Beruflich Dokumente
Kultur Dokumente
Composite Structures
journal homepage: www.elsevier.com/locate/compstruct
Temporary bond strength of partly cured epoxy adhesive for anchoring prestressed
CFRP strips on concrete
Julien Michels a,, Christoph Czaderski a, Raafat El-Hacha b, Rolf Brnnimann c, Masoud Motavalli a,d
a
Structural Engineering Research Laboratory, Swiss Federal Laboratories for Materials Science and Technology (Empa), Dbendorf, Switzerland
Department of Civil Engineering, University of Calgary, Canada
c
Electronics and Metrology Laboratory, Swiss Federal Laboratories for Materials Science and Technology (Empa), Dbendorf, Switzerland
d
Faculty of Engineering, University of Tehran, Iran
b
a r t i c l e
i n f o
Article history:
Available online 9 April 2012
Keywords:
Carbon Fiber Reinforcement Polymer
Concrete strengthening
Prestressing
Gradient anchorage method
Accelerated epoxy curing
Temperature
a b s t r a c t
Externally bonded Carbon Fiber Reinforced Polymer (CFRP) strips have been used for strengthening reinforced concrete structures. This paper presents an experimental study on the debonding of externally
bonded CFRP strips anchored to a concrete substrate by a commercial epoxy adhesive. The study represents the basis for the characterization of an innovative gradient method, giving the possibility to anchor
prestressed CFRP strips to concrete without the use any mechanical anchorage systems such as plates and
bolts. Bond between the two components is achieved by an epoxy adhesive able to carry loads after an
accelerated curing process under elevated temperatures. The effect of heating conguration/duration,
strip thickness and bond length on the temporary bond resistance have been investigated using prestressed and non-prestressed CFRP-strips. Besides the optimization of the heating elements necessary
for the curing process, curing parameters for an optimal temporary bond strength could be determined.
Twenty-ve minutes of heating and curing at 90 C was found to be an optimum heating conguration,
resulting in better short-term mechanical performances than after conventional curing at room temperature for several days. The main reason is a temporarily softer adhesive which allows the use of the full
bond length by reducing shear force peaks.
2012 Elsevier Ltd. All rights reserved.
1. Introduction
Externally bonded (EB) Carbon Fiber Reinforced Polymer (CFRP)
strips have been used extensively as an additional reinforcement for
strengthening reinforced concrete structures. Prestressing EB CFRP
strips generally increases the cracking load, delays yielding and
implicates a better exploitation of the mechanical performances,
such as high tensile strength above 2000 MPa. The prestressed CFRP
strips can be used more efciently and contribute to the load
carrying capacity under both service and ultimate conditions [1].
Combined with the delayed debonding failure [2] compared to
non-prestressed strips, the ultimate load capacity is generally
higher, too.
The following research is part of the development of a novel
anchorage system for prestressed CFRP strips. In contrast to the different developed mechanical anchorage systems described in literature [35], the idea of anchoring prestressed CFRP only with an
epoxy adhesive was proposed by Professor Urs Meier at the Swiss
Federal Laboratories for Materials Science and Technology (Empa)
(refer to [610]). In order to avoid a premature debonding of the
Corresponding author. Tel.: +41 58 765 4339.
E-mail address: julien.michels@empa.ch (J. Michels).
0263-8223/$ - see front matter 2012 Elsevier Ltd. All rights reserved.
http://dx.doi.org/10.1016/j.compstruct.2012.03.037
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Nomenclature
bf
ft,u
fc,cube
fct,s
lb
lb,eff
uf, uc
strip width
uniaxial tensile strength of CFRP
concrete compression strength on cube
concrete splitting tensile strength
bond length
effective anchorage length
horizontal displacement in x-direction of the CFRP strip
and the concrete
sf
relative displacement (slip) between CFRP strip and
concrete
sf,min, sf,max minimum and maximum slips in horizontal direction
tf
strip thickness
tcool
cooling time prior to the test start
x, y
directions, axis
thold
overheating time during the curing process at elevated
temperature
3. Experimental characteristics
3.1. Materials
All CFRP strips used in the presented investigation had a width bf
of 100 mm, whereas three different strip thicknesses tf of 0.6, 0.9
and 1.2 mm were used. Before each test, elastic moduli Ef of the
used CFRP strips (in the ber direction) were determined by
prestressing the strip to several load stages and measuring the corresponding tensile elongation (to derive the strain by dividing the
elongation difference with the measuring length) by means of a
mechanical dial gauge (Table 1).
Direct tensile tests on coupon specimens according to EN ISO
527-5 [19] with strips of 0.6 and 0.9 mm thickness revealed average
uniaxial tensile strengths ftu of 2236 and 2324 MPa, respectively.
According to the quality analysis certicate of the producer, the
uniaxial tensile strength of 1.2 mm strip thickness is 2975 MPa.
Throughout all experiments the epoxy-based S&P epoxy adhesive
220 was used. According to the technical data sheet of the distributor
[20] it offers a compression strength above 90 MPa and bending tensile strength higher than 30 MPa after curing at room temperature.
Its glass transition temperature is higher than 56 C. Further detailed
information is available on the mentioned data sheet.
Concrete substrate, with a maximal aggregate size of 32 mm,
had an average compressive strength fc,cube of 51.1 MPa (tested
Ef
Fl
F1, F2
DF
Fu
Finit
PO
REL
RT
Ta
Tavg
Tn
Th
Tpeak
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a
b
Type
tf (mm)
lb (mm)
Heating system
th (min)
tcool (min)
Tavg (C)
Ef (GPa)
Finit or Fu (kN)
sf,min (mm)
sf,max (mm)
PO
PO
PO
PO
REL
REL
REL
REL
REL
REL
REL
REL
REL
REL
REL
REL
0.6
0.6
0.6
0.6
0.6
0.6
0.6
1.2
1.2
1.2
1.2
1.2
0.9
0.9
0.6
1.2
300
300
300
300
300
300
300
300
200
100
300
200
300
200
300
300
A
RT curing
B
B
C
C
C
C
C
C
C
C
C
C
C
RT curing
15
15
20
30
60
15
25
25
25
25
25
25
25
25
6.6
2 days
6.8
10.7
40.0a
7.7
9.8
15.9
9.2
7.5
18.1
10.4
9.8
10.5
13.9
3 days
39.5
19.2
42.8
40
32.5
53.2
46.2
39.6
45.4
47.9
36.7
42.6
41.8
40.5
37.7
20b
138.1
138.2
131.9
132.9
141.7
133.4
134.6
159.3
157.7
159.2
158.4
158.7
148.2
149.5
143.3
156.5
14.8
35.0
52.2
55.6
44.8
40.3
38.3
58.9
45.0
23.0
67.0
51.2
55.7
35.1
44.6
46.8 (Finit)
57.7 (Fu)
1.14
0.00
0.20
0.10
0.02
0.02
0.18
0.15
0.24
0.17
0.04
0.06
0.36
0.09
0.09
0.00
0.04
1.43
0.20
1.37
1.26
1.12
0.92
1.10
0.72
0.53
0.24
0.57
0.38
1.07
0.34
1.00
0.31
0.57
Longer cooling time due to initial issue with image correlation measurement.
Room temperature not measured.
Fig. 2. Schematic description (side view) of the (a) pull-off and (b) releasing tests.
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Fig. 3. (a) Heating procedure for System C, (b) bottom view of the heating elements and (c) components necessary for the adhesive heating.
Fig. 4. Heating and loading procedure in time for (a) pull-off and (b) releasing tests.
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sf uf uC
with sf is the slip between CFRP strip and concrete; uf the horizontal
displacement (x-direction) of the CFRP strip in Section 1; and uc is
the average horizontal displacement (x-direction) of the concrete
in Section 0 and 2 (see Figs. 5 and 6).
For the present analysis, the CFRP displacement in horizontal
direction (pulling or releasing direction) was evaluated along the
central axis of the strip (Section 1, see Fig. 5), whereas the concrete
displacements were measured in two sections (Section 0 and 2) at a
distance of 15 mm from the strip edge on each side. Fig. 6 presents
the calculation method to obtain the slip values from the experimental measurements. For the evaluation of the slip sf, concrete
displacement uc was obtained by averaging two linear regression
slopes through the measured values in Section 0 and 2. In Table 1,
minimal and maximal slip values sf,min and sf,max at the last stage
of failure are presented for each experimental test.
It has to be mentioned at this point that the slips for the specimens cured at elevated temperature were evaluated at the last
stage of failure, whereas the initiation of debonding-state as
described in Czaderski et al. [24] was considered for the specimens
cured at room temperature. The differences in behavior at debonding between the two categories will be discussed in the following
sections.
4.2. Optimizing the heating elements
Accelerated curing of the epoxy adhesive induces signicant
changes in the horizontal displacement behavior over the strip
width. It can be seen from Fig. 7a that, using the heating System
A, the edges of the strip exhibit larger displacements than the inner
part of the strip. This is due to a less cured and thus less stiff adhesive in the border regions as a consequence of lower temperature
development at the strip edges. This phenomenon is because the
used heating elements from System A offer a homogeneous heat
power over the complete surface, but simultaneously have higher
heat loss at the strip border as explained above. This results in a
different slip behavior than for room temperature-cured specimens, generally exhibiting stronger displacement values in the
central axis [24]. The heating elements with higher border heat
power (System B) induce a more homogeneous adhesive curing,
resulting in a more homogeneous strip displacement in the pulling
direction as shown in Fig. 7b.
Fig. 6. Slip denition between the CFRP strip and the concrete substrate (values at
failure, heating System A, th = 15 min, lb = 300 mm, tf = 0.6 mm).
In addition to the changes in displacement patterns, considerable difference in the debonding force and failure mode can be
observed. Whereas System A with a heating time of 15 min results
in an adhesive failure (Fig. 7a) at a force of only 14.8 kN over a
bond length of 300 mm, the same curing duration with System B
allows the development of a partial concrete failure (see Fig. 7b)
at a force of 52.2 kN, representing a relative enhancement of 253%.
The mentioned difference between heating Systems A and B can
also be explained by analyzing the slip values measured at failure.
As shown in Table 1, it can be concluded that 15 min of curing time
with heating System A exhibits clearly larger slips (sf,min = 1.14 mm,
sf,max = 1.43 mm) than the same testing conguration with heating
System B (sf,min = 0.2, sf,max = 1.35 mm). This is due to a better curing
process and the related transition from a pure adhesive to a mixed
adhesive/concrete failure.
4.3. Optimization of the heating time and comparison with curing
under room temperature
Fig. 8 presents the debonding force versus the heating duration
of three different testing congurations. For temporary curing at
elevated temperature, the debonding resistance increases with
increasing the heating duration with an optimum ranging between
25 and 30 min. For the pull-off test with tf = 0.6 mm, a slight increase of 6.5% in the debonding force is observed when increasing
the heating duration from 15 to 20 min (Fig. 8a). The releasing test
with the same strip type, the debonding force increases by 16.5%
when curing time increases from 15 to 25 min, however almost
no change in the debonding force was observed when the curing
2672
Fig. 7. Failure surface and ICS results for displacements in pull-off direction at failure for (a) heating Systems A and (b) heating System B, tf = 0.6 mm, lb = 300 mm, th = 15 min.
cured after 15 and 20 min, integrates the total bond length into
the anchorage process before failure. The stiffer adhesive after
room temperature curing on the other hand implicates that only
a reduced efcient anchorage length lb,eff of about 125 mm, smaller
than the total bond length, can be involved.
4.3.2. Slip behavior for releasing tests
Fig. 9b shows the force-slip relations for the releasing tests with
a strip thickness of 1.2 mm. Similarly to the presented pull-off tests,
the room temperature cured specimen reveals a clearly stiffer
behavior than its counterpart, temporarily cured for 25 min at high
temperature. However, an important difference between pull-off
and releasing for specimens cured at room temperature can be
pointed out: whilst no further force increase in pull-off test is possible anymore after initiation of debonding, a signicant additional
resistance can be activated after rst crack appearance (see Fig. 9b).
Fig. 11 presents several load stages recorded with the ICS of the
slips sf in the horizontal direction plotted against the total bond
length. The results were recorded with a measurement rate of
1 Hz, which means that there is a time span of 1 s between two consecutive load stages. It can be seen that slip curves for load stages 91
and 92 almost coincide, whereas the transition to load stage 93 is
characterized by a sudden vertical shift in the curves. At this moment, the rst crack appears. The maximum shift in displacement
Ds is pointed out in Figs. 9 and 11. Further anchorage resistance
after rst cracking can be observed. This phenomenon is due to
the particular crack evolution taking place deeper in the concrete
substrate and the resulting crack opening mechanisms. Hence, the
force value of 46.8 kN at loadstage 92 can be increased by10.9 kN
up to the maximum force of 57.7 kN at loadstage 162. Another
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Fig. 9. Forceslip relations for the (a) pull-off with tf = 0.6 mm and (b) releasing
tests with tf = 1.2 mm.
Fig. 10. Slips sf at initiation of debonding or failure level for pull-off with
tf = 0.6 mm and lb = 300 mm.
Fig. 8. Inuence of the heating time th on the anchorage resistance and comparison
with the specimen cured at room temperature ( = prestress force loss of about 5 kN
during heating procedure).
interesting observation from Fig. 11 is the constantly growing participation of the bond length to the shear stress transfer with growing releasing force.
For the releasing specimen cured at elevated temperatures, no
sudden shape change in the slips curve was observed, a continuous
transition between the different load stages was noticed (see
2674
Fig. 11. Slips sf for releasing test cured at room temperature at different load stages,
tf = 1.2 mm, lb = 300 mm.
Fig. 13. Slips sf at rst crack appearance (RT curing) and failure state (RT curing and
25 min accelerated curing) for releasing tests/tf = 1.2 mm, lb = 300 mm/red curve of
specimen with 25 heating time corresponds to stage 115 in Fig. 12. (For
interpretation of the references to color in this gure legend, the reader is referred
to the web version of this article.)
much as possible the total necessary application time. The enhanced short-term anchorage resistance for a dened bond length
allows anchoring higher total prestress forces during the application period. It is worth noticing that, as the curing process in the
adhesive continues, stiffness of the epoxy (initially cured at high
temperature!) rises and eventually reaches the same level than
for the corresponding tests at room temperature [17]. To conclude,
the present investigation exhibits the double advantage the gradient method offers: adhesive curing at high temperature considerably shortens the necessary time span for obtaining sufcient
anchorage capacity and simultaneously, due to the temporary lower epoxy stiffness, even enhances the total resistance values.
4.4. Gradient design
Fig. 12. Slips sf for releasing test temporarily cured at elevated temperature,
tf = 1.2 mm, lb = 300 mm, th = 25 min.
Fig. 14. Debonding failure in the concrete substrate, tf = 1.2 mm, lb = 300 mm,
releasing test, th = 25 min.
2675
Fig. 15. Inuence of the bond length on the temporary anchorage resistance in releasing for (a) tf = 0.9 mm and (b) tf = 1.2 mm/th = 25 min ( = tests performed after a strong
prestress loss of about 5 kN during the heating process).
cured epoxy after temporary heating. Further experiments on longer bond lengths could be useful in order to investigate possible
asymptotic values for the temporary anchorage resistance (and
its corresponding anchorage length) after which an increase in
the bond length does not inuence the anchorage resistance anymore. Eventually, the experiments for the two different strip thicknesses of 0.9 and 1.2 mm and the respective bond length of 200
and 300 mm show the possible anchorage resistances for the practical application of the gradient method.
5. Conclusions and outlook
Locally accelerated curing of epoxy adhesives is essential for the
proposed gradient method for anchoring prestressed CFRP strips
and eliminating the use and or keeping the mechanical anchorage
systems (plates and bolts) at the ends of the strips. The curing by
sequentially heating the individual sectors must be completed
before ambient temperature curing progresses too far. However,
the temperature is limited to avoid heat induced deterioration of
the involved materials. With the developed heating elements, the
temperature gradients over the strip width could be signicantly
reduced. This allows heating the adhesive layer more uniformly,
reducing the curing time. The developed temperature control system accelerates heating the adhesive, further reducing the curing
cycle time.
In order to dene a reasonable force release for the gradient
anchorage, different pull-off and releasing tests allow to summarize adequate application congurations. With optimized heating
elements, it was shown that 25 min of curing time (at 90 C adhesive temperature) represents an optimum time interval regarding
temporary bond strength. After this heating duration, the adhesive
possesses enough strength to transfer the failure from the adhesive
to the concrete substrate with a considerably higher anchorage
resistance, and simultaneously offers a stiffness low enough to
activate the whole bond length for increasing the anchorage resistance. After a longer curing process, the stiffness of the adhesive
would increase and therefore the effective anchorage length decreases, resulting in a lower anchorage resistance. Eventually, the
temporary anchorage resistances for the used strips with 0.9 and
1.2 mm thickness were determined for two different bond lengths
of 200 and 300 mm and thus the force gradient can be designed.
Attention is drawn to the fact that the presented conclusions
are based on one specic concrete strength type. Lower tensile
2676