Digestion

The filter paper were used to weigh and was put into a digestion tube.
Then, 2 kjeltabs and 12 ml of H2SO4 was added and the tube were gently
shake to wet the sample.
The water aspirator had set to full effect with the exhaust system. After
that, the rack with exhaust have been loaded into preheated digestion
block at 250oC for the first 30 minutes.
Next, after 30 minutes, the digestion block was set to 420oC for 45
minutes.

Distillation
-

80 ml f deionized water was added to each cooled tube. The receiver

solution of 25ml of 4% boric acid was placed into distillation unit.
Then, the digestion tube was connected in the distillation unit. Next, 50 ml
of 40% NaOH have been dispensed into the tube for 5minutes.
The distillation flask was light green.

Titration
The distillate was titrated with standardizes HCL and the color have been
changed from light green to light grey.