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GROUP MEMBERS &
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GROUP
SUBMIT TO
No.
1
2
3
4
Title
Procedure
Process Flow Diagram (PFD)
Workbook
Questions & Discussions
TOTAL MARKS
Marks
20
20
20
40
100
Remarks:
Checked by:
Rechecked by:
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)
Date:
PFD
Propylene glycol (C3H8O2) is a very common organic compound that is used in many
applications. It is used as an oil dispersant, a solvent in pharmaceuticals, an antifreeze,
and as a moisturizer, and any other applications. It is produced via the hydrolysis of
propylene oxide which is usually accelerated by acid or base catalysis.
Simulate the propylene glycol production process, including the reaction and separation
processes. Assume a propylene oxide feed stream of 3952 kg/h and a water feed stream
of 4990 kg/h. Both streams have temperature of 25 oC and pressure of 1 bar. The goal is
to produce a final product containing 99.5% propylene glycol. Assume a CSTR with a
volume of 8,000 L and liquid volume of 85%. The outlet temperature of CSTR is 60 oC.
The simplified reaction kinetics are shown below.
C3H6O + H2O C3H8O2
kJ
kgmole
)
RT
75362
k f =( 1.7 1013 h r 1 ) exp (
A distillation column is designed that is capable of producing a product with 99.5% purity.
Questions
1. What is the conversion of propylene glycol after reaction in CSTR?
The conversion of propylene glycol after reaction in CSTR is 23.27%. This
conversion indicate that low composition of propylene glycol would be produced at
the product stream.
2. How you design the distillation column in order to obtain the final product
with 99.5% purity? Explain specification of the distillation column and
assumption made.
In order to obtain the final product with 99.5% purity, the distillation column is
design as follows:
Specification
Pressure (bar)
Number of trays
Feed Tray*
Reflux ratio
Component
Fraction
*Count from the top
1
10
5
1.00
0.995
of DC
Assumption :
1) Used total condenser for the distillation column
3. What is the mole fraction for each component at the bottom and distillate of
distillation column?
The mole fraction for each component at the bottom and distillate of distillation
column are as follows:
Water
Propylene Glycol
Propylene Oxide
Distillate
0.9834
0.0000
0.0166
Bottom
0.0050
0.9950
0.0000
Water
Propylene Glycol
Propylene Oxide
Distillate
0.9827
0.0007
0.0166
Bottom
0.0050
0.9950
0.0000