Amphetamine sulphate synthesis

What we are need is:5g P2NP50ml Isopropanol7,5-8,5g of Aliuminium foil (better t

o use thick foil)50ml 98% acetic acid (can also use 70%, than don t need water)50g
NaOH1ml H2SO4Firstly, you will make mix with acetic acid and water.Water we nee
d, because we areusing 98% of acetic.If will be 70%, than we will not need.Pour
(50ml GAA + 25mldH2O) in to 250ml erlenmeyer flask.
???? ?????? ????????
???? ?? ?????? ???? ???: 5G P2NP1
50ml Isopropanol7?5-8?5g ?? ???? Aliuminium (???? ??? ?? ??????? ????? ???? ????
?) 50ml 98% ???? ????? (?????? ?? ?????? 70% ??????? ????? ?? ?? ???? ?????) 50G
NaOH1ml H2SO4Firstly? ??? ?? ????? ?? ???? ????? ? water.Water ?? ???? ?????? ?
?? ?? ?? areusing 98% ?? acetic.If ????? ??? 70%? ?? ?? ???? need.Pour (GAA ????
? 50ml + 25mldH2O) ?? ???? ?? 250ml.

Prepar solution of 5g P2NP and IPA.Disolve 5g in to 50ml of warm IPA.Let to cool

.

????? ?? 5G P2NP ? IPA.Dissolve 5G ?? ?? 50ml ??? IPA.Let ?? ??? ???.

Prepar solution of 5g P2NP and IPA.Disolve 5g in to 50ml of warm IPA.Let to coo

l.While IPA solutions is cooling, need to make aliuminium amalgam.Cut the square
s1x1.Than put in to 200ml dH2O, add 50mg of Hg(no3) or other Hg salts and stir.A
fter5-10 minutes you will see grey dregs in the jar.That mean, the amalgamation
isstarted.Wait about 10 minutes more and wash aliuminium with water 3 times.Than
alldregs and Hg(no3) wash out.Becouse Hg salts are very dangerous!

??? ?? ?? prepar ?? 5G P2NP ? IPA.Disolve 5G ?? ?? 50ml ??? IPA.Let ?? ??? ?? ??

? cool.While IPA ??? ????? ???? ???? ?? ????? aliuminium amalgam.Cut squares1x1.
Than ?? ???? ???? ? ?? ??? 200ml dH2O? ????? ???? ???? ?? ??? 50mg ???? (NO3 ) ?
?? ???? ??? ??? ???? ? ????? stir.After5-10 ??? ???? ????? ??????? ?? jar.That
???? ????? ????? isstarted.Wait ???? 10 ????? ????? ? aliuminium ?? alldregs ??
3 times.Than ? Hg (NO3 WASH) ????? ??? .Becouse ???? ????? ?????? ???!

You are ready to start reaction.Add aliuminium amalgam in to acetic acid with w
atermix.Wait for about 3-5 minutes, while solution will be grey.You can stir it.

??? ????? ???? ???? reaction.Add ??????? aliuminium ?? ?? ?? ???? ????? ?? water
mix.Wait ???? ???? 3-5 ?????? ?? ???? ?? ??? ?? ????? ??? grey.You ?? ?????? ??
?? ?? ?? ?????.

Than add P2NP solution and stir a little bit.After adition in the 5-10 minutes w
ill startstormy reaction.So let the flask to stay quietly, for about 20-25 minut
es.

?? ????? ???? ????? P2NP ? ?? ????? adition bit.After ??? ?? ????? 5/10 startsto
rmy ????? reaction.So ????? ????? ?? ????? ?? ?? ? ???? ???? ???? 20-25 ?????.

In this time, all solution will boil, so need to put in the erlenmeyer flask so
mecondens
?? ??? ????? ??? ??? ?? ??? ????? ??? ???????? ???? ?? somecondens ?????? ??????
??? ????? ????

SWIM use glass funnel.It works good.

???? ?? ??????? SWIM funnel.It ??? ??? ?? ???.

After storm reaction.When the reaction is over, put the flask on the hotplate a
nd make reflux for 1hour.Atthis moment SWIM doesn t have hotplate, so he is use bo
iling water bath.You canalso don t do the reflux, but the yield will be less than
after reflu

?? ?? ????? reaction.When ????? ?? ????? ????? ???? ???? ???? ????? ?? ???? ???
? ??????? ???? 1hour.Atthis ???? ??? ?? ??? ???? ??? ?? ?????? ???????? ?? ??? b
ath.You ?? canalso ?? ??????? ??? ??????? ?? ???? ??? ?????? ???? ?? ??? ?? refl
u ????? ???

After 45 minutes, you can see that the stuff are pink

??? ?? 45 ?????? ??? ?? ?????? ?????? ?? ?????? ?????

Reflux is over.Let to cool to room temperature.You got red/yellow solution

????? over.Let ??? ???? ??? ???? ?? ???? temperature.You ???? ???? / ??? ?? ???

While the solution is cooling, we need NaOH.Add 50g NaOH in the jar and pour 50
mldH2O.The solution will be very hot.Need to cool it, so put in the freezer camb
er.When two solutions were cooled, start to pour NaOH solution.Pour in the small
amount, because all mix in the erlenmeyer flask will start to heat.So add it slo
wly andgood stir after addition.Need to do this while you will see 2 layers and
the ph will be10-12.When the NaOH is added, wait while all solution will be cool
.Need to picktopest layer, red/yellow.SWIM use syringe to pick it, because he ha
s`nt separate funnel.Extraction withdichlormethane 2x20ml.So, we collected the a
mphetamine freebase.Check the ph.

?? ???? ?? ??? ?? ??? ????? ???? ?? ???? NaOH.Add 50G ??? ?? ???? ?????? ? 50mld
H2O.The ??? ?? ????? ?? ????? hot.Need ?? ?? ???? ?? camber.When ????? ?? ??? ??
??? ?? ?? ???? ???? ????? ???? ?? ????? ????? NaOH .Pour ?? smallamount? ??? ??
??? ????? ?? ?? ???? ?? ?? heat.So ???? ????? ?? ????? ???? ?? ?? ?? ????? ?? ?
???? andgood ?? addition.Need ???? ????? ??? ??? ?? ???? ?? ??? ?? 2 ???? ?? ???
??? ? pH ?? ?? ??? be10-12.When ????? ??? ??? ? ??? ???? ?? ???? ?? ??? ??? ?? ?
???? ?? cool.Need ?? picktopest ????? ???? / yellow.SWIM ??????? ?? ???? ?? ?? ?
? ?????? ????? ??? ?? ?? funnel.Extraction ??????? withdichlormethane 2x20ml.So
has`nt? ?? ???????? freebase.Check ?? pH ??? ???? ???.

Ph is 11.Now need to convert freebase to amphetamine sulphate.This you will do w

ith sulphuracid and isopropanol.Solution H2SO4 + IPA (1ml +5ml).Drop by drop pou
r the acid solution to the freebase and stir a lot.You will see howamphetamine s
ulphate appears.Add acid solution while the ph will be (ph 7).

?? ???? ?? ??? ?? ??? ????? ???? ?? ???? NaOH.Add 50G ??? ?? ???? ?????? ? 50mld
H2O.The ??? ?? ????? ?? ????? hot.Need ?? ?? ???? ?? camber.When ????? ?? ??? ??
??? ?? ?? ???? ???? ????? ???? ?? ????? ????? NaOH .Pour ?? smallamount? ??? ??
??? ????? ?? ?? ???? ?? ?? heat.So ???? ????? ?? ????? ???? ?? ?? ?? ????? ?? ?
???? andgood ?? addition.Need ???? ????? ??? ??? ?? ???? ?? ??? ?? 2 ???? ?? ???
??? ? pH ?? ?? ??? be10-12.When ????? ??? ??? ? ??? ???? ?? ???? ?? ??? ??? ?? ?
???? ?? cool.Need ?? picktopest ????? ???? / yellow.SWIM ??????? ?? ???? ?? ?? ?
? ?????? ????? ??? ?? ?? funnel.Extraction ??????? withdichlormethane 2x20ml.So
has`nt? ?? ???????? freebase.Check ?? pH ??? ???? ???....

Than filtrate all amphetamine sulphate and let to dry in the warm place

?? ?? ????? ??? ???? ?????? ???????? ? ????? ???? ?? ??? ?? ??? ???

Drying SWIM got 3,5g amphetamine sulphate from 5g P2NP.It`s 70% yield.Good luck a
nd be safe.Operacya_Y
??? ???? ... SWIM ?????? ???????? 3?5g ?? 5G P2NP.It`s 70% ???? yield.Good ????
? safe.Operacya_Y