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NaOH + EtOAc
NaOAc + EtOH
This study is one of the arrangements of tests to be done to study the behavior of a CSTR and
shape one for the required changes determined. Hence, past analyses information is obliged and
our perception and results for the present one will be profoundly relying upon the consequences
of the three past labs. These are the hypothesis and data acquired from each of these three
investigations:
The goal of lab one was to adjust two peristaltic pumps. The pumps have a scope of rate settings
that control the volumetric stream rate (Q). In this test the most dependable scope of these
settings as for the exploratory gap of the pumps in deciding flow rate will be resolved. The
analysis will likewise secure a connection between the pump settings and the volumetric stream
rate (Q). The main Limitation for this analysis is the time (2 hours) since the material we were
utilizing was water.
Result from first lab Calibration of Peristaltic Pumps:
Q A (% setting) QA QA
L
min
, in
Q B (% setting) QB QB
, in
L
min
---------- (1)
drained
cylinder to tentatively gauge the volume of liquid in the tank. This volume is called V
during calculations. This is revised for each of the four settings, incorporating the setting with no
baffles.
Result from the second lab, Assessment of Mixing Effectiveness:
For a CSTR flow reactor the perfect mixing was found to be for stirrer setting of 80%.
Volume as a function of the stirrer setting is:
V(stirrer, RPM) V V
.
V = 1087mL [+/- 5.0].
The goal of lab 3 is to focus the energy for the fluid phase "irreversible reaction". Were the
response is between sodium hydroxide (NaOH) and ethyl acetate (EtOAc) in fluid solution for
produce sodium acetate (NaOAc) and ethyl alcohol (EtOH)
NaOH + EtOAc
rA kC A C B
NaOAc + EtOH
Since the response for the analysis is the same as the response that was utilized as a part of the
third lab, the same energy will be utilized. Also the left pump will deliver the reactor with
reactant A (NaOH) which will have the stream rate of (Q1), and the right pump will give the
reactor reactant B (EtOAc) which will have a flow rate of (Q2).
The primary phase of this lap will comprises of outlining the working conditions at an
unfaltering state production for a given transformation level. The CSTR design appraisal must be
utilized:
C AIN ( X A X AIN )
k (T ) C AIN
V
QT
(1 X A ) ( B X A )
(3)
Where:
(4)
Q =Q +Q
(5)
Q A C Ao
QB C B0
(6)
Q A C Ao
C
Q A QB
o
A
(7)
The data acquisition software records the conductivity of the response in the CSTR as a
component of time. So if a particular change is obliged an aggregate volume from the chart is to
be picked and as per this aggregate volume (theta B) and the (conductivity) will be perused from
the Matlab information.
Putting the value of (theta B) in eq #6 and solve it for Q1, then substitute the value of Q1
QT=Q2+Q1 now solve for Q2, once you have the value of Q2 now back calculate the
value of Q1 from eq #5.
Since the value of Q1 and Q2 are both obtained the calculation of the % setting of each
pump can be performed from lab 1 as follow:
Q1=1.0857[+/-.0167] (% setting) 28.19[+/-1.153]
Plug the value of Q1 and solve this equation for pump setting for pump 1.
Similarly for Q2 use
Q2=1.0538[+/-0.0161] (% setting) 11.558[+/-1.1103]
dN A
FAIN FAOUT rAV
dt
(8)
dN B
FBIN FBOUT rBV
dt
(9)
PRODUCTS
This reaction is a liquid phase reaction and can be presumed to be an irretrievable, also has no
catalytic effects, so these simplifications can be made:
dC A QT IN
C A C A rA
dt
V
dC B QT IN
C B C B rB
dt
V
rA kCA C B
With:
(10)
(11)