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Operator:
Page 1/4
22/04/2016 14:59
Laboratory:
De Benikhalled
Mm Farida Karoui
fe04016
22/04/2016 14:18
Version:
Operator:
1
Mm Farida Karoui
Lines
Line
Elem. Wavel.
[nm]
Fe
248.3
Fe248
Current
[mA]
4
Single-beam HCL
Boost
[mA]
-
Slit [nm]
0.2
Evaluation/Background correction
Line
Fe248
Background corr.
D2 background
Int.mode AZDK
Mean
off
Smooth
strong
Flame Parameters
Type:
Burner type:
Line
C2H2/air
50 mm
C2H2/air
[L/h]
65
Fe248
Ox. control:
Burner angle:
off
0 deg
Nebulizer rate:
0 mL/min
Burner height
[mm]
6
Sample Transport
Autosampler:
Dilution if conc.
exceeded:
Injection switch:
Wash:
Yes
none
Delay time:
5s
No
after sample
Wash time:
5s
std. cal.
Std. prep.:
manual
Calibration
Method:
Weighting
none
No.
Type
Pos
Rec
1
2
3
4
Cal-Zero1
Cal-Std1
Cal-Std2
Cal-Std3
1
2
3
4
Check
none
Unit
mg/L
Fe
[mg/L]
0
2
3
4
Statistics Parameters
Statistics:
Repl./sample:
Pre-runs:
ASpect LS 1.5.0.0
Mean stat.
3
0
CI calc.:
absolute
Repl./calib.sample:
3
Grubbs test:
off
conf. level:
Repl./QC:
95.4%
3
Analytik Jena
novAA 350
Operator:
Page 2/4
22/04/2016 14:59
Mm Farida Karoui
Laboratory:
De Benikhalled
QCS Parameters
No entries exist
QCC Parameters
RSD/RR% check:
ASpect LS 1.5.0.0
Calib. check:
Recal. check:
Analytik Jena
novAA 350
Operator:
Page 3/4
22/04/2016 14:59
Laboratory:
De Benikhalled
Mm Farida Karoui
Results
Results file:
Instrument:
Comment:
Line
Load method
C:\Use...\Results-16-04-22 1426.tps
novAA 350 #
Technique:
Mean
fe04016 (1)
SD
Flame
RSD[%]
Flame on
CI
Unit
Date:
Rem.
22/04/2016 14:26
Date:
22/04/2016 14:26
Autozero
fe04016(1)
SIM
Date:
22/04/2016 14:27
Fe248
Cal-Zero1
fe04016(1)
SIM
Date:
22/04/2016 14:27
Fe248
Conc.1
Abs.
0
0.00011
mg/L
0.00010
89.4
Single values (Abs.): #1: 0.00001 #2: 0.00012 #3: 0.00021 (SEV: 300V)
BG (Abs.): #1: -0.00007 #2: 0.00010 #3: -0.00013
Cal-Zero1 Fe248
0.004
Abs.
0.003
0.002
0.001
0.000
0
Time [s]
Cal-Std1
fe04016(1)
Fe248
Conc.1
Abs.
2
0.47514
SIM
Date:
22/04/2016 14:27
mg/L
0.00039
0.1
Single values (Abs.): #1: 0.47551 #2: 0.47475 #3: 0.47517 (SEV: 300V)
BG (Abs.): #1: 0.00010 #2: 0.00016 #3: -0.00010
Cal-Std1 Fe248
0.5
Abs.
0.4
0.3
0.2
0.1
0.0
0
Time [s]
Cal-Std2
fe04016(1)
Fe248
Conc.1
Abs.
3
0.71241
SIM
Date:
22/04/2016 14:27
mg/L
0.00047
0.1
Single values (Abs.): #1: 0.71278 #2: 0.71256 #3: 0.71189 (SEV: 300V)
BG (Abs.): #1: -0.00011 #2: -0.00003 #3: 0.00005
0.8
Cal-Std2 Fe248
Abs.
0.6
0.4
0.2
0.0
0
Time [s]
ASpect LS 1.5.0.0
Analytik Jena
novAA 350
Page 4/4
22/04/2016 14:59
Operator:
Laboratory:
De Benikhalled
Mm Farida Karoui
Line
Cal-Std3
Mean
fe04016(1)
Fe248
Conc.1
Abs.
4
0.95036
SD
RSD[%]
SIM
CI
Unit
Date:
Rem.
22/04/2016 14:28
mg/L
0.00022
0.0
Single values (Abs.): #1: 0.95014 #2: 0.95036 #3: 0.95057 (SEV: 300V)
BG (Abs.): #1: -0.00006 #2: 0.00008 #3: 0.00004
Cal-Std3 Fe248
1.00
Abs.
0.75
0.50
0.25
0.00
0
Time [s]
Compute calib.
Fe248
Date:
22/04/2016 14:28
Date:
22/04/2016 14:28
Fe248
R(adj.): 0.999999442 Slope: 0.23753 Abs./mg/L Char.conc.: 0.01836 mg/L/1%A
Method SD: 0.00090 y=a+bx
a=0.0000623 b=0.2375303
mg/L
Fe248
1.00
Abs.
0.75
0.50
0.25
0.00
Z
0
Sample
2
Conc. [mg/L]
fe04016(1)
Pre-DF: 1
Fe248
Conc.1
Conc.2
Abs.
SIM
Wt.[g]:
2.946
2.946
0.69990
Vol.[mL]: 100
0.0026
0.0026
0.00062
AS-DF: 1.0
0.1
0.1
0.1
0.0028
Blank corr.:
off
mg/L
mg/L
Single values (Abs.): #1: 0.70049 #2: 0.69997 #3: 0.69925 (SEV: 300V)
BG (Abs.): #1: 0.00025 #2: 0.00009 #3: 0.00004
0.8
Sample Fe248
Abs.
0.6
0.4
0.2
0.0
0
Time [s]
Flame off
Date:
22/04/2016 14:28
Lamp off
Date:
22/04/2016 14:28
Cleaning
Date:
22/04/2016 14:28
Clean system
Date:
22/04/2016 14:28
Clean system
Date:
22/04/2016 14:28
ASpect LS 1.5.0.0
Analytik Jena