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Contents
1. Introduction ................................................................................................................. 3
1.1 microPHAZIR Overview ............................................................................................ 4
1.2 Specifications ............................................................................................................ 5
2. Safety ........................................................................................................................... 6
2.1 General Safety Instructions ..................................................................................... 6
2.2 Unsafe operation ....................................................................................................... 7
3. Operation ..................................................................................................................... 8
3.1 Unpacking .................................................................................................................. 8
3.2 microPHAZIRTM Controls ......................................................................................... 9
3.3 Software operation.................................................................................................. 12
3.4 Standby Mode.......................................................................................................... 14
3.5 Downloading data from the microPHAZIRTM ........................................................ 15
4. microPHAZIRTM Configuration Options................................................................... 17
4.1 Application Select ................................................................................................... 18
4.2 PQ (Performance Qualification) ............................................................................. 20
4.3 Take Background .................................................................................................... 20
4.5 Set Group ID ............................................................................................................ 21
4.7 Logout ...................................................................................................................... 25
4.8 Reset Measurement # ............................................................................................. 25
4.9 Version ..................................................................................................................... 26
4.10 Background scans ................................................................................................ 26
4.11 Sample scans ........................................................................................................ 26
4.12 Set date & time ...................................................................................................... 26
4.13 Get Diagnostics Files............................................................................................ 27
4.14 Delete All Data Files .............................................................................................. 28
4.15 Delete App. Data File ............................................................................................ 28
4.16 Turn Speaker ON or OFF ...................................................................................... 28
4.17 Voltages ................................................................................................................. 28
4.18 Set/Unset Euro CSV .............................................................................................. 28
5. Maintenance .............................................................................................................. 29
5.1 The microPHAZIRTM Battery Charger .................................................................... 29
5.2 microPHAZIRTM Batteries and Battery Charging .................................................. 30
5.3 Changing the Bulb .................................................................................................. 31
5.4 Cleaning the Instrument ......................................................................................... 34
6. Fault Diagnosis and Troubleshooting..................................................................... 34
7. Spare Parts and Service ........................................................................................... 35
8. Warranty..................................................................................................................... 36
Appendix A: Usage Guide ............................................................................................ 38
A1 First time operation ................................................................................................ 38
A2 Notes on measurement .......................................................................................... 38
A3 microPHAZIRTM Quick Start .................................................................................. 38
A3.1 Hardware Overview ........................................................................................ 39
A3.2 Collect Mode................................................................................................... 39
A3.3 Downloading Data .......................................................................................... 40
A3.4 Other Applications .......................................................................................... 40
Appendix B: Vial and Cuvette Adaptor Usage ........................................................... 41
Appendix C: Barcode Reader Option .......................................................................... 45
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1. Introduction
The microPHAZIRTM is an integrated handheld spectral analyzer that includes a near
infrared spectrometer, light source, probe, computer, color LCD display and batteries. It
is designed to analyze diffuse reflection measurements from solids, powders or other
reflective materials in a wide range of applications. An accessory for transmission
measurements of materials such as liquids is available as well.
The instrument uses a scripting language to define applications that can be operated by
users with minimal training and little or no spectroscopy experience. Separate scripts
are written for each application, enabling a single device to function successfully for
many applications in many fields.
This manual provides detailed operating instructions and information on the operation
and care of the microPHAZIRTM.
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Sampling area
Reflectance probe
Lanyard
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1.2 Specifications
microPHAZIRTM Handheld NIR Analyzer
Spectral Range
Pixel Spacing
8nm
Optical Resolution
11nm
Stray Light
<0.01%
Measurement Interface
Diffuse reflectance
(Optional, Liquid Vial Adapter)
Contact Thermo Scientific for application specific probes
Weight
Hardware Interface
A/D Converter
24 bit
Detector
Single InGaAs
Display
Color LCD transflective 3.5 diagonal dimension; Black & white rear
LCD display
Controls
Batteries
Battery charger
110/220 AC to 8.4V DC
Recharge time
Reference method
Light source
Water Resistant:
5 to 40C.
-20 to +70C
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2. Safety
STOP
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Steam
High Humidity (moisture condensing conditions)
Extreme ambient temperatures below 5C (40F) or above 45C (110F)
Strong electromagnetic (motors or transformers) or electrostatic fields
Strong vibrations and impacts
Contact with oxidative, corrosive and caustic atmospheres such as, but not
limited to chlorine gas, hydrochloric acid, ammonia.
Contact with oxidative, corrosive and caustic liquids, such as, but not limited to
concentrated hydrogen peroxide, sulfuric acid, aqueous sodium hydroxide.
Failing to follow these instructions may result in harm to the instrument or user. If the
instrument is damaged due to exposure to any of these conditions, even occasional,
your warranty will be voided. Please contact Thermo Scientific if you require
modifications to permit the instrument to work in these harsh conditions.
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3. Operation
3.1 Unpacking
The microPHAZIRTM is shipped in a padded case that can be used for storage and
transport of the instrument.
1 microPHAZIRTM
1 USB cable
1 spare microPHAZIR rechargeable battery**
1 battery charger
1 0.050 Allen key
1 Phillips screwdriver
1 CD or printed operating manual
1 spare bulb
1 internal reference standard
**Please note: A battery comes installed in the microPHAZIR in addition to the spare
battery. Please refer to Section 5: Maintenance for replacement and charging.
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The rear LCD display indicates the operation state of microPHAZIRTM and results.
Under the USB cover is the USB port used to connect microPHAZIRTM to a WindowsTM
based computer. When connected and recognized by the computer, the words
microPHAZIR will appear on the computer as a removable storage device similar to
current digital cameras or USB memory keys:
The USB connection can be used to download scan-data from the microPHAZIRTM and
upload new or upgraded applications to the microPHAZIRTM. There are two additional
ports. The one on the right is a programming port for factory use only. The one on the
left is for future use and will enable operation of the microPHAZIR from an external
power source.
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TOP VIEW
The following items can be found on the top-side of the microPHAZIRTM.
Time
Battery indicator
Scan Number
% full scale signal
Color Display
Soft Keys
Navigation Keys
Power Switch
The Color Display is the main method of communicating analysis data to the user. The
microPHAZIRTM uses a transflective display technology for easy visibility indoors and
outdoors, accommodating a variety of work environments. At the top of the display the
current time, battery state of charge, scan number, and signal level as % full scale
indicators can be found. Other features displayed on the screen will vary depending on
the application used.
The battery indicator is green for an indication of the charge level. The indicator turns
into flashing red when the battery is nearing complete discharge (15 minutes of
operation left).
Navigation Keys: These buttons can be used to navigate up, down, left and right
between the various menu items.
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Soft Keys: The function of these buttons is displayed on the screen directly above them.
In the picture above the right soft key is labeled Config. The functions of the soft keys
can change for different screens and applications.
Power Switch: To turn the microPHAZIRTM on, press and release this button. To turn
the microPHAZIRTM off hold the button down until the screen indicates the
microPHAZIRTM is powering down. A short wait period is required while the onboard
computer initializes or shuts down properly.
In addition to the above controls there is a trigger (see microPHAZIR overview) that
initiates the measurement of a spectrum. An optional barcode reader is also available.
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This process should take approximately 30 seconds. The next screen will indicate the
light source is turned on and performing an initial calibration. The microPHAZIRTM uses a
harmless tungsten light source requiring no precautions when operating it.
If the User Login function is enabled, the user selection screen, shown above, will be
displayed. Factory default is for the User Login feature to be disabled, but it will be
enabled upon customer request.
Each microPHAZIRTM is configured with two user accounts named Admin and Guest.
These user accounts are configured with no password required as the default. User
accounts including passwords can be configured by the system administrator using the
PHAZIR Setup Utility software.
The Admin user has full access rights to all Configuration menu functions on the
microPHAZIRTM. In Section 4, all menu items are described.
To select the user, use the navigation keys to highlight the user and press the Accept
soft-key.
Once the initial calibration is complete the microPHAZIRTM is ready for operation. It is
wise to perform a PQ (Performance Qualification) test periodically or after any event,
such as dropping the instrument, which might cause misalignment. The PQ test will
verify the instrument is operating properly. This test is described in section 4.2.
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During the measurement, the user should keep the sample in contact with the
microPHAZIRTM and should not move it. The Scan progress is indicated on the main
LCD screen by a progress bar during the measurement. In addition, the rear LCD
screen says scanning and measurement complete at the end of the scan. The
number of scans may vary depending on the application in use. The rear LCD screen
will also indicate when the measurement is complete and contact with the sample is no
longer required. The result is displayed on both LCD screens.
Note: Each time a sample is measured on the microPHAZIRTM, the Scan Number
indicator located at the very top of the screen is incremented. This number is recorded
in all data files to identify the particular measurement and can be used to match data
with sample information. The number displayed AFTER the scan is complete is the
value that is recorded with the scan that was just completed.
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set for each application in the script. During Standby Mode the following screen is
displayed:
To resume operation from Standby Mode, press any button. The light warm up screen
will be displayed, followed by a new background scan.
Application scripts reside in the Applications Folder which can be accessed to add new
applications or upgrade current applications (e.g. adding additional materials to be
identified etc).
The Config and firmware folders contain information used by the microPHAZIRTM and
normally should not be accessed by users. The Config folder also contains the group ID
and Sample Info files.
Logged scan data files can be found in the top level of the drive. In the example above,
the file Collected-data-1003.csv is a data file containing measured spectra. 1003 is the
instrument serial number. Data files are saved in an ASCII comma separated value
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format (csv). The csv extension is added to the file name so that it can be opened with
Excel by simply clicking on it.
To review a data file, it is best to copy it from the microPHAZIRTM to the PC using
standard Windows methods (copy and paste, or drag and drop) and open the file with
Excel by double clicking on it. Below is a typical view from Excel:
The column headings in this file have been designed to be self-explanatory. Each
spectrum occupies a row of the spreadsheet. Starting with column F, the wavelengths
are displayed in the top row with the Log (1/R) data below. The data saved in this format
is compatible with most chemometric software packages with minimal editing.
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While this format is typical, other formats are possible. The data
file format is determined by the Application. Some Applications
save only the identification results, for example Cotton from the
fabric identification script might only be saved in the file and not
the spectral information. Other Applications may save no data at
all.
After transferring data to the PC, click on the Safely Remove Hardware icon in the task
bar. Safely Remove the microPHAZIR from the USB connection list before unplugging
the USB cable.
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To select a configuration option, navigate to the option using the directional navigation
keys and then press the Select Item soft-key.
Of the 4 applications listed here, Collect is the only standard application included on all
microPHAZIRTM units. The additional applications are commercially available from
Thermo Scientific.
Note that after selecting a new application from this menu, a new background
measurement will be performed automatically.
4.1.1 Collect
The data Collect application is for recording raw spectra without data pretreatment or
predictions. The spectral data can be later downloaded to a PC. This application is
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typically used for collecting raw data that will subsequently be used for chemometric
modeling and application development. At this point, hold the microPHAZIRTM against
the sample, press the trigger, and record the new spectra. The screen will appear as
shown below. Pressing the more button will show an expanded view of the spectrum.
Record the scan number for the resulting spectra. Once spectra of all samples are
collected, the data can be downloaded from the microPHAZIRTM into your PC. See
section 3.5 for further instructions.
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Example 1:
Example 2:
The file should be re-saved under the same name and it must be saved as a csv file
type. (Normally this file type will be saved automatically by Excel since it was the
original file type).
Group IDs are selected by using the up/down arrow keys to highlight the desired text
field. The Accept button is used to select that value. The Group ID will appear in the
Collect application on the main screen so the user can easily see the current value. As
previously mentioned, the Group ID is also saved in the data file with each spectrum. By
selecting skip the user is returned to the config menu.
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New Group IDs may also be entered manually (character-by-character) directly on the
microPHAZIR by selecting new. The first character can be selected using the up/down
arrow. Additional characters can be selected by using the right arrow key. Once editing
is complete, press the Accept soft button.
See the PHAZIR Tools User manual for more detailed information regarding Group IDs.
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The default Sample Information categories are listed below but these can be customized
as required.
Sample Information entries are automatically stored in the microPHAZIR data files along
with the spectrum, predicted results, time/date, operator etc.
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4.7 Logout
The Logout menu option logs the current user out and prompts a new user to login to the
microPHAZIRTM.
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4.9 Version
This function displays the current version of Firmware running on the microPHAZIRTM,
the serial number of the microPHAZIRTM and the FPGA version number.
Note: The microPHAZIR serial number can also be found in the battery
compartment.
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4.17 Voltages
This function displays the percentage of maximum voltage that is being supplied to the
lamp (light source). This value is determined by the application in use and may be a
fixed value or it may be automatically set by the application during calibration. In
addition this function provides a measure of the battery voltage.
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5. Maintenance
5.1 The microPHAZIRTM Battery Charger
The battery charger was developed specifically for this battery system and provides the
means for a fast and safe charging of the battery pack in the microPHAZIRTM instrument.
It is easy to use and enables the maximum use of the battery pack capacity, while at the
same time providing the highest possible protection.
STOP
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STOP
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Final Steps:
Step 5: Insert a new bulb into the socket as far as it will go. Orient the mark on the
light bulb with the arrow on the mount (as shown below) and secure it by tightening
the set screw.
Step 6: Attach the wire connector on the bulb to the plug connector on the
microPHAZIRTM.
Step 7: Attach the nose cover using the two screws.
Step 8: Power on the microPHAZIRTM to verify that the new bulb is working properly. It
is necessary to run the Cal Internal Reference function under the config menu before
anything else. Then run a PQ test and one of the applications on the microPHAZIRTM to
ensure that everything is functioning properly.
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STOP
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8. Warranty
Thermo Scientific, Inc. (Thermo Scientific or Seller) warrants that its products will be free
from defects in materials and workmanship under normal use and service in general
process conditions for the effective period set out below. This warranty and its remedies
are in lieu of all other warranties expressed or implied, oral or written, either in fact or by
operation of law, statutory or otherwise, including warranties of merchantability and fitness
for a particular purpose, which Thermo Scientific specifically disclaims. Thermo Scientific
shall have no liability for incidental or consequential damages of any kind arising out of the
sale, installation, or use of its products.
Thermo Scientifics obligation under this warranty shall not arise until Buyer notifies
Thermo Scientific of the defect. Thermo Scientifics sole responsibility under this warranty
is, at its option, to replace or repair any defective component part of the product within the
warranty period.
Except in the case of an authorized distributor or seller, authorized in writing by Seller to
extend this warranty to the distributors customers, the warranty herein applies only to
Buyer as the original purchaser from Seller and may not be assigned, sold, or otherwise
transferred to a third party.
No warranty is made with respect to used, reconstructed, refurbished, or previously owned
Products, which will be so marked on the sales order and will be sold As Is.
BUYERS SOLE AND EXCLUSIVE REMEDY UNDER THIS WARRANTY IS THAT THE
SELLER EITHER AGREES TO REPAIR OR REPLACE, AT SELLERS SOLE OPTION,
ANY PART OR PARTS OF SUCH PRODUCTS THAT UNDER PROPER AND NORMAL
CONDITIONS OF USE, PROVE(S) TO BE DEFECTIVE WITHIN THE APPLICABLE
WARRANTY PERIOD. ALTERNATELY, SELLER MAY AT ANY TIME, IN ITS SOLE
DISCRETION, ELECT TO DISCHARGE ITS WARRANTY OBLIGATION HEREUNDER
BY ACCEPTING THE RETURN OF ANY DEFECTIVE PRODUCT PURSUANT TO THE
TERMS SET FORTH HEREIN AND REFUNDING THE PURCHASE PRICE PAID BY
BUYER.
Place of Service
Seller shall use its best efforts to assist buyer to resolve all warranty related issues
through Thermo Scientific customer and technical support as soon as reasonably
practicable after notification by the Buyer of a possible defect. However, the Seller
reserves the right to require the Buyer return the Product to Sellers production facility,
transportation charges prepaid, when necessary, to provide proper warranty service.
Effective Date
The effective date of this warranty shall begin on the date of shipment/date of invoice,
whichever is later. Products are warranted to be free from defects in materials and
workmanship for parts and labor for 1 year with the exceptions indicated below:
Limitations
Products are warranted to be free from defects in materials and workmanship for parts
and labor for 1 year with the following exceptions:
Any components of the system that are in direct contact with corrosive materials
are warranted to be free from defects in materials and workmanship at time of
delivery but cannot be further warranted due to the unknown nature of the use of
the product.
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Consumable items such as lamps, cuvettes and optical filters are excluded from
this warranty. If a lamp undergoes a catastrophic failure (e.g., no light at all) within
90 days of shipment from the factory, it will be replaced at no charge.
The sole and exclusive warranty applicable to software and firmware products
provided by Seller for use with a processor internal or external to the Product will
be as follows: Seller warrants that such software and firmware will conform to
Sellers program manuals or other publicly available documentation made
available by Seller current at the time of shipment to Buyer when properly installed
on that processor, provided however that Seller does not warrant the operation of
the processor or software or firmware will be uninterrupted or error-free.
The warranty herein applies only to Products within the country of original
delivery. Products transferred outside the country of original delivery, either
by the Seller at the direction of the Buyer or by Buyers actions subsequent to
delivery, may be subject to additional charges prior to warranty repair or
replacement of such Products based on the actual location of such Products
and Sellers warranty and/or service surcharges for such location(s).
The warranty period for data processing equipment, including data storage
devices, processors, printers, terminals, communication interfaces, tape
drives, and/or all similar devices, is in all cases limited to ninety (90) days
from the date of shipment to Buyer.
Repaired products are warranted for 90 days with the above exceptions.
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A2 Notes on measurement
The microPHAZIRTM makes diffuse reflection measurements of materials that are placed
in contact with the nose of the instrument. These are usually solids or powders. The
material must be reflective enough so that the light level reaching the instrument is
above a threshold set by the application.
General Notes
The sample to be measured must be in contact with the nose of the
microPHAZIRTM to make a measurement and it must not be moved during the
measurement time.
Light must reach the material of interest to be properly measured. The
microPHAZIRTM cannot measure through thick paint, paper, or metals.
Transparent materials do not reflect much light and will be difficult to measure.
Sheets of thin transparent material can be measured by using a diffuse reflection,
reference material such as Spectralon or Flourilon behind the film.
Some dark materials, notably those filled with or covered with carbon-black, do
not reflect sufficient light for measurement.
Small pieces of material can be analyzed by carefully placing the sample on a
well lit portion of the window.
To perform a measurement
Verify that the application you wish to use, such as Data collection, is loaded.
Press the nose of the instrument against the sample to be measured and pull the trigger.
Do not hold the trigger down as this will delay the measurement. The parameters for the
measurement, such as the number of spectra/scans to average, are set by the
application loaded in the microPHAZIR.
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Time
Battery indicator
Scan Number
% full scale signal
Color Display
Soft Keys
Navigation Keys
Power Switch
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B1.
B2.
B3.
B4.
Introduction
Attaching and de-attaching adaptors
Use of the Collect Cuvette application (cuvette and liquid adaptors
only)
Making applications using Thermo Scientific MG for use with Cuvette
and Liquid Vial Adaptors
B1. Introduction:
The microPHAZIR has several available sample adaptors. The adaptors include:
-Cuvette adaptor for transmission measurements on liquid samples.
-Liquid vial adaptor for transmission measurement on small vials.
-Solids vial adaptor for measuring diffuse reflectance from powder
(typically) samples.
-Quick-disk adaptor for locating quick-disk vials and measurement of
diffuse reflectance from samples.
All of the adaptors use the same attachment method which is described in section B2.
Note that for transmission measurements (cuvette and liquid vial adaptors) the
microPHAZIR internal reference should NOT be used since that is only for diffuse
reflectance measurements. Instead, reference measurements for transmission
measurements are made on either empty adaptors or adaptors with empty cells (cuvette
or vial). In order to prevent the microPHAZIR from automatically using the internal
reference, a special Collect-Cuvette application should be used for collecting data
(section B3). When creating applications in Thermo Scientific Method Generator
software, an option is available to disable the reference shutter and is described in
section B4.
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Figure B1. Slide on adaptor until locking clips snap into place (indicated by the
blue arrows).
The adaptor is removed by squeezing the two metal release springs simultaneously as
shown in figure B2:
Figure B2. Squeeze the metal release springs as shown and the adaptor should
release and slide off of the nose. Note: Care should be taken not to over stress
the adaptor arms during removal.
B3. Use of the Collect Cuvette application (cuvette and liquid adaptors only):
The Collect Cuvette application is intended for use with the cuvette and liquid vial
adaptors and may be downloaded here:
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http://www.Thermo Scientific.com/PMG/Collect-Cuvette.zip
This application functions exactly as the normal Collect application except that it will
ask the user to manually take a reference/background measurement. At this time the
user should have the adaptor attached with an empty cell in place (cuvette or vial).
Figure B3. Request for manual background measurement when using the
Collect-Cuvette application.
B4. Making applications using Thermo Scientific MG for use with Cuvette and
Liquid Vial Adaptors:
Applications made using Thermo Scientific Method Generator (PMG) software for use
with the Cuvette or Liquid Vial adaptors should be saved with the Internal Reference
disabled. The ability to disable the internal reference is a new PMG feature present only
in PMG version 3.101 or greater:
http://www.Thermo Scientific.com/PMG/PMG-MostRecent.zip
The internal reference can be disabled from the Model Parameters screen that is
displayed when the Create Application button is pushed:
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Figure 1
The bar code reader is activated when the Set Group ID or Set Sample Information
menu items are selected in the microPHAZIR Config menu. These functions can be
accessed by pressing the Config soft key and selecting either Set Sample Info or Set
Group ID.
Note: Hold the microPHAZIR so that the barcode reader is at a right angle to barcode.
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6. When the barcode is successfully read you will see the barcode information
displayed on the microPHAZIR display. Press Accept to save the barcode data.
(see Figure 3 and Figure 4)
7. Proceed to the next operation step. Note: the bar code value will automatically
be saved with subsequent measurements.
Figure 2
Figure 3
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Figure 4
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