Beruflich Dokumente
Kultur Dokumente
4
Paper ID GTJ14093
Available online at: www.astm.org
ABSTRACT: To better characterize a bulk soil electrically, both the electrical conductivity and dielectric permittivity should be measured. This
study developed a time domain reflectometry TDR penetrometer to allow simultaneous measurements of dielectric permittivity and electrical
conductivity during cone penetration. A TDR penetrometer is formed by placing a multiple-conductor waveguide around a nonconducting shaft.
Probe design considerations and calibration methods for measuring dielectric constant were first theoretically discussed and then evaluated through
laboratory investigations. A prototype TDR penetrometer was fabricated and used to perform simulated penetration tests in a calibration chamber.
The effect of penetration disturbance on dielectric constant is quantitatively reported and explained. The implications of the data that can be measured by the TDR penetrometer are also discussed.
KEYWORDS: dielectric permittivity, electrical conductivity, time domain reflectometry TDR, CPT
Introduction
The soil physical properties, such as water content, void ratio, and
physical chemistry of pore water, are of great interest in geoenvironmental and hydrogeological problems. Furthermore, soil-water
interaction and soil microstructure are important to the renewed
focus on the fundamentals of soil behavior. These physical properties of soils are usually investigated using laboratory techniques on
samples retrieved from a borehole. Hence, questions arise as to how
representative laboratory samples are of the actual field conditions.
In particular, it is relatively difficult to obtain undisturbed samples
in sand deposits. It is also costly and time consuming to obtain soil
physical properties using traditional drilling and laboratory techniques. Conventional in situ testing methods, be it standard penetration test SPT, cone penetration test CPT, or dilatometer test
DMT, focuses on the mechanical response of the soil under test.
Electrical methods are more feasible for characterizing soil physical parameters in situ, since electrical properties are related to the
soil composition and less affected by the stress state.
Electrical properties of a bulk soil include its electrical conductivity and frequency-dependent dielectric permittivity. Much laboratory and theoretical work has been done on the relation between
soil electrical and physical parameters Santamarina et al. 2001.
These results encourage further development of field measurement
techniques and more effective homogenization models for electrical properties of porous media. While laboratory and theoretical
development continues to advance, electrical characterization in
situ lags behind. Campanella and Weemees 1990 developed an
electrical resistivity module in CPT using the four-electrode array
under low frequency excitation. Several similar modules are now
commercially available. However, interpretation of the resistivity
alone for soil properties is difficult because it is sensitive to many
Manuscript received March 10, 2005; accepted for publication March 30,
2006; published online May 2006.
1
Associate Professor and Graduate Students, respectively, of Civil Engineering, National Chiao Tung University, Hsinchu, Taiwan, e-mail:
cplin@mail.nctu.edu.tw
factors, such as water content, soil type, and groundwater characteristics. CPT dielectric modules have been reported more recently
for soil moisture measurements based on resonant frequency
modulation or time domain reflectometry Knowlton et al. 1995;
Singh et al. 1997; Young et al. 1999; Vaz and Hopmans 2001. On
the contrary, these probes measure only the dielectric constant in a
certain frequency range. To better characterize the soil electrically,
both the resistivity reciprocal of electrical conductivity and dielectric permittivity in a wide band are desired. The spatial sensitivity and penetration effect of both resistivity and dielectric penetrometer should also be studied.
Time domain reflectometry TDR is a geophysical method
based on electromagnetic waves. It can be used to make simultaneous measurements of electrical conductivity, apparent dielectric
constant, and dielectric spectrum of a soil Topp et al. 1980; Dalton
et al. 1984; Heimovaara 1994. Much work has been published in
soil science regarding the measurements of soil water content and
salinity using apparent dielectric constant and electrical conductivity. More recently, Hilhorst 1998 showed that dielectric spectrum
in a wide band can provide extra information related to characteristics of soil-water interaction. Lin 2003a reported a field technique for soil dielectric spectroscopy using TDR. However, current
TDR probes can only apply to soils near ground surface.
A four-phase research project is undertaken at National Chiao
Tung University in Taiwan to develop an efficient field method for
estimating various physical properties of soils using time domain
reflectometry. The four phases are 1 development of field probes
suitable for TDR measurements of soils at various depths, 2 construction of homogenization models for soil electrical properties as
functions of soil compositions, 3 development of dielectric spectroscopy of soils using the new field probe, and 4 development of
theoretical or semi-empirical relationships to extract soil physical
properties from electrical properties. In phase one, a TDR probe
was developed to be used in conjunction with the cone penetration
test CPT or deployed as a permanent sensor. The probe was specifically designed to be directly inserted into soils without the need
for digging, drilling, or other types of soil preparation. The present
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*f = f + jiif = f j f +
2f0
Since the dielectric permittivity of the insulating material depends on frequency, the propagation velocity is also a function of
frequency. The TDR waveform recorded by the sampling oscilloscope is a result of multiple reflections and dispersion. A typical
TDR output waveform is shown in Fig. 1. The experimental timedomain information may be treated in the frequency domain to obtain the dielectric permittivity as a function of frequency Heimovaara 1994; Lin 2003a. This involves deriving the system
function as a function of the impedance, propagation constant, and
boundary conditions and it has different forms depending on the
configuration of the probe. In this study, the TDR penetrometer was
developed in the context of apparent dielectric constant and electrical conductivity.
The propagation velocity of an electromagnetic wave that
travels in a material with equivalent dielectric permittivity * is a
function of frequency since the dielectric permittivity depends on
frequency. It can be written as Ramo et al. 1994
f =
f
1+
2
iif
1+
f
where c is the speed of light. The denominator in Eq 2 can be considered as the apparent dielectric permittivity of each frequency
component. Topp et al. 1980 ignored the dielectric relaxation and
loss and assumed the denominator to be a constant. Accordingly,
the denominator in Eq 2 was replaced by the apparent dielectric
constant Ka and the corresponding propagation velocity was
called apparent velocity a. a is determined from the time difference T between the arrivals of the two reflections as shown in
Fig. 1 and the round-trip length of the probe 2L in the soil.
Hence, Ka can be determined from the travel time analysis as
Ka =
c cT
=
a 2L
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or spacing. The PVC tubes were used as the shaft and copper
strips as the waveguide conductors. The configurations of the trial
probes are summarized in Table 1. A later section will present the
performance of these probes through laboratory investigations.
Probe Design
Standard waveguides or probes for TDR measurements are primarily of two types: coaxial type and multi-conductor type, as shown
in Figs. 2a and 2b. The coaxial type of probe is composed of a
cylinder acting as the outer conductor and a rod along the centerline
of the cylinder acting as a central conductor. The multi-conductor
type of probe is composed of one or more rods acting as the outer
conductors and a center rod as the inner conductor. The coaxial
type of probe is adopted for laboratory measurements such as in the
compaction mold or in a Shelby tube, using the cylinder as the outer
conductor with the inner conductor being a steel rod inserted along
the centerline of the soil in the mold. The multi-conductor probes
can be used for in-place measurements Siddiqui et al. 2000. Conventional multi-conductor probes are around 30 cm long and only
applicable to top soils. In order to adapt the TDR technique to a
cone penetrometer application, a new design is required for the
probe. The multiple conductors are placed around a nonconducting
shaft to form a TDR probe as shown in Fig. 2c.
Also shown in Fig. 2 are the electrical potential distributions
corresponding to the cross sections of different probe types. The
electrical field is contained in the cylinder for a coaxial probe while
it is open in a multi-conductor probe. Placing multiple conductors
around a nonconducting shaft allows the waveguide to sense the
material around the shaft. It should be noted that the material inside
the shaft of the TDR cone penetrometer is different from the surrounding material to be measured by the probe design. Therefore, a
new calibration procedure is required for measurements of the apparent dielectric constant and electrical conductivity using the TDR
penetrometer. Previous studies on two-conductor probes have
shown that the unequal spatial weighting in the plane transverse to
the probe is inherent in the TDR measurement and cannot be eliminated Baker and Lascano 1989; Knight 1992. Hence, the probe
should be designed to minimize the effect of the material inside the
shaft and maximize the influence zone in the surrounding medium.
A series of trial probes were constructed in the laboratory to determine the optimal configuration for the waveguide. The variables
considered included the number of conductors and conductor width
Ka,soil =
Ka,eff b
a
n
1/n
cT
2L
2n
1/n
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pulse down the cable and some of the wave energy is reflected from
both the beginning and end of the probe as shown in Fig. 3 and 4.
The first positive reflection is due to the impedance change at the
connector between the cable and the probe. The sudden drop of the
waveform resulting from the negative reflection occurs when the
pulse enters the probe section. The second positive reflection occurs at the end of the probe. From a practical perspective, the data
shown in Fig. 3 and Fig. 4 suggests any of the five-probe configurations can be used in the aspect of identifying reflection points.
However, as the number of conductors and conductor width increases, the impedance of the probe decreases and the negative reflection at the beginning of the probe increases, causing the waveform to drop down to a lower level. Hence, the reflection points in
probe T1 are the clearest. This becomes more obvious especially
when the dielectric constant of the surrounding medium decreases
e.g., soils with low water contents.
The travel time per unit length of the penetrometer probe is
about 70 % of that of the coaxial probe. All penetrometer probes
perform similarly in this aspect. The dielectric constant of the tap
water Ka,water should be about 80 if measured by a conventional
TDR probe. Due to the interference of the insulator in between the
conductors, the effective dielectric constants of the tap water
Ka,eff measured by the penetrometer probes listed in Table 1 are all
near 41. The theoretical value of n in Eq 4 is n = 1 for the TDR
penetrometer. The insulator in between the conductors is comprised
of a PVC tube and air inside the tube. The dielectric constant of the
insulator Ka,probe is about 2. The a value in Eq 5 can be set at a
= 1 / 2 i.e., Ka,eff of water= Ka,water + Ka,probe / 2, Therefore, Eq 5
can be simplified as
Ka,eff
Ka,soil + Ka,probe
2
for all probe configurations. Regardless of the waveguide configuration, the material inside the probe weights the same as the material surrounding the probe in Ka measurements.
Sensitivity of Ka Measurements
The material surrounding the TDR penetrometer contributes 50 %
to the effective dielectric constant and electrical conductivity. This
percentage cannot be increased by changing the conductor configuration. Placing multiple conductors around a nonconducting shaft
allows the waveguide to sense the material around the shaft at
depths, but decreases the sensitivity of dielectric and conductivity
measurements. It is therefore necessary to investigate the amount
of loss in sensitivity for dielectric measurements using the TDR
penetrometer.
The measurement sensitivity is defined here as the derivative of
the TDR response i.e., the T with respect to the dielectric constant
of the material under test. The sensitivity of the dielectric measurement using the conventional probe and the TDR penetrometer can
be derived from Eq 3 and Eq 6 as
SKa =
dT
L
=
dKa,soil c Ka,soil
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SKa =
dT
=
dKa,soil
2c
L
Ka,soil + Ka,probe
2
8
Assuming Ka,probe = 2 and L = 30 cm, the sensitivity of the dielectric
measurement is shown as a function of the dielectric constant of the
material under test in Fig. 5a. The measurement sensitivity decreases with increasing dielectric constant. The relative sensitivity
sensitivity of the TDR penetrometer relative to the conventional
probe as a function of the dielectric constant is shown in Fig. 5b.
The sensitivity of the TDR penetrometer is about 70 % of the coaxial or conventional multi-conductor probes. This reduction in
sensitivity should be acceptable in practice. The measurement sensitivity may be increased by increasing the probe length, as suggested by Eqs 7 and 8, but increasing probe length may decrease the
spatial resolution.
Ka,r
100 %
Ka,eff
where Ka,r is the effective dielectric constant measured in a waterfilled PVC tube with inner diameter r and Ka,eff is the effective dielectric constant measured in a large water-filled tank. Ka,eff is rep-
resentative of the effective dielectric constant measured in a waterfilled PVC tube with inner diameter r = .
The Ka spatial weighting functions for different probe configurations are also shown in Fig. 6. The effective dielectric constant
approaches an asymptotic value at a distance of 100 mm and
greater. The majority of the electromagnetic response occurs within
the first several centimetres in the radial direction. The fourconductor probe T1 and three-conductor probe T2 have similar
spatial weighting functions; and the spatial weighting appears to be
insensitive to the conductor width for the two-conductor configuration see T3, T4, and T5. In Ka measurements, the radial sampling of the four-conductor probe T1 and three-conductor probe
T2 is more focused on the vicinity of the probe than that of the
two-conductor probes T3, T4, and T5.
Observations from Fig. 6 raise the concern for the penetration
disturbance effect on Ka in soil measurements. The soil displaced
by the penetrometer may change the density of the soil adjacent to
the penetrometer, and hence the dielectric constant.
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function for electrical conductivity appeared extremely biased towards the probe Lin et al. this issue and the penetration may induce significant disturbance.
Figure 7 shows the design and a photo of the probe. The diameter of the prototype is the same as a standard CPT module
35 mm and the sensing waveguide is 20-cm long. The probe consists of four arc-shape stainless steel plates and a Delrin shaft. The
thickness of the stainless steel was maximized to increase the axial
strength of the probe. The stainless steel plates were fit into four
grooves in the Delrin shaft and fastened with screws. This probe
was used to perform simulated penetration tests in a calibration
chamber.
FIG. 8Dielectric constant measured by TDR penetrometer compared to actual dielectric constant in calibration tests.
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the apparent dielectric constant, increases. Therefore, the penetration effect is more pronounced for the soil with lower Ka, as Fig. 10
shows. In summary, the penetration effect induces a coherent Ka
error which increases with decreasing soil density. For the soils
tested dry density ranging from 1.58 to 1.67 g / cm3, this error is
within the uncertainty associated with the Ka- correlation. But
caution should be taken when performing tests in looser soils. The
simulated tests demonstrate the effectiveness and limitations of the
prototype TDR penetrometer. The penetration effect on electrical
conductivity measurement will be examined in the companion
paper Lin et al. this issue and further refinement of the TDR penetrometer will be suggested accordingly.
lationship was shown by Topp et al. 1980 to be relatively independent of soil type and electrical conductivity of pore water. Time
domain reflectometry can integrate all electrical measurements.
The apparent dielectric constant alone can be used for estimating
volumetric water content or void ratio when the soil is saturated.
Future study on electrical conductivity and dielectric dispersion
can provide extra information for characterization of soil type and
pore water.
In addition to measurements using the TDR penetrometer, TDR
measurements were also performed using a 4-rod MRP probe
measurements which were much less disturbed. Figure 10 shows
the comparison for Ka measurements. The effect of penetration can
be noticed in Ka measurements as expected. Ka increases as soil
density increases due to penetration because the volumetric water
content increases with density when gravimetric water content remained unchanged. This increase in apparent dielectric constant
depends on the degree and extent of the soil densification. As the
original soil density increases, the densification due to penetration
is less significant but the disturbed zone becomes larger. Therefore,
the Ka measurement is less affected by the penetration effect for
dense soil than for loose soil. This can explain the effect of penetration shown in Fig. 10. The soil samples prepared for the simulated
penetration tests were compacted at dry side of optimum. At dry
side, the density increases as gravimetric water content, and hence
Conclusions
The objective of this study is to develop a TDR penetrometer for
simultaneously measuring dielectric constant Ka and electrical
conductivity during cone penetration. The present paper discusses the probe development in the context of dielectric measurement. A TDR penetrometer can be formed by placing a multipleconductor waveguide around a nonconducting shaft. The
theoretical relationship between the dielectric constant of the surrounding material and the TDR responses travel time T may be
formulated by the Birchaks exponential mixing model. The calibration parameters involved in the theoretical relationship can be
easily determined by calibration tests with several liquids of known
Ka. A TDR penetrometer allows the waveguide to sense the surrounding soils at depths, but the sensitivity of Ka is decreased by
about 30 % compared with the conventional TDR probes. Changing the conductor configuration seems unable to improve the measurement sensitivity but could change the characteristic impedance
and radial sampling characteristics. The majority of the electromagnetic response occurs within the first several centimetres measured from the probe surface. Experimental results indicate that the
penetration disturbance induces a coherent Ka error which increases with decreasing soil density. Future refinement and applications will be based on the results obtained in this study and a
companion paper discussing the electrical conductivity measurement using the TDR penetrometer.
Acknowledgments
The research was partially sponsored by the National Science
Council of ROC under contract numbers 89-2218-009-100 and 902611-E-009-004.
References
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