

---

30%

1-Methylnaphthalene

ND

---

0.0137

"

"

---

ND

---

---

---

30%

2-Methylnaphthalene

ND

---

0.0137

"

"

---

ND

---

---

---

30%

Naphthalene

ND

---

0.0137

"

"

---

ND

---

---

---

30%

Phenanthrene

ND

---

0.0137

"

"

---

ND

---

---

---

30%

Pyrene

ND

---

0.0137

"

"

---

ND

---

---

---

30%

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 47 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

QUALITY CONTROL (QC) SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

RPD
Limit

Notes

Soil

Batch 6020836 - EPA 3546 (Fuels)

Prepared: 02/27/16 10:02 Analyzed: 02/27/16 17:43

Duplicate (6020836-DUP4)
QC Source Sample: 3C (A6B0900-10)
Surr: 2-Fluorobiphenyl (Surr)

Recovery: 88 %

Limits: 44-115 %

Dilution: 1x

108 %

54-127 %

"

p-Terphenyl-d14 (Surr)

Prepared: 02/27/16 10:02 Analyzed: 02/27/16 23:03

Matrix Spike (6020836-MS1)


QC Source Sample: Ex Sidewall E (A6B0900-21)
EPA 8270D (SIM)

Acenaphthene

0.751

---

0.0107

mg/kg dry

0.852

ND

88

40-122%

---

---

Acenaphthylene

0.758

---

0.0107

"

"

"

0.0181

87

32-132%

---

---

Anthracene

0.774

---

0.0107

"

"

"

0.0526

85

47-123%

---

---

Benz(a)anthracene

0.752

---

0.0107

"

"

"

0.635

14

49-126%

---

---

Benzo(a)pyrene

0.779

---

0.0107

"

"

"

0.219

66

45-129%

---

---

Benzo(b)fluoranthene

0.795

---

0.0107

"

"

"

0.603

22

45-132%

---

---

Benzo(k)fluoranthene

0.782

---

0.0107

"

"

"

0.206

68

47-132%

---

---

Benzo(g,h,i)perylene

0.580

---

0.0107

"

"

"

0.0799

59

43-134%

---

---

Chrysene

0.753

---

0.0107

"

"

"

0.947

-23

50-124%

---

---

Dibenz(a,h)anthracene

0.665

---

0.0107

"

"

"

0.0306

74

45-134%

---

---

Dibenzofuran

0.777

---

0.0107

"

"

"

0.00750

90

44-120%

---

---

Fluoranthene

0.792

---

0.0107

"

"

"

1.86

-125

50-127%

---

---

Fluorene

0.768

---

0.0107

"

"

"

ND

90

43-125%

---

---

Indeno(1,2,3-cd)pyrene

0.625

---

0.0107

"

"

"

0.116

60

45-133%

---

---

1-Methylnaphthalene

0.727

---

0.0107

"

"

"

0.00568

85

40-120%

---

---

2-Methylnaphthalene

0.765

---

0.0107

"

"

"

0.0135

88

38-122%

---

---

Naphthalene

0.724

---

0.0107

"

"

"

ND

85

35-123%

---

---

Phenanthrene

0.775

---

0.0107

"

"

"

0.0119

90

50-121%

---

---

Pyrene

0.784

---

0.0107

"

"

"

1.60

-96

47-127%

---

---

Surr: 2-Fluorobiphenyl (Surr)

Recovery: 92 %

Limits: 44-115 %

Dilution: 1x

112 %

54-127 %

"

p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Q-04

Q-04

Q-04

Q-04

Q-04

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 48 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

QUALITY CONTROL (QC) SAMPLE RESULTS


Percent Dry Weight
Analyte

Result

MDL

Reporting
Limit

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

RPD
Limit

Notes

Soil

Batch 6020837 - Total Solids (Dry Weight)

Prepared: 02/27/16 10:49 Analyzed: 02/27/16 13:34

Duplicate (6020837-DUP1)
QC Source Sample: 1A (A6B0900-01)
EPA 8000C

% Solids

52.0

---

1.00

% by
Weight

---

65.4

---

---

23

10%

10%

0.7

10%

10%

Q-04

Prepared: 02/27/16 10:49 Analyzed: 02/27/16 13:34

Duplicate (6020837-DUP2)
QC Source Sample: 3C (A6B0900-10)
EPA 8000C

% Solids

64.6

---

1.00

% by
Weight

---

67.6

---

---

Prepared: 02/27/16 10:49 Analyzed: 02/27/16 13:34

Duplicate (6020837-DUP3)
QC Source Sample: Ex Sidewall E (A6B0900-21)
EPA 8000C

% Solids

83.4

---

1.00

% by
Weight

---

82.9

---

---

Prepared: 02/27/16 13:01 Analyzed: 02/27/16 13:34

Duplicate (6020837-DUP4)
QC Source Sample: 0B (A6B0900-17)
EPA 8000C

% Solids

57.3

---

1.00

% by
Weight

---

55.4

---

---

No Client related Batch QC samples analyzed for this batch. See notes page for more information.

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 49 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

SAMPLE PREPARATION INFORMATION


Diesel and/or Oil Hydrocarbons by NWTPH-Dx
Prep: EPA 3546 (Fuels)
Lab Number

Matrix

Method

Sampled

Prepared

Sample

Default

RL Prep

Initial/Final

Initial/Final

Factor

Batch: 6020835

A6B0900-03
A6B0900-06

Soil
Soil

NWTPH-Dx
NWTPH-Dx

02/26/16 10:00
02/26/16 10:10

02/27/16 10:01
02/27/16 10:01

10.94g/5mL
11.18g/5mL

10g/5mL
10g/5mL

0.91
0.89

Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil

NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx

02/26/16 09:40
02/26/16 09:50
02/26/16 10:55
02/26/16 11:00
02/26/16 10:05
02/26/16 10:40
02/26/16 10:45
02/26/16 10:50
02/26/16 10:15
02/26/16 10:35
02/26/16 10:30
02/26/16 10:25
02/26/16 10:20
02/26/16 12:00
02/26/16 12:05
02/26/16 12:10
02/26/16 12:20
02/26/16 12:30
02/26/16 12:40

02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02

10.7g/5mL
10.83g/5mL
10.51g/5mL
11.24g/5mL
10.31g/5mL
10.74g/5mL
10.36g/5mL
10.97g/5mL
11.43g/5mL
10.38g/5mL
10.86g/5mL
10.21g/5mL
10.87g/5mL
11.77g/5mL
10.8g/5mL
10.49g/5mL
10.19g/5mL
10.53g/5mL
11.5g/5mL

10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL

0.94
0.92
0.95
0.89
0.97
0.93
0.97
0.91
0.88
0.96
0.92
0.98
0.92
0.85
0.93
0.95
0.98
0.95
0.87

Batch: 6020836

A6B0900-01
A6B0900-02
A6B0900-04
A6B0900-05
A6B0900-07
A6B0900-08
A6B0900-09
A6B0900-10
A6B0900-11
A6B0900-12
A6B0900-13
A6B0900-14RE1
A6B0900-15
A6B0900-16
A6B0900-17
A6B0900-18
A6B0900-19
A6B0900-20
A6B0900-21

RBDM Compounds (BTEX+) by EPA 8260B


Prep: EPA 5035A
Lab Number

Matrix

Method

Sampled

Prepared

02/26/16 09:40
02/26/16 09:50
02/26/16 10:55
02/26/16 11:00
02/26/16 10:05
02/26/16 10:40

02/26/16 09:40
02/26/16 09:50
02/26/16 10:55
02/26/16 11:00
02/26/16 10:05
02/26/16 10:40

Sample

Default

RL Prep

Initial/Final

Initial/Final

Factor

Batch: 6020833

A6B0900-01
A6B0900-02
A6B0900-04
A6B0900-05
A6B0900-07
A6B0900-08

Soil
Soil
Soil
Soil
Soil
Soil

5035/8260B
5035/8260B
5035/8260B
5035/8260B
5035/8260B
5035/8260B

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

4.67g/5mL
4.4g/5mL
5.47g/5mL
4.01g/5mL
3.04g/5mL
4.31g/5mL

5g/5mL
5g/5mL
5g/5mL
5g/5mL
5g/5mL
5g/5mL

1.07
1.14
0.91
1.25
1.64
1.16

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 50 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

SAMPLE PREPARATION INFORMATION


RBDM Compounds (BTEX+) by EPA 8260B
Sample

Default

RL Prep

Initial/Final

Initial/Final

Factor

Prep: EPA 5035A


Lab Number

A6B0900-09
A6B0900-10
A6B0900-11
A6B0900-12
A6B0900-13

Matrix

Method

Sampled

Prepared

Soil
Soil
Soil
Soil
Soil

5035/8260B
5035/8260B
5035/8260B
5035/8260B
5035/8260B

02/26/16 10:45
02/26/16 10:50
02/26/16 10:15
02/26/16 10:35
02/26/16 10:30

02/26/16 10:45
02/26/16 10:50
02/26/16 10:15
02/26/16 10:35
02/26/16 10:30

5.25g/5mL
6.83g/5mL
5.61g/5mL
5.14g/5mL
5.22g/5mL

5g/5mL
5g/5mL
5g/5mL
5g/5mL
5g/5mL

0.95
0.73
0.89
0.97
0.96

Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil

5035/8260B
5035/8260B
5035/8260B
5035/8260B
5035/8260B
5035/8260B
5035/8260B
5035/8260B

02/26/16 10:25
02/26/16 10:20
02/26/16 12:00
02/26/16 12:05
02/26/16 12:10
02/26/16 12:20
02/26/16 12:30
02/26/16 12:40

02/26/16 10:25
02/26/16 10:20
02/26/16 12:00
02/26/16 12:05
02/26/16 12:10
02/26/16 12:20
02/26/16 12:30
02/26/16 12:40

7.9g/5mL
9.59g/5mL
4.61g/5mL
4.71g/5mL
4.05g/5mL
7.98g/5mL
9.02g/5mL
11.83g/5mL

5g/5mL
5g/5mL
5g/5mL
5g/5mL
5g/5mL
5g/5mL
5g/5mL
5g/5mL

0.63
0.52
1.08
1.06
1.23
0.63
0.55
0.42

Batch: 6020834

A6B0900-14
A6B0900-15
A6B0900-16
A6B0900-17
A6B0900-18
A6B0900-19
A6B0900-20
A6B0900-21

Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM


Prep: EPA 3546 (Fuels)
Lab Number

Matrix

Method

Sampled

Prepared

02/26/16 09:40
02/26/16 09:50
02/26/16 10:55
02/26/16 11:00
02/26/16 10:05
02/26/16 10:40
02/26/16 10:45
02/26/16 10:50
02/26/16 10:15
02/26/16 10:35
02/26/16 10:30
02/26/16 10:25
02/26/16 10:20
02/26/16 12:00
02/26/16 12:05

02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02

Sample

Default

RL Prep

Initial/Final

Initial/Final

Factor

Batch: 6020836

A6B0900-01
A6B0900-02
A6B0900-04
A6B0900-05
A6B0900-07
A6B0900-08
A6B0900-09
A6B0900-10
A6B0900-11
A6B0900-12
A6B0900-13
A6B0900-14
A6B0900-15
A6B0900-16
A6B0900-17

Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil

EPA 8270D (SIM)


EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

10.7g/5mL
10.83g/5mL
10.51g/5mL
11.24g/5mL
10.31g/5mL
10.74g/5mL
10.36g/5mL
10.97g/5mL
11.43g/5mL
10.38g/5mL
10.86g/5mL
10.21g/5mL
10.87g/5mL
11.77g/5mL
10.8g/5mL

10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL
10g/5mL

0.94
0.92
0.95
0.89
0.97
0.93
0.97
0.91
0.88
0.96
0.92
0.98
0.92
0.85
0.93

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 51 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

SAMPLE PREPARATION INFORMATION


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Prep: EPA 3546 (Fuels)
Lab Number

A6B0900-18
A6B0900-19
A6B0900-20
A6B0900-21

Matrix

Soil
Soil
Soil
Soil

Method

EPA 8270D (SIM)


EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)

Sampled

Prepared

02/26/16 12:10
02/26/16 12:20
02/26/16 12:30
02/26/16 12:40

02/27/16 10:02
02/27/16 10:02
02/27/16 10:02
02/27/16 10:02

Sample

Default

RL Prep

Initial/Final

Initial/Final

Factor

10.49g/5mL
10.19g/5mL
10.53g/5mL
11.5g/5mL

10g/5mL
10g/5mL
10g/5mL
10g/5mL

0.95
0.98
0.95
0.87

Percent Dry Weight


Prep: Total Solids (Dry Weight)
Lab Number

Matrix

Method

Sampled

Prepared

02/26/16 09:40
02/26/16 09:50
02/26/16 10:00
02/26/16 10:55
02/26/16 11:00
02/26/16 10:10
02/26/16 10:05
02/26/16 10:40
02/26/16 10:45
02/26/16 10:50
02/26/16 10:15
02/26/16 10:35
02/26/16 10:30
02/26/16 10:25
02/26/16 10:20
02/26/16 12:00
02/26/16 12:05
02/26/16 12:10
02/26/16 12:20
02/26/16 12:30
02/26/16 12:40

02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49
02/27/16 10:49

Sample

Default

RL Prep

Initial/Final

Initial/Final

Factor

Batch: 6020837

A6B0900-01
A6B0900-02
A6B0900-03
A6B0900-04
A6B0900-05
A6B0900-06
A6B0900-07
A6B0900-08
A6B0900-09
A6B0900-10
A6B0900-11
A6B0900-12
A6B0900-13
A6B0900-14
A6B0900-15
A6B0900-16
A6B0900-17
A6B0900-18
A6B0900-19
A6B0900-20
A6B0900-21

Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil
Soil

EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C
EPA 8000C

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A

1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A
1N/A/1N/A

NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 52 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/28/16 12:19

Notes and Definitions


Qualifiers:
F-17

No fuel pattern detected. The Diesel result represents carbon range C12 to C24, and the Oil result represents >C24 to C40.

M-02

Due to matrix interference, this analyte cannot be accurately quantified. The reported result is estimated.

M-04

Due to matrix interference, this analyte cannot be accurately quantified. The reported result may contain a high bias.

Q-04

Spike recovery and/or RPD is outside control limits due to a non-homogeneous sample matrix.

Q-05

Analyses are not controlled on RPD values from sample and duplicate concentrations are below 5 times the reporting level.

Q-42

Matrix Spike and/or Duplicate analysis was performed on this sample. % Recovery or RPD for this analyte is outside laboratory control
limits. (Refer to the QC Section of Analytical Report.)

R-02

The Reporting Limit for this analyte has been raised to account for interference from coeluting organic compounds present in the sample.

S-01

Surrogate recovery for this sample is not available due to sample dilution required from high analyte concentration and/or matrix
interference.

S-05

Surrogate recovery is estimated due to sample dilution required for high analyte concentration and/or matrix interference.

Notes and Conventions:


DET

Analyte DETECTED

ND

Analyte NOT DETECTED at or above the reporting limit

NR

Not Reported

dry

Sample results reported on a dry weight basis. Results listed as 'wet' or without 'dry'designation are not dry weight corrected.

RPD

Relative Percent Difference

MDL

If MDL is not listed, data has been evaluated to the Method Reporting Limit only.

WMSC

Water Miscible Solvent Correction has been applied to Results and MRLs for volatiles soil samples per EPA 8000C.

Batch
QC

Unless specifically requested, this report contains only results for Batch QC derived from client samples included in this report. All
analyses were performed with the appropriate Batch QC (including Sample Duplicates, Matrix Spikes and/or Matrix Spike Duplicates) in
order to meet or exceed method and regulatory requirements. Any exceptions to this will be qualified in this report. Complete Batch QC
results are available upon request. In cases where there is insufficient sample provided for Sample Duplicates and/or Matrix Spikes, a
Lab Control Sample Duplicate (LCS Dup) is analyzed to demonstrate accuracy and precision of the extraction and analysis.

Blank
Policy

Apex assesses blank data for potential high bias down to a level equal to the method reporting limit (MRL), except for conventional
chemistry and HCID analyses which are assessed only to the MRL. Sample results flagged with a B or B-02 qualifier are potentially
biased high if they are less than ten times the level found in the blank for inorganic analyses or less than five times the level found in the
blank for organic analyses.
For accurate comparison of volatile results to the level found in the blank; water sample results should be divided by the dilution factor,
and soil sample results should be divided by 1/50 of the sample dilution to account for the sample prep factor.
Results qualified as reported below the MRL may include a potential high bias if associated with a B or B-02 qualified blank. B and B-02
qualifications are not applied to J qualified results reported below the MRL.

---

QC results are not applicable. For example, % Recoveries for Blanks and Duplicates, % RPD for Blanks, Blank Spikes and Matrix
Spikes, etc.

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 53 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
NRC-CB&I

Project: AT&T Hall Ridge

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

***

Reported:

02/28/16 12:19

Used to indicate a possible discrepancy with the Sample and Sample Duplicate results when the %RPD is not available. In this case,
either the Sample or the Sample Duplicate has a reportable result for this analyte, while the other is Non Detect (ND).

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 54 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
NRC-CB&I

Project: AT&T Hall Ridge

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Reported:

02/28/16 12:19

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 55 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
NRC-CB&I

Project: AT&T Hall Ridge

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Reported:

02/28/16 12:19

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 56 of 57

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
NRC-CB&I

Project: AT&T Hall Ridge

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Reported:

02/28/16 12:19

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 57 of 57

Apex Labs

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Sunday, February 21, 2016


Ron Malec
NRC-CB&I
6211 N Ensign St
Portland, OR 97217

RE: AT&T Hall Ridge / [none]


Enclosed are the results of analyses for work order A6B0661, which was received by the laboratory on
2/19/2016 at 9:30:00AM.
Thank you for using Apex Labs. We appreciate your business and strive to provide the highest quality
services to the environmental industry.
If you have any questions concerning this report or the services we offer , please feel free to contact me by
email at: dthomas@apex-labs.com, or by phone at 503-718-2323.

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 1 of 18

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: [none]

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/21/16 15:02

ANALYTICAL REPORT FOR SAMPLES


SAMPLE INFORMATION
Sample ID

Laboratory ID

Matrix

Date Sampled

Date Received

SW-01

A6B0661-01
A6B0661-02
A6B0661-03
A6B0661-04

Water
Water
Water
Water

02/19/16 07:00
02/19/16 07:30
02/19/16 08:00
02/19/16 08:30

02/19/16 09:30
02/19/16 09:30
02/19/16 09:30
02/19/16 09:30

SW-02
SW-03
SW-04

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 2 of 18

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: [none]

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/21/16 15:02

ANALYTICAL SAMPLE RESULTS


Diesel and/or Oil Hydrocarbons by NWTPH-Dx
Analyte

Result

MDL

SW-01 (A6B0661-01)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Diesel

ND

104

208

ug/L

2.5

02/19/16 23:07

NWTPH-Dx

Oil

ND

208

417

"

"

"

"

"

"

"

Surrogate: o-Terphenyl (Surr)

Recovery: 84 %

SW-02 (A6B0661-02)

Limits: 50-150 %

Matrix: Water

Batch: 6020602

Diesel

ND

104

208

ug/L

2.5

02/19/16 23:29

NWTPH-Dx

Oil

ND

208

417

"

"

"

"

"

"

"

Surrogate: o-Terphenyl (Surr)

Recovery: 85 %

SW-03 (A6B0661-03)

Limits: 50-150 %

Matrix: Water

Diesel

ND

100

Oil

ND

200

Surrogate: o-Terphenyl (Surr)

200
400
Recovery: 83 %

SW-04 (A6B0661-04)

Batch: 6020602

ug/L

2.5

02/19/16 23:51

NWTPH-Dx

"

"

"

"

"

"

"

Limits: 50-150 %

Matrix: Water

Batch: 6020602

Diesel

ND

97.1

194

ug/L

2.5

02/20/16 00:13

NWTPH-Dx

Oil

ND

194

388

"

"

"

"

"

"

"

Surrogate: o-Terphenyl (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Recovery: 90 %

Notes

Batch: 6020602

Limits: 50-150 %

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 3 of 18

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: [none]

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/21/16 15:02

ANALYTICAL SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Result

Analyte

MDL

SW-01 (A6B0661-01)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Benzene

ND

0.100

0.200

ug/L

02/19/16 14:00

EPA 8260B

Toluene

ND

0.500

1.00

"

"

"

"

Ethylbenzene

ND

0.250

0.500

"

"

"

"

Xylenes, total

ND

0.750

1.50

"

"

"

"

Naphthalene

ND

1.00

2.00

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

0.500

1.00

"

"

"

"

Isopropylbenzene

ND

0.500

1.00

"

"

"

"

n-Propylbenzene

ND

0.250

0.500

"

"

"

"

1,2,4-Trimethylbenzene

ND

0.500

1.00

"

"

"

"

1,3,5-Trimethylbenzene

ND

0.500

1.00

"

"

"

"

1,2-Dibromoethane (EDB)

ND

0.250

0.500

"

"

"

"

1,2-Dichloroethane (EDC)

ND

0.250

0.500

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 99 %

Limits: 80-120 %

"

"

"

1,4-Difluorobenzene (Surr)

99 %

Limits: 80-120 %

"

"

"

Toluene-d8 (Surr)

97 %

Limits: 80-120 %

"

"

"

4-Bromofluorobenzene (Surr)

95 %

Limits: 80-120 %

"

"

"

SW-02 (A6B0661-02)

Matrix: Water

Batch: 6020583

Benzene

ND

0.100

0.200

ug/L

02/19/16 14:28

EPA 8260B

Toluene

ND

0.500

1.00

"

"

"

"

Ethylbenzene

ND

0.250

0.500

"

"

"

"

Xylenes, total

ND

0.750

1.50

"

"

"

"

Naphthalene

ND

1.00

2.00

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

0.500

1.00

"

"

"

"

Isopropylbenzene

ND

0.500

1.00

"

"

"

"

n-Propylbenzene

ND

0.250

0.500

"

"

"

"

1,2,4-Trimethylbenzene

ND

0.500

1.00

"

"

"

"

1,3,5-Trimethylbenzene

ND

0.500

1.00

"

"

"

"

1,2-Dibromoethane (EDB)

ND

0.250

0.500

"

"

"

"

1,2-Dichloroethane (EDC)

ND

0.250

0.500

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 100 %

Limits: 80-120 %

"

"

"

100 %

Limits: 80-120 %

"

"

"

Toluene-d8 (Surr)

97 %

Limits: 80-120 %

"

"

"

4-Bromofluorobenzene (Surr)

96 %

Limits: 80-120 %

"

"

"

02/19/16 14:57

EPA 8260B

1,4-Difluorobenzene (Surr)

SW-03 (A6B0661-03)

Benzene

Matrix: Water

ND

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

0.100

0.200

Notes

Batch: 6020583

Batch: 6020583

ug/L

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 4 of 18

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: [none]

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/21/16 15:02

ANALYTICAL SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Result

Analyte

MDL

SW-03 (A6B0661-03)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Toluene

ND

0.500

1.00

ug/L

"

EPA 8260B

Ethylbenzene

ND

0.250

0.500

"

"

"

"

Xylenes, total

ND

0.750

1.50

"

"

"

"

Naphthalene

ND

1.00

2.00

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

0.500

1.00

"

"

"

"

Isopropylbenzene

ND

0.500

1.00

"

"

"

"

n-Propylbenzene

ND

0.250

0.500

"

"

"

"

1,2,4-Trimethylbenzene

ND

0.500

1.00

"

"

"

"

1,3,5-Trimethylbenzene

ND

0.500

1.00

"

"

"

"

1,2-Dibromoethane (EDB)

ND

0.250

0.500

"

"

"

"

1,2-Dichloroethane (EDC)

ND

0.250

0.500

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 99 %

Limits: 80-120 %

"

"

"

1,4-Difluorobenzene (Surr)

99 %

Limits: 80-120 %

"

"

"

Toluene-d8 (Surr)

95 %

Limits: 80-120 %

"

"

"

4-Bromofluorobenzene (Surr)

97 %

Limits: 80-120 %

"

"

"

SW-04 (A6B0661-04)

Matrix: Water

Batch: 6020583

Benzene

ND

0.100

0.200

ug/L

02/19/16 15:26

EPA 8260B

Toluene

ND

0.500

1.00

"

"

"

"

Ethylbenzene

ND

0.250

0.500

"

"

"

"

Xylenes, total

ND

0.750

1.50

"

"

"

"

Naphthalene

ND

1.00

2.00

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

0.500

1.00

"

"

"

"

Isopropylbenzene

ND

0.500

1.00

"

"

"

"

n-Propylbenzene

ND

0.250

0.500

"

"

"

"

1,2,4-Trimethylbenzene

ND

0.500

1.00

"

"

"

"

1,3,5-Trimethylbenzene

ND

0.500

1.00

"

"

"

"

1,2-Dibromoethane (EDB)

ND

0.250

0.500

"

"

"

"

1,2-Dichloroethane (EDC)

ND

0.250

0.500

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 102 %

Limits: 80-120 %

"

"

"

101 %

Limits: 80-120 %

"

"

"

Toluene-d8 (Surr)

96 %

Limits: 80-120 %

"

"

"

4-Bromofluorobenzene (Surr)

96 %

Limits: 80-120 %

"

"

"

1,4-Difluorobenzene (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020583

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 5 of 18

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: [none]

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/21/16 15:02

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

SW-01 (A6B0661-01)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Acenaphthene

ND

0.0208

0.0417

ug/L

02/19/16 18:13

EPA 8270D (SIM)

Acenaphthylene

ND

0.0208

0.0417

"

"

"

"

Anthracene

ND

0.0208

0.0417

"

"

"

"

Benz(a)anthracene

ND

0.0208

0.0417

"

"

"

"

Benzo(a)pyrene

ND

0.0208

0.0417

"

"

"

"

Benzo(b)fluoranthene

ND

0.0208

0.0417

"

"

"

"

Benzo(k)fluoranthene

ND

0.0208

0.0417

"

"

"

"

Benzo(g,h,i)perylene

ND

0.0208

0.0417

"

"

"

"

Chrysene

ND

0.0208

0.0417

"

"

"

"

Dibenz(a,h)anthracene

ND

0.0208

0.0417

"

"

"

"

Dibenzofuran

ND

0.0208

0.0417

"

"

"

"

Fluoranthene

ND

0.0208

0.0417

"

"

"

"

Fluorene

ND

0.0208

0.0417

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

0.0208

0.0417

"

"

"

"

1-Methylnaphthalene

ND

0.0417

0.0833

"

"

"

"

2-Methylnaphthalene

ND

0.0417

0.0833

"

"

"

"

Naphthalene

ND

0.0417

0.0833

"

"

"

"

Phenanthrene

ND

0.0208

0.0417

"

"

"

"

Pyrene

ND

0.0208

0.0417

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020602

Recovery: 54 %

Limits: 44-120 %

"

"

"

96 %

Limits: 50-133 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 6 of 18

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: [none]

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/21/16 15:02

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

SW-02 (A6B0661-02)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Acenaphthene

ND

0.0208

0.0417

ug/L

02/19/16 18:39

EPA 8270D (SIM)

Acenaphthylene

ND

0.0208

0.0417

"

"

"

"

Anthracene

ND

0.0208

0.0417

"

"

"

"

Benz(a)anthracene

ND

0.0208

0.0417

"

"

"

"

Benzo(a)pyrene

ND

0.0208

0.0417

"

"

"

"

Benzo(b)fluoranthene

ND

0.0208

0.0417

"

"

"

"

Benzo(k)fluoranthene

ND

0.0208

0.0417

"

"

"

"

Benzo(g,h,i)perylene

ND

0.0208

0.0417

"

"

"

"

Chrysene

ND

0.0208

0.0417

"

"

"

"

Dibenz(a,h)anthracene

ND

0.0208

0.0417

"

"

"

"

Dibenzofuran

ND

0.0208

0.0417

"

"

"

"

Fluoranthene

ND

0.0208

0.0417

"

"

"

"

Fluorene

ND

0.0208

0.0417

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

0.0208

0.0417

"

"

"

"

1-Methylnaphthalene

ND

0.0417

0.0833

"

"

"

"

2-Methylnaphthalene

ND

0.0417

0.0833

"

"

"

"

Naphthalene

ND

0.0417

0.0833

"

"

"

"

Phenanthrene

ND

0.0208

0.0417

"

"

"

"

Pyrene

ND

0.0208

0.0417

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020602

Recovery: 61 %

Limits: 44-120 %

"

"

"

95 %

Limits: 50-133 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 7 of 18

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: [none]

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/21/16 15:02

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

SW-03 (A6B0661-03)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Acenaphthene

ND

0.0200

0.0400

ug/L

02/19/16 19:06

EPA 8270D (SIM)

Acenaphthylene

ND

0.0200

0.0400

"

"

"

"

Anthracene

ND

0.0200

0.0400

"

"

"

"

Benz(a)anthracene

ND

0.0200

0.0400

"

"

"

"

Benzo(a)pyrene

ND

0.0200

0.0400

"

"

"

"

Benzo(b)fluoranthene

ND

0.0200

0.0400

"

"

"

"

Benzo(k)fluoranthene

ND

0.0200

0.0400

"

"

"

"

Benzo(g,h,i)perylene

ND

0.0200

0.0400

"

"

"

"

Chrysene

ND

0.0200

0.0400

"

"

"

"

Dibenz(a,h)anthracene

ND

0.0200

0.0400

"

"

"

"

Dibenzofuran

ND

0.0200

0.0400

"

"

"

"

Fluoranthene

ND

0.0200

0.0400

"

"

"

"

Fluorene

ND

0.0200

0.0400

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

0.0200

0.0400

"

"

"

"

1-Methylnaphthalene

ND

0.0400

0.0800

"

"

"

"

2-Methylnaphthalene

ND

0.0400

0.0800

"

"

"

"

Naphthalene

ND

0.0400

0.0800

"

"

"

"

Phenanthrene

ND

0.0200

0.0400

"

"

"

"

Pyrene

ND

0.0200

0.0400

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020602

Recovery: 52 %

Limits: 44-120 %

"

"

"

93 %

Limits: 50-133 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 8 of 18

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: [none]

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/21/16 15:02

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

SW-04 (A6B0661-04)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Acenaphthene

ND

0.0194

0.0388

ug/L

02/19/16 19:32

EPA 8270D (SIM)

Acenaphthylene

ND

0.0194

0.0388

"

"

"

"

Anthracene

ND

0.0194

0.0388

"

"

"

"

Benz(a)anthracene

ND

0.0194

0.0388

"

"

"

"

Benzo(a)pyrene

ND

0.0194

0.0388

"

"

"

"

Benzo(b)fluoranthene

ND

0.0194

0.0388

"

"

"

"

Benzo(k)fluoranthene

ND

0.0194

0.0388

"

"

"

"

Benzo(g,h,i)perylene

ND

0.0194

0.0388

"

"

"

"

Chrysene

ND

0.0194

0.0388

"

"

"

"

Dibenz(a,h)anthracene

ND

0.0194

0.0388

"

"

"

"

Dibenzofuran

ND

0.0194

0.0388

"

"

"

"

Fluoranthene

ND

0.0194

0.0388

"

"

"

"

Fluorene

ND

0.0194

0.0388

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

0.0194

0.0388

"

"

"

"

1-Methylnaphthalene

ND

0.0388

0.0777

"

"

"

"

2-Methylnaphthalene

ND

0.0388

0.0777

"

"

"

"

Naphthalene

ND

0.0388

0.0777

"

"

"

"

Phenanthrene

ND

0.0194

0.0388

"

"

"

"

Pyrene

ND

0.0194

0.0388

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020602

Recovery: 81 %

Limits: 44-120 %

"

"

"

99 %

Limits: 50-133 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 9 of 18

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: [none]

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/21/16 15:02

QUALITY CONTROL (QC) SAMPLE RESULTS


Diesel and/or Oil Hydrocarbons by NWTPH-Dx
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

RPD
Limit

Notes

Water

Batch 6020602 - EPA 3510C (Acid Extraction)

Prepared: 02/19/16 12:32 Analyzed: 02/19/16 22:01

Blank (6020602-BLK2)
NWTPH-Dx

Diesel

ND

90.9

182

ug/L

2.5

---

---

---

---

---

---

Oil

ND

182

364

"

"

---

---

---

---

---

---

---

---

Surr: o-Terphenyl (Surr)

Recovery: 88 %

Limits: 50-150 %

Dilution: 2.5x

Prepared: 02/19/16 12:32 Analyzed: 02/19/16 22:23

LCS (6020602-BS2)
NWTPH-Dx

Diesel

991

Surr: o-Terphenyl (Surr)

100

200

Recovery: 90 %

ug/L

2.5

Limits: 50-150 %

1250

---

79

58-115%

Dilution: 2.5x

Prepared: 02/19/16 12:32 Analyzed: 02/19/16 22:45

LCS Dup (6020602-BSD2)

Q-19

NWTPH-Dx

Diesel
Surr: o-Terphenyl (Surr)

1060

100

200

Recovery: 93 %

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

ug/L

2.5

Limits: 50-150 %

1250

---

84

58-115%

20%

Dilution: 2.5x

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 10 of 18

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: [none]

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/21/16 15:02

QUALITY CONTROL (QC) SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

RPD
Limit

Notes

Water

Batch 6020583 - EPA 5030B

Prepared: 02/19/16 10:11 Analyzed: 02/19/16 12:34

Blank (6020583-BLK1)
EPA 8260B

Benzene

ND

0.100

0.200

ug/L

---

---

---

---

---

---

Toluene

ND

0.500

1.00

"

"

---

---

---

---

---

---

Ethylbenzene

ND

0.250

0.500

"

"

---

---

---

---

---

---

Xylenes, total

ND

0.750

1.50

"

"

---

---

---

---

---

---

Naphthalene

ND

1.00

2.00

"

"

---

---

---

---

---

---

Methyl tert-butyl ether


(MTBE)
Isopropylbenzene

ND

0.500

1.00

"

"

---

---

---

---

---

---

ND

0.500

1.00

"

"

---

---

---

---

---

---

n-Propylbenzene

ND

0.250

0.500

"

"

---

---

---

---

---

---

1,2,4-Trimethylbenzene

ND

0.500

1.00

"

"

---

---

---

---

---

---

1,3,5-Trimethylbenzene

ND

0.500

1.00

"

"

---

---

---

---

---

---

1,2-Dibromoethane (EDB)

ND

0.250

0.500

"

"

---

---

---

---

---

---

1,2-Dichloroethane (EDC)

ND

0.250

0.500

"

"

---

---

---

---

---

---

---

---

Surr: Dibromofluoromethane (Surr)

Recovery: 97 %

Limits: 80-120 %

Dilution: 1x

1,4-Difluorobenzene (Surr)

98 %

80-120 %

"

Toluene-d8 (Surr)

97 %

80-120 %

"

4-Bromofluorobenzene (Surr)

97 %

80-120 %

"

Prepared: 02/19/16 10:11 Analyzed: 02/19/16 11:37

LCS (6020583-BS1)
EPA 8260B

Benzene

19.6

0.100

0.200

ug/L

20.0

---

98

70-130%

Toluene

20.3

0.500

1.00

"

"

"

---

102

"

---

---

Ethylbenzene

20.7

0.250

0.500

"

"

"

---

103

"

---

---

Xylenes, total

62.4

0.750

1.50

"

"

60.0

---

104

"

---

---

Naphthalene

18.5

1.00

2.00

"

"

20.0

---

93

"

---

---

Methyl tert-butyl ether


(MTBE)
Isopropylbenzene

18.8

0.500

1.00

"

"

"

---

94

"

---

---

21.8

0.500

1.00

"

"

"

---

109

"

---

---

n-Propylbenzene

20.0

0.250

0.500

"

"

"

---

100

"

---

---

1,2,4-Trimethylbenzene

20.5

0.500

1.00

"

"

"

---

103

"

---

---

1,3,5-Trimethylbenzene

20.4

0.500

1.00

"

"

"

---

102

"

---

---

1,2-Dibromoethane (EDB)

20.4

0.250

0.500

"

"

"

---

102

"

---

---

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 11 of 18

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: [none]

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/21/16 15:02

QUALITY CONTROL (QC) SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

%REC
Limits RPD

RPD
Limit

Notes

Prepared: 02/19/16 10:11 Analyzed: 02/19/16 11:37

LCS (6020583-BS1)
Surr: Dibromofluoromethane (Surr)

%REC

Water

Batch 6020583 - EPA 5030B


1,2-Dichloroethane (EDC)

Source
Result

18.4

0.250

0.500

ug/L

"

"

---

Recovery: 94 %

Limits: 80-120 %

Dilution: 1x

1,4-Difluorobenzene (Surr)

96 %

80-120 %

"

Toluene-d8 (Surr)

96 %

80-120 %

"

4-Bromofluorobenzene (Surr)

97 %

80-120 %

"

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

92

"

---

---

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 12 of 18

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: [none]

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/21/16 15:02

QUALITY CONTROL (QC) SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

RPD
Limit

Notes

Water

Batch 6020602 - EPA 3510C (Acid Extraction)

Prepared: 02/19/16 12:32 Analyzed: 02/19/16 16:54

Blank (6020602-BLK1)
EPA 8270D (SIM)

Acenaphthene

ND

0.0182

0.0364

ug/L

---

---

---

---

---

---

Acenaphthylene

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

Anthracene

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

Benz(a)anthracene

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

Benzo(a)pyrene

ND

0.0182

0.0364

"

"

---

---

---

---

---

-----

Benzo(b)fluoranthene

ND

0.0182

0.0364

"

"

---

---

---

---

---

Benzo(k)fluoranthene

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

Benzo(g,h,i)perylene

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

Chrysene

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

Dibenz(a,h)anthracene

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

Dibenzofuran

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

Fluoranthene

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

Fluorene

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

Indeno(1,2,3-cd)pyrene

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

1-Methylnaphthalene

ND

0.0364

0.0727

"

"

---

---

---

---

---

---

2-Methylnaphthalene

ND

0.0364

0.0727

"

"

---

---

---

---

---

---

Naphthalene

ND

0.0364

0.0727

"

"

---

---

---

---

---

---

Phenanthrene

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

Pyrene

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

---

Surr: 2-Fluorobiphenyl (Surr)

Recovery: 74 %

Limits: 44-120 %

Dilution: 1x

97 %

50-133 %

"

p-Terphenyl-d14 (Surr)

Prepared: 02/19/16 12:32 Analyzed: 02/19/16 17:20

LCS (6020602-BS1)
EPA 8270D (SIM)

Acenaphthene

6.61

0.0200

0.0400

ug/L

8.00

---

83

47-122%

---

Acenaphthylene

6.67

0.0200

0.0400

"

"

"

---

83

41-130%

---

---

Anthracene

7.42

0.0200

0.0400

"

"

"

---

93

57-123%

---

---

Benz(a)anthracene

7.09

0.0200

0.0400

"

"

"

---

89

58-125%

---

---

Benzo(a)pyrene

7.37

0.0200

0.0400

"

"

"

---

92

54-128%

---

---

Benzo(b)fluoranthene

7.15

0.0200

0.0400

"

"

"

---

89

53-131%

---

---

Benzo(k)fluoranthene

7.57

0.0200

0.0400

"

"

"

---

95

57-129%

---

---

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 13 of 18

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: [none]

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/21/16 15:02

QUALITY CONTROL (QC) SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

%REC

%REC
Limits RPD

RPD
Limit

Notes

Water

Batch 6020602 - EPA 3510C (Acid Extraction)

Prepared: 02/19/16 12:32 Analyzed: 02/19/16 17:20

LCS (6020602-BS1)

Benzo(g,h,i)perylene

Source
Result

6.33

0.0200

0.0400

"

"

"

---

79

50-134%

---

---

Chrysene

7.06

0.0200

0.0400

"

"

"

---

88

59-123%

---

---

Dibenz(a,h)anthracene

7.13

0.0200

0.0400

"

"

"

---

89

51-134%

---

---

Dibenzofuran

6.82

0.0200

0.0400

"

"

"

---

85

53-120%

---

---

Fluoranthene

7.26

0.0200

0.0400

"

"

"

---

91

57-128%

---

---

Fluorene

7.07

0.0200

0.0400

"

"

"

---

88

52-124%

---

---

Indeno(1,2,3-cd)pyrene

6.17

0.0200

0.0400

"

"

"

---

77

52-133%

---

---

1-Methylnaphthalene

5.76

0.0400

0.0800

"

"

"

---

72

41-120%

---

---

2-Methylnaphthalene

5.98

0.0400

0.0800

"

"

"

---

75

40-121%

---

---

Naphthalene

5.76

0.0400

0.0800

"

"

"

---

72

"

---

---

Phenanthrene

6.99

0.0200

0.0400

"

"

"

---

87

59-120%

---

---

Pyrene

7.40

0.0200

0.0400

"

"

"

---

93

57-126%

---

---

Surr: 2-Fluorobiphenyl (Surr)

Recovery: 79 %

Limits: 44-120 %

Dilution: 1x

94 %

50-133 %

"

p-Terphenyl-d14 (Surr)

Prepared: 02/19/16 12:32 Analyzed: 02/19/16 17:47

LCS Dup (6020602-BSD1)

Q-19

EPA 8270D (SIM)

Acenaphthene

6.83

0.0200

0.0400

ug/L

8.00

---

85

47-122%

30%

Acenaphthylene

6.79

0.0200

0.0400

"

"

"

---

85

41-130%

30%

Anthracene

7.61

0.0200

0.0400

"

"

"

---

95

57-123%

30%

Benz(a)anthracene

7.28

0.0200

0.0400

"

"

"

---

91

58-125%

30%

Benzo(a)pyrene

7.59

0.0200

0.0400

"

"

"

---

95

54-128%

30%

Benzo(b)fluoranthene

7.57

0.0200

0.0400

"

"

"

---

95

53-131%

30%

Benzo(k)fluoranthene

7.43

0.0200

0.0400

"

"

"

---

93

57-129%

30%

Benzo(g,h,i)perylene

6.45

0.0200

0.0400

"

"

"

---

81

50-134%

30%

Chrysene

7.30

0.0200

0.0400

"

"

"

---

91

59-123%

30%

Dibenz(a,h)anthracene

7.31

0.0200

0.0400

"

"

"

---

91

51-134%

30%

Dibenzofuran

7.06

0.0200

0.0400

"

"

"

---

88

53-120%

30%

Fluoranthene

7.45

0.0200

0.0400

"

"

"

---

93

57-128%

30%

Fluorene

7.21

0.0200

0.0400

"

"

"

---

90

52-124%

30%

Indeno(1,2,3-cd)pyrene

8.20

0.0200

0.0400

"

"

"

---

103

52-133%

28

30%

1-Methylnaphthalene

6.08

0.0400

0.0800

"

"

"

---

76

41-120%

30%

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 14 of 18

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: [none]

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/21/16 15:02

QUALITY CONTROL (QC) SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

Prepared: 02/19/16 12:32 Analyzed: 02/19/16 17:47

LCS Dup (6020602-BSD1)

Q-19

2-Methylnaphthalene

6.25

0.0400

0.0800

"

"

"

---

78

Naphthalene

5.97

0.0400

0.0800

"

"

"

---

75

Phenanthrene

7.12

0.0200

0.0400

"

"

"

---

89

Pyrene

7.53

0.0200

0.0400

"

"

"

---

94

57-126%

Recovery: 81 %

Limits: 44-120 %

Dilution: 1x

94 %

50-133 %

"

p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Water

Batch 6020602 - EPA 3510C (Acid Extraction)

Surr: 2-Fluorobiphenyl (Surr)

RPD
Limit

40-121%

30%

"

30%

59-120%

30%

30%

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 15 of 18

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: [none]

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/21/16 15:02

SAMPLE PREPARATION INFORMATION


Diesel and/or Oil Hydrocarbons by NWTPH-Dx
Sample

Default

RL Prep

Initial/Final

Initial/Final

Factor

1000mL/5mL
1000mL/5mL
1000mL/5mL
1000mL/5mL

0.42
0.42
0.40
0.39

Prep: EPA 3510C (Acid Extraction)


Lab Number

Matrix

Method

Sampled

Prepared

02/19/16 07:00
02/19/16 07:30
02/19/16 08:00
02/19/16 08:30

02/19/16 12:32
02/19/16 12:32
02/19/16 12:32
02/19/16 12:32

Batch: 6020602

A6B0661-01
A6B0661-02
A6B0661-03
A6B0661-04

Water
Water
Water
Water

NWTPH-Dx
NWTPH-Dx
NWTPH-Dx
NWTPH-Dx

960mL/2mL
960mL/2mL
1000mL/2mL
1030mL/2mL

RBDM Compounds (BTEX+) by EPA 8260B


Sample

Default

RL Prep

Initial/Final

Initial/Final

Factor

Prep: EPA 5030B


Lab Number

Matrix

Method

Sampled

Prepared

02/19/16 07:00
02/19/16 07:30
02/19/16 08:00
02/19/16 08:30

02/19/16 12:34
02/19/16 12:34
02/19/16 12:34
02/19/16 12:34

Batch: 6020583

A6B0661-01
A6B0661-02
A6B0661-03
A6B0661-04

Water
Water
Water
Water

EPA 8260B
EPA 8260B
EPA 8260B
EPA 8260B

5mL/5mL
5mL/5mL
5mL/5mL
5mL/5mL

5mL/5mL
5mL/5mL
5mL/5mL
5mL/5mL

1.00
1.00
1.00
1.00

Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM


Prep: EPA 3510C (Acid Extraction)
Lab Number

Matrix

Method

Sampled

Prepared

02/19/16 07:00
02/19/16 07:30
02/19/16 08:00
02/19/16 08:30

02/19/16 12:32
02/19/16 12:32
02/19/16 12:32
02/19/16 12:32

Sample

Default

RL Prep

Initial/Final

Initial/Final

Factor

1000mL/2mL
1000mL/2mL
1000mL/2mL
1000mL/2mL

1.04
1.04
1.00
0.97

Batch: 6020602

A6B0661-01
A6B0661-02
A6B0661-03
A6B0661-04

Water
Water
Water
Water

EPA 8270D (SIM)


EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

960mL/2mL
960mL/2mL
1000mL/2mL
1030mL/2mL

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 16 of 18

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: [none]

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/21/16 15:02

Notes and Definitions


Qualifiers:
Q-19

Blank Spike Duplicate (BSD) sample analyzed in place of Matrix Spike/Duplicate samples due to limited sample amount available for
analysis.

Notes and Conventions:


DET

Analyte DETECTED

ND

Analyte NOT DETECTED at or above the reporting limit

NR

Not Reported

dry

Sample results reported on a dry weight basis. Results listed as 'wet' or without 'dry'designation are not dry weight corrected.

RPD

Relative Percent Difference

MDL

If MDL is not listed, data has been evaluated to the Method Reporting Limit only.

WMSC

Water Miscible Solvent Correction has been applied to Results and MRLs for volatiles soil samples per EPA 8000C.

Batch
QC

Unless specifically requested, this report contains only results for Batch QC derived from client samples included in this report. All
analyses were performed with the appropriate Batch QC (including Sample Duplicates, Matrix Spikes and/or Matrix Spike Duplicates) in
order to meet or exceed method and regulatory requirements. Any exceptions to this will be qualified in this report. Complete Batch QC
results are available upon request. In cases where there is insufficient sample provided for Sample Duplicates and/or Matrix Spikes, a
Lab Control Sample Duplicate (LCS Dup) is analyzed to demonstrate accuracy and precision of the extraction and analysis.

Blank
Policy

Apex assesses blank data for potential high bias down to a level equal to the method reporting limit (MRL), except for conventional
chemistry and HCID analyses which are assessed only to the MRL. Sample results flagged with a B or B-02 qualifier are potentially
biased high if they are less than ten times the level found in the blank for inorganic analyses or less than five times the level found in the
blank for organic analyses.
For accurate comparison of volatile results to the level found in the blank; water sample results should be divided by the dilution factor,
and soil sample results should be divided by 1/50 of the sample dilution to account for the sample prep factor.
Results qualified as reported below the MRL may include a potential high bias if associated with a B or B-02 qualified blank. B and B-02
qualifications are not applied to J qualified results reported below the MRL.

---

QC results are not applicable. For example, % Recoveries for Blanks and Duplicates, % RPD for Blanks, Blank Spikes and Matrix
Spikes, etc.

***

Used to indicate a possible discrepancy with the Sample and Sample Duplicate results when the %RPD is not available. In this case,
either the Sample or the Sample Duplicate has a reportable result for this analyte, while the other is Non Detect (ND).

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 17 of 18

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
NRC-CB&I

Project: AT&T Hall Ridge

6211 N Ensign St

Project Number: [none]

Portland, OR 97217

Project Manager: Ron Malec

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Reported:

02/21/16 15:02

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 18 of 18

Apex Labs

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Monday, February 22, 2016


Ron Malec
NRC-CB&I
6211 N Ensign St
Portland, OR 97217

RE: AT&T Hall Ridge / 156319


Enclosed are the results of analyses for work order A6B0703, which was received by the laboratory on
2/22/2016 at 8:30:00AM.
Thank you for using Apex Labs. We appreciate your business and strive to provide the highest quality
services to the environmental industry.
If you have any questions concerning this report or the services we offer , please feel free to contact me by
email at: dthomas@apex-labs.com, or by phone at 503-718-2323.

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 1 of 16

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/22/16 18:29

ANALYTICAL REPORT FOR SAMPLES


SAMPLE INFORMATION
Sample ID

Laboratory ID

Matrix

Date Sampled

Date Received

SW-01

A6B0703-01
A6B0703-02
A6B0703-03
A6B0703-04

Water
Water
Water
Water

02/21/16 07:30
02/21/16 08:10
02/21/16 08:40
02/21/16 09:00

02/22/16 08:30
02/22/16 08:30
02/22/16 08:30
02/22/16 08:30

SW-02
SW-03
SW-04

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 2 of 16

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/22/16 18:29

ANALYTICAL SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Result

Analyte

MDL

SW-01 (A6B0703-01)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Benzene

ND

0.100

0.200

ug/L

02/22/16 13:47

EPA 8260B

Toluene

ND

0.500

1.00

"

"

"

"

Ethylbenzene

ND

0.250

0.500

"

"

"

"

Xylenes, total

ND

0.750

1.50

"

"

"

"

Naphthalene

ND

1.00

2.00

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

0.500

1.00

"

"

"

"

Isopropylbenzene

ND

0.500

1.00

"

"

"

"

n-Propylbenzene

ND

0.250

0.500

"

"

"

"

1,2,4-Trimethylbenzene

ND

0.500

1.00

"

"

"

"

1,3,5-Trimethylbenzene

ND

0.500

1.00

"

"

"

"

1,2-Dibromoethane (EDB)

ND

0.250

0.500

"

"

"

"

1,2-Dichloroethane (EDC)

ND

0.250

0.500

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 98 %

Limits: 80-120 %

"

"

"

97 %

Limits: 80-120 %

"

"

"

Toluene-d8 (Surr)

100 %

Limits: 80-120 %

"

"

"

4-Bromofluorobenzene (Surr)

100 %

Limits: 80-120 %

"

"

"

1,4-Difluorobenzene (Surr)

SW-02 (A6B0703-02)

Matrix: Water

Batch: 6020629

Benzene

ND

0.100

0.200

ug/L

02/22/16 14:16

EPA 8260B

Toluene

ND

0.500

1.00

"

"

"

"

Ethylbenzene

ND

0.250

0.500

"

"

"

"

Xylenes, total

ND

0.750

1.50

"

"

"

"

Naphthalene

ND

1.00

2.00

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

0.500

1.00

"

"

"

"

Isopropylbenzene

ND

0.500

1.00

"

"

"

"

n-Propylbenzene

ND

0.250

0.500

"

"

"

"

1,2,4-Trimethylbenzene

ND

0.500

1.00

"

"

"

"

1,3,5-Trimethylbenzene

ND

0.500

1.00

"

"

"

"

1,2-Dibromoethane (EDB)

ND

0.250

0.500

"

"

"

"

1,2-Dichloroethane (EDC)

ND

0.250

0.500

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 97 %

Limits: 80-120 %

"

"

"

1,4-Difluorobenzene (Surr)

97 %

Limits: 80-120 %

"

"

"

Toluene-d8 (Surr)

99 %

Limits: 80-120 %

"

"

"

4-Bromofluorobenzene (Surr)

97 %

Limits: 80-120 %

"

"

"

02/22/16 14:44

EPA 8260B

SW-03 (A6B0703-03)

Benzene

Matrix: Water

ND

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

0.100

0.200

Notes

Batch: 6020629

Batch: 6020629

ug/L

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 3 of 16

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/22/16 18:29

ANALYTICAL SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Result

Analyte

MDL

SW-03 (A6B0703-03)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Toluene

ND

0.500

1.00

ug/L

"

EPA 8260B

Ethylbenzene

ND

0.250

0.500

"

"

"

"

Xylenes, total

ND

0.750

1.50

"

"

"

"

Naphthalene

ND

1.00

2.00

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

0.500

1.00

"

"

"

"

Isopropylbenzene

ND

0.500

1.00

"

"

"

"

n-Propylbenzene

ND

0.250

0.500

"

"

"

"

1,2,4-Trimethylbenzene

ND

0.500

1.00

"

"

"

"

1,3,5-Trimethylbenzene

ND

0.500

1.00

"

"

"

"

1,2-Dibromoethane (EDB)

ND

0.250

0.500

"

"

"

"

1,2-Dichloroethane (EDC)

ND

0.250

0.500

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)


1,4-Difluorobenzene (Surr)
Toluene-d8 (Surr)
4-Bromofluorobenzene (Surr)

SW-04 (A6B0703-04)

Recovery: 99 %

Limits: 80-120 %

"

"

"

97 %

Limits: 80-120 %

"

"

"

100 %

Limits: 80-120 %

"

"

"

98 %

Limits: 80-120 %

"

"

"

Matrix: Water

Batch: 6020629

Benzene

ND

0.100

0.200

ug/L

02/22/16 15:13

EPA 8260B

Toluene

ND

0.500

1.00

"

"

"

"

Ethylbenzene

ND

0.250

0.500

"

"

"

"

Xylenes, total

ND

0.750

1.50

"

"

"

"

Naphthalene

ND

1.00

2.00

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

0.500

1.00

"

"

"

"

Isopropylbenzene

ND

0.500

1.00

"

"

"

"

n-Propylbenzene

ND

0.250

0.500

"

"

"

"

1,2,4-Trimethylbenzene

ND

0.500

1.00

"

"

"

"

1,3,5-Trimethylbenzene

ND

0.500

1.00

"

"

"

"

1,2-Dibromoethane (EDB)

ND

0.250

0.500

"

"

"

"

1,2-Dichloroethane (EDC)

ND

0.250

0.500

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)


1,4-Difluorobenzene (Surr)
Toluene-d8 (Surr)
4-Bromofluorobenzene (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020629

Recovery: 99 %

Limits: 80-120 %

"

"

"

98 %

Limits: 80-120 %

"

"

"

100 %

Limits: 80-120 %

"

"

"

97 %

Limits: 80-120 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 4 of 16

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/22/16 18:29

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

SW-01 (A6B0703-01)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Acenaphthene

ND

0.0196

0.0392

ug/L

02/22/16 16:34

EPA 8270D (SIM)

Acenaphthylene

ND

0.0196

0.0392

"

"

"

"

Anthracene

ND

0.0196

0.0392

"

"

"

"

Benz(a)anthracene

ND

0.0196

0.0392

"

"

"

"

Benzo(a)pyrene

ND

0.0196

0.0392

"

"

"

"

Benzo(b)fluoranthene

ND

0.0196

0.0392

"

"

"

"

Benzo(k)fluoranthene

ND

0.0196

0.0392

"

"

"

"

Benzo(g,h,i)perylene

ND

0.0196

0.0392

"

"

"

"

Chrysene

ND

0.0196

0.0392

"

"

"

"

Dibenz(a,h)anthracene

ND

0.0196

0.0392

"

"

"

"

Dibenzofuran

ND

0.0196

0.0392

"

"

"

"

Fluoranthene

ND

0.0196

0.0392

"

"

"

"

Fluorene

ND

0.0196

0.0392

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

0.0196

0.0392

"

"

"

"

1-Methylnaphthalene

ND

0.0392

0.0784

"

"

"

"

2-Methylnaphthalene

ND

0.0392

0.0784

"

"

"

"

Naphthalene

ND

0.0392

0.0784

"

"

"

"

Phenanthrene

ND

0.0196

0.0392

"

"

"

"

Pyrene

ND

0.0196

0.0392

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020635

Recovery: 75 %

Limits: 44-120 %

"

"

"

106 %

Limits: 50-133 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 5 of 16

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/22/16 18:29

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

SW-02 (A6B0703-02)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Acenaphthene

ND

0.0208

0.0417

ug/L

02/22/16 17:00

EPA 8270D (SIM)

Acenaphthylene

ND

0.0208

0.0417

"

"

"

"

Anthracene

ND

0.0208

0.0417

"

"

"

"

Benz(a)anthracene

ND

0.0208

0.0417

"

"

"

"

Benzo(a)pyrene

ND

0.0208

0.0417

"

"

"

"

Benzo(b)fluoranthene

ND

0.0208

0.0417

"

"

"

"

Benzo(k)fluoranthene

ND

0.0208

0.0417

"

"

"

"

Benzo(g,h,i)perylene

ND

0.0208

0.0417

"

"

"

"

Chrysene

ND

0.0208

0.0417

"

"

"

"

Dibenz(a,h)anthracene

ND

0.0208

0.0417

"

"

"

"

Dibenzofuran

ND

0.0208

0.0417

"

"

"

"

Fluoranthene

ND

0.0208

0.0417

"

"

"

"

Fluorene

ND

0.0208

0.0417

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

0.0208

0.0417

"

"

"

"

1-Methylnaphthalene

ND

0.0417

0.0833

"

"

"

"

2-Methylnaphthalene

ND

0.0417

0.0833

"

"

"

"

Naphthalene

ND

0.0417

0.0833

"

"

"

"

Phenanthrene

ND

0.0208

0.0417

"

"

"

"

Pyrene

ND

0.0208

0.0417

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020635

Recovery: 70 %

Limits: 44-120 %

"

"

"

102 %

Limits: 50-133 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 6 of 16

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/22/16 18:29

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

SW-03 (A6B0703-03)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Acenaphthene

ND

0.0206

0.0412

ug/L

02/22/16 17:26

EPA 8270D (SIM)

Acenaphthylene

ND

0.0206

0.0412

"

"

"

"

Anthracene

ND

0.0206

0.0412

"

"

"

"

Benz(a)anthracene

ND

0.0206

0.0412

"

"

"

"

Benzo(a)pyrene

ND

0.0206

0.0412

"

"

"

"

Benzo(b)fluoranthene

ND

0.0206

0.0412

"

"

"

"

Benzo(k)fluoranthene

ND

0.0206

0.0412

"

"

"

"

Benzo(g,h,i)perylene

ND

0.0206

0.0412

"

"

"

"

Chrysene

ND

0.0206

0.0412

"

"

"

"

Dibenz(a,h)anthracene

ND

0.0206

0.0412

"

"

"

"

Dibenzofuran

ND

0.0206

0.0412

"

"

"

"

Fluoranthene

ND

0.0206

0.0412

"

"

"

"

Fluorene

ND

0.0206

0.0412

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

0.0206

0.0412

"

"

"

"

1-Methylnaphthalene

ND

0.0412

0.0825

"

"

"

"

2-Methylnaphthalene

ND

0.0412

0.0825

"

"

"

"

Naphthalene

ND

0.0412

0.0825

"

"

"

"

Phenanthrene

ND

0.0206

0.0412

"

"

"

"

Pyrene

ND

0.0206

0.0412

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020635

Recovery: 72 %

Limits: 44-120 %

"

"

"

106 %

Limits: 50-133 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 7 of 16

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/22/16 18:29

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

SW-04 (A6B0703-04)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Acenaphthene

ND

0.0198

0.0396

ug/L

02/22/16 17:52

EPA 8270D (SIM)

Acenaphthylene

ND

0.0198

0.0396

"

"

"

"

Anthracene

ND

0.0198

0.0396

"

"

"

"

Benz(a)anthracene

ND

0.0198

0.0396

"

"

"

"

Benzo(a)pyrene

ND

0.0198

0.0396

"

"

"

"

Benzo(b)fluoranthene

ND

0.0198

0.0396

"

"

"

"

Benzo(k)fluoranthene

ND

0.0198

0.0396

"

"

"

"

Benzo(g,h,i)perylene

ND

0.0198

0.0396

"

"

"

"

Chrysene

ND

0.0198

0.0396

"

"

"

"

Dibenz(a,h)anthracene

ND

0.0198

0.0396

"

"

"

"

Dibenzofuran

ND

0.0198

0.0396

"

"

"

"

Fluoranthene

ND

0.0198

0.0396

"

"

"

"

Fluorene

ND

0.0198

0.0396

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

0.0198

0.0396

"

"

"

"

1-Methylnaphthalene

ND

0.0396

0.0792

"

"

"

"

2-Methylnaphthalene

ND

0.0396

0.0792

"

"

"

"

Naphthalene

ND

0.0396

0.0792

"

"

"

"

Phenanthrene

ND

0.0198

0.0396

"

"

"

"

Pyrene

ND

0.0198

0.0396

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020635

Recovery: 78 %

Limits: 44-120 %

"

"

"

106 %

Limits: 50-133 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 8 of 16

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/22/16 18:29

QUALITY CONTROL (QC) SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

RPD
Limit

Notes

Water

Batch 6020629 - EPA 5030B

Prepared: 02/22/16 10:56 Analyzed: 02/22/16 13:18

Blank (6020629-BLK1)
EPA 8260B

Benzene

ND

0.100

0.200

ug/L

---

---

---

---

---

---

Toluene

ND

0.500

1.00

"

"

---

---

---

---

---

---

Ethylbenzene

ND

0.250

0.500

"

"

---

---

---

---

---

---

Xylenes, total

ND

0.750

1.50

"

"

---

---

---

---

---

---

Naphthalene

ND

1.00

2.00

"

"

---

---

---

---

---

---

Methyl tert-butyl ether


(MTBE)
Isopropylbenzene

ND

0.500

1.00

"

"

---

---

---

---

---

---

ND

0.500

1.00

"

"

---

---

---

---

---

---

n-Propylbenzene

ND

0.250

0.500

"

"

---

---

---

---

---

---

1,2,4-Trimethylbenzene

ND

0.500

1.00

"

"

---

---

---

---

---

---

1,3,5-Trimethylbenzene

ND

0.500

1.00

"

"

---

---

---

---

---

---

1,2-Dibromoethane (EDB)

ND

0.250

0.500

"

"

---

---

---

---

---

---

1,2-Dichloroethane (EDC)

ND

0.250

0.500

"

"

---

---

---

---

---

---

---

---

Surr: Dibromofluoromethane (Surr)

Recovery: 98 %

Limits: 80-120 %

Dilution: 1x

98 %

80-120 %

"

100 %

80-120 %

"

97 %

80-120 %

"

1,4-Difluorobenzene (Surr)
Toluene-d8 (Surr)
4-Bromofluorobenzene (Surr)

Prepared: 02/22/16 10:56 Analyzed: 02/22/16 12:21

LCS (6020629-BS1)
EPA 8260B

Benzene

19.1

0.100

0.200

ug/L

20.0

---

95

70-130%

Toluene

20.1

0.500

1.00

"

"

"

---

100

"

---

---

Ethylbenzene

20.4

0.250

0.500

"

"

"

---

102

"

---

---

Xylenes, total

61.6

0.750

1.50

"

"

60.0

---

103

"

---

---

Naphthalene

17.8

1.00

2.00

"

"

20.0

---

89

"

---

---

Methyl tert-butyl ether


(MTBE)
Isopropylbenzene

18.3

0.500

1.00

"

"

"

---

92

"

---

---

21.5

0.500

1.00

"

"

"

---

107

"

---

---

n-Propylbenzene

19.6

0.250

0.500

"

"

"

---

98

"

---

---

1,2,4-Trimethylbenzene

20.4

0.500

1.00

"

"

"

---

102

"

---

---

1,3,5-Trimethylbenzene

20.3

0.500

1.00

"

"

"

---

102

"

---

---

1,2-Dibromoethane (EDB)

20.3

0.250

0.500

"

"

"

---

102

"

---

---

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 9 of 16

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/22/16 18:29

QUALITY CONTROL (QC) SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

%REC
Limits RPD

RPD
Limit

Notes

Prepared: 02/22/16 10:56 Analyzed: 02/22/16 12:21

LCS (6020629-BS1)
Surr: Dibromofluoromethane (Surr)

%REC

Water

Batch 6020629 - EPA 5030B


1,2-Dichloroethane (EDC)

Source
Result

18.0

0.250

0.500

ug/L

"

"

---

Recovery: 95 %

Limits: 80-120 %

Dilution: 1x

1,4-Difluorobenzene (Surr)

96 %

80-120 %

"

Toluene-d8 (Surr)

99 %

80-120 %

"

4-Bromofluorobenzene (Surr)

98 %

80-120 %

"

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

90

"

---

---

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 10 of 16

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/22/16 18:29

QUALITY CONTROL (QC) SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

RPD
Limit

Notes

Water

Batch 6020635 - EPA 3510C (Acid Extraction)

Prepared: 02/22/16 11:20 Analyzed: 02/22/16 15:15

Blank (6020635-BLK1)
EPA 8270D (SIM)

Acenaphthene

ND

0.0182

0.0364

ug/L

---

---

---

---

---

---

Acenaphthylene

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

Anthracene

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

Benz(a)anthracene

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

Benzo(a)pyrene

ND

0.0182

0.0364

"

"

---

---

---

---

---

-----

Benzo(b)fluoranthene

ND

0.0182

0.0364

"

"

---

---

---

---

---

Benzo(k)fluoranthene

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

Benzo(g,h,i)perylene

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

Chrysene

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

Dibenz(a,h)anthracene

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

Dibenzofuran

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

Fluoranthene

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

Fluorene

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

Indeno(1,2,3-cd)pyrene

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

1-Methylnaphthalene

ND

0.0364

0.0727

"

"

---

---

---

---

---

---

2-Methylnaphthalene

ND

0.0364

0.0727

"

"

---

---

---

---

---

---

Naphthalene

ND

0.0364

0.0727

"

"

---

---

---

---

---

---

Phenanthrene

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

Pyrene

ND

0.0182

0.0364

"

"

---

---

---

---

---

---

---

Surr: 2-Fluorobiphenyl (Surr)

Recovery: 92 %

Limits: 44-120 %

Dilution: 1x

114 %

50-133 %

"

p-Terphenyl-d14 (Surr)

Prepared: 02/22/16 11:20 Analyzed: 02/22/16 15:41

LCS (6020635-BS1)
EPA 8270D (SIM)

Acenaphthene

7.34

0.0200

0.0400

ug/L

8.00

---

92

47-122%

---

Acenaphthylene

7.43

0.0200

0.0400

"

"

"

---

93

41-130%

---

---

Anthracene

7.74

0.0200

0.0400

"

"

"

---

97

57-123%

---

---

Benz(a)anthracene

7.61

0.0200

0.0400

"

"

"

---

95

58-125%

---

---

Benzo(a)pyrene

7.92

0.0200

0.0400

"

"

"

---

99

54-128%

---

---

Benzo(b)fluoranthene

8.27

0.0200

0.0400

"

"

"

---

103

53-131%

---

---

Benzo(k)fluoranthene

7.91

0.0200

0.0400

"

"

"

---

99

57-129%

---

---

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 11 of 16

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/22/16 18:29

QUALITY CONTROL (QC) SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

%REC

%REC
Limits RPD

RPD
Limit

Notes

Water

Batch 6020635 - EPA 3510C (Acid Extraction)

Prepared: 02/22/16 11:20 Analyzed: 02/22/16 15:41

LCS (6020635-BS1)

Benzo(g,h,i)perylene

Source
Result

6.86

0.0200

0.0400

"

"

"

---

86

50-134%

---

---

Chrysene

7.46

0.0200

0.0400

"

"

"

---

93

59-123%

---

---

Dibenz(a,h)anthracene

7.31

0.0200

0.0400

"

"

"

---

91

51-134%

---

---

Dibenzofuran

7.57

0.0200

0.0400

"

"

"

---

95

53-120%

---

---

Fluoranthene

8.05

0.0200

0.0400

"

"

"

---

101

57-128%

---

---

Fluorene

7.68

0.0200

0.0400

"

"

"

---

96

52-124%

---

---

Indeno(1,2,3-cd)pyrene

7.04

0.0200

0.0400

"

"

"

---

88

52-133%

---

---

1-Methylnaphthalene

6.80

0.0400

0.0800

"

"

"

---

85

41-120%

---

---

2-Methylnaphthalene

7.18

0.0400

0.0800

"

"

"

---

90

40-121%

---

---

Naphthalene

6.93

0.0400

0.0800

"

"

"

---

87

"

---

---

Phenanthrene

7.70

0.0200

0.0400

"

"

"

---

96

59-120%

---

---

Pyrene

8.13

0.0200

0.0400

"

"

"

---

102

57-126%

---

---

Surr: 2-Fluorobiphenyl (Surr)

Recovery: 91 %

Limits: 44-120 %

Dilution: 1x

104 %

50-133 %

"

p-Terphenyl-d14 (Surr)

Prepared: 02/22/16 11:20 Analyzed: 02/22/16 16:07

LCS Dup (6020635-BSD1)

Q-19

EPA 8270D (SIM)

Acenaphthene

7.41

0.0200

0.0400

ug/L

8.00

---

93

47-122%

30%

Acenaphthylene

7.60

0.0200

0.0400

"

"

"

---

95

41-130%

30%

Anthracene

7.78

0.0200

0.0400

"

"

"

---

97

57-123%

0.5

30%

Benz(a)anthracene

7.63

0.0200

0.0400

"

"

"

---

95

58-125%

0.3

30%

Benzo(a)pyrene

8.00

0.0200

0.0400

"

"

"

---

100

54-128%

30%

Benzo(b)fluoranthene

8.28

0.0200

0.0400

"

"

"

---

103

53-131%

0.08

30%

Benzo(k)fluoranthene

7.87

0.0200

0.0400

"

"

"

---

98

57-129%

0.5

30%

Benzo(g,h,i)perylene

7.12

0.0200

0.0400

"

"

"

---

89

50-134%

30%

Chrysene

7.66

0.0200

0.0400

"

"

"

---

96

59-123%

30%

Dibenz(a,h)anthracene

7.62

0.0200

0.0400

"

"

"

---

95

51-134%

30%

Dibenzofuran

7.56

0.0200

0.0400

"

"

"

---

94

53-120%

0.2

30%

Fluoranthene

7.98

0.0200

0.0400

"

"

"

---

100

57-128%

0.8

30%

Fluorene

7.65

0.0200

0.0400

"

"

"

---

96

52-124%

0.4

30%

Indeno(1,2,3-cd)pyrene

7.20

0.0200

0.0400

"

"

"

---

90

52-133%

30%

1-Methylnaphthalene

6.96

0.0400

0.0800

"

"

"

---

87

41-120%

30%

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 12 of 16

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/22/16 18:29

QUALITY CONTROL (QC) SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

Prepared: 02/22/16 11:20 Analyzed: 02/22/16 16:07

LCS Dup (6020635-BSD1)

Q-19

2-Methylnaphthalene

7.34

0.0400

0.0800

"

"

"

---

92

Naphthalene

7.22

0.0400

0.0800

"

"

"

---

90

Phenanthrene

7.76

0.0200

0.0400

"

"

"

---

97

Pyrene

8.10

0.0200

0.0400

"

"

"

---

101

57-126%

Recovery: 92 %

Limits: 44-120 %

Dilution: 1x

104 %

50-133 %

"

p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Water

Batch 6020635 - EPA 3510C (Acid Extraction)

Surr: 2-Fluorobiphenyl (Surr)

RPD
Limit

40-121%

30%

"

30%

59-120%

0.8

30%

0.4

30%

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 13 of 16

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/22/16 18:29

SAMPLE PREPARATION INFORMATION


RBDM Compounds (BTEX+) by EPA 8260B
Sample

Default

RL Prep

Initial/Final

Initial/Final

Factor

Prep: EPA 5030B


Lab Number

Matrix

Method

Sampled

Prepared

02/21/16 07:30
02/21/16 08:10
02/21/16 08:40
02/21/16 09:00

02/22/16 12:40
02/22/16 12:40
02/22/16 12:40
02/22/16 12:40

Batch: 6020629

A6B0703-01
A6B0703-02
A6B0703-03
A6B0703-04

Water
Water
Water
Water

EPA 8260B
EPA 8260B
EPA 8260B
EPA 8260B

5mL/5mL
5mL/5mL
5mL/5mL
5mL/5mL

5mL/5mL
5mL/5mL
5mL/5mL
5mL/5mL

1.00
1.00
1.00
1.00

Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM


Prep: EPA 3510C (Acid Extraction)
Lab Number

Matrix

Method

Sampled

Prepared

02/21/16 07:30
02/21/16 08:10
02/21/16 08:40
02/21/16 09:00

02/22/16 11:20
02/22/16 11:20
02/22/16 11:20
02/22/16 11:20

Sample

Default

RL Prep

Initial/Final

Initial/Final

Factor

1000mL/2mL
1000mL/2mL
1000mL/2mL
1000mL/2mL

0.98
1.04
1.03
0.99

Batch: 6020635

A6B0703-01
A6B0703-02
A6B0703-03
A6B0703-04

Water
Water
Water
Water

EPA 8270D (SIM)


EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

1020mL/2mL
960mL/2mL
970mL/2mL
1010mL/2mL

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 14 of 16

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/22/16 18:29

Notes and Definitions


Qualifiers:
Q-19

Blank Spike Duplicate (BSD) sample analyzed in place of Matrix Spike/Duplicate samples due to limited sample amount available for
analysis.

Notes and Conventions:


DET

Analyte DETECTED

ND

Analyte NOT DETECTED at or above the reporting limit

NR

Not Reported

dry

Sample results reported on a dry weight basis. Results listed as 'wet' or without 'dry'designation are not dry weight corrected.

RPD

Relative Percent Difference

MDL

If MDL is not listed, data has been evaluated to the Method Reporting Limit only.

WMSC

Water Miscible Solvent Correction has been applied to Results and MRLs for volatiles soil samples per EPA 8000C.

Batch
QC

Unless specifically requested, this report contains only results for Batch QC derived from client samples included in this report. All
analyses were performed with the appropriate Batch QC (including Sample Duplicates, Matrix Spikes and/or Matrix Spike Duplicates) in
order to meet or exceed method and regulatory requirements. Any exceptions to this will be qualified in this report. Complete Batch QC
results are available upon request. In cases where there is insufficient sample provided for Sample Duplicates and/or Matrix Spikes, a
Lab Control Sample Duplicate (LCS Dup) is analyzed to demonstrate accuracy and precision of the extraction and analysis.

Blank
Policy

Apex assesses blank data for potential high bias down to a level equal to the method reporting limit (MRL), except for conventional
chemistry and HCID analyses which are assessed only to the MRL. Sample results flagged with a B or B-02 qualifier are potentially
biased high if they are less than ten times the level found in the blank for inorganic analyses or less than five times the level found in the
blank for organic analyses.
For accurate comparison of volatile results to the level found in the blank; water sample results should be divided by the dilution factor,
and soil sample results should be divided by 1/50 of the sample dilution to account for the sample prep factor.
Results qualified as reported below the MRL may include a potential high bias if associated with a B or B-02 qualified blank. B and B-02
qualifications are not applied to J qualified results reported below the MRL.

---

QC results are not applicable. For example, % Recoveries for Blanks and Duplicates, % RPD for Blanks, Blank Spikes and Matrix
Spikes, etc.

***

Used to indicate a possible discrepancy with the Sample and Sample Duplicate results when the %RPD is not available. In this case,
either the Sample or the Sample Duplicate has a reportable result for this analyte, while the other is Non Detect (ND).

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 15 of 16

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
NRC-CB&I

Project: AT&T Hall Ridge

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Reported:

02/22/16 18:29

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 16 of 16

Apex Labs

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Friday, February 26, 2016


Ron Malec
NRC-CB&I
6211 N Ensign St
Portland, OR 97217

RE: AT&T Hall Ridge / 156319


Enclosed are the results of analyses for work order A6B0868, which was received by the laboratory on
2/26/2016 at 6:35:00AM.
Thank you for using Apex Labs. We appreciate your business and strive to provide the highest quality
services to the environmental industry.
If you have any questions concerning this report or the services we offer , please feel free to contact me by
email at: dthomas@apex-labs.com, or by phone at 503-718-2323.

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 1 of 12

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/26/16 16:36

ANALYTICAL REPORT FOR SAMPLES


SAMPLE INFORMATION
Sample ID

Laboratory ID

Matrix

Date Sampled

Date Received

SW-05

A6B0868-01

Water

02/25/16 13:00

02/26/16 06:35

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 2 of 12

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/26/16 16:36

ANALYTICAL SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Result

Analyte

MDL

SW-05 (A6B0868-01)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Benzene

ND

---

0.200

ug/L

02/26/16 13:07

EPA 8260B

Toluene

ND

---

1.00

"

"

"

"

Ethylbenzene

ND

---

0.500

"

"

"

"

Xylenes, total

ND

---

1.50

"

"

"

"

Naphthalene

ND

---

2.00

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

1.00

"

"

"

"

Isopropylbenzene

ND

---

1.00

"

"

"

"

n-Propylbenzene

ND

---

0.500

"

"

"

"

1,2,4-Trimethylbenzene

ND

---

1.00

"

"

"

"

1,3,5-Trimethylbenzene

ND

---

1.00

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.500

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.500

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)


1,4-Difluorobenzene (Surr)
Toluene-d8 (Surr)
4-Bromofluorobenzene (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020814

Recovery: 100 %

Limits: 80-120 %

"

"

"

99 %

Limits: 80-120 %

"

"

"

102 %

Limits: 80-120 %

"

"

"

98 %

Limits: 80-120 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 3 of 12

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/26/16 16:36

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

SW-05 (A6B0868-01)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Acenaphthene

ND

---

0.0440

ug/L

02/26/16 12:14

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0440

"

"

"

"

Anthracene

ND

---

0.0440

"

"

"

"

Benz(a)anthracene

ND

---

0.0440

"

"

"

"

Benzo(a)pyrene

ND

---

0.0440

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0440

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0440

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0440

"

"

"

"

Chrysene

ND

---

0.0440

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0440

"

"

"

"

Dibenzofuran

ND

---

0.0440

"

"

"

"

Fluoranthene

ND

---

0.0440

"

"

"

"

Fluorene

ND

---

0.0440

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0440

"

"

"

"

1-Methylnaphthalene

ND

---

0.0879

"

"

"

"

2-Methylnaphthalene

ND

---

0.0879

"

"

"

"

Naphthalene

ND

---

0.0879

"

"

"

"

Phenanthrene

ND

---

0.0440

"

"

"

"

Pyrene

ND

---

0.0440

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020786

Recovery: 75 %

Limits: 44-120 %

"

"

"

112 %

Limits: 50-133 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 4 of 12

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/26/16 16:36

QUALITY CONTROL (QC) SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

RPD
Limit

Notes

Water

Batch 6020814 - EPA 5030B

Prepared: 02/26/16 10:15 Analyzed: 02/26/16 12:39

Blank (6020814-BLK1)
EPA 8260B

Benzene

ND

---

0.200

ug/L

---

---

---

---

---

---

Toluene

ND

---

1.00

"

"

---

---

---

---

---

---

Ethylbenzene

ND

---

0.500

"

"

---

---

---

---

---

---

Xylenes, total

ND

---

1.50

"

"

---

---

---

---

---

---

Naphthalene

ND

---

2.00

"

"

---

---

---

---

---

---

Methyl tert-butyl ether


(MTBE)
Isopropylbenzene

ND

---

1.00

"

"

---

---

---

---

---

---

ND

---

1.00

"

"

---

---

---

---

---

---

n-Propylbenzene

ND

---

0.500

"

"

---

---

---

---

---

---

1,2,4-Trimethylbenzene

ND

---

1.00

"

"

---

---

---

---

---

---

1,3,5-Trimethylbenzene

ND

---

1.00

"

"

---

---

---

---

---

---

1,2-Dibromoethane (EDB)

ND

---

0.500

"

"

---

---

---

---

---

---

1,2-Dichloroethane (EDC)

ND

---

0.500

"

"

---

---

---

---

---

---

---

---

Surr: Dibromofluoromethane (Surr)

Recovery: 99 %

Limits: 80-120 %

Dilution: 1x

99 %

80-120 %

"

Toluene-d8 (Surr)

101 %

80-120 %

"

4-Bromofluorobenzene (Surr)

100 %

80-120 %

"

1,4-Difluorobenzene (Surr)

Prepared: 02/26/16 10:15 Analyzed: 02/26/16 11:13

LCS (6020814-BS1)
EPA 8260B

Benzene

18.8

---

0.200

ug/L

20.0

---

94

70-130%

Toluene

20.2

---

1.00

"

"

"

---

101

"

---

---

Ethylbenzene

20.1

---

0.500

"

"

"

---

101

"

---

---

Xylenes, total

61.4

---

1.50

"

"

60.0

---

102

"

---

---

Naphthalene

17.9

---

2.00

"

"

20.0

---

90

"

---

---

Methyl tert-butyl ether


(MTBE)
Isopropylbenzene

18.2

---

1.00

"

"

"

---

91

"

---

---

20.8

---

1.00

"

"

"

---

104

"

---

---

n-Propylbenzene

19.8

---

0.500

"

"

"

---

99

"

---

---

1,2,4-Trimethylbenzene

20.4

---

1.00

"

"

"

---

102

"

---

---

1,3,5-Trimethylbenzene

20.4

---

1.00

"

"

"

---

102

"

---

---

1,2-Dibromoethane (EDB)

20.5

---

0.500

"

"

"

---

102

"

---

---

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 5 of 12

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/26/16 16:36

QUALITY CONTROL (QC) SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

%REC
Limits RPD

RPD
Limit

Notes

Prepared: 02/26/16 10:15 Analyzed: 02/26/16 11:13

LCS (6020814-BS1)
Surr: Dibromofluoromethane (Surr)

%REC

Water

Batch 6020814 - EPA 5030B


1,2-Dichloroethane (EDC)

Source
Result

17.7

---

0.500

ug/L

"

"

---

Recovery: 96 %

Limits: 80-120 %

Dilution: 1x

95 %

80-120 %

"

Toluene-d8 (Surr)

100 %

80-120 %

"

4-Bromofluorobenzene (Surr)

101 %

80-120 %

"

1,4-Difluorobenzene (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

88

"

---

---

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 6 of 12

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/26/16 16:36

QUALITY CONTROL (QC) SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

RPD
Limit

Notes

Water

Batch 6020786 - EPA 3510C (Acid Extraction)

Prepared: 02/26/16 07:39 Analyzed: 02/26/16 10:52

Blank (6020786-BLK1)
EPA 8270D (SIM)

Acenaphthene

ND

---

0.0364

ug/L

---

---

---

---

---

---

Acenaphthylene

ND

---

0.0364

"

"

---

---

---

---

---

---

Anthracene

ND

---

0.0364

"

"

---

---

---

---

---

---

Benz(a)anthracene

ND

---

0.0364

"

"

---

---

---

---

---

---

Benzo(a)pyrene

ND

---

0.0364

"

"

---

---

---

---

---

-----

Benzo(b)fluoranthene

ND

---

0.0364

"

"

---

---

---

---

---

Benzo(k)fluoranthene

ND

---

0.0364

"

"

---

---

---

---

---

---

Benzo(g,h,i)perylene

ND

---

0.0364

"

"

---

---

---

---

---

---

Chrysene

ND

---

0.0364

"

"

---

---

---

---

---

---

Dibenz(a,h)anthracene

ND

---

0.0364

"

"

---

---

---

---

---

---

Dibenzofuran

ND

---

0.0364

"

"

---

---

---

---

---

---

Fluoranthene

ND

---

0.0364

"

"

---

---

---

---

---

---

Fluorene

ND

---

0.0364

"

"

---

---

---

---

---

---

Indeno(1,2,3-cd)pyrene

ND

---

0.0364

"

"

---

---

---

---

---

---

1-Methylnaphthalene

ND

---

0.0727

"

"

---

---

---

---

---

---

2-Methylnaphthalene

ND

---

0.0727

"

"

---

---

---

---

---

---

Naphthalene

ND

---

0.0727

"

"

---

---

---

---

---

---

Phenanthrene

ND

---

0.0364

"

"

---

---

---

---

---

---

Pyrene

ND

---

0.0364

"

"

---

---

---

---

---

---

---

Surr: 2-Fluorobiphenyl (Surr)

Recovery: 84 %

Limits: 44-120 %

Dilution: 1x

108 %

50-133 %

"

p-Terphenyl-d14 (Surr)

Prepared: 02/26/16 07:39 Analyzed: 02/26/16 11:19

LCS (6020786-BS1)
EPA 8270D (SIM)

Acenaphthene

6.55

---

0.0400

ug/L

8.00

---

82

47-122%

---

Acenaphthylene

6.52

---

0.0400

"

"

"

---

82

41-130%

---

---

Anthracene

7.27

---

0.0400

"

"

"

---

91

57-123%

---

---

Benz(a)anthracene

7.29

---

0.0400

"

"

"

---

91

58-125%

---

---

Benzo(a)pyrene

7.85

---

0.0400

"

"

"

---

98

54-128%

---

---

Benzo(b)fluoranthene

7.84

---

0.0400

"

"

"

---

98

53-131%

---

---

Benzo(k)fluoranthene

7.60

---

0.0400

"

"

"

---

95

57-129%

---

---

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 7 of 12

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/26/16 16:36

QUALITY CONTROL (QC) SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

%REC

%REC
Limits RPD

RPD
Limit

Notes

Water

Batch 6020786 - EPA 3510C (Acid Extraction)

Prepared: 02/26/16 07:39 Analyzed: 02/26/16 11:19

LCS (6020786-BS1)

Benzo(g,h,i)perylene

Source
Result

7.13

---

0.0400

"

"

"

---

89

50-134%

---

---

Chrysene

7.26

---

0.0400

"

"

"

---

91

59-123%

---

---

Dibenz(a,h)anthracene

7.46

---

0.0400

"

"

"

---

93

51-134%

---

-----

Dibenzofuran

6.69

---

0.0400

"

"

"

---

84

53-120%

---

Fluoranthene

7.26

---

0.0400

"

"

"

---

91

57-128%

---

---

Fluorene

6.83

---

0.0400

"

"

"

---

85

52-124%

---

---

Indeno(1,2,3-cd)pyrene

7.14

---

0.0400

"

"

"

---

89

52-133%

---

---

1-Methylnaphthalene

5.60

---

0.0800

"

"

"

---

70

41-120%

---

---

2-Methylnaphthalene

5.84

---

0.0800

"

"

"

---

73

40-121%

---

---

Naphthalene

5.78

---

0.0800

"

"

"

---

72

"

---

---

Phenanthrene

7.19

---

0.0400

"

"

"

---

90

59-120%

---

---

Pyrene

7.29

---

0.0400

"

"

"

---

91

57-126%

---

---

Surr: 2-Fluorobiphenyl (Surr)

Recovery: 83 %

Limits: 44-120 %

Dilution: 1x

100 %

50-133 %

"

p-Terphenyl-d14 (Surr)

Prepared: 02/26/16 07:39 Analyzed: 02/26/16 11:47

LCS Dup (6020786-BSD1)

Q-19

EPA 8270D (SIM)

Acenaphthene

6.86

---

0.0400

ug/L

8.00

---

86

47-122%

30%

Acenaphthylene

6.91

---

0.0400

"

"

"

---

86

41-130%

30%

Anthracene

7.76

---

0.0400

"

"

"

---

97

57-123%

30%

Benz(a)anthracene

7.26

---

0.0400

"

"

"

---

91

58-125%

0.5

30%

Benzo(a)pyrene

7.87

---

0.0400

"

"

"

---

98

54-128%

0.2

30%

Benzo(b)fluoranthene

7.58

---

0.0400

"

"

"

---

95

53-131%

30%

Benzo(k)fluoranthene

7.81

---

0.0400

"

"

"

---

98

57-129%

30%

Benzo(g,h,i)perylene

7.11

---

0.0400

"

"

"

---

89

50-134%

0.4

30%

Chrysene

7.26

---

0.0400

"

"

"

---

91

59-123%

0.05

30%

Dibenz(a,h)anthracene

7.42

---

0.0400

"

"

"

---

93

51-134%

0.5

30%

Dibenzofuran

6.91

---

0.0400

"

"

"

---

86

53-120%

30%

Fluoranthene

7.28

---

0.0400

"

"

"

---

91

57-128%

0.3

30%

Fluorene

7.03

---

0.0400

"

"

"

---

88

52-124%

30%

Indeno(1,2,3-cd)pyrene

7.07

---

0.0400

"

"

"

---

88

52-133%

30%

1-Methylnaphthalene

6.30

---

0.0800

"

"

"

---

79

41-120%

12

30%

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 8 of 12

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/26/16 16:36

QUALITY CONTROL (QC) SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

%REC

%REC
Limits RPD

RPD
Limit

Prepared: 02/26/16 07:39 Analyzed: 02/26/16 11:47

LCS Dup (6020786-BSD1)

2-Methylnaphthalene

6.60

Naphthalene
Phenanthrene
Pyrene

Q-19

---

0.0800

"

"

"

---

82

6.56

---

0.0800

"

"

"

---

82

7.24

---

0.0400

"

"

"

---

91

7.39

---

"

"

"

---

92

57-126%

0.0400
Recovery: 91 %

Limits: 44-120 %

Dilution: 1x

100 %

50-133 %

"

p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Water

Batch 6020786 - EPA 3510C (Acid Extraction)

Surr: 2-Fluorobiphenyl (Surr)

Source
Result

40-121%

12

30%

"

13

30%

59-120%

0.7

30%

30%

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 9 of 12

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/26/16 16:36

SAMPLE PREPARATION INFORMATION


RBDM Compounds (BTEX+) by EPA 8260B
Sample

Default

RL Prep

Initial/Final

Initial/Final

Factor

Prep: EPA 5030B


Lab Number

Matrix

Method

Sampled

Prepared

02/25/16 13:00

02/26/16 12:03

Batch: 6020814

A6B0868-01

Water

EPA 8260B

5mL/5mL

5mL/5mL

1.00

Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM


Prep: EPA 3510C (Acid Extraction)
Lab Number

Matrix

Method

Sampled

Prepared

02/25/16 13:00

02/26/16 09:16

Sample

Default

RL Prep

Initial/Final

Initial/Final

Factor

910mL/2mL

1000mL/2mL

1.10

Batch: 6020786

A6B0868-01

Water

EPA 8270D (SIM)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 10 of 12

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/26/16 16:36

Notes and Definitions


Qualifiers:
Q-19

Blank Spike Duplicate (BSD) sample analyzed in place of Matrix Spike/Duplicate samples due to limited sample amount available for
analysis.

Notes and Conventions:


DET

Analyte DETECTED

ND

Analyte NOT DETECTED at or above the reporting limit

NR

Not Reported

dry

Sample results reported on a dry weight basis. Results listed as 'wet' or without 'dry'designation are not dry weight corrected.

RPD

Relative Percent Difference

MDL

If MDL is not listed, data has been evaluated to the Method Reporting Limit only.

WMSC

Water Miscible Solvent Correction has been applied to Results and MRLs for volatiles soil samples per EPA 8000C.

Batch
QC

Unless specifically requested, this report contains only results for Batch QC derived from client samples included in this report. All
analyses were performed with the appropriate Batch QC (including Sample Duplicates, Matrix Spikes and/or Matrix Spike Duplicates) in
order to meet or exceed method and regulatory requirements. Any exceptions to this will be qualified in this report. Complete Batch QC
results are available upon request. In cases where there is insufficient sample provided for Sample Duplicates and/or Matrix Spikes, a
Lab Control Sample Duplicate (LCS Dup) is analyzed to demonstrate accuracy and precision of the extraction and analysis.

Blank
Policy

Apex assesses blank data for potential high bias down to a level equal to the method reporting limit (MRL), except for conventional
chemistry and HCID analyses which are assessed only to the MRL. Sample results flagged with a B or B-02 qualifier are potentially
biased high if they are less than ten times the level found in the blank for inorganic analyses or less than five times the level found in the
blank for organic analyses.
For accurate comparison of volatile results to the level found in the blank; water sample results should be divided by the dilution factor,
and soil sample results should be divided by 1/50 of the sample dilution to account for the sample prep factor.
Results qualified as reported below the MRL may include a potential high bias if associated with a B or B-02 qualified blank. B and B-02
qualifications are not applied to J qualified results reported below the MRL.

---

QC results are not applicable. For example, % Recoveries for Blanks and Duplicates, % RPD for Blanks, Blank Spikes and Matrix
Spikes, etc.

***

Used to indicate a possible discrepancy with the Sample and Sample Duplicate results when the %RPD is not available. In this case,
either the Sample or the Sample Duplicate has a reportable result for this analyte, while the other is Non Detect (ND).

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 11 of 12

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
NRC-CB&I

Project: AT&T Hall Ridge

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Reported:

02/26/16 16:36

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 12 of 12

Apex Labs

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Monday, February 29, 2016


Ron Malec
NRC-CB&I
6211 N Ensign St
Portland, OR 97217

RE: AT&T Hall Ridge / 156319


Enclosed are the results of analyses for work order A6B0905, which was received by the laboratory on
2/29/2016 at 6:36:00AM.
Thank you for using Apex Labs. We appreciate your business and strive to provide the highest quality
services to the environmental industry.
If you have any questions concerning this report or the services we offer , please feel free to contact me by
email at: dthomas@apex-labs.com, or by phone at 503-718-2323.

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 1 of 19

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/29/16 17:54

ANALYTICAL REPORT FOR SAMPLES


SAMPLE INFORMATION
Sample ID

Laboratory ID

Matrix

Date Sampled

Date Received

SW-01

A6B0905-01
A6B0905-02
A6B0905-03
A6B0905-04
A6B0905-05

Water
Water
Water
Water
Water

02/28/16 07:15
02/28/16 07:30
02/28/16 07:45
02/28/16 08:00
02/28/16 09:15

02/29/16 06:36
02/29/16 06:36
02/29/16 06:36
02/29/16 06:36
02/29/16 06:36

SW-02
SW-03
SW-04
SW-05

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 2 of 19

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/29/16 17:54

ANALYTICAL SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Result

Analyte

MDL

SW-01 (A6B0905-01)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Benzene

ND

---

0.200

ug/L

02/29/16 12:13

EPA 8260B

Toluene

ND

---

1.00

"

"

"

"

Ethylbenzene

ND

---

0.500

"

"

"

"

Xylenes, total

ND

---

1.50

"

"

"

"

Naphthalene

ND

---

2.00

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

1.00

"

"

"

"

Isopropylbenzene

ND

---

1.00

"

"

"

"

n-Propylbenzene

ND

---

0.500

"

"

"

"

1,2,4-Trimethylbenzene

ND

---

1.00

"

"

"

"

1,3,5-Trimethylbenzene

ND

---

1.00

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.500

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.500

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 102 %

Limits: 80-120 %

"

"

"

99 %

Limits: 80-120 %

"

"

"

Toluene-d8 (Surr)

101 %

Limits: 80-120 %

"

"

"

4-Bromofluorobenzene (Surr)

100 %

Limits: 80-120 %

"

"

"

1,4-Difluorobenzene (Surr)

SW-02 (A6B0905-02)

Matrix: Water

Batch: 6020841

Benzene

ND

---

0.200

ug/L

02/29/16 13:10

EPA 8260B

Toluene

ND

---

1.00

"

"

"

"

Ethylbenzene

ND

---

0.500

"

"

"

"

Xylenes, total

ND

---

1.50

"

"

"

"

Naphthalene

ND

---

2.00

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

1.00

"

"

"

"

Isopropylbenzene

ND

---

1.00

"

"

"

"

n-Propylbenzene

ND

---

0.500

"

"

"

"

1,2,4-Trimethylbenzene

ND

---

1.00

"

"

"

"

1,3,5-Trimethylbenzene

ND

---

1.00

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.500

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.500

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)


1,4-Difluorobenzene (Surr)
Toluene-d8 (Surr)
4-Bromofluorobenzene (Surr)

SW-03 (A6B0905-03)

Benzene

Recovery: 102 %

Limits: 80-120 %

"

"

"

98 %

Limits: 80-120 %

"

"

"

102 %

Limits: 80-120 %

"

"

"

99 %

Limits: 80-120 %

"

"

"

02/29/16 13:39

EPA 8260B

Matrix: Water

ND

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

---

0.200

Notes

Batch: 6020841

Batch: 6020841

ug/L

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 3 of 19

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/29/16 17:54

ANALYTICAL SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Result

Analyte

MDL

SW-03 (A6B0905-03)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Toluene

ND

---

1.00

ug/L

"

EPA 8260B

Ethylbenzene

ND

---

0.500

"

"

"

"

Xylenes, total

ND

---

1.50

"

"

"

"

Naphthalene

ND

---

2.00

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

1.00

"

"

"

"

Isopropylbenzene

ND

---

1.00

"

"

"

"

n-Propylbenzene

ND

---

0.500

"

"

"

"

1,2,4-Trimethylbenzene

ND

---

1.00

"

"

"

"

1,3,5-Trimethylbenzene

ND

---

1.00

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.500

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.500

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 104 %

Limits: 80-120 %

"

"

"

1,4-Difluorobenzene (Surr)

100 %

Limits: 80-120 %

"

"

"

Toluene-d8 (Surr)

102 %

Limits: 80-120 %

"

"

"

98 %

Limits: 80-120 %

"

"

"

4-Bromofluorobenzene (Surr)

SW-04 (A6B0905-04)

Matrix: Water

Batch: 6020841

Benzene

ND

---

0.200

ug/L

02/29/16 14:08

EPA 8260B

Toluene

ND

---

1.00

"

"

"

"

Ethylbenzene

ND

---

0.500

"

"

"

"

Xylenes, total

ND

---

1.50

"

"

"

"

Naphthalene

ND

---

2.00

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

1.00

"

"

"

"

Isopropylbenzene

ND

---

1.00

"

"

"

"

n-Propylbenzene

ND

---

0.500

"

"

"

"

1,2,4-Trimethylbenzene

ND

---

1.00

"

"

"

"

1,3,5-Trimethylbenzene

ND

---

1.00

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.500

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.500

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)


1,4-Difluorobenzene (Surr)
Toluene-d8 (Surr)
4-Bromofluorobenzene (Surr)

SW-05 (A6B0905-05)

Recovery: 105 %

Limits: 80-120 %

"

"

"

99 %

Limits: 80-120 %

"

"

"

101 %

Limits: 80-120 %

"

"

"

97 %

Limits: 80-120 %

"

"

"

Matrix: Water

Batch: 6020841

Benzene

ND

---

0.200

ug/L

02/29/16 14:36

EPA 8260B

Toluene

ND

---

1.00

"

"

"

"

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020841

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 4 of 19

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/29/16 17:54

ANALYTICAL SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Result

Analyte

MDL

SW-05 (A6B0905-05)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Ethylbenzene

ND

---

0.500

ug/L

"

EPA 8260B

Xylenes, total

ND

---

1.50

"

"

"

"

Naphthalene

ND

---

2.00

"

"

"

"

Methyl tert-butyl ether (MTBE)

ND

---

1.00

"

"

"

"

Isopropylbenzene

ND

---

1.00

"

"

"

"

n-Propylbenzene

ND

---

0.500

"

"

"

"

1,2,4-Trimethylbenzene

ND

---

1.00

"

"

"

"

1,3,5-Trimethylbenzene

ND

---

1.00

"

"

"

"

1,2-Dibromoethane (EDB)

ND

---

0.500

"

"

"

"

1,2-Dichloroethane (EDC)

ND

---

0.500

"

"

"

"

Surrogate: Dibromofluoromethane (Surr)

Recovery: 105 %

Limits: 80-120 %

"

"

"

1,4-Difluorobenzene (Surr)

101 %

Limits: 80-120 %

"

"

"

Toluene-d8 (Surr)

101 %

Limits: 80-120 %

"

"

"

99 %

Limits: 80-120 %

"

"

"

4-Bromofluorobenzene (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020841

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 5 of 19

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/29/16 17:54

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

SW-01 (A6B0905-01)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Acenaphthene

ND

---

0.0392

ug/L

02/29/16 12:57

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0392

"

"

"

"

Anthracene

ND

---

0.0392

"

"

"

"

Benz(a)anthracene

ND

---

0.0392

"

"

"

"

Benzo(a)pyrene

ND

---

0.0392

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0392

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0392

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0392

"

"

"

"

Chrysene

ND

---

0.0392

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0392

"

"

"

"

Dibenzofuran

ND

---

0.0392

"

"

"

"

Fluoranthene

ND

---

0.0392

"

"

"

"

Fluorene

ND

---

0.0392

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0392

"

"

"

"

1-Methylnaphthalene

ND

---

0.0784

"

"

"

"

2-Methylnaphthalene

ND

---

0.0784

"

"

"

"

Naphthalene

ND

---

0.0784

"

"

"

"

Phenanthrene

ND

---

0.0392

"

"

"

"

Pyrene

ND

---

0.0392

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020838

Recovery: 83 %

Limits: 44-120 %

"

"

"

114 %

Limits: 50-133 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 6 of 19

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/29/16 17:54

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

SW-02 (A6B0905-02)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Acenaphthene

ND

---

0.0404

ug/L

02/29/16 13:24

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0404

"

"

"

"

Anthracene

ND

---

0.0404

"

"

"

"

Benz(a)anthracene

ND

---

0.0404

"

"

"

"

Benzo(a)pyrene

ND

---

0.0404

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0404

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0404

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0404

"

"

"

"

Chrysene

ND

---

0.0404

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0404

"

"

"

"

Dibenzofuran

ND

---

0.0404

"

"

"

"

Fluoranthene

ND

---

0.0404

"

"

"

"

Fluorene

ND

---

0.0404

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0404

"

"

"

"

1-Methylnaphthalene

ND

---

0.0808

"

"

"

"

2-Methylnaphthalene

ND

---

0.0808

"

"

"

"

Naphthalene

ND

---

0.0808

"

"

"

"

Phenanthrene

ND

---

0.0404

"

"

"

"

Pyrene

ND

---

0.0404

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020838

Recovery: 82 %

Limits: 44-120 %

"

"

"

115 %

Limits: 50-133 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 7 of 19

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/29/16 17:54

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

SW-03 (A6B0905-03)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Acenaphthene

ND

---

0.0421

ug/L

02/29/16 13:52

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0421

"

"

"

"

Anthracene

ND

---

0.0421

"

"

"

"

Benz(a)anthracene

ND

---

0.0421

"

"

"

"

Benzo(a)pyrene

ND

---

0.0421

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0421

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0421

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0421

"

"

"

"

Chrysene

ND

---

0.0421

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0421

"

"

"

"

Dibenzofuran

ND

---

0.0421

"

"

"

"

Fluoranthene

ND

---

0.0421

"

"

"

"

Fluorene

ND

---

0.0421

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0421

"

"

"

"

1-Methylnaphthalene

ND

---

0.0842

"

"

"

"

2-Methylnaphthalene

ND

---

0.0842

"

"

"

"

Naphthalene

ND

---

0.0842

"

"

"

"

Phenanthrene

ND

---

0.0421

"

"

"

"

Pyrene

ND

---

0.0421

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020838

Recovery: 67 %

Limits: 44-120 %

"

"

"

109 %

Limits: 50-133 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 8 of 19

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/29/16 17:54

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

SW-04 (A6B0905-04)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Acenaphthene

ND

---

0.0408

ug/L

02/29/16 14:19

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0408

"

"

"

"

Anthracene

ND

---

0.0408

"

"

"

"

Benz(a)anthracene

ND

---

0.0408

"

"

"

"

Benzo(a)pyrene

ND

---

0.0408

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0408

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0408

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0408

"

"

"

"

Chrysene

ND

---

0.0408

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0408

"

"

"

"

Dibenzofuran

ND

---

0.0408

"

"

"

"

Fluoranthene

ND

---

0.0408

"

"

"

"

Fluorene

ND

---

0.0408

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0408

"

"

"

"

1-Methylnaphthalene

ND

---

0.0816

"

"

"

"

2-Methylnaphthalene

ND

---

0.0816

"

"

"

"

Naphthalene

ND

---

0.0816

"

"

"

"

Phenanthrene

ND

---

0.0408

"

"

"

"

Pyrene

ND

---

0.0408

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020838

Recovery: 86 %

Limits: 44-120 %

"

"

"

110 %

Limits: 50-133 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 9 of 19

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/29/16 17:54

ANALYTICAL SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Result

Analyte

MDL

SW-05 (A6B0905-05)

Reporting
Limit

Dilution

Units

Matrix: Water

Date Analyzed

Method

Acenaphthene

ND

---

0.0440

ug/L

02/29/16 14:46

EPA 8270D (SIM)

Acenaphthylene

ND

---

0.0440

"

"

"

"

Anthracene

ND

---

0.0440

"

"

"

"

Benz(a)anthracene

ND

---

0.0440

"

"

"

"

Benzo(a)pyrene

ND

---

0.0440

"

"

"

"

Benzo(b)fluoranthene

ND

---

0.0440

"

"

"

"

Benzo(k)fluoranthene

ND

---

0.0440

"

"

"

"

Benzo(g,h,i)perylene

ND

---

0.0440

"

"

"

"

Chrysene

ND

---

0.0440

"

"

"

"

Dibenz(a,h)anthracene

ND

---

0.0440

"

"

"

"

Dibenzofuran

ND

---

0.0440

"

"

"

"

Fluoranthene

ND

---

0.0440

"

"

"

"

Fluorene

ND

---

0.0440

"

"

"

"

Indeno(1,2,3-cd)pyrene

ND

---

0.0440

"

"

"

"

1-Methylnaphthalene

ND

---

0.0879

"

"

"

"

2-Methylnaphthalene

ND

---

0.0879

"

"

"

"

Naphthalene

ND

---

0.0879

"

"

"

"

Phenanthrene

ND

---

0.0440

"

"

"

"

Pyrene

ND

---

0.0440

"

"

"

"

Surrogate: 2-Fluorobiphenyl (Surr)


p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Batch: 6020838

Recovery: 78 %

Limits: 44-120 %

"

"

"

115 %

Limits: 50-133 %

"

"

"

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 10 of 19

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/29/16 17:54

QUALITY CONTROL (QC) SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Analyte

Result

MDL

Reporting
Limit

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

RPD
Limit

Notes

Water

Batch 6020841 - EPA 5030B

Prepared: 02/29/16 09:00 Analyzed: 02/29/16 11:45

Blank (6020841-BLK1)
EPA 8260B

Benzene

ND

---

0.200

ug/L

---

---

---

---

---

---

Toluene

ND

---

1.00

"

"

---

---

---

---

---

---

Ethylbenzene

ND

---

0.500

"

"

---

---

---

---

---

---

Xylenes, total

ND

---

1.50

"

"

---

---

---

---

---

---

Naphthalene

ND

---

2.00

"

"

---

---

---

---

---

---

Methyl tert-butyl ether


(MTBE)
Isopropylbenzene

ND

---

1.00

"

"

---

---

---

---

---

---

ND

---

1.00

"

"

---

---

---

---

---

---

n-Propylbenzene

ND

---

0.500

"

"

---

---

---

---

---

---

1,2,4-Trimethylbenzene

ND

---

1.00

"

"

---

---

---

---

---

---

1,3,5-Trimethylbenzene

ND

---

1.00

"

"

---

---

---

---

---

---

1,2-Dibromoethane (EDB)

ND

---

0.500

"

"

---

---

---

---

---

---

1,2-Dichloroethane (EDC)

ND

---

0.500

"

"

---

---

---

---

---

---

---

---

Surr: Dibromofluoromethane (Surr)

Recovery: 100 %

Limits: 80-120 %

Dilution: 1x

99 %

80-120 %

"

101 %

80-120 %

"

99 %

80-120 %

"

1,4-Difluorobenzene (Surr)
Toluene-d8 (Surr)
4-Bromofluorobenzene (Surr)

Prepared: 02/29/16 09:00 Analyzed: 02/29/16 10:19

LCS (6020841-BS1)
EPA 8260B

Benzene

18.9

---

0.200

ug/L

20.0

---

94

70-130%

Toluene

20.0

---

1.00

"

"

"

---

100

"

---

---

Ethylbenzene

20.2

---

0.500

"

"

"

---

101

"

---

---

Xylenes, total

61.0

---

1.50

"

"

60.0

---

102

"

---

---

Naphthalene

17.1

---

2.00

"

"

20.0

---

86

"

---

---

Methyl tert-butyl ether


(MTBE)
Isopropylbenzene

18.7

---

1.00

"

"

"

---

93

"

---

---

20.5

---

1.00

"

"

"

---

103

"

---

---

n-Propylbenzene

19.6

---

0.500

"

"

"

---

98

"

---

---

1,2,4-Trimethylbenzene

20.2

---

1.00

"

"

"

---

101

"

---

---

1,3,5-Trimethylbenzene

19.9

---

1.00

"

"

"

---

100

"

---

---

1,2-Dibromoethane (EDB)

20.7

---

0.500

"

"

"

---

103

"

---

---

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 11 of 19

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/29/16 17:54

QUALITY CONTROL (QC) SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

%REC

%REC
Limits RPD

RPD
Limit

Notes

Water

Batch 6020841 - EPA 5030B

Prepared: 02/29/16 09:00 Analyzed: 02/29/16 10:19

LCS (6020841-BS1)

1,2-Dichloroethane (EDC)

Source
Result

19.0

---

Surr: Dibromofluoromethane (Surr)

0.500

ug/L

"

"

---

Recovery: 98 %

Limits: 80-120 %

Dilution: 1x

1,4-Difluorobenzene (Surr)

95 %

80-120 %

"

Toluene-d8 (Surr)

99 %

80-120 %

"

4-Bromofluorobenzene (Surr)

99 %

80-120 %

"

95

"

---

---

Prepared: 02/29/16 11:35 Analyzed: 02/29/16 12:43

Duplicate (6020841-DUP1)
QC Source Sample: SW-01 (A6B0905-01)
EPA 8260B

Benzene

ND

---

0.200

ug/L

---

ND

---

---

---

30%

Toluene

ND

Ethylbenzene

ND

---

1.00

"

"

---

ND

---

---

---

30%

---

0.500

"

"

---

ND

---

---

---

30%

Xylenes, total
Naphthalene

ND

---

1.50

"

"

---

ND

---

---

---

30%

ND

---

2.00

"

"

---

ND

---

---

---

30%

Methyl tert-butyl ether


(MTBE)
Isopropylbenzene

ND

---

1.00

"

"

---

ND

---

---

---

30%

ND

---

1.00

"

"

---

ND

---

---

---

30%

n-Propylbenzene

ND

---

0.500

"

"

---

ND

---

---

---

30%

1,2,4-Trimethylbenzene

ND

---

1.00

"

"

---

ND

---

---

---

30%

1,3,5-Trimethylbenzene

ND

---

1.00

"

"

---

ND

---

---

---

30%

1,2-Dibromoethane (EDB)

ND

---

0.500

"

"

---

ND

---

---

---

30%

1,2-Dichloroethane (EDC)

ND

---

0.500

"

"

---

ND

---

---

---

30%

Surr: Dibromofluoromethane (Surr)

Recovery: 102 %

Limits: 80-120 %

Dilution: 1x

99 %

80-120 %

"

102 %

80-120 %

"

98 %

80-120 %

"

1,4-Difluorobenzene (Surr)
Toluene-d8 (Surr)
4-Bromofluorobenzene (Surr)

Prepared: 02/29/16 11:35 Analyzed: 02/29/16 15:05

Matrix Spike (6020841-MS1)


QC Source Sample: SW-05 (A6B0905-05)
EPA 8260B

Benzene

20.8

---

0.200

ug/L

20.0

ND

104

70-130%

---

---

Toluene

21.5

---

1.00

"

"

"

ND

108

"

---

---

Ethylbenzene

21.8

---

0.500

"

"

"

ND

109

"

---

---

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 12 of 19

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/29/16 17:54

QUALITY CONTROL (QC) SAMPLE RESULTS


RBDM Compounds (BTEX+) by EPA 8260B
Analyte

Result

MDL

Reporting
Limit

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

RPD
Limit

Notes

Water

Batch 6020841 - EPA 5030B

Prepared: 02/29/16 11:35 Analyzed: 02/29/16 15:05

Matrix Spike (6020841-MS1)


QC Source Sample: SW-05 (A6B0905-05)

Xylenes, total

65.0

---

1.50

ug/L

"

60.0

ND

108

"

---

---

Naphthalene

16.8

---

2.00

"

"

20.0

ND

84

"

---

---

Methyl tert-butyl ether


(MTBE)
Isopropylbenzene

19.3

---

1.00

"

"

"

ND

96

"

---

---

22.2

---

1.00

"

"

"

ND

111

"

---

---

n-Propylbenzene

20.8

---

0.500

"

"

"

ND

104

"

---

---

1,2,4-Trimethylbenzene

20.8

---

1.00

"

"

"

ND

104

"

---

---

1,3,5-Trimethylbenzene

21.0

---

1.00

"

"

"

ND

105

"

---

---

1,2-Dibromoethane (EDB)

21.6

---

0.500

"

"

"

ND

108

"

---

---

1,2-Dichloroethane (EDC)

20.5

---

0.500

"

"

"

ND

102

"

---

---

Surr: Dibromofluoromethane (Surr)

Recovery: 100 %

Limits: 80-120 %

Dilution: 1x

1,4-Difluorobenzene (Surr)

97 %

80-120 %

"

Toluene-d8 (Surr)

99 %

80-120 %

"

4-Bromofluorobenzene (Surr)

97 %

80-120 %

"

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 13 of 19

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/29/16 17:54

QUALITY CONTROL (QC) SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

Source
Result

%REC

%REC
Limits RPD

RPD
Limit

Notes

Water

Batch 6020838 - EPA 3510C (Acid Extraction)

Prepared: 02/29/16 07:30 Analyzed: 02/29/16 10:42

Blank (6020838-BLK1)
EPA 8270D (SIM)

Acenaphthene

ND

---

0.0364

ug/L

---

---

---

---

---

---

Acenaphthylene

ND

---

0.0364

"

"

---

---

---

---

---

---

Anthracene

ND

---

0.0364

"

"

---

---

---

---

---

---

Benz(a)anthracene

ND

---

0.0364

"

"

---

---

---

---

---

---

Benzo(a)pyrene

ND

---

0.0364

"

"

---

---

---

---

---

-----

Benzo(b)fluoranthene

ND

---

0.0364

"

"

---

---

---

---

---

Benzo(k)fluoranthene

ND

---

0.0364

"

"

---

---

---

---

---

---

Benzo(g,h,i)perylene

ND

---

0.0364

"

"

---

---

---

---

---

---

Chrysene

ND

---

0.0364

"

"

---

---

---

---

---

---

Dibenz(a,h)anthracene

ND

---

0.0364

"

"

---

---

---

---

---

---

Dibenzofuran

ND

---

0.0364

"

"

---

---

---

---

---

---

Fluoranthene

ND

---

0.0364

"

"

---

---

---

---

---

---

Fluorene

ND

---

0.0364

"

"

---

---

---

---

---

---

Indeno(1,2,3-cd)pyrene

ND

---

0.0364

"

"

---

---

---

---

---

---

1-Methylnaphthalene

ND

---

0.0727

"

"

---

---

---

---

---

---

2-Methylnaphthalene

ND

---

0.0727

"

"

---

---

---

---

---

---

Naphthalene

ND

---

0.0727

"

"

---

---

---

---

---

---

Phenanthrene

ND

---

0.0364

"

"

---

---

---

---

---

---

Pyrene

ND

---

0.0364

"

"

---

---

---

---

---

---

---

Surr: 2-Fluorobiphenyl (Surr)

Recovery: 97 %

Limits: 44-120 %

Dilution: 1x

126 %

50-133 %

"

p-Terphenyl-d14 (Surr)

Prepared: 02/29/16 07:30 Analyzed: 02/29/16 11:09

LCS (6020838-BS1)
EPA 8270D (SIM)

Acenaphthene

6.88

---

0.0400

ug/L

8.00

---

86

47-122%

---

Acenaphthylene

6.99

---

0.0400

"

"

"

---

87

41-130%

---

---

Anthracene

7.45

---

0.0400

"

"

"

---

93

57-123%

---

---

Benz(a)anthracene

7.32

---

0.0400

"

"

"

---

92

58-125%

---

---

Benzo(a)pyrene

7.90

---

0.0400

"

"

"

---

99

54-128%

---

---

Benzo(b)fluoranthene

7.86

---

0.0400

"

"

"

---

98

53-131%

---

---

Benzo(k)fluoranthene

8.18

---

0.0400

"

"

"

---

102

57-129%

---

---

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 14 of 19

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/29/16 17:54

QUALITY CONTROL (QC) SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

%REC

%REC
Limits RPD

RPD
Limit

Notes

Water

Batch 6020838 - EPA 3510C (Acid Extraction)

Prepared: 02/29/16 07:30 Analyzed: 02/29/16 11:09

LCS (6020838-BS1)

Benzo(g,h,i)perylene

Source
Result

6.28

---

0.0400

"

"

"

---

78

50-134%

---

---

Chrysene

7.23

---

0.0400

"

"

"

---

90

59-123%

---

---

Dibenz(a,h)anthracene

7.25

---

0.0400

"

"

"

---

91

51-134%

---

-----

Dibenzofuran

7.12

---

0.0400

"

"

"

---

89

53-120%

---

Fluoranthene

7.07

---

0.0400

"

"

"

---

88

57-128%

---

---

Fluorene

7.17

---

0.0400

"

"

"

---

90

52-124%

---

---

Indeno(1,2,3-cd)pyrene

6.66

---

0.0400

"

"

"

---

83

52-133%

---

---

1-Methylnaphthalene

6.48

---

0.0800

"

"

"

---

81

41-120%

---

---

2-Methylnaphthalene

6.84

---

0.0800

"

"

"

---

85

40-121%

---

---

Naphthalene

6.62

---

0.0800

"

"

"

---

83

"

---

---

Phenanthrene

7.43

---

0.0400

"

"

"

---

93

59-120%

---

---

Pyrene

7.02

---

0.0400

"

"

"

---

88

57-126%

---

---

Surr: 2-Fluorobiphenyl (Surr)

Recovery: 91 %

Limits: 44-120 %

Dilution: 1x

112 %

50-133 %

"

p-Terphenyl-d14 (Surr)

Prepared: 02/29/16 07:30 Analyzed: 02/29/16 11:36

LCS Dup (6020838-BSD1)

Q-19

EPA 8270D (SIM)

Acenaphthene

6.36

---

0.0400

ug/L

8.00

---

80

47-122%

30%

Acenaphthylene

6.48

---

0.0400

"

"

"

---

81

41-130%

30%

Anthracene

7.06

---

0.0400

"

"

"

---

88

57-123%

30%

Benz(a)anthracene

7.19

---

0.0400

"

"

"

---

90

58-125%

30%

Benzo(a)pyrene

7.78

---

0.0400

"

"

"

---

97

54-128%

30%

Benzo(b)fluoranthene

8.07

---

0.0400

"

"

"

---

101

53-131%

30%

Benzo(k)fluoranthene

7.91

---

0.0400

"

"

"

---

99

57-129%

30%

Benzo(g,h,i)perylene

6.03

---

0.0400

"

"

"

---

75

50-134%

30%

Chrysene

7.16

---

0.0400

"

"

"

---

89

59-123%

30%

Dibenz(a,h)anthracene

7.05

---

0.0400

"

"

"

---

88

51-134%

30%

Dibenzofuran

6.67

---

0.0400

"

"

"

---

83

53-120%

30%

Fluoranthene

6.63

---

0.0400

"

"

"

---

83

57-128%

30%

Fluorene

6.79

---

0.0400

"

"

"

---

85

52-124%

30%

Indeno(1,2,3-cd)pyrene

6.49

---

0.0400

"

"

"

---

81

52-133%

30%

1-Methylnaphthalene

5.81

---

0.0800

"

"

"

---

73

41-120%

11

30%

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 15 of 19

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/29/16 17:54

QUALITY CONTROL (QC) SAMPLE RESULTS


Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM
Analyte

Result

Reporting
Limit

MDL

Units

Dil.

Spike
Amount

%REC

%REC
Limits RPD

RPD
Limit

Prepared: 02/29/16 07:30 Analyzed: 02/29/16 11:36

LCS Dup (6020838-BSD1)

2-Methylnaphthalene

6.05

Naphthalene
Phenanthrene
Pyrene

---

0.0800

"

"

"

---

76

5.95

---

0.0800

"

"

"

---

7.07

---

0.0400

"

"

"

---

6.59

---

"

"

"

---

0.0400
Recovery: 83 %

Limits: 44-120 %

Dilution: 1x

113 %

50-133 %

"

p-Terphenyl-d14 (Surr)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Notes

Water

Batch 6020838 - EPA 3510C (Acid Extraction)

Surr: 2-Fluorobiphenyl (Surr)

Source
Result

Q-19

40-121%

12

30%

74

"

11

30%

88

59-120%

30%

82

57-126%

30%

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 16 of 19

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/29/16 17:54

SAMPLE PREPARATION INFORMATION


RBDM Compounds (BTEX+) by EPA 8260B
Sample

Default

RL Prep

Initial/Final

Initial/Final

Factor

Prep: EPA 5030B


Lab Number

Matrix

Method

Sampled

Prepared

02/28/16 07:15
02/28/16 07:30
02/28/16 07:45
02/28/16 08:00
02/28/16 09:15

02/29/16 11:35
02/29/16 11:35
02/29/16 11:35
02/29/16 11:35
02/29/16 11:35

Batch: 6020841

A6B0905-01
A6B0905-02
A6B0905-03
A6B0905-04
A6B0905-05

Water
Water
Water
Water
Water

EPA 8260B
EPA 8260B
EPA 8260B
EPA 8260B
EPA 8260B

5mL/5mL
5mL/5mL
5mL/5mL
5mL/5mL
5mL/5mL

5mL/5mL
5mL/5mL
5mL/5mL
5mL/5mL
5mL/5mL

1.00
1.00
1.00
1.00
1.00

Polyaromatic Hydrocarbons (PAHs) by EPA 8270D SIM


Prep: EPA 3510C (Acid Extraction)
Lab Number

Matrix

Method

Sampled

Prepared

02/28/16 07:15
02/28/16 07:30
02/28/16 07:45
02/28/16 08:00
02/28/16 09:15

02/29/16 10:09
02/29/16 10:09
02/29/16 10:09
02/29/16 10:09
02/29/16 10:09

Sample

Default

RL Prep

Initial/Final

Initial/Final

Factor

1000mL/2mL
1000mL/2mL
1000mL/2mL
1000mL/2mL
1000mL/2mL

0.98
1.01
1.05
1.02
1.10

Batch: 6020838

A6B0905-01
A6B0905-02
A6B0905-03
A6B0905-04
A6B0905-05

Water
Water
Water
Water
Water

EPA 8270D (SIM)


EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)
EPA 8270D (SIM)

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

1020mL/2mL
990mL/2mL
950mL/2mL
980mL/2mL
910mL/2mL

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 17 of 19

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
Project: AT&T Hall Ridge

NRC-CB&I

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

Reported:

02/29/16 17:54

Notes and Definitions


Qualifiers:
Q-19

Blank Spike Duplicate (BSD) sample analyzed in place of Matrix Spike/Duplicate samples due to limited sample amount available for
analysis.

Notes and Conventions:


DET

Analyte DETECTED

ND

Analyte NOT DETECTED at or above the reporting limit

NR

Not Reported

dry

Sample results reported on a dry weight basis. Results listed as 'wet' or without 'dry'designation are not dry weight corrected.

RPD

Relative Percent Difference

MDL

If MDL is not listed, data has been evaluated to the Method Reporting Limit only.

WMSC

Water Miscible Solvent Correction has been applied to Results and MRLs for volatiles soil samples per EPA 8000C.

Batch
QC

Unless specifically requested, this report contains only results for Batch QC derived from client samples included in this report. All
analyses were performed with the appropriate Batch QC (including Sample Duplicates, Matrix Spikes and/or Matrix Spike Duplicates) in
order to meet or exceed method and regulatory requirements. Any exceptions to this will be qualified in this report. Complete Batch QC
results are available upon request. In cases where there is insufficient sample provided for Sample Duplicates and/or Matrix Spikes, a
Lab Control Sample Duplicate (LCS Dup) is analyzed to demonstrate accuracy and precision of the extraction and analysis.

Blank
Policy

Apex assesses blank data for potential high bias down to a level equal to the method reporting limit (MRL), except for conventional
chemistry and HCID analyses which are assessed only to the MRL. Sample results flagged with a B or B-02 qualifier are potentially
biased high if they are less than ten times the level found in the blank for inorganic analyses or less than five times the level found in the
blank for organic analyses.
For accurate comparison of volatile results to the level found in the blank; water sample results should be divided by the dilution factor,
and soil sample results should be divided by 1/50 of the sample dilution to account for the sample prep factor.
Results qualified as reported below the MRL may include a potential high bias if associated with a B or B-02 qualified blank. B and B-02
qualifications are not applied to J qualified results reported below the MRL.

---

QC results are not applicable. For example, % Recoveries for Blanks and Duplicates, % RPD for Blanks, Blank Spikes and Matrix
Spikes, etc.

***

Used to indicate a possible discrepancy with the Sample and Sample Duplicate results when the %RPD is not available. In this case,
either the Sample or the Sample Duplicate has a reportable result for this analyte, while the other is Non Detect (ND).

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 18 of 19

12232 S.W. Garden Place


Tigard, OR 97223
503-718-2323 Phone
503-718-0333 Fax

Apex Labs
NRC-CB&I

Project: AT&T Hall Ridge

6211 N Ensign St

Project Number: 156319

Portland, OR 97217

Project Manager: Ron Malec

DRAFT REPORT

DRAFT REPORT, DATA SUBJECT TO CHANGE

Reported:

02/29/16 17:54

The results provided in this report are PRELIMINARY and are subject to change based
on subsequent analysis, QC validation or final data review. Please use these results
with the understanding that they may have not been finalized by the laboratory

Page 19 of 19

AppendixB
BiostimulationProductInformation

Overview'of'OSE'II!
OSE$II:$
! Invented$in$1989.$$
! Manufactured$in$the$USA.$
! Used$in$more$than$40$countries$across$the$world.$$
! Remediated$more$than$28,000$spills$and$contaminated$sites.$

$
$
Features$of$OSE$II$include:$
! 100%$biodegradable$and$nonItoxic.$
! Effective$in$remediating$all$types$of$hydrocarbons$$fresh$and$weathered.$
! Easily$applied$and$no$need$for$special$protective$clothing.$
! Effective$in$a$large$range$of$temperatures.$
! Enhances$natures$process$for$bioIremediating$hydrocarbons.$

How$OSE$II$works:$

Process'and'benets!
When$combined$with$fresh$or$salt$water,$OSE$II$breaks$down$the$molecular$
structure$of$hydrocarbons$through$the$effects$of$bioIsurfactants,$followed$
by$enzymes$developing$protein$binding$sites$and$acting$as$a$catalyst,$while$
enhancing$indigenous$bacteria$to$rapidly$colonize.$$$
$

The$enhanced$bacteria$use$the$detoxiSied$hydrocarbons$as$a$food$source$via$
the$enzymatic$catalyst,$digesting$the$hydrocarbon$based$material$to$carbon$
dioxide$and$water.$
BeneSits$of$using$OSE$II:$$
!

Remediating$hydrocarbon$contaminated$soil,$water$and$waste.$$
The$toxins$and$contaminants$are$removed$from$the$environment,$
not$transferred.$

Cleaning$up$oil$spills$/$contaminated$areas$without$having$to$
separate$and$dispose$of$hydrocarbon$contaminated$waste.$$$

OSE$II$is$effective$in$cleaning$large$contaminated$sites$enabling$
land$to$be$returned$to$preIspill$conditions$and$re#vegetated$and$
restored$for$beneSicial$use.$$$

Kadhema$ScientiSic$Consultancy$&$Services$will$manage$the$
revegetation$for$the$project.$

Its$ability$to$be$used$in$sensitive$environments$as$it$is$nonI
hazardous$and$can$be$applied$in$a$variety$of$ways$preventing$
physical$damage$as$a$result$of$access$to$difSicult$to$reach$
locations.$

Comparing'OSE'II'with'tradi;onal'methods!
Excavation$
Contaminated$materials$are$
dug$up$and$loaded$into$trucks$
for$transport$I$expensive$
process$and$risks$associated$
with$transporting$hazardous$
waste.$
Dust$is$generated$from$the$
excavation$and$truck$
movements.$
Waste$requires$disposal$at$
facility$licensed$to$receive$
hazardous$waste.$$Expensive$
to$dispose$of$hazardous$waste$
I$limited$facilities$available.$
Equipment$used$for$
extraction$must$be$thoroughly$
cleaned$and$decontaminated$
prior$to$leaving$the$site.$
Digging$up$and$hauling$off$
soil$/$sand$may$have$impacts$
on$local$ecology.$

Incineration$
Requires$extremely$high$
temperatures$(therefore$
energy)$to$break$down$
contaminants$into$nontoxic$
substances,$such$as$water,$
carbon$dioxide,$and$nitrogen$
oxides.$
Unlikely$that$100%$of$the$
hazardous$waste$is$destroyed$
during$the$incineration$
process.$
Leftover$ash$and$material$
removed$from$the$incinerator$
is$hazardous$and$requires$
disposal$at$a$facility$licenced$
to$receive$hazardous$waste.$
Air$emissions$and$odour$
possible$if$process$is$not$
efSicient.$

Thermal$desorption$
Extreme$safety$precautions$
required$due$to$elevated$
heating$at$the$site.$
Responders$need$to$wear$
special$protective$gear.$
Size$of$particles$can$restrict$
clean$up,$or$produce$a$
secondary$required$process.$

Bioremediation$OSE$II$
No$speciSic$precautions$need$
to$be$taken.$
No$speciSic$protective$clothing$
required$when$handling$OSE$
II.$
Particle$size$does$not$affect$
remediation.$
No$vapours$emitted.$

Harmful$vapours$given$off$
that$need$to$be$captured$for$
secondary$processing.$
Soil$needs$reprocessing$to$
complete$removal$of$
contaminants.$
Area$to$be$heated$up,$or$
mobile$unit$has$limitations$of$
size$or$amount$of$soil$to$be$
addressed$at$one$time.$
Potentially$higher$risks$and$
insurance$costs.$
In$relation$to$soil.$$Sterilizes$
soil,$making$it$virtually$
useless.$

OSE$II$is$a$oneItime$
application$and$treats$
contamination$at$the$source.$$
No$disposal$of$waste$is$
required.$
OSE$II$can$be$applied$to$an$
indeSinite$area.$
Emulates$natures$process$
allowing$soil$to$be$returned$to$
pre$contamination$conditions,$
converting$soil$into$a$valuable$
top$soil$for$resale.$

Tes;ng'&'approval'across'the'world'!
Extensive$efSicacy$and$toxicity$testing$have$contributed$to$OSE$II$being$recognized$as$an$effective$oil$spill$and$
bioremediation$product$and$is$approved$for$the$following:$
!

Regional$Organization$for$the$Protection$of$the$Marine$Environment$(ROPME)$Marine$Emergency$Mutual$
Aid$Centre$(MEMAC)$Oil$Spill$Combating$Product$(approval$Ref:$337/12IRHD).$$This$includes:$

o State$of$Kuwait$
o State$of$Oman$
o State$of$Qatar$
$
$
$
$
$
$
o Kingdom$of$Saudi$
o United$Arab$Emirates$
o Kingdom$of$Bahrain$
o Islamic$Republic$of$Iran$
o Republic$of$Iraq$
US$Environmental$Protection$Agencys$National$Contingency$Plan$for$Oil$Spills$(US$EPA$NCP$#$B53).$

UK$Marine$Management$Organization$(ODA$241/2015).$

Australian$Maritime$Safety$Authoritys$National$Plan$to$Combat$the$Pollution$of$the$Sea$by$Oil$and$Other$
Noxious$and$Hazardous$Substances$(#OBA$Bioremediation$Oil$Spill$Control$Agent).$

New$Zealand$Environment$Protection$Authority,$Status$of$Substance$(SOS$#1001797).$

Greece$(ID$no:$17554);$Philippines$(accreditation$#PCGI14I06I112);$Nigeria$(NOSDRA$cert:$189);$Mexico;$
Israel;$Trinidad$and$Tobago;$and$South$Korea$(cert$no:$SI007).$$

$$

Business'case'for'OSE'II!
OSE$II$is$suited$to$large$contaminated$areas$due$to$the$ease$of$application$and$ability$to$treat$
contaminated$soil$at$the$source.$
$$
The$following$expenses$are$eliminated$when$OSE$II$is$used:$
! Clean$up$and$/$or$disposal$of$equipment$and$material$contaminated$with$hydrocarbons.$
! Treatment$of$contaminated$soil,$contaminated$water,$oily$sludge$or$mud$prior$to$disposal.$
! Extraction,$transport$and$disposal$of$contaminated$soil$(including$mud,$sludge)$and$water.$
$$
The$following$risks$are$eliminated$when$OSE$II$is$used:$
! Accidental$release$and$spill$during$transit$to$waste$facility.$
! Contaminants$not$completely$removed$from$the$environment$resulting$in$long$term$impact.$
! Having$to$relocate$the$contaminated$soil$for$treatment$at$another$facility.$
$$

Conclusion!
Clean$up$using$OSE$II$will$return$contaminated$land$to$pre$spill$conditions,$suitable$for$reI
vegetating$and$restoring.$$

OIL SPILL EATER II | NCP Product Schedule | Emergency Management | US EPA

Page 1 of 4

Emergency Management
You are here: EPA Home Emergency Management
Schedule OIL SPILL EATER II

NCP Subpart J

NCP Product

OIL SPILL EATER II

TECHNICAL PRODUCT BULLETIN #B-53


USEPA, OFFICE OF EMERGENCY MANAGEMENT
REGULATION AND POLICY DEVELOPMENT DIVISION
ORIGINAL LISTING DATE: AUGUST 26, 1996
REMOVAL DATE: AUGUST 16, 2005
RELISTING DATE: SEPTEMBER 18, 2009
"OIL SPILL EATER II (OSE II)"
I. NAME, BRAND, OR TRADEMARK
OIL SPILL EATER II (OSE II)
Type of Product: Bioremediation Agent (Biological Enzyme Additive [previously listed as a
Nutrient Additive])
II. NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
OSEI Corporation (Formerly Sky Blue Chems)
P.O. Box 515429
Dallas, TX 75251-5429
Phone: (972) 669-3390
E-mail: oseicorp@msn.com
Web Site: www.osei.us
(Mr. Steven Pedigo, Chairman, CEO, Inventor)
III. NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
OSEI Corporation (Formerly Sky Blue Chems)
P.O. Box 515429
Dallas, TX 75251-5429
Phone: (972) 669-3390
E-mail: oseicorp@msn.com
Web Site: www.osei.us
(Mr. Steven Pedigo, Chairman, CEO, Inventor)

IV. SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION
1. Flammability: Water-based, non-flammable
2. Ventilation: Needs no ventilation; aqueous-based product; does not emit hazardous
vapors
3. Skin and eye contact; protective clothing; treatment in case of contact: OSE II is not a
primary dermal irritant. Avoid eye contact, and wear goggles if possible for the spray to
come in direct contact with eyes. Facilities for quick and copious eye flushing should be
provided and prompt medical attention should be sought if exposure and irritation persists.
Protective rubber gloves are suggested during handling. Before mixing the product has a
smell of fermentation. The product does not give off any harmful vapors.
4.a. Maximum storage temperature: 120F

http://www.epa.gov/emergencies/content/ncp/products/oseater.htm

4/3/2011

OIL SPILL EATER II | NCP Product Schedule | Emergency Management | US EPA

Page 2 of 4

4.b. Minimum storage temperature: None; OSE II can freeze and thaw without adverse
effects
4.c. Optimum storage temperature range: 72F
4.d. Temperatures of phase separations and chemical changes: 120F
V. SHELF LIFE
OSE II has a recommended shelf life of 5 years. After 5 years at optimum storage
temperature, there is an approximate 10% decrease per year in product capability.
VI. RECOMMENDED APPLICATION PROCEDURE
1. Application Method:
A. Use surface spray apparatus, such as small hand held tanks, back pack, large mixing
tanks with mechanical pumping devices, vessels with booms for spraying wide paths, or
spray devices on airplanes or helicopters.
B. OSE II can be applied by eductor systems from vessels, fire trucks, etc. Set the eductor
system to 2% and apply 1 gallon of mixed OSE II to each spilled gallon of hydrocarbon.
2. Concentration/Application Rate:
General - OSE II generally takes 3 to 30 minutes to penetrate the molecular walls of
hydrocarbons. However, once you spray OSE II on the hydrocarbons, OSE II attaches itself
and will eventually engulf the hydrocarbons regardless of where the hydrocarbons may
spread on the surface of salt or fresh water. Additionally, once you spray OSE II, the
hydrocarbons cannot attach itself to the shoreline, rocks, or any equipment in its path. OSE
II breaks down the adhesion properties of hydrocarbons and causes hydrocarbons to float,
thereby, eliminating secondary contamination of the water column or any other areas, and
holding the contaminated area to the waters surface, the original contaminated area.
If OSE II is to be used on ocean spills or on intertidal zones OSE II should be mixed
with ocean water.
If OSE II is to be used on lakes, rivers, streams, ponds, or on land mix the product
with water from a lake, stream, or pond.
If you are performing a clean up, make sure the water used to mix with OSE II, and
the water used to keep the area saturated, is the type of water normally associated
with that area.
If you use fresh water in an area normally contacted with salt water or vice versa,
the different types of bacteria and competition could occur, not to mention the
problems with salinity for fresh water organisms.
[Note: Do not mix tap water with OSE II if possible: Chlorine in tap water slows bacterial
enhancement]
Spills on Water:
Dilute each gallon of OSE II with 50 gallons of fresh, brackish, or salt water - depending on
the water associated with the area that has been impacted by the spill. Apply OSE II at a
ratio of 1 gallon mixed OSE II to each gallon of hydrocarbon spilled. Apply using hand held
sprayers, tank sprayers, booms from vessels, helicopters, or airplanes; by spraying the
perimeter first then working toward the middle of the spilled area. Next spray the entire
surface of the spill. If the spill is very heavy (more than 2 inches thick) it is recommended
that OSE II be applied every day until you have met a 1:1 ratio of OSE II and water
mixture to spilled oil/hydrocarbons.
Use 1 gallon OSE II for every 50 gallons of hydrocarbons.
Use 1 drum of OSE II for every 2,750 gallons of hydrocarbons.
If you know gallons of hydrocarbons spilled, multiply gallons of hydrocarbons by
0.02 to get amount of OSE II needed [gallons of hydrocarbons x 0.02 = gallons of
OSE II].
If you know barrels of crude oil spilled, multiply barrels of crude oil by 0.015 to get
drums of OSE II needed [barrels of crude oil x 0.015 = drums of OSE II].
If you do not know gallons of hydrocarbons or barrels of crude oil, multiply size of
spill by 0.0023 to get drums of OSE II needed or by 0.12 to get gallons of OSE II

http://www.epa.gov/emergencies/content/ncp/products/oseater.htm

4/3/2011

OIL SPILL EATER II | NCP Product Schedule | Emergency Management | US EPA

Page 3 of 4

needed [(yards long x yards wide x inches thick) x 0.0.0023 = drums of OSE II or
(yards long x yards wide x inches thick) x 0.015 = gallons of OSE II].
Intertidal Zone:
Mix each 55 gallon drum of OSE II with 2,750 gallons of fresh, brackish, or salt water. The
water used is determined by the type of water associated with the site. OSE II should be
applied as the tide recedes (if there is a tide) and once the tide comes in the application
should cease until the tide recedes again. Additional applications should only be warranted
if spill has been allowed time to percolate into the depths of the soil.
If there is no tide, but waves have pushed the spill into the intertidal zone, then there will
be direct access to the spill at all times. If possible use string or stakes to grid off the beach
or intertidal zone area, and then you can calculate how much premixed OSE II to apply to a
given area. If unable to grid off an area then calculate how much OSE II to apply and then
determine how much premixed OSE II will flow through a nozzle (gallons per minute) then
let application technician know how many gallons to apply in a given area and this can be
determined by applying product for a certain time period to get the correct amount of OSE
II applied to gain the 1:1 ratio.
Note: If the intertidal zone is associated with the sea then mix OSE II with salt water. If the
spill area is in an area of brackish water then mix OSE II with brackish water. If the
intertidal zone is associated with fresh water such as lakes, rivers, streams, ponds, creeks,
aquifers, or drinking water wells then use fresh water to mix OSE II.
3. Conditions for Use:
OSE II can remediate hydrocarbon-based material including chlorinated
hydrocarbons, PCB's, dioxins, and some pesticides.
As the age of spilled hydrocarbons increases, the time necessary for bioremediation
increases. In general, fresh crude, gasoline of BTEX takes from 72 hours to 30 days
to completely bioremediate.
Variations of sea water salinity should have no effect, but as long as microbial life
can exist, then OSE II will be effective.
OSE II bioremediation slows somewhat at temperatures below 40F. OSE II
however, will continue to work at any liquid water temperature that will sustain
microbial life.

VII. TOXICITY AND EFFECTIVENESS


a. Effectiveness:
Summary Data Table:
PRODUCT
TOTAL MEAN
DAYS
3
ALKANES
REPS/PROD
(ppm)

RED%
28
DAYS

TOTAL MEAN
AROMATICS
(ppm)

RED%
28
DAYS

CONTROL
NUTRIENT
OSE II

43,170
40,569
41,730

11,435
11,785
12,155

CONTROL
NUTRIENT
OSE II

39,250
34,815
26,316

9.1
14.2
36.9

10,355
9,898
8,072

9.4
16.0
33.6

28

CONTROL
NUTRIENT
OSE II

35,797
26,507
4,273

17.1
34.7
89.8

9,534
8,938
1,268

16.6
24.2
89.6

Results of Gravimetric Analysis:


Percentage (%) Decrease in Weight of Oil on Day 28

http://www.epa.gov/emergencies/content/ncp/products/oseater.htm

4/3/2011

OIL SPILL EATER II | NCP Product Schedule | Emergency Management | US EPA

Control: 16.5%
Nutrient: 52.0%
Product: 85.4%

Page 4 of 4

http://www.epa.gov/emergencies/content/ncp/products/oseater.htm
Last updated on Thursday, January 27, 2011

VIII. MICROBIOLOGICAL ANALYSIS


1. Listing of each component of the total formulation, other than enzymes, by chemical
name and percentage by weight: CONFIDENTIAL
2. Enzyme Names: CONFIDENTIAL
3. I.U.B.: CONFIDENTIAL
4. Source of Enzymes: Fermentation process
5. Units: No less than 1% and no more than 50% by weight
6. Specific Gravity: 1.05
7. Optimum Conditions:
a.
b.
c.
d.
e.
f.

pH: 7.0
Temperature: 72F
Salinity Ranges: Fresh water to salt water
Maximum and Minimum pH: 3.5 - 8.0
Maximum and Minimum Temperature: 28F - 128F
Maximum and Minimum Salinity Levels - Salinity level above that will support
microbial activity will adversely effect OSE II's performance
g. Enzyme Shelf Life: Up to 5 years when properly stored
h. Enzyme Optimal Storage Conditions: 72F is optimal, enzyme range is freezing to
120F, never leave OSE II in direct sunlight for more than a couple of hours

IX. PHYSICAL PROPERTIES


NA
X. ANALYSIS OF HEAVY METALS, CYANIDE, AND CHLORINATED HYDROCARBONS
NA

http://www.epa.gov/emergencies/content/ncp/products/oseater.htm

4/3/2011

23

US Safety Data Sheet


Issued: June 1, 2015
1. IDENTIFICATION OF THE SUBSTANCE PREPARATION AND
COMPANY
Product Name:

Oil Spill Eater II, OSE II

Product Code, GHS code:


(Export Code)

3821000000

Product Type:

Hydrocarbon Bioremediation Product

Supplier:

Oil Spill Eater International Corporation

Address:

P.O. Box 515429


Dallas, Texas 75251
USA

Contact Numbers:
Telephone:

(972) 669-3390

Fax:

(469)241-0896

E-mail:

oseicorp@msn.com

Emergency Telephone Number:

(972) 669-3390

Emergency Covers:

24 hours a day 7 days a week

2. HAZARDOUS IDENTIFICATION
Human Health Hazards:

None. Potentially toxic if more than 1liter


ingested.

Safety Hazards:

Will not burn. Is, in fact, a fire retardant.

Environmental Hazards:

None. Protects environment;100%biodegradable;


no known allergens.

Page 2 of 9 US Safety Data Sheet

3. COMPOSITION INFORMATION ON INGREDIENTS


Preparation Description:

A hydrocarbon bioremediation product containing


all natural nonhazardous ingredients.
Contains:
Ingredient
CAS Number
80-90%
7732-18-5
1) Water
2) Nitrogen (Urea)
0.01-0.09% 57 -13-6
3) Molasses
1-2%
None
4) Bio Surfactant
0.06-0.08% 68131-40-8
5) Sugar
1.5%-2%
50-99-7
6) Protease
0.01-0.03% 9000/90/2
7) Amylase
0.01-0.03% 9014-01-1
8) Malt
1-2%
8029-43-4

4. FIRST AID MEASURES


Symptoms and Effects:

Prolonged exposure would have minimal effect,


if any at all.

First Aid - Inhalation:

Inhalation of vapors from this product pose


no acute or chronic hazard.

First Aid - Skin:

Prolonged exposure to skin may cause some


drying of the skin. Wash off with water.

First Aid - Eye:

Flush eyes with copious quantities of water. If


irritation persists, seek medical attention.

First Aid - Ingestion:

If less than 59 ml / 2 ounces is ingested, no toxic


symptoms should occur, to most humans
Wash out mouth and seek medical attention if
more than59ml or 2 ounces is ingested.

Advice to Physicians:

Treat symptomatically. Wash skin or eyes


thoroughly. Treat as you would for any large
ingestion of mild soap or tooth paste.

5. FIRE FIGHTING MEASURES


Specific Hazards:

OSE ll is a fire retardant. However, if applied to


a burning fire, there can be a slight flash before
fire goes out.

Extinguishing Media:

None required. Product is a fire retardant.


Method - ASTM-D56.

Unsuitable Extinguishing Media:

None required. Product is a fire retardant.

Page 3 of 9 US Safety Data Sheet


Protective Equipment:

Proper protective equipment including breathing


apparatus must be worn when approaching any
fire.

6. ACCIDENTAL RELEASE MEASURES


Personal Precautions:

Avoid contact with eyes. Wash from skin or


eyes as needed.

Personal Protection:

Wear goggles if applying in windy conditions.


Wear protective rubber gloves if applying
directly in a prolonged situation.

Environmental Precautions:

Wash down with water. Will help clean soil,


drains, or water.

Clean-up methods - small spillage:

Wash down with water. Non-toxic to the


environment.

Clean-up methods - large spillage:

Same as for small spills.

7. HANDLING AND STORAGE


Handling:

When handling product in drums, safety


Footwear should be worn. However No
special handling procedures required.

Storage:

Keep in cool, dry area. A void direct sunlight


and excessive heat.

Storage Temperatures:

Do not store where temperature exceeds


120 F.

Recommended Materials:

Polyethylene drums or PVC are acceptable.

Unsuitable Materials:

None known.

Other Information:

Product can freeze / thaw without any negative


effect on product.

Page 4 of 9 US Safety Data Sheet


8. EXPOSURE CONTROL/PERSONAL PROTECTION
Occupational Exposure Standards:

None established (none toxic).

Hygiene Measures:

Wash hands before eating or drinking.

Respiratory Protection:

Not normally required.

Hand Protection:

Any plastic or rubber glove if needed; not


normally required.

Eye Protection:

Wear safety glasses or goggles if applying


in windy conditions.

Body Protection:

Not normally required.

9. PHYSICAL AND CHEMICAL PROPERTIES


Physical State:

Liquid with the same density of H20.

Color:

Amber to brown .

Odor:

Some smell of ferment.

Vapor Pressure:

Same as H20.1.0215

Density:

Same as H20. 1.0215

Vapor Density:

Same as H20. 1.0215

Dropping Point:

Same as H20.

Flash Point:

Same as H20 in excess of 7000 F.

Flammability Limit - Lower:

Nonflammable.

Flammability Limit - Upper:

Nonflammable.

Auto-ignition Temperature:

Non-igniting

Solubility in Water:

100%

N-octanol/water Partition Coefficient:

100% soluble - non partitioning

Elements Content:

None.

Page 5 of 9 US Safety Data Sheet


10. STABILITY REACTIVITY
Stability:

Stable.

Conditions to Avoid:

Temperatures in excess of 120 F and


direct sunlight during storage or transporting.

Materials to Avoid:

Strong oxidizing agents.

Hazardous Decomposition Products:

None decomposes to CO2 and H20.

11. TOXICOLOGICAL INFORMATION


Basis for Assessment:

Toxicity tests have been performed


Determining OSE II is (virtually nontoxic).

Acute Toxicity - Oral:

Can become toxic if more than 60 ml ot 2


ounces is ingested.

Acute Toxicity - Dermal:

None.

Eye Irritation:

Slight irritant alleviated by copious eye


washing.

Skin Irritation:

Skin can dry slightly if prolonged direct


exposure occurs.

Respiratory Irritation:

Virtually none.

Skin Sensitization:

Not expected to be a skin sensitizer.

(Sub )chronic Toxicity:

None expected.

Carcinogenicity:

Not a carcinogen.

Mutagenicity:

Not a mutagenic.

Human Effects:

None expected.

Other Information:

Not applicable.

12. ECOLOGICAL INFORMATION


Basis for Assessment:

Ecotoxicological data has been determined


specifically for this product. Information
given is for specific sensitive (aquatic)
species in fresh and salt water.

Page 6 of 9 US Safety Data Sheet


Mobility:

Liquid that floats on water and solubilizes


rapidly. If it comes in contact with soil
will percolate at the same rate as H20 and
will biodegrade rapidly.

PersistencelDegradability:

Product completely biodegrades in water


or soil environments and will not persist.
100% biodegradable as testing has
confirmed

Bioaccumulation:

None

Ecotoxicity:
US EAP

100% soluble.
LC50 Brine shrimp: >1,900
mg/l up to 10,000 mg/l.
LC50 Fundulus Heterocletus
96 hour: 5,258 mg/l.
Environment Canada
LC50 Rainbow Trout:10,000
mg/l.
OSEI with the city of Plano Tx LC50 Fathead Minnows
(Pimephale promelas): 9,300
mg/l.
Australia NATA test results:
IC10(milky oyster,
Saccostrea echinata): 11.0
(10.0-11.9)mg/l/48h
EC50(milky oyster,
Saccostrea echinata): 16.5
(16.0-17.1)mg/l/48h
NOEC(milky oyster,
Saccostrea echinata):
10.0mg/l
LOEC(milky oyster,
Saccostrea echinata):
20.0mg/l
EC10(mussel, Mytilus
galloprovincialis):
>20.0mg/l/72h
EC50(mussel, Mytilus
galloprovincialis):
>20.0mg/l/72h
NOEC(mussel, Mytilus
galloprovincialis):
20.0mg/l
LOEC(mussel, Mytilus
galloprovincialis):
>20.0mg/l

Page 7 of 9 US Safety Data Sheet


13. DISPOSAL CONSIDERATIONS

Waste Disposal:

No special disposal.

Product Disposal:

No special disposal.

Container Disposal:

No special disposal.

Local Legislation:

Not applicable.

14. TRANSPORT INFORMATION

Not dangerous for conveyance under UN, IMO, ADRiRID.


Marine Transport (IMO/IMDG): Not classified as Dangerous
Goods by the criteria of the International Maritime
Dangerous Goods Code (IMDG Code) for transport by sea.
Air Transport (ICAO/IATA): Not classified as Dangerous
Goods by the criteria of the International Air Transport
Association (IATA) Dangerous Goods Regulations for
transport by air.
IMDG Marine No
15. REGULATORY INFORMATION

EC Classification:

Not Known.

EC Symbols:

Not Known.

EC Risk Phrases:

Not Known.

EINECS (EC):

Not Known.

TSCA (USA):
Other Information:

US DOT class 55 non hazardous

Dangerous Constituents:

None.

Page 8 of 9 US Safety Data Sheet


16. OTHER INFORMATION
Only bioremediation product successfully used to permanently remove oil on U.S. navigable
waters under U.S. EPA Government observation.
Government approvals or approved listings:

!!
!
!
!
!
!

US!EPA!NCP!#!B53,!!
New!Zealand!EPA!SOS # 1001797,
Australia #OBA
Oil Spill Control agent Greek registration ID
no:17554
Gulf States MEMAC approval Ref:337/12RHD,
Philippine accreditation #PCG-14-06-112
Nigeria NOSDRA cert: 189,
Mexico Coatzacoalcos.Ver.,a 30 de Julio de
2014,
Israel approval,
UK approval #ODA 241/2015 ,
Trinidad and Tobago approval#
MEEA:12.1.5 Vol. XXXXII, South Korea cert
no: S-007 !

Uses and Restrictions:

Bioremediation product that converts


hydrocarbons, chlorinated
hydrocarbons,
and most organic based material or
waste to CO2 and H20.

Technical Contact Point:

Steven Pedigo

Technical Contact Number:

(972) 669-3390

Fax Number:

(469) 241-0896

E-Mail:

oseicorp@msn.com

SDS History:

Not Applicable

Revisions Highlighted

None.

Page 9 of 9 US Safety Data Sheet


!
last!revision!of!SDS!
Literature!References!
SDS Created: June 2015
Preparation of Safety Data Sheets for Hazardous Chemicals
Code of Practice. Standard for the Uniform Scheduling of
Medicines and Poisons. Australian Code for the Transport of
Dangerous Goods by Road & Rail. Model Work Health and
Safety Regulations, Schedule 10: Prohibited carcinogens,
restricted carcinogens and restricted hazardous chemicals.
Workplace exposure standards for airborne contaminants,
Safe work Australia. American Conference of Industrial
Hygienists (ACGIH). Globally Harmonised System of
classification and labelling of chemicals. ...End Of
MSDS...
!
!

Written and Compiled


by the

Science & Technology Advisory Board


Marynette Herndon, Environ Eng, REM (Registered Environmental Manager),
CHMM (Certied Hazardous Materials Manager)
President, Herndon & Associates, Inc.
Chairperson, LAEO Science & Technology Advisory Board
Paul W. Sammarco, PhD
Professor and Senior Scientist
Louisiana Universities Marine Consortium (LUMCON)
Alex Nicholson, Mech Eng, MBA, PE
Former NASA Aerospace Engineer
Environmental Specialist
Jeanne Pascal, Esq
EPA Northwest District Debarment Counsel, retired (19842010)
Former in-house EPA attorney for oil spill relief
Barbara Wiseman
International President
Lawrence Anthony Earth Organization
Diane Wagenbrenner
Advisory Board Member
Lawrence Anthony Earth Organization

Identication of Nontoxic Methods


for Contingency Plans
The establishment and enactment of new
contingency plans associated with remediation
of oil spills (including those response plans
submitted by oil companies requesting permits)
is urgently needed, using methodologies other
than intensive application of chemical dispersants. The commencement and acceleration
of new deep-water drilling in the Gulf of
Mexico and the Beaufort Sea in Alaska, for
instance, particularly in the absence of
updated contingency plans in the event of
a spill, is quite concerning. In other words,
hundreds of permits have been issued since
September 2010 with no signicant change in
spill contingency planningother than more
advanced deep-water dispersant injection
systems that have been added to plans, which
would produce a repeat of the Deepwater
Horizon toxic response.
The information presented here is for distribution to Regional/Area Committees and all
stakeholders responsible for maintaining upto-date contingency plans for safeguarding our
aquatic, marine, and terrestrial environments.
The article included regarding bioremediation
category denitions and their modes of action,
along with further information below, should overwrite previous guidance on bioremediation
because it clarifies use of the Bioremediation
Agent EA Type as a FIRST-RESPONSE agent.

Bioremediation Agent Enzyme Additive


Type can clearly serve as a rst-response
alternative to the use of chemical
dispersants, which no longer have a
place in modern-day oil spill cleanup in
US navigable waters.

NCP-Listed Bioremediation Agent


(EA Type) as a Solution and
Alternative to Chemical Dispersants
We encourage independent investigation of
EA Type as a promising potential solution to
oil spill response in deep-water drilling and
difcult access environments, particularly as a
rst-response method for open-water oil spills,
in lieu of chemical dispersants of any kind.
It is the position of the Science & Technology
Advisory Board of the Lawrence Anthony
Earth Organization that Bioremediation Agent
Enzyme Additive Type can clearly serve as a
rst-response alternative to the use of chemical dispersants, which no longer have a place
in modern-day oil spill cleanup in US
navigable waters.
The EPA is now being pressed to nd safer
response agents to replace these outdated
modes, which, when combined with oil
pollutants, are more toxic than the oil itself
and therefore contrary to the intent of the US
Clean Water Act (CWA).29 To reiterate, the
CWA stipulates that, for a response method
to be utilized, it must REMOVE oil from the
environment. Dispersants do not fulll this
requirement; in fact, studies have shown that
use of dispersants prolongs the time that oil
plus chemical dispersants remain in the
environment, resulting in adverse impacts to
ora and fauna for up to ve years or longer.30,31
The good news is that there are developed
protocols for identifying and assessing
the degree of usefulness of spill-response
products, and they are not complicated.

20

How Oil Spill Cleanup Products


Should Be Assessed and Prioritized

Its use and application must be economically


reasonable and within acceptable ranges of
expected remediation costs.
The LAEO has conducted nearly three years Eliminates or signicantly reduces the
of research to nd methods for remediating
necessity for secondary cleanup, such as
oil spills that are more effective and less toxic
cleaning up tar mats formed by sinking the
than those currently used. We have also been
oil using dispersants, disposal of hydroworking to gain the necessary authorizations
carbon-based material in landlls, or other
for utilizing these more effective techniques to
methods of disposal.
clean up the waters of the Gulf and its shorelines
Our extensive search revealed only one product
still impacted by the Macondo spill.
that fullled all of these requirementsone
Our rst step was to vet the applicable products under the Bioremediation subcategory EA
on the EPA NCP Product Schedule. We developed
on the NCP list: Oil Spill Eater II (OSE II).
a set of guidelines by which to review products
We continue to look for other products that
and determine their eligibility for use in US
fulll these criteria, but in the meantime, at
navigable waters. We were not looking for any least there is one bioremediation category
given product but merely those that fell under that could effectively lead response methods
our criteria for desired effectiveness, as follows:
into the twenty-rst century; and as of the
writing of this paper, the only product that
On the NCP list.
has been able to meet our guidelines has been
Swift and effective removal of the oil, not
OSE II.
just dispersal of it by solubilizing or disLAEO produced a documentary lm to
solving it into the water column.
educate the public on bioremediation and to
Nontoxic with no destructive trade-offs
encourage researchers and companies with
associated with its application.
products that meet the above criteria to step
Able to also detoxify chemical disperforward.32 Several products have since been
santse.g., the two types of Corexit that
submitted to us for our advocacy, and some,
have been broadly used domestically and
although promoted as nontoxic, were found
internationally.
to be at least as toxic as crude oil.
Using neither nonindigenous microbes nor
New and innovative solutions utilizing all
genetically modied organisms.
available technology are needed for the
Complete scientic documentation subsituation in the Gulf of Mexico, as well as
stantiating the products efcacy.
future hydrocarbon-based spills that will
A track record of success in the eld.
continue to occur in all the waters of the
world. If we stay on the same track, we run the
Pretested and screened as usable anyrisk of having sheries collapse, a chemically
whereopen water, sandy beaches,
stressed ecosystem worldwide, and progresmarshes, etc., as a rst-response method
sively worsening human health issues.33
(i.e., predetermined as applicable in all
environments to enable rapid response
Characteristics of an
without the need for assessment during an
Effective Solution
emergency).
Feasibility Assessment Criteria
The manufacturer has sufcient quantities in
stock and immediate production capabilities
The protection of human health should be
to handle a spill of signicance.
the foremost concern of any oil spill cleanup
21

decision-making process. Human health is


4. Understanding that nature uses surfactantsxiii
dependent upon the relative health of the
in the natural process of cleaning up an oil
surrounding environment; hence it is important
spill, an effective product would have no
to understand the criteria by which cleanup
toxic surfactants such as are contained
methods must be gauged as to their value and
in both Corexit 9527 and 9500. (For instance,
effectiveness. To reiterate, the primary reason
Bioremediation EA Type OSE II contains no
to clean up an oil spill or hazardous materials
toxic surfactants and is fully tested and valiis to rapidly reduce the impact of their toxicity
dated as nontoxic. Comparing toxicity levels
so that all living organisms can survive. And
using established EPA standards cited earlier,
again, if even the smallest organisms can
Corexit 9500 had a high toxicity level of
survive, then the ecosystem will be able to
0.065 to 0.354 ppm compared to OSE II,
sustain itself.
which had a reading of 10,000 ppm for one
of the most sensitive marine species tested
Thus, our recommended standards for the
[the higher the number, the lower the toxicity
ideal technology or agent for use in cleaning
level]. This means that Corexit is as much
up a hazardous spill would be these:
as 150,000 times more toxic than the bioremediation alternative. See Toxicity Values
1. Must swiftly and thoroughly detoxify the
chart below.)
oil or hazardous substances as a rst step
in order to protect the indigenous microbial
populations and all life forms.

5. Must have a scientically substantiated


and predictable end point that could be
standardly achieved from its proper
2. Must nullify the oils adhesive qualities so
application. This end point would be that
that it does not stick to marine life, wildlife,
within
a matter of days to, maximally, a few
marsh grass, rocky shorelines, sandy beaches,
weeks, close to 100 percent of the oil would
or seabed sediment.
have been converted into CO2 and water
two benign substanceswithout any adverse
3. Must keep the oil on the surface so that it
side
effects, or trade-offs related to its applican most rapidly be digested by indigenous
cation, thereby protecting the responders,
microbes, utilizing existing airborne oxygen
wildlife, and marine life.
and protecting the 60 percent of marine life
that resides in the subsurface area. (Note:
6. Its application must be economically
This also makes it accessible for physical
viablefor example, comparable in cost
removal methods working in tandem with
to current methods and, ideally,
nontoxic agents.)
signicantly less.

LC 50 = Lethal concentration values in parts per million measuring level in which there is mortality with 50 percent of
species being tested over a specific period of time. Higher # = less toxic, lower # = greater toxicity in ppm.

Sample Toxic ity Com par ison, Envi ronment Canada and US EPA Tests,
Bioremediation vs. Corexits 34
xiii. surfactant. A substance that lowers the surface tension of water, making it easier for organic compounds to be dissolved in the water.
There are toxic and nontoxic surfactants; i.e., chemical based with various degrees of toxicity, and plant/living-organism based = nontoxic.

22

Our research found that an EA Type bioremediation technology that meets the above
criteria exists today and is being used in over
30 countries. Its results contrast strongly with
those derived from dispersants predominantly
used in US navigable waters. Additionally,
it costs a fraction of the other methods and
would therefore represent an economic boon,
not only to the responsible parties, who could
avoid damage claims and heavy nes, but also
to those living in the environment, reducing
business disruptions with rapid cleanup,
bringing a quick return to their livelihoods.
In other words, in addition to preserving the
health and safety of the waters, there would

be little impact on tourism, coastal


businesses, and fisheries.
The value of a product could be rated and
characterized by how rapidly and thoroughly
it meets the above criteria while introducing
no additional toxicity to the scene already
created by the hazardous spill.
Due to the many common misconceptions
about bioremediation, and especially the
subcategory EA Type on the NCP list, LAEOs
Science & Technology Advisory Board has
provided the above summary of our vetting
process of spill-response methods for use by
all interested parties.

We encourage independent investigation of EA Type as a promising potential


solution to oil spill response in deep-water drilling and difcult access environments,
particularly as a rst-response method for open-water oil spills, in lieu of chemical
dispersants of any kind. To reiterate, the primary reason to clean up an oil spill or
hazardous materials is to rapidly reduce the impact of their toxicity so that all living
organisms can survive. And again, if even the smallest organisms can survive, then
the ecosystem will be able to sustain itself.

Because None Survive Alone

23

Material Safety Data Sheet

U.S. Department of Labor

May be used to comply with OSHAs Hazard


Communication Standard, 29 CFR 1910 1200. Standard
must be consulted for specific requirements.

Occupational Safety and Health Administration


(Non-Mandatory Form)
Form Approved
OMB No. 1218-0072
Note: Blank spaces are not permitted. If any item is not
applicable or no information is available, the space
must be marked to indicate that.

IDENTITY)

Micro-Blaze
Non-Formulated

Section I
Manufacturers name
Address

Verde Environmental, Inc.

Emergency Telephone Number

9223 Eastex Freeway


Houston, Texas 77093-7001

Telephone Number for Information


Date Prepared

800 / 626-6598
713 / 691-6468

01/01/13

Signature of Preparer
William L. Scogin, President

Section IIHazardous Ingredients/Identity Information


Hazardous Components (Specific Chemical Identity, Common Name(s))

PART A HAZARDOUS INGREDIENTS

CAS Number:

NONE

OSHA PEL

N/A

Other Limits
Recommended

ACGIH TLV

N/A

% (optional)

N/A

PART B OTHER INGREDIENTS


Water and viable Non-Pathogenic and Non-Toxic
Bacillus Spore Forming Bacteria Cultures
7732-18-5

Components not listed are either proprietary, or non-hazardous.


Section IIIPhysical/Chemical Characteristics
Boiling Point

100C

Specific Gravity (H20 = 1)

Vapor Pressure (mm Hg)

Equiv. water

Melting Point

N/A

Equiv. water

Evaporation Rate (Butyl Acetate = 1)

N/A

Vapor Density (AIR = 1)


Solubility in Water
Appearance and Odor

1.0

100%
Opaque liquid, slight odor

Section IVFire and Explosion Hazard Data


Flammable Limits

Flash Point (Method Used)

Extinguishing Media

N/A

Non-flammable

LEL

UEL

----

----

Non-flammable

Special Fire Fighting Procedures

Unusual Fire and Explosion Hazards

None

None - NON-FLAMMABLE
OSHA 174 Sept. 1985

Section VReactivity Data


Stability

Unstable

Conditions to Avoid

Stable
Incompatibility (Materials to Avoid)

XXXX

Strong acids or alkali compounds may inactivate biological cultures.

Hazardous Decomposition or Byproducts


May Occur

Hazardous
Polymerization

Conditions to Avoid

Will Not Occur

XXXX
Section VIHealth Hazard Data
Route(s) of Entry

Inhalation?

Health Hazards (Acute and Chronic)

Skin?

Ingestion?

May cause diarrhea if ingested in large amounts.

Organisms used are non-pathogenic. These organisms are susceptible to commonly used antibiotics.
Carcinogenicity

NTP?

N/A

IARC Monographs?

N/A

N/A

OSHA Regulated?

N/A

Signs and Symptoms of Exposure

Skin: slight redness on hands and forearms if individual has a history of dermal allergic
reaction. Inhalation: if inhaled, remove victim to fresh air. Give oxygen or artificial respiration as needed. Obtain
emergency medical attention.
Medical Conditions
Generally Aggravated by Exposure Dermal
Emergency and First Aid Procedures

allergic reaction on skin if susceptible person has continual exposure.

Ingestion: Drink water or milk to dilute. Induce vomiting only if advised by


physician or poison control center.
Section VIIPrecautions for Safe Handling and Use
Steps to Be Taken in Case Material Is Released or Spilled

May mop up spills; may flush down sanitary drain into waste water

treatment lines.
Waste Disposal Method

Disposal of this product or its residue must be done in accordance with all local, state and

federal requirements.
Precautions to Be Taken in Handling and Storing

Avoid eye contact.

Other Precautions

To maintain shelf life, avoid temperatures under 32 F or over 120 F for long periods of time.
Microbes are viable up to 180 F. KEEP FROM PROLONGED FREEZING.
Section VIIControl Measures
Respiratory Protection (Specify Type
Ventilation

) Avoid breathing mists; mask advised if spraying in enclosed, unventilated spaces.

Local Exhaust

Special

Mechanical (General)

Other

Protective Gloves

Use if prolonged exposure or dermal


sensitivity to surfactants.
Other Protective Clothing or Equipment
Work/Hygienic Practices

Eye Protection

Normal room ventilation.


Avoid splashing in eyes; may irritate.

None required; rubber or latex recommended.

Minimize exposure in accordance with good hygiene practices.

We believe the statements, technical information and recommendations herein


are reliable, but they are given without warranty or guarantee of any kind,
express or implied, and we assume no responsibility for any loss, damage, or
expense, direct or consequential, arising out of their use.

VERDE ENVIRONMENTAL, INC.


HOME OF

Non-Formulated

Verde Environmental, Inc.


9223 Eastex Freeway
Houston, TX 77093
Office: 713.691.6468
Toll Free: 800.626.6598
Fax: 713.691.2331
www.micro-blaze.com

Partnering with Nature for a Cleaner Tomorr ow

Non-Formulated

Product Details
Appearance:
Light brown

pH:

7.0 8.0

Shelf Life:
10 Years

Storage:

Avoid temperatures over 48C for long


periods of time. Avoid prolonged
freezing.

Micro-Blaze Non-Formulated is a safe


non-toxic microbial formulation used
for bioremediation where the use of
surfactants are not desired or permited. It
is used primarily in contaminated ground
water clean-up and also in and around
surface water, such as creeks, rivers, ponds,
and lakes. It breaks down, degrades, and
digests waste. The residue and run-off can
be safely sent to the facility waste water
treatment plant. The numerous strains of
microbes in Micro-Blaze Non-Formulated
provide a synergistic degradation of the
organic and hydrocarbon pollutants.
Uses:

Remediation

of

ground

water

contamination

Packaging:

Remediation of contamination in and

1-Gallon Pail
5-Gallon Pail
55-Gallon Drum
275-Gallon Tote

around creeks, rivers, ponds, and lakes

SURFACTANT FREE
* Always obtain regulatory approval prior to putting any
product into a waterway

To receive more information:

Other Micro-Blaze Microbial


Products:

0912

Emergency Liquid Spill Control FOG


Micro-Blaze Out AGRO APT Budkicker
CSR Turf Care