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INTRODUCTION ABSTRACT
Since the initial applications of Statement of problem. Framework longevity is a key factor for the success of complete-arch
titanium (Ti) in the early 1950s, prostheses and commonly depends on the welding methods. However, no consensus has been
reached on the joint design and welding type for improving framework resistance.
this metal has been used in nu-
merous industrial processes.1-3 Purpose. The purpose of this study was to assess the effect of different joint designs and welding
Titanium is attractive because methods with tungsten inert gas (TIG) or laser to join titanium alloy bars (Ti-6Al-4V).
of its low specic weight, high Material and methods. Seventy titanium alloy bar specimens were prepared (3.18 mm in diam-
strength-to-weight ratio, and eter 40.0 mm in length) and divided into 7 groups (n=10): the C-control group consisting of intact
good resistance to fatigue and specimens without joints and the remaining 6 groups consisting of specimens sectioned perpen-
corrosion.1,2 In dentistry, tita- dicular to the long-axis and rejoined using an I-, X30-, or X45-shaped joint design with TIG welding
(TI, TX30, and TX45) or laser welding (LI, LX30, and LX45). The specimens were tested with 3-point
nium was initially used to fabri-
bending. The fracture surfaces were rst evaluated with stereomicroscopy to measure the weld
cate dental implants because penetration area and then analyzed with scanning electron microscopy (SEM). The data were
of its biocompatibility, while statistically analyzed with 2-way ANOVA and the Tukey post hoc test, 1-way ANOVA and the
prosthetic implant-based in- Dunnett test, and the Pearson correlation test (a=.05).
frastructures were initially made
Results. Specimens from the X30 and X45 groups showed higher exural strength (P<.05) and
of precious metals.3 However, welded area (P<.05) than specimens from the I groups, regardless of the welding type. TIG welded
with the rising price of gold and groups showed signicantly higher exural strength than the laser groups (P<.05), regardless of the
the occurrence of allergic reac- joint design. TIG welding also resulted in higher welded areas than laser welding for the I-shaped
tions to some nickel-chromium specimens. No signicant differences were found for the weld penetration area in the X45 group,
and other base-metal alloys, either for laser or TIG welding. SEM analysis showed more pores at the fracture surfaces of the laser
economically feasible alloys specimens. Fracture surfaces indicative of regions of increased ductility were detected for the TIG
specimens.
with reduced risks to patients
were sought.4-6 Conclusions. TIG welding resulted in higher exural strength for the joined titanium specimens
Interest in titanium as a than laser welding. For both welding methods, X30- and X45-shaped joint designs resulted in
dental restorative material has higher exural strength and welding penetration than the I-shaped joint design. (J Prosthet Dent
2015;-:---)
increased, because this mate-
rial has adequate physical and
This study was supported by the National Counsel of Technological and Scientic Development (CNPq) and the Minas Gerais State Research Foundation (FAPEMIG).
a
Professor, Department of Occlusion, Fixed Prosthodontics and Dental Materials, School of Dentistry, Federal University of Uberlndia, MG, Brazil.
b
Professor, Department of Operative Dentistry and Dental Materials, School of Dentistry, Federal University of Uberlndia, MG, Brazil.
c
Graduate student, Department of Occlusion, Fixed Prosthodontics, and Dental Materials, School of Dentistry, Federal University of Uberlndia, MG, Brazil.
d
Professor, Department of Operative Dentistry and Dental Materials, School of Dentistry, Federal University of Uberlndia, MG, Brazil.
e
Professor, Department of Occlusion, Fixed Prosthodontics and Dental Materials, School of Dentistry, Federal University of Uberlndia, MG, Brazil.
40 mm
Clinical Implications 3.18 mm
TIG is a viable option for welding titanium alloy
A
frameworks when high exural strength is required.
40 mm
The X30- and X45- shaped joint designs are also
preferred under these circumstances. 3.18 mm
60 B
Table 1. Two-way ANOVA (32) for exural strength values Table 2. Mean exural strength (MPa) and standard deviation ()
Sources of Variation df Sum of Square Mean Square F P Groups Flexural Strength P
Welding type 1 5716901.8 5716901.8 74.8 <.001 Control 2311.0 55.4 -
Joint design 2 3415932.9 1707966.5 22.3 <.001 LI 1134.9 400.3* <.001
Welding type joint design 2 249786.0 124893.2 1.7 .205 LX30 1831.8 259.8* .002
Residual 54 4127947.7 76443.5 LX45 1673.3 340.2* <.001
Total 59 13510568.4 228992.7 TI 1906.3 184.5* .013
TX30 2287.4 226.0 .990
TX45 2298.3 173.4 .995
*Signicant difference from control group. Data analyzed by 1-way ANOVA and Dunnett
Table 3. Mean exural strength (MPa) and standard deviation () test (P<.05).
comparing factors welding type and joint design
Welding Type
Joint design Laser TIG Table 4. Two-way ANOVA (32) for weld penetration area values
I 1134.9 400.3Bb 1906.3 184.5Ab Sum of Mean
Sources of Variation df Square Square F P
X30 1831.8 259.8Ba 2287.4 226.0Aa
Ba Aa
Welding type 1 0.2 0.1 0.7 .408
X45 1673.3 340.2 2298.3 173.4
Joint design 2 84.4 42.2 145.9 <.001
Different uppercase letters indicate signicant difference in rows (welding type). Different Welding type joint design 2 9.0 4.5 15.6 <.001
lowercase letters indicate signicant difference in columns (joint design) (statistical categories
dened by Tukey test; a=.05). Residual 54 15.6 0.3
Total 59 109.2 1.9
Figure 3. SEM images of fracture joints from laser welded specimens. A, LI specimen fracture surface (25 magnication). B, LX30 specimen fracture
surface (25 magnication). C, LX45 specimen fracture surface (25 magnication). D, Magnication of fracture surface from LX45 specimen indicating
presence of pores (500 magnication).
resulting from insufcient welding penetration, which also agrees with results already reported for I-shaped
were represented by radiolucent areas at the central re- specimens joined with different welding parameters.33
gion of the joint. However, distinguishing internal voids, The assessments for weld penetration area showed
pores, and cracks was not possible. Limitations can exist signicantly lower values for the I-shaped design than for
with this technique, and the possibility of detecting X-shaped joints with both welding methods (Table 5).
small defects depends on the accuracy of the x-ray unit This occurred because of the limited welding capability of
and digital sensor. Analysis with computed micro- both welding processes for the I-shaped design. The
tomography can be more responsive.15 In contrast, minor incomplete welding of the central region in I-shaped
defects at the joints of prosthetic frameworks can usually specimens resulted in voids, with a signicant decrease in
be accepted; however, they often result in premature the exural strength (Figs. 3A, 4A). Studies have shown
failures.31 A dyeing liquid was employed in this study to that weld penetration can be impaired when I-shaped
detect discontinuities at the framework surfaces, but the design is used in Ti alloy specimens greater than 3 mm
specimens showed no evidence of surface defects, sug- in diameter, with a consequent decrease in joint
gesting that both welding processes were effective in strength.27,30 These ndings are corroborated by our re-
providing smooth surfaces. sults, in that the I-shaped joint design resulted in lower
The exural strength of the X-shaped TIG specimens strength values, regardless of the welding method
was statistically similar to that of the control group (Table 3).
(Table 2). These results are comparable to previous The chamfering on X-shaped joints is designed to
ndings using intact nonwelded titanium beams as con- reduce the cross-sectional area of the piece, allowing the
trol specimens.33 Despite the higher values observed heat generated by the welding equipment to reach the
with TIG welding, the I-shaped specimens presented center of the joint region, thus obtaining complete
lower exural strength than that of the X-shaped design, joining of the parts.28,29 This procedure was effective in
regardless of the welding method (Table 3). This nding overcoming the penetration limitations of both welding
Figure 4. SEM images of fracture joints from TIG welded specimens. A, TI specimen fracture surface (25 magnication). B, TX30 specimen fracture
surface (25 magnication). C, TX45 specimen fracture surface (25 magnication). D, Magnication of fracture surface from TX45 specimen, indicating
presence of dimples (white arrows) (500 magnication).
methods used. The angle variation (30 or 45 degree specimens (Fig. 3D). The presence of pores can probably
chamfer), however, did not signicantly affect the exural be attributed to the incorporation of gases such as argon
strength of the specimens (Table 3). Despite the higher and oxygen present in the equipment chamber during
welded areas veried for the X45 specimens, the X30 welding.12 This fact associated with the limited penetra-
joint design is more useful because less time is required tion of laser welding seems to explain the lower exural
to ll the chamfer completely and less lling material and strength for this method.21 Another relevant factor
gas is consumed for the 2 welding methods. observed at the SEM evaluation was the presence of
TIG welding associated with X-shaped design resul- ripples, called dimples, on the fracture surface of TIG
ted in higher joint resistance and was the only combi- specimens (Fig. 4D).21 The fracture surfaces of the TIG
nation to perform similarly to the control group (Table 2). groups clearly show a more complex joint arrangement
In this welding method, the joint lling has more volume when compared with the laser specimens. Studies have
for each pulse applied because of the higher diameter of shown that the formation of dimples in the fractured
the fusion point promoted by the increased heating welded areas is characteristic of ductile materials.21
input. This is advantageous because it allows for com- Ductile fractures of metals, in general, are character-
plete welding in less time and requires less gas shielding. ized by dimpled fracture surfaces caused by the micro-
This fact can also justify the increased resistance obtained scale mechanism of microvoid coalescence, which
by X-shaped joints compared with I- shaped design for typically is associated with macroscopic ductile fractures
TIG welding, because nal weld volume tends to be and is accepted as the dominant fracture mechanism in
higher. Thus, the joints of titanium-based frameworks engineering materials.34 The presence of dimples on the
can be inuenced by the welding techniques and by the fracture surfaces of the specimens from TIG groups
operator.13 shows that this welding process was more effective in
The SEM analysis of the fracture surfaces showed preserving some ductility from the original material than
higher occurrence of pores on the surface of laser-welded the laser method. However, the limits of the elastic
exure formula for the mechanical testing of ductile Future research using microtomographic analysis and
materials, such as titanium alloy, should be respected, cyclic fatigue would provide valuable data.
because ductile materials under compression loading can
only swell or buckle without fracture. Thus, the elastic CONCLUSIONS
limit of specimens must be taken into consideration
Within the limitations of this in vitro study, the X-shaped
during testing to avoid misunderstandings.
design resulted in higher exural strength (P<.001) and
All joint designs welded by TIG exhibited higher
weld penetration area (P<.001) for TIG and laser welding.
exural strength than laser joints; however, differences
The variation on the chamfer angle (30 and 45 degrees)
were found for weld penetration. For this factor, results
for the X-shaped design had no signicant inuence on
varied according to the joint design used, and superiority
the exural strength of either of the welding methods
of the welding methods was not detected (Table 5).
(P=.67). TIG welding resulted in higher exural strength
Although laser welding has obtained satisfactory results
for the joined titanium specimens than laser welding, and
in terms of welded area, this fact was not related to
weld penetration area varied for the welding methods
higher mechanical joint strength, possibly due to the
according to the joint design (P<.001).
increased incidence of pores and to the lower ductility of
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