Oiw-hbo-0017-Hd-001 Handheld Operation With 1.3.3 Update A4

Worlds Best
Oil in Water
Analyzers
USER HANDBOOK:
OIW HANDHELD SERIES - HD-1000
OIL IN WATER ANALYZERS
for PORTABLE APPLICATIONS
DOCUMENT CODE:
0IW - HBO - 001
VERSION: +'-001
OIW-HBO-0017-HD-001
OIW SERIES HANDHELD
OPERATION
MANUAL
Rev. 001 NOVEMBER 2014
TABLE OF C ONTENTS
TABLE OF CONTENTS ....................................................................................................................................................................... 1
DOCUMENT HISTORY ....................................................................................................................................................................... 3
SYMBOLS USED IN THIS MANUAL ................................................................................................................................................ 3
SECTION 1 INTRODUCTION ..........................................................................................................................................................4
1.1 GENERAL INFORMATION ...........................................................................................................................................................4
1.2 GENERAL HEALTH & SAFETY .................................................................................................................................................. 5
1.3 E LECTRICAL S AFETY ............................................................................................................................................................... 5
1.4 MECHANICAL SAFETY ............................................................................................................................................................. 5
1.5 OPTICAL SAFETY .................................................................................................................................................................... 6
SECTION 2 UNIT OVERVIEW........................................................................................................................................................ 7
2.1 OVERVIEW OF UNIT HARDWARE ............................................................................................................................................... 7
2.2 OVERVIEW OF MEASUREMENT CYCLE .................................................................................................................................... 10
SECTION 3 OVERVIEW OF SOFTWARE OPERATION .............................................................................................................. 11
3.1 THE HD-1000 SERIES BASIC OPERATING FUNCTIONS ........................................................................................................... 11
3.1.1 Starting the HD-1000 .................................................................................................................................................................. 11
3.1.1.1 Charging the Unit ............................................................................................................................................................................................. 12
3.1.2 Basic Unit Functions .................................................................................................................................................................... 14

3.1.2.1 Screen Navigation ............................................................................................................................................................................................ 14
3.1.2.2 On Screen Keyboard........................................................................................................................................................................................ 15
3.1.2.3 Button Definitions ........................................................................................................................................................................................... 15
3.2 M AIN S OFTWARE M ENU ........................................................................................................................................................ 16

3.2.1 Quick Measurement ..................................................................................................................................................................... 17
3.2.2 Logged Measurement ................................................................................................................................................................ 20
3.2.3 Saved Data .....................................................................................................................................................................................21
3.2.3.1 Measurement Data ......................................................................................................................................................................................... 21
3.2.3.1.1 Data Export ..................................................................................................................................................................................................... 22
3.2.3.1.2 Data Saving .................................................................................................................................................................................................... 22
3.2.3.1.3 Deleting Data ................................................................................................................................................................................................. 22
3.2.3.2Spectra Data ..................................................................................................................................................................................................... 23
3.2.3.2.1 Scale Function ............................................................................................................................................................................................... 24
3.2.4 Oil Calibration............................................................................................................................................................................... 25

3.2.4.1 Download Calibration Files ...........................................................................................................................................................................25
3.2.4.1.1 Viewing and Editing Downloaded Calibration Files ........................................................................................................................... 27
3.2.4.2 Generate New Calibration Files ..................................................................................................................................................................29
3.2.4.3 Upload New Calibration Files ......................................................................................................................................................................35
3.2.5 Options........................................................................................................................................................................................... 36
8 Meadowbank Road, Carrickfergus, BT38 8YF, Northern Ireland
www.advancedsensors.co.uk
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APPENDIX 1 CALIBRATION PROCEDURE: MANUAL MIXING ............................................................................................... 37

A1.1 PURPOSE AND S COPE ......................................................................................................................................................... 37
A1.2 M ATERIALS LIST ................................................................................................................................................................ 37
A1.3 PREPARATION OF STANDARDS ............................................................................................................................................ 38
A1.4 E VALUATING THE LINEARITY OF THE CALIBRATION CURVE ..................................................................................................... 42
A1.5 CORRELATION TO AN ALTERNATE M ETHOD ......................................................................................................................... 42
APPENDIX 2 SAMPLE PREPARATION AND MEASUREMENT .............................................................................................. 43
A2.1 PURPOSE AND S COPE ......................................................................................................................................................... 43
A2.2 S AMPLE M EASUREMENT .................................................................................................................................................... 43
APPENDIX 3 ADDITIONAL CONNECTIVITY FEATURES ......................................................................................................... 44
A3.1 CONNECTING TO WI-FI....................................................................................................................................................... 44
A3.2 B LUETOOTH ...................................................................................................................................................................... 46
A3.3 PRODUCT REGISTRATION ONLINE ....................................................................................................................................... 50
A3.4 UPDATING THE S OFTWARE .................................................................................................................................................. 51
APPENDIX 4 TECHNICAL SPECIFICATIONS ............................................................................................................................ 53
APPENDIX 5 DECLARATION OF CONFORMITY ...................................................................................................................... 54
APPENDIX 6 PRODUCT UPDATES ........................................................................................................................................... 55
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DOCUMENT H ISTORY
Change No.
Version
Description
Released
00a (Draft)
First Draft for review
28th January 2014
00b (Draft)
Addition of laser safety label and update of laser safety

standards.
13th August 2014
00c (Draft)
Addition of calibration and sampling procedures.
21st November 2014
001
Final approval for release.
28th November 2014
SYMBOLS USED IN THIS MANUAL

The
symbol is used throughout this document to highlight important information.
The definitions of each term used where it is found are as follows:

CAUTION
An instruction that draws attention to the risk of damage to the product, process or
surroundings.
INFORMATION
Further reference for more detailed information or technical details.
NOTE
Clarification of an instruction or additional information.
WARNING
An instruction that draws attention to the risk of injury or death.
WARNING: Although Warning hazards are related to potential personal injury, and Caution hazards are
associated with material damage, it must be understood that operation of damaged equipment
could lead to personal injury or death. All Warning and Caution hazards must be complied with.
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SECTION 1 INTRODUCTION
1.1 GENERAL INFORMATION
This manual provides user information for the functions required in the routine operation of the Advanced Sensors Ltd
HD-1000 Portable Oil in Water Monitor System.
Functions not required for the routine function of the HD-1000 fall
outside the scope of this manual and will not be detailed. These analysers are designed to conform to EN 55011, EN 300
328, EN 61326-1: 2006, EN 61000-4-2 & -3 and EN61010-1 2001 Part 1. The HD-1000 is designed for portable use within
Safe Areas to measure the residual hydrocarbon content of Produced Water.
The oil content is determined using a technique known as Laser Induced Fluorescence (LIF). The resulting oil
fluorescence value is used to calculate the proportion of hydrocarbons in the water. The HD-1000 analyser is equipped
with a fibre optic probe and uses an Android based software interface, with touch screen, to simply and accurately
measure the concentration of oil in water. The stainless steel jacketed probe is detachable for convenient storage.
HD-1000 facilitates these phenomena and with intuitive Android interface becomes a tool that allows user to easily
measure oil in water concentration with 2% accuracy 1 instantly.
Unauthorised use of the HD-1000 outside the recommended use described within this manual will invalidate product
warrantee and support. Should you have any questions or comments regarding any information contained within this
manual, please contact us at address shown below:
Advanced Sensors Ltd
8 Meadowbank Road
Carrickfergus
BT38 8YF
UK
Tel: +44 (0)28 93 32 89 22
Fax: +44 (0)28 93 32 86 69
Web: www.advancedsensors.co.uk
NOTE: This manual addresses ONLY THE ROUTINE OPERATION of the HD Series of Portable Analyser
systems.
Dependent upon application.
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1.2 GENERAL HEALTH & S AFETY

1.
The equipment is designed for use in SAFE AREAS ONLY.
2.
All warning labels on the equipment and packaging shall be observed.
3.
There are NO USER-SERVICEABLE PARTS within the unit. Therefore no requirement exists for the unit to be
opened. Any unauthorized repairs or modifications shall not be under-written by the manufacturer.
4.
Ensure the HD-1000 is handled with care to avoid damage to the unit or personal injury.
5.
Ensure mains power to the system has been disconnected prior to use, i.e. mains charger.
6.
If any physical damage occurs to the enclosure, display window or probe connections, then the power must be
removed immediately and the manufacturer, or their approved agent, contacted for servicing and repairs.
1.3 ELECTRICAL S AFETY

Power requirements for the HD-1000 are minimal as the unit requires mains power for recharging only. The HD-1000
system is designed to operate off one of 2 nominal power variants: 115VAC or 230VAC. Use only the charger and cable
supplied with the instrument. It is the responsibility of the USER to ensure compliance with the regional requirements
for electrical safety. After 2 minutes of idle use the unit will automatically enter power save mode and after 30 minutes
shut down to save power.
1.4 MECHANICAL S AFETY

1.
An assembled system weighs approximately 1 kg (including the detachable probe).
2.
The probe has a maximum bend radius of 16cm and should not be exceeded.
3.
Installations where the process water temperature may be high it is the customers responsibility to comply
with any regional H&S signage requirements.
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1.5 OPTICAL S AFETY

The system uses a Class 3R laser as part of its measurement process. The light source is contained within the analyser
and transmitted along an optical cable housed within the jacketing of the probe ensuring safety during routine use.
Therefore to prevent accidental eye exposure to the laser users shall ensure the dust caps (Figure 2) be fitted when the
probe is not connected. Power to the laser, or the unit, should not be applied when the unit is disassembled or the dust
caps removed. All labels are in accordance with the requirements outlined in EN 60825-1:2007 Safety of laser products
Part 1: Equipment classification and requirements.
The upper probe port is labelled with the following 8mm (h) x 16mm (l) warning, and users should take caution to avoid
direct eye contact as per the Class 3R laser warning below:
A 32mm (h) x 64mm (l) information and warning label, shown below, is affixed to the back of the unit which provides
additional laser warnings, laser information, manufacturing details, CE declaration and power information.
CAUTION: USE OF CONTROLS OR ADJUSTMENTS OR PERFORMANCE OF PROCEDURES OTHER THAN THOSE

SPECIFIED HEREIN MAY RESULT IN HAZARDOUS RADIATION EXPOSURE.
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SECTION 2 UNIT OVERVIEW

2.1 OVERVIEW OF UNIT HARDWARE
The following section provides an overview of the HD-1000 hardware. The HD-1000 is a portable handheld unit with a
detachable probe for insertion into a light tight sampling vessel as shown below in Figure 1. The main unit is an encased
touch screen display (1) with a detachable probe. The probe is a stainless steel jacketed bifurcated fibre assembly,
where one leg carries input signal and the other output signal, which converges into the probe ferrule. Each leg
attaches to the ports on the right hand side of the unit as shown in Figure 1 (and #2 in Figure 2). The calibration
chamber (3) can be used for both calibration and as a sampling vessel. It is used to provide a light tight environment
that enables the probe to accurately measure oil droplets fluorescing in water.
Figure 1: The HD-1000 portable analyser with sampling vessel.

1. Main analyser unit 2. Probe - with flexible jacketing 3. Calibration Chamber (light tight)
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Figures 2 and 3 below depict the right and left sides of the unit. The right side, Figure 2, is equipped with the Power On
button (1) and two probe ports (2) fitted with dust caps (3). The upper port supplies the laser output while the lower
port supplies the return signal to the spectrometer. The dust caps should always be fitted when the probe is not in use
to prevent accidental exposure to the laser and from dust or liquids damaging the unit. The left side, Figure 3, is fitted
with the Power Supply Outlet (4) for charging when required.
Figure 2: Right side of analyzer unit with: 1. Power On

button 2. Probe ports & 3. Dust caps
Figure 3: Left side of analyzer unit 4. Power supply outlet.
The back of the analyser is embossed with the Advanced Sensors logo and the Serial Number (5) of the unit.
Figure 4: Rear of the analyzer unit with: 2. Probe ports with dust caps and 5. Serial Number.
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The detachable probe, Figure 5, is jacketed in stainless steel (3), is approximately 1.2 meters in length and bifurcated at 1
meter into two legs, each approximately 0.2 meters in length. At one terminal is the probe ferrule (1), a stainless steel
tube which houses and protects the fibre assembly. Each leg (2) terminates in connectors for the separate input and
output of signals.
Figure 5: Detachable probe; 1. Probe ferrule 2. Legs & 3. Stainless Steel Jacket
CAUTION: Do not exceed the probe bend radius of 16cm.

the fibres within the jacketing.
Exceeding this radius will result in damage to
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2.2 OVERVIEW OF MEASUREMENT PRINCIPLE

The HD-1000 uses laser induced fluorescence to quantify the proportion of hydrocarbons in the water. Fluorescence is
proportional to the concentration of hydrocarbons in water, in particular residual oil content found in process water.
Therefore fluorescence will increase, or decrease, with oil concentrations in water and is translated into quantifiable
readings; such as PPM or PPB. Each type of oil has a unique spectral shape which will only differ in amplitude relative to
concentration as shown in Figure 6. In other words, the shape of the spectra peak is unique to each oil type and as
concentration decreases the peak decreases in height. Knowing the spectra shape for 2 concentrations, for example 100
and 0 PPM, will typically provide sufficient information to measure the oil content in water.
Figure 6: Example of spectra obtained by the HD-1000 for one oil type at 4 different concentrations.
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SECTION 3 OVERVIEW OF SOFTWARE OPERATION

3.1 THE HD-1000 SERIES B ASIC OPERATING FUNCTIONS
The HD-1000 analyser runs an Android based interface for routine operation. This manual assumes that the user has a
basic competence, or familiarity, with Android based technology (i.e. smart phones and tablets).
3.1.1 Starting the HD-1000

Turn on the main power supply by firmly pressing and holding the button on the right side of the analyser unit (#1 in
Figure 2) for 3 seconds or until the Samsung prompt appears. Once power up of the unit is complete, the lock screen
will appear as below in Figure 7. The analyser software is set to automatically start up when the unit is powered on.
Swiping the screen to unlock, as indicated on screen in Figure 7, will open up to the main menu of the analyser software
as shown in Figure 8 below.
Figure 7: Lock screen of the HD-1000
Figure 8: Analyser Main Menu
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To exit or manually close the analyser software, press the home button (Figure 9 - #2) at the bottom of the main display
screen. When the software is closed the Home Screen, Figure 10 below, is displayed. Touching the Launch Analyzer
field will load the analyzer software.
Figure 9: Front Main Menu display on the analyzer.

1. Analyzer software Main Menu 2. Home screen button.
Figure 10: Home screen display with the Launch Analyser

selection field.
3.1.1.1 Charging the Unit

Charge the unit with only the mains charger and cable supplied with the instrument. When the battery power is low a
warning message will appear on screen alerting users to connect the unit to a charging device, as follows in Figure 11.
Figure 11: Low battery warnings; as the battery level decreases the first Battery Low message is then followed by a second
warning Battery critically low indicating less than 5% charge remains and the unit must be connected to a charger.
Connect only the supplied charger cable to the power supply outlet on the left side of the unit (#4 in Figure 3 p. 8). Then
plug the charger into the mains power supply and charge the unit fully. Mains power supply shall be readily available for
charging the unit as required.
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Measurement functions will not be available while the unit is charging and the Main Menu screen will display Charging
Mode as follows:
Figure 12: Charging Mode Main Menu Options.
Once charged, and the charger cable removed, the HD-1000 will automatically restart. This is required to stabilize the
power on the device and enable power saving features.
NOTE: Ensure the unit is switched on to charge. If the unit is switched off, restart the unit.
Connecting the unit to the charger DURING CALIBRATION ONLY will result in a software reset. The following warning
will appear if the user attempts to calibrate the unit while in charge mode:
NOTE: Advanced Sensors recommend calibrating the unit when fully charged and avoid connecting the
device to a charger during calibration as this will reset the software.
NOTE: POWER SAVING MODES: when idle (not measuring) the HD-1000 will exit either Quick or Logged
Measurement menus after 2 minutes as the spectrometer shuts down to save power. After 30
minutes the unit will power down completely.
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3.1.2 Basic Unit Functions

The following sections will outline basic functionality for the routine operation of the HD-1000. Functions for routine
operation include, but are not limited to: screen navigation, on screen keyboard, Wi-Fi and Bluetooth connectivity.
3.1.2.1 Screen Navigation

Accessing different analysis options requires users move either to the previous screen or between screens within a
selected menu.
INFORMATION: The HD-1000 display screen will Auto-rotate adjusting to the position of the unit. Screen
captures in this manual are in portrait format. When in landscape format, while the
orientation has changed, the information remains the same.
Navigating Between Screens
The Advanced Sensors logo
, located in the upper left corner of menu screens, functions as a Back button
returning users to the previous menu screen.

Alternatively, users can press the Back Key (1) located at the base of the screen and to the right of the Home button as
shown in Figure 12. Note that these Touch Keys are not permanently illuminated however the display duration can be
adjusted according to the Manufacturers instructions. Users press this part of the screen to illuminate the button and
complete the action.
Figure 13: 1. Back Key and 2. Option Key (not required for operation)
Scroll Views
Within a selected menu, multiple viewing options may be available. Users navigate, or scroll, between each view by
placing a finger on the screen and swiping it to the left or right. Swiping to the left moves forward one screen while
swiping to the right moves backward one screen. Specific information for each menu, the additional options and
screen views are further described in Section3.2 Main Software Menu.
Zoom In / Out
In graphical displays users can zoom in or out and move through graphical data by pinching (spreading 2 fingers apart
or bringing together), using the magnifying options at the bottom of screen or by placing a finger in the centre of the
graph and scrolling in any direction. The magnifying options include: + to zoom in, - to zoom out and return to origin.
Increasing PPM Reading Display Font Size
Hard press the PPM value on screen to increase the font size. There are 3 sizes available for users to select.
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3.1.2.2 On Screen Keyboard

When text input is required an on screen key board, alphabetic as in Figure 14 or numeric as in Figure 15, will
automatically open when the user selects a text box. Once the required information is entered select the next text box,
press Done or the
button to return to the previous screen.
Figure 14: Alphabetic on screen keyboard.
NOTE: When using the
Figure 15: Numeric on screen keyboard.
button, pressing it twice will return to the previous screen.
3.1.2.3 Button Definitions

The following table lists the most commonly used buttons and their functions for reference:
Button:
Function:
Start: Begins measurement. Turns into the Stop
button once pressed.
Stop: Ends measurement. Reverts back into Start
button once pressed.
Take / Save Spectra: Saves the current spectrum.
Save: Saves results data only. Appears after the
measurement has finished.
Open Menu: Opens popup menus displaying
selectable options.
Delete: Select to delete a file or data point.
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3.2 MAIN SOFTWARE MENU

The HD-1000 uses a simple Android based user interface with user intuitive icons and menu features. The following
sections will provide a detailed overview of the softwares functionality. Information for additional non analytical
functions, such as connectivity, is described in Appendix 1. The Main Menu screen, Figure 16 below, has 5 main
functional menus including software version for quick reference:
Figure 16: HD-1000 Main Software Menu. Menu options are: 1. Quick Measurement 2. Logged Measurement 3. Saved Data
4. Oil Calibration and 5. Options. 6. The current version of software on the unit.
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3.2.1 Quick Measurement

The Quick Measurement menu allows the user to take measurements but the data must be saved manually to prevent
accumulation of unnecessary data. The Quick Measurement functions primarily to assist in optimizing oil type settings
allowing users to save only measurements of interest. An oil type file should be loaded prior to measurement (see
Section 3.2.4 Oil Calibration p. 25) or the Oil Type Recognition function turned on (see Section 3.2.5 Options p. 36).
INFORMATION: For more accurate results samples should be prepared as described in Appendix 2 p.43.
1.
Select the Quick Measurement button from the Main Analysis menu. The main screen, by default, will always
open with the Spectra graphic display at the bottom. There are 3 lower screen viewing options, as shown
below in Figure 17. Scroll, left or right, to view each screen.
A. Raw data display
B. Spectral graph display
C. Measurement readings display

(PPM currently only available)
Figure 17: Quick Measurement menu screens from left to right: Raw data, Spectra and Reading graphical displays.
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2.
From the samples list select the arrow to open the popup menu as shown in Figure 18. Select the number of
samples required for a quick measurement.
Figure 18: Main Quick Measurement screen. Press the arrow and the sample selection window will pop up.
INFORMATION:
Custom Options: When selecting the Custom samples option a Custom Measurement Schedule will then
pop up as shown below in Figure 19. Scroll up or down through the numerical options selecting a measurement
time and interval between samples. Press OK to apply the settings for the current quick measurement and
close the scheduler.
Figure 19: Schedule for defining Custom Sample Measurement parameters.
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3.
Once the parameters have been selected and the sample prepared as previously described, insert the probe into
the sample and press the blue start button. Once pressed it will change to the red stop button which can be
pressed to stop measurements at any time. Readings will be displayed in PPM at the top of the display screen
while spectra or raw data are displayed in the lower part of the screen.
A. Start Display.
B. Display during measurement.
C. Display at end of measurement.
Figure 20: Measurement reading display before measurement showing the start button (A), during measurement (B) and at
the end of measurement (C).
IMPORTANT: The data will not automatically save. Press the Save and/or Save Spectra button(s) to
retain the Quick Measurement data otherwise it will not be saved.
4.
Press the Save Spectra button to save spectral data. A Spectra Saved message will appear on screen.
Press the Save button to save the measurement data. The Save Data screen opens displaying the number of
samples taken, average reading and a comment box for the user to enter additional reference information (a
touch screen keyboard will open). Press the large blue Save Data button to save the measurement data.
Results can be stored on the unit or transferred to another device for analysis.
See Appendix A3.2 for Bluetooth data transfers.
Figure 21: Save data screen; comments area to enter reference or comment identifier.
5.
Once the measurement(s) are completed remove the probe from the sample and clean with a damp cloth.
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3.2.2 Logged Measurement

To use the Logged Measurements function follow the same procedure as described above in Section 3.2.1 for Quick
Measurements. The only exception is the results data are automatically saved; spectral data must still be saved
manually using the Save Spectra as shown in Figure 22 B and C.
A. Start Display.
B. Display during measurement.
C. Display at end of measurement.
Figure 22: Measurement reading display before measurement showing the start button (A), during measurement (B) and at
the end of measurement (C).
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3.2.3 Saved Data

All data saved to the HD-1000 can be accessed from the Saved Data
menu. Data is saved as two
separate types: Measurements and Spectra.
3.2.3.1 Measurement Data

Measurement data are listed chronologically starting with the latest measurement data and ending with the oldest data
as shown in Figure 23 A. The listed information per measurement includes: the oil type name, file creation date/time,
the average PPM reading and any added comments. Selecting a measurement will open a graphical display of the data
as shown in Figure 23 B.
A. Measurement data list
B. Data graphical display
Figure 23: Saved Data Measurements list and display. Selecting a measurement from the list (A) will open a data display as
shown in (B).
Saved data can be exported (1), saved (2) or deleted (3) using the following buttons (Figure 24):
Figure 24: Saved data option buttons: 1. Export 2. Save 3. Delete.
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3.2.3.1.1 Data Export

Data can be exported by selecting the Export
icon. Formats for export are: Short Text or CSV file. Selecting an
export option will open the Complete Action Using menu as shown in Figure 25. Users can select to export data using
Bluetooth, dropbox, email, gmail or Wi-Fi direct. Connection to Wi-Fi and Bluetooth enabled devices is detailed in
Appendix 1 of this manual. Once a method of export has been selected, users can choose to perform transfers by the
selected method Always or Just once.
Figure 25: Options available for data export.
3.2.3.1.2 Saving Data

To save the current data select the Save
icon. The following save location message will appear at the bottom of
the on-screen graph:
Figure 26: File save location message.
3.2.3.1.3 Deleting Data

To delete the current data select the Delete
icon. The following message will open to confirm the delete action:
Figure 27: Confirm result deletion pop up.

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3.2.3.2Spectra Data
Spectral data are listed chronologically starting with the latest measurement data and ending with the oldest data as
shown in Figure 28 A. The listed information per measurement includes: the oil type name, creation date/time and the
average PPM reading. The tick box next to each entry can be selected to compare up to 8 spectra. Selecting the
Compare button will open a graphical display comparing the selected data as shown in Figure 28 B.
A. Saved Spectral data
B. Compared spectral data
Figure 28: (A) Saved measurement spectra and (B) comparison display.
Saved spectral data can be scaled (1), exported (2), saved (3) or deleted (4) using the following buttons (Figure 24). The
export, save and delete functions are the same as previously described for Measurement Data in the previous section.
In addition to these users can also select spectra to compare using the scaling function.
Figure 29: Saved spectral measurement options: 1. Scale settings 2. Share / Export 3. Save 4. Delete.
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3.2.3.2.1 Scale Function

The scaling function enables comparison of up to 8 spectral graphs. Selecting the Scale settings
icon will open
the available scaling options: Normalize to Highest Value and Reset To Original, as shown below in Figure 30.
Figure 30: Scaling options.
From the list of options select Normalize to Highest Value. This will scale all the comparison spectra to relative to the
spectra with the highest value.
This adjustment enables users to compare spectral measurements for different
concentrations of the same oil or to compare spectral measurements between different oil types. Figure 31 A below is
an example comparing 5 spectra taken for 1 oil type.
The fluorescence, or signal intensity, varies with PPM
concentration accordingly. However when the spectra are Normalized to Highest Value the highest value of all spectra
are made equal and fit into approximately the same curve shape (Figure 31 B).
When comparing different oil types
normalizing to the highest value will highlight any differences in the spectral curve, simplifying the comparison.
A. Original (Non Normalized) Data
B. Normalized Data
Figure 31: Graphical display of spectra for comparison. (A) Original NON Normalised spectra and (B) Normalized spectra for
comparison.
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3.2.4 Oil Calibration

Oil type files contain all the calibration parameters required for the specific oil type being analyzed. The HD-1000 is
supplied with generic default oil type files for calibration however these may not be suitable for the type of oil being
analyzed. Calibrations may require simple adjustment, gain and/or PPM offsets, or a new calibration may be required.
When analysis of a new oil type is required the HD-1000 must be calibrated with at least 2 different concentrations of
the new oil. This calibration will generate the oil type file required for the unit to recognize and accurately measure that
oil type. Calibration files can be uploaded for file sharing between units or facilities. Multiple oil type files can be stored
on the system each displayed with basic reference information for each.
To access calibration options press the Oil Calibration
button from the analyzer main menu. Oil
type calibration files can be downloaded or a new one can be generated and uploaded. The following sections describe
how to download files, how to generate new files and upload files. To perform a calibration see Appendix 1 - Calibration
Procedure: Manual Mixing.
3.2.4.1 Download Calibration Files

Oil type calibration files can be downloaded onto the HD-1000 as follows:
1.
Ensure the device has been registered. See Appendix A3.3 Product Registration Online for information.
2.
Connect to wireless network. See Appendix A3.1 Connecting to Wi-Fi for additional information.
3.
Press the Oil Calibration button from the main menu. The main screen will open and list all the loaded oil type
files on the unit, shown below in Figure 32.
Figure 32: Main Oil Calibration screen.

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4.
Press the Download
button at the top of the screen.
5.
The HD-1000 will initialize and load all possible oil type files for download. These are divided into Local and
Global files. Figure 33 displays a sample listing of oil type files available for download. Swipe to change
between Local and Global listing screens. Local files are Customer specific oil type files for sharing between
devices. Global files are publicly available oil type files for all HD-1000 users to download.
Figure 33: Available local oil type calibration files for download.
6.
Select the required file and the following message will pop up: Downloading Oil Type File. Please Wait. Once
the download is complete the following message will pop up: Oil file downloaded successfully.
7.
If the file has already been downloaded the message This file is already downloaded will pop up.
8.
Select
to return to the list of downloaded oil type files.
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3.2.4.1.1 Viewing and Editing Downloaded Calibration Files

Once a file has been downloaded, or created, users can view or edit basic parameters to optimize the calibration curve
for a particular oil type.
1.
Select the file of interest. The Stored Spectra graphical display will open as shown in Figure 34 below. The
Calibration Curve and Data Points can be viewed by swiping to the right.
A. Spectral calibration graph.
B. Calibration curve.
C. Data points for the curve.
Figure 34: Stored information for downloaded spectra showing graphical display, calibration curve and data points.
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2.
To make minor adjustments to the oil type calibration file, select the Settings
icon to open the list of
available options as shown in Figure 35. Users can adjust the Gain factor, PPM offset, Upper and lower
detection masks or auto correction of the curve.
Figure 35: Adjustment settings for calibration curves.
3.
From the options list select a parameter for adjustment. The following editable fields, Figure 36, will open for
the respective option. An on screen keyboard will open when an editable text field is selected. See Section
3.1.2.2 On Screen Keyboard for keyboard details p.15.
A. Gain factor
B. PPM offset
C. Lower/Upper mask
D. Auto correction
Figure 36: Editable fields for the selected calibration file. A. Gain factor B. PPM offset C. Mask detection limits and
D. Auto correction values.
4.
To apply the new settings select
or the return key. A Save Changes prompt will pop up to confirm and
apply the changes.
Figure 37: Save changes prompt. Select Ok to save new calibration curve parameters or Cancel to discard.
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3.2.4.2 Generate New Calibration Files

A calibration file must be generated for each oil type. A pipette, light tight sample container (the unit is supplied with a
light tight calibration chamber), mixer and pure oil sample are required to perform the calibration. The first oil sample is
prepared at the maximum required concentration, as described in Appendix 1, as this will be the highest expected
fluorescence for the given oil type. Subsequent samples will be serial diluted to the Users requirements with the final
sample being 0 PPM or pure water. Users can generate calibration files for each new oil type as follows:
1.
Press the Oil Calibration button from the main menu. The main screen will open and list all the loaded oil type
files on the unit as shown in Figure 32.
2.
Select New
from the top right of the screen. At this point the software begins a guided step by
step calibration process.

3.
Users must give each new calibration file a name. The first step is to type a New Oil Name in the text box as
shown below in Figure 38. Note that the file name must be at least 3 characters in length. The on screen
keyboard will open when inside of the text box is touched.
Figure 38: Naming a new oil calibration file.
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4.
File names can be any combination of alphanumeric characters. Once the 3 character minimum is entered, the
Maximum PPM Range text box will open as shown in Figure 39, but users can continue entering a file name.
The measurement range text box will remain open until a value is entered.
Figure 39: Measurement range parameters.
5.
Once the maximum measurement value has been entered either press Done on the number pad or select the
Open Menu icon to open the Guide Calibration By: options list. Users can select the Recommended
option or Dilution by Quarter, Equal Distribution or Custom.
Figure 40: Available dilution options for calibration.
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INFORMATION:
Custom Options: When selecting Equal Distribution or Custom calibration users are required to input
additional information as described in the following section.
Equal Distribution: Users can select to calibrate for an equal number of sample points or dilutions. Once the
Equal Distribution option has been selected a text box will open where users enter the Number of Data
Points: required as shown in Figure 41. Proceed with the calibration detailed in the remainder of this section.
Figure 41: Equal distribution options.
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Custom Distribution: Users selecting to calibrate with a custom distribution, Figure 42 A, set the maximum
PPM which serves as the starting measurement.
After selecting to Start Calibration, subsequent
measurements are then defined using the slider or entering a value, using the pop up keyboard, in the text box
as shown in Figure 42 B. Then proceed with the calibration as detailed in the remainder of this section.
A. Input selection screen.
B. Input next measurement screen.
Figure 42: A. Selection of Custom calibration as the Guide Calibration By method. B. Next value input screen;
input using the pop up keyboard or the slider.
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6.
Once the Guide Calibration By method has been selected, press the blue Start Calibration button. The
following screens, Figure 43, will open to guide users to the first calibration point. Once each step is complete
users press the OK button to proceed to the next step.
A. Prepare sample for measurement.
B. Ensure probe is cleaned before adding to sample solution.
Figure 43: The first calibration reading guide screens: prepare maximum measurement sample (A) then ensure the probe is
cleaned prior to adding to the sample (B).
7.
Once the measurement is complete the following popup message will open to confirm the addition of the new
data point (Figure 44). Click Cancel if the value is not acceptable. For the first measurement this will end the
new calibration session and return to the main calibration list screen. For all other additional measurements
this will return to the measurement screen and allow the user to measure the sample again. Click OK to save
the current data point and proceed to the next measurement.
Figure 44: Confirm addition of a new data point.
INFORMATION: When problems obtaining a data point arise an on screen message will appear to
notify the user of the issue after 2 Bad Data Point messages a Bad Calibration
message will open. Users can select to Discard the calibration or Try Again to
obtain a more accurate result. Difficulty obtaining a data point may be the result of
oil separating out of solution or oil sample may have low fluorescent properties.
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8.
The next measurement value will automatically be displayed for measurement. On screen prompts will guide
users stepwise through the measurement, Figure 45. Note press the OK button at each step to proceed with
the measurement.
A. Next measurement preparation screen.
B. Instruction to clean probe and insert into sample

container.
Figure 45: Measurement screens indicating: A. the next measurement point with B. instructions to proceed
9.
Once the measurement is complete the Add New Datapoint message, as shown in Figure 44 of step 7, will
open and users select Cancel or OK to proceed to the next measurement.
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10. The final calibration must be for a 0 PPM measurement. Once the final measurement has been taken, and the
data point saved, a Calibration Completed prompt will appear between the graph and the measurement
instruction guide shown in Figure 46 A. Select OK to proceed and a Calibration Completed confirmation
message, shown in Figure 46 B, will open to confirm or cancel the calibration.
A. Final measurement screen
B. Confirmation calibration is complete.
Figure 46: A. Final 0 PPM reading screens, select OK to complete. B. Confirm Calibration Completed.
11. The completed calibration will be stored in the main calibrations list. From the list users can select the
calibration for viewing, to use or to upload.
3.2.4.3 Upload New Calibration Files

Users can upload oil type calibration files onto a secured server to backup the device files, to download on additional
units or for use on site for data analysis. Upload files as follows:
1.
Ensure the Wi-Fi is connected and the unit Registered. See the following for more information: Appendix 1.1
Connecting to Wi-Fi and Appendix 1.3 Product Registration.
2.
Select the Oil Calibration
3.
Then select the oil calibration file for uploading.
4.
From the icons at the top of the screen, select the Upload
5.
An Uploading timer will open during to indicate upload progress. When complete, an Upload successful
menu.
icon.
message will appear at the bottom of the screen.
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3.2.5 Options
From the Options menu, users can configure Oil type recognition, load oil type files, set sampling frequency and open
an electronic copy of the operation manual.
Oil Type:
The HD-1000 can be set to recognize oil types. Essentially the analyzer will measure the sample, compare the resulting
spectra against the oil type files downloaded on the unit and select the calibration oil type file which best fits the data.
To enable this feature select the ON switch next to Oil Type Recognition as shown in Figure 47 A.
If the specific oil type calibration file has been saved or downloaded onto the unit deselect the Oil Type Recognition
feature and select the file from the drop down list as shown in Figure 47 B.
Figure 47: Oil type recognition options: A. On and B. Off with the required oil type file selected from the drop down list,
sampling frequency can then be set.
Once the oil type file selection has been made, users can set the sampling frequency or the period of time between each
sample measurement. This can be adjusted to suit the user and the type of oil to obtain the most accurate results. A
shorter sampling frequency would be required for oils which separate out faster compared to a longer frequency for oils
which do not separate quickly. Then return to the Quick Measurement or Logged Measurement menu to begin
analyzing samples.
Other Options:
The final available option is Help. Selecting this option will open and display on screen this Operators Manual for the
user to consult.
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APPENDIX 1 CALIBRATION PROCEDURE: MANUAL MIXING

A1.1 PURPOSE AND S COPE
The purpose of this procedure is to provide instructions to calibrate the HD-1000 handheld unit using manually mixed
standards prepared from light crude oil samples, with an API gravity greater than 31. It is recommended this procedure
be followed when suitable laboratory mixers are not available.
This procedure describes a standardized method for calibrating the HD-1000 for 100, 1000 and 3000 ppm
concentrations only; requirements for additional concentrations shall be requested from Advanced Sensors. In future
this procedure shall be updated to include any additional concentrations and made available accordingly.
NOTE: This procedure is only for calibrating light crude oils with an API gravity greater than 31.
A1.2 MATERIALS LIST

The following materials are required, and were used, to perform this calibration:
1. Crude oil Sample (100 ml)
2. Surfactant: Loctite 7840 / Loctite Natural Blue Cleaner (North America)
3. Clean tap water (De-Ionized is recommended if available) (3L)
4. 500ml graduated capped brown glass bottle
5. 200ml graduated beaker
6. 100 ml graduated cylinder*
7. 100 l Sartorius Proline Mechanical Pipette* (range 10 100 l) with disposable tips*
8. Calibration Chamber*
9. Optical cleaning tissues (3M Super Clear Lens Cleaning Tissues); any lint free optical tissue can be used.
* Items 6 & 7 (including disposable tips) are included in the HD-1000 Optional Calibration Kit.
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A1.3 PREPARATION OF S TANDARDS

Standards are prepared from a crude oil sample (with an API greater than 31) with the addition of a surfactant, or
surface active agent, to increase the oil dispersion in the water.
Standards for 100, 1000 and 3000 ppm are prepared according to Table 1. Additional standards are then prepared by
stepwise dilution with the final standard being a water blank, or 0 ppm.
Table 1: Oil Volumes required in preparation of standards
100 ppm
1000 ppm
3000 ppm
Volume of Oil
20 l
200 l
600 l
Volume of Surfactant
10 l
100 l
300 l
Total Volume in Water
200 ml
200 ml
200 ml
Step 1: Prepare Standard Solution

1. Measure 200 ml of clean water in the graduated cylinder and add to the 500ml graduated glass bottle.
2. Using the pipette, with a fresh tip, add the required amount of surfactant (see Table 1 for volumes) to the water.
3. Next, using the pipette with the same tip, add he required amount of oil (see Table 1 for volumes) to the water &
surfactant mixture.
4. Rinse the pipette in the water to clean the tip of any residue.
5. Cap the graduated glass bottle and shake it vigorously to mix for 2 minutes. Ensure that the oil and surfactant are
well mixed.
6. Allow the sample to settle for 2 minutes.
Step 2: Preparing the HD-1000

1. Ensure the cleanliness of the analyzer probe and calibration chamber. Rinse the entire probe ferrule in a beaker
of clean water and dry with an optical tissue. Do not detach the probe from the analyzer unit.
2. Ensure mains power to the system is disconnected prior starting the oil calibration. (Disconnecting the charger
will restart the system).
3. From the main menu select Oil Calibration.
4. The Oil Type Management screen will open listing all oil type files loaded on the unit.
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5. Select New from the Oil Type Management screen.
6. The Adding New Oil screen will open and display all the options for entering new oil calibration details. Using
the pop up keyboard, enter the new calibration details as follows:
6.1. Enter a New Oil Name: The file name must be at least 3 characters in length.
6.2. Enter the Maximum ppm Range: enter the highest ppm value for the
current calibration.
6.3. Select the Guide Calibration By: Select Custom.
7. Press the Start Calibration button to begin the calibration process.
This will open the first standard
preparation screen which reads: XXXX PPM PREPARED.

Step 3: Calibration with Prepared Standards
1. Ensure the cleanliness of the analyzer calibration chamber.
2. Empty the first standard into the analyzer calibration chamber and mix well. (Transfer the sample between the
calibration chamber and the 200 ml graduated beaker and repeat 3 times to ensure a thorough mix)
NOTE: Ensure the cleanliness of the analyzer calibration chamber and 200 ml graduated beaker prior to
running a standard. Make sure the prepared standard is well mixed before taking the reading.
3. Press the OK button to proceed to the next step.
4. The next screen will open displaying CLEANED PROBE IN THE BEAKER instructing users to insert the clean
probe into the chamber. Ensure the probe is clean and dry then insert into the analyzer calibration chamber.
NOTE: Use only standard optical cleaning tissues to remove any dirt or residual oil that might be
present on the probe including the optical end.
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5. Press OK button to proceed to the next step. This will open the measurement screen. Once the measurement is
complete a pop up message will confirm the addition of the fluorescence value for the first standard.
6. Press the OK button to proceed to the next step. This will open the next measurement preparation screen.
Diluted Standards
7. For the remaining dilutions, always ensure the cleanliness of the calibration chamber, the 200 ml graduated
beaker and cylinder between standards.
8. Mix the sample in the calibration chamber, then using the graduated cylinder, remove 100 ml of the previous
standard solution. Pour into the 200 ml graduated beaker.
9. Add 100 ml of clean water to bring up to 200 ml in the beaker.
10. Remove the remaining sample from the calibration chamber into a separate beaker.
11. Transfer the next standard from the 200ml beaker into the calibration chamber and mix well.
12. (Transfer the sample between the analyzer calibration chamber and the 200 ml graduated beaker and repeat 3
times to get a good mix)
13. Enter the next measurement value (XX ppm) and press OK.
14. The next screen will open displaying CLEANED PROBE IN THE BEAKER instructing users to insert the clean
probe into the chamber.
15. Repeat Steps 7 through 13 for all remaining cut down dilutions. When all required dilutions are completed
perform a Blank, or 0 ppm, calibration.
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NOTE:
1. Ensure the calibration chamber, the 200ml graduated beaker and graduated cylinder are clean prior to
running each standard.
2. For most accurate results ensure the prepared standard is well mixed before taking the reading.
3. Collect the left over sample it is used at the end for evaluating the linearity of the constructed
calibration curve as described in Section 4.
Calibration Blank: 0 ppm

1. Ensure the cleanliness of the 200 ml graduated beaker and the calibration chamber.
2. Prepare a blank solution by adding the same volume of surfactant as used for the highest standard into 200 ml
of clean water in the 200 ml graduated beaker.
3. Empty the blank into the analyzer calibration chamber and mix well. (Transfer the sample between the analyzer
calibration chamber and the 200 ml graduated beaker and repeat it for 3 times to get a good mix).
4. Repeat Steps 7 through 13.
5. Press the OK button next to Calibration Completed. This will complete the calibration, storing the results in
the main calibrations list.
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A1.4 EVALUATING THE LINEARITY OF THE CALIBRATION CURVE

Following the calibration, test the linear range of a calibration curve for the sample under study.
1. Ensure the cleanliness of the probe and analyzer calibration chamber prior to running any sample.
2. Prepare a solution of unknown concentration by combining left over standards used in the calibration.
3. Load the produced calibration curve prior to measurement.
4. Press the Quick Measurement button from the main menu to open the measurement menu.
5. Empty the solution of unknown concentration into the calibration chamber and mix well ensure that the
sample is very well mixed.
6. Insert the probe and press the START button to take a measurement of the unknown solution.
7. Check the displayed ppm reading. This result is the concentration of the solution as determined from the
constructed calibration curve.
8. Prepare the next unknown sample by diluting the first solution by a factor of 2 with clean water (100mls of
sample + 100mls of clean water).
9. Pour the prepared new unknown sample into the calibration chamber and mix well.
10. Follow steps 5 through 7 to obtain the next reading.
NOTE: If the displayed ppm of the second unknown is greater than half the ppm of the first unknown
measured, the calibration curve is proved to be non-linear and conducting a calibration linear
range check or constructing a new calibration curve is recommended.
A1.5 CORRELATION TO AN A LTERNATE METHOD

If the HD-1000 measured concentration is greater, or less, than the alternate method (i.e. laboratory analysis) ppm
reading, adjust the HD-1000 instrument gain factor to match the difference.
NOTE: To adjust instrument gain, go to the oil calibration and the constructed oil curve file should be
visible in the oil calibration list. Select the file, press the settings icon
the analyzer reads the required concentration.
and adjust the gain factor until
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APPENDIX 2 SAMPLE PREPARATION AND MEASUREMENT

A2.1 PURPOSE AND SCOPE
Procedure for analysing representative oil in water samples using the HD-1000. Samples should be obtained using the
applicable corporate procedures.
Advanced Sensors recommend samples are taken using clean GLASS bottles only, preferably using brown glass. Bottles
shall be 200ml or higher volume and sealed to prevent leakage. DO NOT use plastic bottles at any time. A label
containing the following information should be affixed to the sample bottle for traceability:
1.
Location from which the sample was taken
2.
The date and time (start and finish times) the sample was taken
3.
Site and/or facility name
4.
Name of the person taking the sample

NOTE: If the produced water sample is to be transported to a different location from the sampling point,
ensure the sample is stored in a light tight container and clearly labeled.
A2.2 SAMPLE MEASUREMENT

Sample measurement is simple and easy to perform with no need for solvent preparation. Follow these simple steps to
determine the content of oil in water using the HD-1000:
1.
Rinse the entire probe ferrule in a beaker of clean water and dry with an optical tissue. Do not detach the
probe from the analyzer unit.
2.
Ensure the produced calibration curve is loaded prior to measurement (*see Section 3.2.4 Oil Calibration).
3.
Press the Quick Measurement button from the main menu to open the measurement menu.
4.
Mix the sample well in the glass bottle then add to the supplied calibration chamber until it is - full.
5.
Press the
6.
Check the displayed ppm reading. This result is the concentration of oil in the sample as determined from
calibration curve for that oil type.
button to measure the unknown sample concentration.
NOTE: If the oil has an API gravity greater than 31, has stratified and/or hard to achieve a good mix
through manual mixing, the addition of surfactant (Advanced Sensors recommend Loctite
7840 / Loctite Natural Blue Cleaner) may be required. When adding surfactant follow the
recommended volumes per PPM as indicated in the calibration procedure.
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APPENDIX 3 ADDITIONAL CONNECTIVITY F EATURES

A3.1 CONNECTING TO WI-FI
The HD-1000 is equipped with Wi-Fi allowing users to up or down load oil type files. Oil type files can be shared
between HD-1000 units, stored and/or shared worldwide. Enabling Wi-Fi on the HD-1000 can be performed as follows.
Turning Wi-Fi On and Off:
1.
Navigate to the Home Screen (Figure 10) by pressing the home screen button (2) in Figure 9.
2.
Locate the Status Bar at the top of the Home Screen, as shown in Figure 48 A.
3.
Press along the Status Bar until the display changes to the drop down option as shown in Figure 48 B.
4.
Drag downward to open the Notifications Panel as shown in Figure 48 C.
A. Locate Status Bar.
B. Press and drag down to open.
C. Open Notifications Panel.
Figure 48: Accessing the Status Bar notifications panel to access Wi-Fi and Bluetooth settings.
5.
To turn ON the Wi-Fi, press the Wi-Fi button once and it will change to green, as shown below.
To turn OFF the Wi-Fi press the Wi-Fi button again and it will return to grey.
6.
Alternatively Wi-Fi can be switched on or off under the Settings options, Figure 16, by selecting the switch as
shown below:
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Joining a Wi-Fi Network

1.
2.
Select the Settings icon from the Home Screen.
3.
From the Wireless and networks list select the Wi-Fi menu, Figure 49, to display the list of available
networks, Figure 50 below.
4.
Select a network from the list of detected networks, Figure 50. If required enter the network password and
select the Connect button as shown in Figure 51.
Figure 49: Settings options.
Figure 50: List of available Wi-Fi

networks.
Figure 51: Password entry.
Note: Networks that require a password will appear with a lock icon.
5.
Once the device is connected to a Wi-Fi network a connection message will appear at the bottom of the screen
to confirm, as shown in the example below:
6.
Additionally once connected to a specified Wi-Fi network the device will automatically connect to it any time it
is available.
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A3.2 B LUETOOTH
The HD-1000 is Bluetooth enabled to transmit data wirelessly over short distances to another paired device.
To send
files using Bluetooth ensure the feature is activated on both devices (the HD-1000 & the other device) prior to pairing.
Activating Bluetooth on the HD-1000
Bluetooth can be activated from the Notifications Panel or from the Settings options.
1.
2.
Locate the Status Bar at the top of the Home Screen, as shown in Figure 48 A, and open the Notifications
Panel as shown in Figure 48 C.
3.
To activate Bluetooth, press the Bluetooth button once and it will change to green, as shown below.
To de-activate Bluetooth press the Bluetooth button again and it will return to grey.
4.
Alternatively Bluetooth can be switched on or off under the Settings options, Figure 16, by selecting the switch
as shown below:
5.
Once switched on the Bluetooth device options screen will open to select device visibility and display all
available devices, as shown in Figure 52.
Figure 52: Bluetooth device visibility screen.

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Pairing Additional Devices

Additional devices are paired from the device visibility screen as follows:
1.
Tick the Not visible to other Bluetooth devices box to enable the HD-1000s visibility, Figure 53 .
2.
Press the Scan button. The HD-1000 will scan and display available Bluetooth devices on screen.
Figure 53: Bluetooth device visibility screen.
3.
Figure 54: Available devices for pairing.
Select the device to pair with, Figure 54, and accept the Bluetooth pairing request passkey on both devices to
confirm. The Bluetooth pairing request will appear on the HD-1000 as shown below in the example:
4.
Once accepted the devices are paired and then listed in the Bluetooth device options screen, Figure 55.
Figure 55: Bluetooth device options screen showing paired and available devices.
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Sending and Receiving Data via Bluetooth

The HD-1000 is equipped with Bluetooth capability to support data transfer between other Bluetooth compatible
devices, such as additional HD-1000 units. Share, or transfer, files using the Bluetooth function as follows:
1.
Ensure the Bluetooth feature is activated; see Section Activating Bluetooth for more information.
2.
Open the Saved Data
3.
Select the required measurement to open the data file.
4.
From the icons along the top of the screen press Export
menu to view the list of stored data on the unit.
. A list of export options will open as shown in
Figure 56 below:
Figure 56: File export format options.
5.
Select the required format for export and from the open options list, Figure 57, select Bluetooth as shown
followed by either Always or Just Once to complete the action:
Figure 57: Export by Bluetooth selection.
Selecting Always will export data by Bluetooth each time data is exported. Selecting Just Once will export
only the current data by Bluetooth and users will have to select Bluetooth for subsequent exports.
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INFORMATION: If Bluetooth has not been activated the following message will open to prompt users
to activate Bluetooth. Selecting OK will open up the Bluetooth menu on the unit so
the user can activate the feature. Selecting Cancel will return users back to the
data screen.
6.
Once Bluetooth has been accepted for export, the list of available devices will open as shown in Figure 58.
Select the required device from the list and ensure the devices are paired (see Appendix 3.2 Bluetooth).
Figure 58: Options for Bluetooth export transfer; listing available devices paired and unpaired.
7.
The transfer will start automatically. Note the file transfer may need to be accepted on the other paired device.
8.
The transferred file is saved in the Bluetooth folder.
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A3.3 PRODUCT REGISTRATION ONLINE

Product registration is optional, however it is recommended, as it enables software updates and provides access to
online calibration files. Note that to register the HD-1000 unit access to a wireless internet connection is required.
Registration can only be completed once per device.
To un-register a device contact your Advanced Sensors
representative.
Register the unit as follows:
1.
Ensure the Wi-Fi is connected (Appendix 3.1 Connecting to Wi-Fi )
2.
From the Main Menu select Oil Calibration
3.
In the Oil Calibration menu select the Download
4.
The Product Registration screen, Figure 59 below, will open.
5.
Users should enter the Company name and location 2 (country of use).
6.
Select the Register button to complete the registration.
icon.
Figure 59: Product registration screen with on screen key board for information entry.
7.
Once the device is registered users can upload, download or export files between devices and/or the secured
server.
For units used in multiple locations enter only the primary location or country of use.
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A3.4 UPDATING THE S OFTWARE

The HD-1000 software will automatically update at regular intervals. Periodically, however the HD-1000 software will
require a manual update. Update the unit as follows:
1.
Ensure the Wi-Fi is enabled.
2.
From the Main Menu press the Option key on the bottom left (see Figure 13).
3.
Select the Check for Update option as shown in Figure 60 below.
Figure 60: Check for update from the options menu.
4.
If a new update is available it will begin to download automatically and the following message will open:
Figure 61: Confirmation of automatic software update.
5.
Once the download is complete the user is required to confirm the replacement of the existing application.
Select OK to proceed with the installation.
Figure 62: Confirm replacement of the current application with the update.
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6.
Once the replacement is confirmed the following screen will open, Figure 63, then select Install to complete
the installation.
Figure 63: Install confirmation screen.
7.
The final step in the updating process is to Grant the Superuser request as shown below in Figure 64:
Figure 64: Superuser request prompt. Select Grant to complete installation.
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APPENDIX 4 TECHNICAL SPECIFICATIONS

Measurement Performance
Measurement principle
Laser Induced Fluorescence (LIF)
Range
0-3,000ppm
Accuracy
2% of measurement range
Response time
<1 second, continuous results
Operating conditions
Process temperature
Operational ambient temperature
0C to 100C
0C to +50C
Spectral Analysis Specification

Emission wavelength range
Resolution
400-1,100nm
0.5nm
Utilities
Power
Rechargeable battery (3,000 mAh)

5Vdc (Charging device required: input 100-240VAC, Output 2A)
Material
Enclosure material
Aluminium
Weight and Dimensions

Weight
Dimensions
Flexible probe length
0.8kg
85W x 152D x 52H mm
1.2m (additional length optional)
Communications
Wireless (Wi-Fi)
Bluetooth
Internal data storage
Security
Standard
Standard
9GB (expandable to 41GB)
Password protection
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APPENDIX 5 DECLARATION OF CONFORMITY

DECLARATION OF CONFORMITY
We, the manufacturer declare under our sole responsibility that the product; Portable Handheld Oil-in-Water Analyzer
Model HD-1000, to which this document relates, are in conformity with the following:
DIRECTIVES:
Low Voltage Directive 72/23/EEC

EMC Directive 89/336EEC and 92/31/EEC
STANDARDS:
EN 55011: 2009 + A1: 2010: Radio-Frequency Disturbance Characteristics

EN 60825-1 (2007): Safety of laser products-Part 1: Equipment classification and requirements.
EN 61010-1: 2010 Electrical Safety Requirements
EN 61326-1: 2006 Electrical Equipment for Measurement, Control & Laboratory use
EN 61000-4-2: 2009 Electromagnetic (EMC)
EN 61000-4-3: 2006+A1:2007+A2:2010 Radiated / Immunity tests
EN 61000-4-8: 2010 Power Frequency Magnetic Immunity
ADDITIONAL NORTH AMERICAN STANDARDS:
21 CFR 1040.10 & 1040.11: Performance standards for light-emitting products.
The associated mains to 5V charger provided with the HD-1000, as declared by the manufacturer XP Power LLC, has
been manufactured in conformity with the following (additional safety information available upon request):
EN55022, class B: Information Technology Equipment: Radiated Immunity

EN61000-3-2: Conducted Immunity
EN61000-3-3: Magnetic Field
EN61000-4-2: Electromagnetic (EMC)
EN61000-4-3: Radiated / Immunity tests
EN61000-4-4: Transient/Burst Immunity tests
EN61000-4-5: Surge Immunity Tests
EN61000-4-6: Conducted Disturbances Immunity
EN61000-4-8: Power Frequency Magnetic Immunity
EN61000-4-11: Voltage Dips, Variations, Interruptions Immunity.
We hereby declare that the above named products are in conformity to the declared directives and standards. The
technical documentation is kept at the address below and is available for inspection.
R. Acheson, Quality Manager.
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APPENDIX 6 PRODUCT UPDATES (INSERT ANY UPDATES IN THIS SECTION)

SOFTWARE RELEASE NOTE
HD-1000 SOFTWARE UPDATE REVISION 1.3.3
The HD-1000 portable oil in water analyzer software will be upgraded to Version 1.3.3. This new
version of software will address a number of issues aimed at overall product improvement of the
user interface and system.
The following improvements affecting the User Interface include:
1. PPM value displays:
a.
b.
c.
d.
to one decimal place for values above 100 PPM

to two decimal places for values above 10 PPM
to two decimal places for values above 1PPM
to three decimal places for values below 1 PPM
2. Calculated PPM estimation is now displayed on the measurement

screen when the maximum set PPM threshold is exceeded. This value
is indicative of the measured PPM when it exceeds the threshold value.
3. New Integration Time features which make the unit more sensitive in applications with low
fluorescence signal:
a. Configuration of the Integration Time is now an option
during Calibration.
b. Integration time is configurable up to 5000 ms and
recorded in the oil type file for traceability and reference.
4. New Calibration features:
a. Default Calibration File is now the last selected oil type file from the options menu.
b. Users can select to take 3, 5 or 10 replicates of a given PPM standard then the
average value used. The number of replicates taken is recorded in the oil type file
for traceability and reference.
c. Calibration points can be re-measured or removed if the data point is significantly
out of line with the expected value. This applies only to mid-point calibration
samples; high and low endpoints are fixed.
d. Calibration Data Points record includes fields which display values for both
Integrated Fluorescence and Fluorescence Peak Points.
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3.1.2 Basic Unit Functions .................................................................................................................................................................... 14

3.2 M AIN S OFTWARE M ENU ........................................................................................................................................................ 16

3.2.4 Oil Calibration............................................................................................................................................................................... 25

8 Meadowbank Road, Carrickfergus, BT38 8YF, Northern Ireland

APPENDIX 1 CALIBRATION PROCEDURE: MANUAL MIXING ............................................................................................... 37

8 Meadowbank Road, Carrickfergus, BT38 8YF, Northern Ireland

First Draft for review

28th January 2014

Addition of laser safety label and update of laser safety

13th August 2014

Addition of calibration and sampling procedures.

21st November 2014

Final approval for release.

28th November 2014

SYMBOLS USED IN THIS MANUAL

symbol is used throughout this document to highlight important information.

The definitions of each term used where it is found are as follows:

Further reference for more detailed information or technical details.

Clarification of an instruction or additional information.

An instruction that draws attention to the risk of injury or death.

8 Meadowbank Road, Carrickfergus, BT38 8YF, Northern Ireland

Dependent upon application.

8 Meadowbank Road, Carrickfergus, BT38 8YF, Northern Ireland

1.2 GENERAL HEALTH & S AFETY

The equipment is designed for use in SAFE AREAS ONLY.

All warning labels on the equipment and packaging shall be observed.

1.3 ELECTRICAL S AFETY

1.4 MECHANICAL S AFETY

An assembled system weighs approximately 1 kg (including the detachable probe).

8 Meadowbank Road, Carrickfergus, BT38 8YF, Northern Ireland

1.5 OPTICAL S AFETY

CAUTION: USE OF CONTROLS OR ADJUSTMENTS OR PERFORMANCE OF PROCEDURES OTHER THAN THOSE

8 Meadowbank Road, Carrickfergus, BT38 8YF, Northern Ireland

SECTION 2 UNIT OVERVIEW

Figure 1: The HD-1000 portable analyser with sampling vessel.

8 Meadowbank Road, Carrickfergus, BT38 8YF, Northern Ireland

Figure 2: Right side of analyzer unit with: 1. Power On

Figure 3: Left side of analyzer unit 4. Power supply outlet.

8 Meadowbank Road, Carrickfergus, BT38 8YF, Northern Ireland

CAUTION: Do not exceed the probe bend radius of 16cm.

8 Meadowbank Road, Carrickfergus, BT38 8YF, Northern Ireland

Exceeding this radius will result in damage to

2.2 OVERVIEW OF MEASUREMENT PRINCIPLE

8 Meadowbank Road, Carrickfergus, BT38 8YF, Northern Ireland

SECTION 3 OVERVIEW OF SOFTWARE OPERATION

3.1.1 Starting the HD-1000

Figure 7: Lock screen of the HD-1000

8 Meadowbank Road, Carrickfergus, BT38 8YF, Northern Ireland

Figure 8: Analyser Main Menu

Figure 9: Front Main Menu display on the analyzer.

Figure 10: Home screen display with the Launch Analyser

3.1.1.1 Charging the Unit

8 Meadowbank Road, Carrickfergus, BT38 8YF, Northern Ireland

Figure 12: Charging Mode Main Menu Options.

8 Meadowbank Road, Carrickfergus, BT38 8YF, Northern Ireland

3.1.2 Basic Unit Functions

3.1.2.1 Screen Navigation

returning users to the previous menu screen.

8 Meadowbank Road, Carrickfergus, BT38 8YF, Northern Ireland

3.1.2.2 On Screen Keyboard

button to return to the previous screen.

Figure 14: Alphabetic on screen keyboard.