Beruflich Dokumente
Kultur Dokumente
RADIOGRAPHIC STANDARDS
SE-280 Standard Reference Radiographs for Heavy-Walled [412 to 12-in. (114 to 305-
(ASTM E 280-93) mm)] Steel Castings . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 313
SE-747 Standard Practice for Design, Manufacture, and Material Grouping Classification
(ASTM E 747-97) of Wire Image Quality Indicators (IQI) Used for Radiology . . . . . . . . . . . . . . . . . . . . 321
SE-1025 Standard Practice for Design, Manufacture, and Material Grouping Classification
(ASTM E 1025-95) of Hole-Type Image Quality Indicators (IQI) Used for Radiology . . . . . . . . . . . . . . . 339
SE-1030 Standard Test Method for Radiographic Examination of Metallic Castings. . . . . . . . . . 347
(ASTM E 1030-95)
283 A99
SE-1165 Standard Test Method for Measurement of Focal Spots of Industrial X-Ray
[ASTM E 1165-92 Tubes by Pinhole Imaging . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 360.7
(R1996)]
SE-1815 Standard Test Method for Classification of Film Systems for Industrial
(ASTM E 1815-96) Radiography . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 385
A99 284
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SE-94 1998 SECTION V SE-94
PH2.22 Methods for Determining Safety Times of Photo- first determining that these quality levels can be main-
graphic Darkroom Illumination tained in production radiography.
PH4.8 Methylene Blue Method for Measuring Thiosul-
NOTE 2 The first number of the quality level designation refers
fate and Silver Densitometric Method for Measuring to IQI thickness expressed as a percentage of specimen thickness;
Residual Chemicals in Films, Plates, and Papers the second number refers to the diameter of the IQI hole that must
T9.1 Imaging Media (Film) Silver-Gelatin Type Speci- be visible on the radiograph, expressed as a multiple of penetrameter
thickness, T.
fications for Stability
T9.2 Imaging Media Photographic Processed Films, 5.2 If IQIs of material radiographically similar to
Plates, and Papers Filing Enclosures and Storage that being examined are not available, IQIs of the
Containers required dimensions but of a lower-absorption material
may be used.
3. Terminology 5.3 The quality level required using wire IQIs shall
be equivalent to the 2-2T level of Practice E 1025
3.1 Definitions For definitions of terms used in unless a higher or lower quality level is agreed upon
this guide, refer to Terminology E 1316. between purchaser and supplier. Table 4 of Test Method
E 747 gives a list of various hole-type IQIs and the
diameter of the wires of corresponding EPS with the
4. Significance and Use applicable 1T, 2T, and 4T holes in the plaque IQI.
4.1 Within the present state of the radiographic art, Appendix XI of Test Method E 747 gives the equation
this guide is generally applicable to available materials, for calculating other equivalencies, if needed.
processes, and techniques where industrial X-ray films
are used as the recording media.
4.2 Limitations This guide does not take into 6. Energy Selection
consideration special benefits and limitations resulting 6.1 X-ray energy affects image quality. In general,
from the use of nonfilm recording media or readouts the lower the energy of the source utilized the higher
such as paper, tapes, xeroradiography, fluoroscopy, and the achievable radiographic contrast, however, other
electronic image intensification devices. Although refer- variables such as geometry and scatter conditions may
ence is made to documents that may be used in override the potential advantage of higher contrast. For
the identification and grading, where applicable, of a particular energy, a range of thicknesses, which are
representative discontinuities in common metal castings a multiple of the half value layer, may be radiographed
and welds, no attempt has been made to set standards to an acceptable quality level utilizing a particular X-
of acceptance for any material or production process. ray machine or gamma ray source. In all cases the
Radiography will be consistent in sensitivity and resolu- specified IQI (penetrameter) quality level must be shown
tion only if the effect of all details of techniques, such on the radiograph. In general, satisfactory results can
as geometry, film, filtration, viewing, etc., is obtained normally be obtained for X-ray energies between 100
and maintained. kV to 500 kV in a range between 2.5 to 10 half value
layers (HVL) of material thickness (see Table 1). This
range may be extended by as much as a factor of 2
PART I EQUIPMENT AND PROCEDURE in some situations for X-ray energies in the 125 MV
range primarily because of reduced scatter.
5. Radiographic Quality Level
5.1 The quality level usually required for radiography
is 2% (2-2T when using hole type IQI) unless a higher
7. Radiographic Equivalence Factors
or lower quality is agreed upon between the purchaser
and the supplier. At the 2% subject contrast level, three 7.1 The radiographic equivalence factor of a material
quality levels of inspection, levels 2-1T, 2-2T, and 2- is that factor by which the thickness of the material
4T, are available through the design and application must be multiplied to give the thickness of a standard
of the IQI Practice E 1025, Table 1. The level of material (often steel) which has the same absorption.
inspection specified should be based on the service Radiographic equivalence factors of several of the more
requirements of the product. Great care should be taken common metals are given in Table 2, with steel arbi-
in specifying quality levels 2-1T, 1-1T, and 1-2T by trarily assigned a factor of 1.0. The factors may be used:
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SE-94 ARTICLE 22 RADIOGRAPHIC STANDARDS SE-94
TABLE 1
TYPICAL STEEL HVL THICKNESS IN INCHES (MM)
FOR COMMON ENERGIES
TABLE 2
APPROXIMATE RADIOGRAPHIC EQUIVALENCE FACTORS FOR SEVERAL METALS
(RELATIVE TO STEEL)
Energy Level
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SE-94 1998 SECTION V SE-94
7.1.1 To determine the practical thickness limits 9.4.2 Thickness of the material radiographed.
for radiation sources for materials other than steel, and
9.4.3 Variation of thickness of the material radio-
7.1.2 To determine exposure factors for one metal graphed.
from exposure techniques for other metals.
9.4.4 Energy spectrum of the radiation used.
9.4.5 The improvement desired (increasing or de-
8. Film creasing contrast). Filter thickness and material can be
calculated or determined empirically.
8.1 Various industrial X-ray film types are available
to meet the needs of production radiographic work.
However, definite rules on the selection of film are
10. Masking
difficult to formulate because the choice depends on
individual user requirements. Some user requirements 10.1 Masking or blocking (surrounding specimens
are as follows: radiographic quality levels, exposure or covering thin sections with an absorptive material)
times, and various cost factors. Several methods are is helpful in reducing scattered radiation. Such a material
available for assessing image quality levels (see Method can also be used to equalize the absorption of different
E 142, Test Methods E 746 and E 747, and Practice sections, but the loss of detail may be high in the
E 801). Information about specific products can be thinner sections.
obtained from the manufacturers.
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SE-94 ARTICLE 22 RADIOGRAPHIC STANDARDS SE-94
screen thickness, or for that matter, any metallic screen on active surfaces. Grease and lint may be removed
thickness, is subject to the same considerations as from lead screens with a solvent. Fluorescent screens
outlined in 9.4. Lead screens lessen the scatter reaching should be cleaned in accordance with the recommenda-
the film regardless of whether the screens permit a tions of the manufacturer. Screens showing evidence
decrease or necessitate an increase in the radiographic of physical damage should be discarded.
exposure. To avoid image unsharpness due to screens,
there should be intimate contact between the lead screen
and the film during exposure. 13. Radiographic Contrast
12.1.2 Lead foil screens of appropriate thickness 13.1 The various radiation intensities that penetrate
should be used whenever they improve radiographic an object are rendered as different photographic densities
quality or penetrameter sensitivity or both. The thickness in a radiograph. Using transmitted or reflected light to
of the front lead screens should be selected with care view a radiograph, an observed change in film density
to avoid excessive filtration in the radiography of over a background is defined as contrast. Radiographic
thin or light alloy materials, particularly at the lower contrast depends mostly upon subject contrast and film
kilovoltages. In general, there is no exposure advantage gradient.
to the use of 0.005 in. in front and back lead screens
13.2 Subject contrast is the ratio of radiation intensi-
below 125 kV in the radiography of 1 / 4-in. (6.35-mm)
or lesser thickness steel. As the kilovoltage is increased ties transmitted by two selected portions of a specimen.
to penetrate thicker sections of steel, however, there 13.3 The film gradient is the value of the slope of
is a significant exposure advantage. In addition to the tangent line drawn to a particular density point on
intensifying action, the back lead screens are used as the characteristic curve to the abscissa. Film manufactur-
protection against back-scattered radiation (see Section ers can furnish characteristic curves of their products.
11) and their thickness is only important for this
function. As exposure energy is increased to penetrate 13.4 The quality of radiography is influenced by
greater thicknesses of a given subject material, it is many variables; the effects of changes in some of these
customary to increase lead screen thickness. For radiog- variables are illustrated in Fig. 1.
raphy using radioactive sources, the minimum thickness
of the front lead screen should be 0.005 in. (0.13 mm)
for iridium-192, and 0.010 in. (0.25 mm) for cobalt-60. 14. Geometry
12.2 Other Metallic Screen Materials: 14.1 The focus-film distance necessary to reduce
geometric unsharpness to a negligible amount depends
12.2.1 Lead oxide screens perform in a similar upon the film or film-screen combinations, focal-spot
manner to lead foil screens except that their equivalence size, and objectfilm distance. Geometric unsharpness
in lead foil thickness approximates 0.0005 in. (0.013 is given [see Fig. 2(a)] by the equation:
mm).
12.2.2 Copper screens have somewhat less absorp- Ug p Ft /do
tion and intensification than lead screens, but may
provide somewhat better radiographic sensitivity with where:
higher energy above 1 MV. Ug p geometric unsharpness,
F p size of the radiation source,
12.2.3 Gold, tantalum, or other heavy metal screens t p specimen thickness, when in contact with the
may be used in cases where lead cannot be used. film, and
do p sourceobject distance.
12.3 Fluorescent Screens In general, for a given
source of radiation, fluorescent screens should be used NOTE 3 do and t must be in the same units of measure; the
only when the exposure necessary without them would units of Ug will be in the same units as F.
NOTE 4 A nomogram for the determination of Ug is given
be prohibitively long. In any event, if fluorescent screens in Fig. 3 (inch-pound units). Fig. 4 represents a nomogram in
must be used, they should be proven capable of achiev- metric units.
ing the required quality level. Good screenfilm contact
Example:
is essential for the successful use of fluorescent screens.
Given:
12.4 Screen Care All screens should be handled
carefully to avoid dents and scratches, dirt, or grease Sourcefilm distance (do) p 40 in.,
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SE-94 1998 SECTION V SE-94
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SE-94 ARTICLE 22 RADIOGRAPHIC STANDARDS SE-94
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SE-94 1998 SECTION V SE-94
Source size (F) p 500 mils, and NOTE 5 For detailed information of film density and density
Source side of specimen to film distance (t) p 1.5 in. measurement calibration, see Practice E 1079.
15.2 The essential elements of an exposure chart or 16.2.1 Description or sketch of the object,
calculator must relate the following: 16.2.2 Material type and thickness,
15.2.1 Source or machine, 16.2.3 Source or focusfilm distance,
15.2.2 Material type, 16.2.4 Film type,
15.2.3 Material thickness, 16.2.5 Film density,
15.2.4 Film type (relative speed), 16.2.6 Screen type and thickness,
15.2.5 Film density (see Note 5), 16.2.7 Isotope or X-ray machine identification,
15.2.6 Source or focus-film distance, 16.2.8 Curie or milliampere minutes,
15.2.7 Kilovoltage or isotope type, 16.2.9 Film placement for nonstandard items,
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SE-94 ARTICLE 22 RADIOGRAPHIC STANDARDS SE-94
16.2.10 Source position for nonstandard items, and method by which identification is achieved shall
be as agreed upon between the customer and inspector.
16.2.11 Penetrameter and shim thickness,
16.2.12 Special masking or filters,
18.1.2 The minimum identification should at least
16.2.13 Collimator or field limitation device, and include the following: the radiographic facilitys name,
the date, part number and serial number, if used,
16.2.14 Processing method. for unmistakable identification of radiographs with the
16.3 The recommendations of 16.2 are not mandatory, specimen. The letter R should be used to designate a
but are essential in reducing the overall cost of radiogra- radiograph of a repair area, and may include -1 , -2,
phy, and serve as a communication link between the etc., for the number of repair.
radiographic interpreter and the radiographic operator.
18.2 Location Markers:
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manufacturers recommendation should be followed in 24.9.2 For specific washing recommendations, con-
choosing a development time. When the temperature sult the film manufacturer.
is higher or lower, development time must be changed.
24.10 Wetting Agent Dip the film for approxi-
Again, consult manufacturer-recommended development
mately 30 s in a wetting agent. This makes water drain
time versus temperature charts. Other recommendations
evenly off film which facilitates quick, even drying.
of the manufacturer to be followed are replenishment
rates, renewal of solutions, and other specific instruc- 24.11 Residual Fixer Concentrations If the fixing
tions. chemicals are not removed adequately from the film,
they will in time cause staining or fading of the
24.5 Agitation Shake the film horizontally and
developed image. Residual fixer concentrations permis-
vertically, ideally for a few seconds each minute during sible depend upon whether the films are to be kept
development. This will help film develop evenly. for commercial purposes (3 to 10 years) or must
24.6 Stop Bath or Rinse After development is be of archival quality. Archival quality processing is
complete, the activity of developer remaining in the desirable for all radiographs whenever average relative
emulsion should be neutralized by an acid stop bath humidity and temperature are likely to be excessive,
or, if this is not possible, by rinsing with vigorous as is the case in tropical and subtropical climates. The
agitation in clear water. Follow the film manufacturers method of determining residual fixer concentrations may
recommendation of stop bath composition (or length be ascertained by reference to ANSI PH4.8, PH1.28, and
of alternative rinse), time immersed, and life of bath. PH1.41.
24.7 Fixing The films must not touch one another 24.12 Drying Drying is a function of (1) film
in the fixer. Agitate the hangers vertically for about (base and emulsion); (2) processing (hardness of emul-
10 s and again at the end of the first minute, to ensure sion after washing, use of wetting agent); and (3)
uniform and rapid fixation. Keep them in the fixer until drying air (temperature, humidity, flow). Manual drying
fixation is complete (that is, at least twice the clearing can vary from still air drying at ambient temperature
time), but not more than 15 min in relatively fresh to as high as 140F (60C) with air circulated by a
fixer. Frequent agitation will shorten the time of fixation. fan. Film manufacturers should again be contacted for
recommended drying conditions. Take precaution to
24.8 Fixer Neutralizing The use of a hypo elimina- tighten film on hangers, so that it cannot touch in the
tor or fixer neutralizer between fixation and washing may dryer. Too hot a drying temperature at low humidity
be advantageous. These materials permit a reduction of can result in uneven drying and should be avoided.
both time and amount of water necessary for adequate
washing. The recommendations of the manufacturers
as to preparation, use, and useful life of the baths 25. Testing Developer
should be observed rigorously.
25.1 It is desirable to monitor the activity of the
24.9 Washing The washing efficiency is a function radiographic developing solution. This can be done by
of wash water, its temperature, and flow, and the film periodic development of film strips exposed under
being washed. Generally, washing is very slow below carefully controlled conditions, to a graded series of
60F (16C). When washing at temperatures above radiation intensities or time, or by using a commercially
85F (30C), care should be exercised not to leave available strip carefully controlled for film speed and
films in the water too long. The films should be washed latent image fading.
in batches without contamination from new film brought
over from the fixer. If pressed for capacity, as more
films are put in the wash, partially washed film should 26. Viewing Radiographs
be moved in the direction of the inlet.
26.1 Transmission The illuminator must provide
24.9.1 The cascade method of washing uses less light of an intensity that will illuminate the average
water and gives better washing for the same length of density areas of the radiographs without glare and it
time. Divide the wash tank into two sections (may be must diffuse the light evenly over the viewing area.
two tanks). Put the films from the fixer in the outlet Commercial fluorescent illuminators are satisfactory for
section. After partial washing, move the batch of film radiographs of moderate density; however, high light
to the inlet section. This completes the wash in fresh intensity illuminators are available for densities up to
water. 3.5 or 4.0. Masks should be available to exclude any
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SE-94 1998 SECTION V SE-94
extraneous light from the eyes of the viewer when book, or other record) constituting a record of each job
viewing radiographs smaller than the viewing port or performed, be maintained. This record should comprise,
to cover low-density areas. initially, a job number (which should appear also on
the films), the identification of the parts, material or
26.2 Reflection Radiographs on a translucent or area radiographed, the date the films are exposed, and
opaque backing may be viewed by reflected light. It a complete record of the radiographic procedure, in
is recommended that the radiograph be viewed under sufficient detail so that any radiographic techniques
diffuse lighting conditions to prevent excess glare. may be duplicated readily. If calibration data, or other
Optical magnification can be used in certain instances records such as card files or procedures, are used to
to enhance the interpretation of the image. determine the procedure, the log need refer only to
the appropriate data or other record. Subsequently, the
interpreters findings and disposition (acceptance or
27. Viewing Room rejection), if any, and his initials, should be entered
for each job.
27.1 Subdued lighting, rather than total darkness, is
preferable in the viewing room. The brightness of the
surroundings should be about the same as the area of 30. Reports
interest in the radiograph. Room illumination must be
so arranged that there are no reflections from the surface 30.1 When written reports of radiographic examina-
of the film under examination. tions are required, they should include the following,
plus such other items as may be agreed upon:
30.1.1 Identification of parts, material, or area.
28. Storage of Processed Radiographs
30.1.2 Radiographic job number.
28.1 Radiographs should be stored using the same
30.1.3 Findings and disposition, if any. This infor-
care as for any other valuable record.
mation can be obtained directly from the log.
28.2 Envelopes having an edge seam, rather than a
center seam, and joined with a nonhygroscopic adhesive,
are preferred, since occasional staining and fading of 31. Identification of Completed Work
the image is caused by certain adhesives used in the 31.1 Whenever radiography is an inspective (rather
manufacture of envelopes (see ANSI PH1.53). than investigative) operation whereby material is ac-
cepted or rejected, all parts and material that have been
accepted should be marked permanently, if possible,
PART IV RECORDS, REPORTS, AND with a characteristic identifying symbol which will
IDENTIFICATION OF ACCEPTED indicate to subsequent or final inspectors the fact of
MATERIAL radiographic acceptance.
31.2 Whenever possible, the completed radiographs
29. Records
should be kept on file for reference. The custody of
29.1 It is recommended that an X-ray log (a log radiographs and the length of time they are preserved
may consist of a card file, punched card system, a should be agreed upon between the contracting parties.
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SE-94 ARTICLE 22 RADIOGRAPHIC STANDARDS SE-94
APPENDIX
(Nonmandatory Information)
X1. USE OF FLUORESCENT SCREENS layer thickness, is minimized by using screens having
small, evenly spaced crystals in a thin crystalline layer.
X1.1 Description Fluorescent intensifying screens
Fluorescent screens are highly sensitive to longer wave-
have a cardboard or plastic support coated with a
length scattered radiation. Consequently, to maximize
uniform layer of inorganic phosphor (crystalline sub-
contrast when this non-image forming radiation is exces-
stance). The support and phosphor are held together by
sive, fluorometallic intensifying screens or fluorescent
a radiotransparent binding material. Fluorescent screens
screens backed by lead screens of appropriate thickness
derive their name from the fact that their phosphor
are recommended. Screen technology has seen signifi-
crystals fluoresce (emit visible light) when struck by
cant advances in recent years, and todays fluorescent
X or gamma radiation. Some phosphors like calcium
screens have smaller crystal size, more uniform crystal
tungstate (CaWO4) give off blue light while others
packing, and reduced phosphor thickness. This translates
known as rare earth emit light green.
into greater screen /film speed with reduced unsharpness
and mottle. These improvements can represent some
X1.2 Purpose and Film Types Fluorescent screen meaningful benefits for industrial radiography, as indi-
exposures are usually much shorter than those made cated by the three examples as follows:
without screens or with lead intensifying screens, be-
cause radiographic films generally are more responsive
to visible light than to direct X-radiation, gamma radia- X1.3.1 Reduced Exposure (Increased Productiv-
tion, and electrons. ity) There are instances where prohibitively long
exposure times make conventional radiography impracti-
X1.2.1 Films fall into one of two categories: non- cal. An example is the inspection of thick, high atomic
screen type film having moderate light response, and number materials with low curie isotopes. Depending
screen type film specifically sensitized to have a very on many variables, exposure time may be reduced by
high blue or green light response. Fluorescent screens factors ranging from 2 to 105 when the appropriate
can reduce conventional exposures by as much as 150 fluorescent screen /film combination is used.
times, depending on film type.
X1.3.2 Improved Safety Conditions (Field Sites)
X1.3 Image Quality and Use The image quality Because fluorescent screens provide reduced exposure,
associated with fluorescent screen exposures is a func- the length of time that non-radiation workers must
tion of sharpness, mottle, and contrast. Screen sharpness evacuate a radiographic inspection site can be reduced
depends on phosphor crystal size, thickness of the significantly.
crystal layer, and the reflective base coating. Each
crystal emits light relative to its size and in all directions
thus producing a relative degree of image unsharpness. X1.3.3 Extended Equipment Capability Utiliz-
To minimize this unsharpness, screen to film contact ing the speed advantage of fluorescent screens by
should be as intimate as possible. Mottle adversely translating it into reduced energy level. An example
affects image quality in two ways. First, a quantum is that a 150 kV X-ray tube may do the job of a 300
mottle is dependent upon the amount of X or gamma kV tube, or that iridium 192 may be used in applications
radiation actually absorbed by the fluorescent screen, normally requiring cobalt 60. It is possible for overall
that is, faster screen /film systems lead to greater mottle image quality to be better at the lower kV with fluores-
and poorer image quality. A structural mottle, which cent screens than at a higher energy level using lead
is a function of crystal size, crystal uniformity, and screens.
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SE-142 1998 SECTION V SE-142
placed as close as possible to the item being examined, 6.5 When shims are used with penetrameters in the
and the resulting radiographic density of the block radiography of welds, or when the penetrameters are
image is within prescribed penetrameter /area of interest placed on separate blocks, the shims or blocks may
density variation tolerances. be made of any material in the pertinent materials
group. For materials not categorized, the shims or
6.2 When radiographing welds, the penetrameters blocks may be made of the penetrameter material or
shall be placed on the source side adjacent to the of material of similar specification analysis as the
weld being radiographed. When weld reinforcement or material being radiographed.
protruding backing ring is not removed, a shim of the
same type parent metal shall be placed under the 6.6 It is the intent of the foregoing stipulations for
penetrameter to provide the same thickness of material shims and separate blocks that wrought materials may
under the penetrameter as the average thickness through be used for these items when castings or welds are being
the weld. Shims shall exceed the penetrameter dimen- radiographed. This is to permit equitable evaluation
sions such that the outline of at least three sides of of the penetrameter where diffraction effects may be
the penetrameter image shall be placed so as not to encountered in the radiography of some cast or weld
overlap the backing strip or ring. deposit materials.
6.3 When examining double-walled parts such as
piping or duct with a radiation source outside the pipe,
the penetrameter shall be placed, where practicable, on
the outside of the pipe alongside the weld nearest the
source of radiation. 7. Number of Penetrameters
7.1 One penetrameter shall represent an area within
6.3.1 In cases where placement of the penetrameter
which radiographic densities do not vary more than
on the source side is impracticable, the penetrameter
15% or +30% (Note 2). At least one penetrameter per
may be placed on the film side if one of the following
radiograph, exposed simultaneously with the specimen,
conditions is met.
shall be used except as noted in 7.1.1 and 7.1.2 (Note
6.3.2 The radiographic technique shall be demon- 3). The radiographic density of the penetrameter shall
strated with the applicable penetrameter set placed on be measured through the body of the penetrameter.
the source side and a continuous series of penetrameters
placed on the film side of a like pipe section. The 7.1.1 When the film density varies more than
series of penetrameters shall range in thickness from 15% or +30% from that through to the penetrameter,
2% to 0.5% of the material thickness. If the penetrameter two penetrameters used in the following manner will
on the source side indicates the required sensitivity, be satisfactory. If one penetrameter shows an acceptable
the image of the smallest penetrameter hole visible on sensitivity at the most dense portion of the radiograph
the film side shall be used to determine the penetrameter and the second penetrameter, placed in accordance with
and penetrameter hole which shall be used on production Section 6, shows an acceptable sensitivity at the least
radiographs. dense portion of the radiograph, these two penetrameters
will serve to qualify the radiograph.
6.3.3 When radiographing welds in which only
the portion of the weld next to the film is viewed, the 7.1.2 Simultaneous Exposures When a part or
radiographic technique shall be demonstrated on a parts of the same design are exposed simultaneously
similar pipe section with the applicable penetrameters under the same geometrical condition in a 360 radiation
placed on the inside along the root of the weld, and beam, a minimum of one penetrameter shall be required
a series of penetrameters, chosen as in 6.3.2, placed in each quadrant.
on the film side. If the penetrameter on the source
side indicates the required sensitivity, the image of the NOTE 2 Radiographic densities may be measured by Practice E
smallest penetrameter hole visible on the film side shall 1079. When films are exposed simultaneously in one film holder,
density variations should be determined on the single or superimposed
be used to determine the penetrameter and penetrameter films, referred to the manner in which they are interpreted.
holes which shall be used on production radiographs.
6.4 In the inspection of irregular objects, the pene- NOTE 3 For parts of irregular geometry or widely varying
thickness, it may be necessary to radiograph the first unit of a given
trameter shall be placed on the part of the object design to determine proper placement of penetrameters for subsequent
farthest from the film. radiography.
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SE-142 ARTICLE 22 RADIOGRAPHIC STANDARDS SE-142
9. Identification of Radiograph
9.1 A system of positive identification of the radio- 14. Records
graph shall be provided. Any or all of the following 14.1 Complete records of the technique details shall
may appear: the name of the inspection laboratory, the accompany the radiographs and shall be maintained by
date, the part number, the view, and whether original the inspecting laboratory.
or subsequent exposure.
10.1 Film techniques with two or more films of 15.1 Radiographic procedure shall be carried out
equal or different speeds in the same holder will be under protected conditions so that the radiographer will
permitted provided that the appropriate penetrameter not receive a maximum whole body radiation dosage
sensitivity for a specific area is demonstrated. exceeding that permitted by city, state, or national
codes.
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SE-186 ARTICLE 22 RADIOGRAPHIC STANDARDS SE-186
1.3 These reference radiographs consist of three 1.4.5 Category E Hot tear; one illustration D3
separate sets as follows: in pre-1972 documents.
1.3.1 1 MV X-rays and Iridium-192 radiation 1.4.6 Category F Insert; one illustration EB3
(called 1 to 2-MeV X-rays in previous editions). in pre-1972 documents.
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SE-186 1998 SECTION V SE-186
2. Referenced Documents
5. Classification Specifications
2.1 ASTM Standard:
E 94 Guide for Radiographic Testing 5.1 The applicable radiographic severity classification
should be designated by the contracting agency in
2.2 Adjuncts: formal specifications or drawings and in the specific
Reference Radiographs for Heavy-Walled [2 to 41 / 2-in. contract or order. The specifications, drawings, contract,
(51 to 114-mm)] Steel Castings or order should also designate the sampling plan for
Volume I, 1-MV X-Rays and Iridium-192 the castings to be radiographed and the extent of
Volume II, 2-MV X-Rays and Cobalt-60 radiographic coverage, as well as the classification or
Volume III, 4-MV to 30-MV X-Rays degree of acceptable discontinuity.
306
SE-186 ARTICLE 22 RADIOGRAPHIC STANDARDS SE-186
govern without regard to the other categories of disconti- 6.8.1 When the source has been placed perpendicu-
nuities, and the casting rejected until satisfactorily re- lar to the length of the gas hole, evaluate the production
paired. radiograph with a shrinkage reference radiograph.
6.5 When two or more categories of discontinuity 6.8.2 When the source has been placed diametri-
are present to an extent equal to the maximum permissi- cally or into the diameter of the gas hole, evaluate the
ble level as shown in the pertinent standards for each production radiograph with a gas reference radiograph.
category, then that part of the casting shall be judged
by the most representative reference radiograph. 6.9 A diffraction mottling pattern can occur on
radiographs of parts and sections where the grain size
6.6 Reference radiographs are provided showing a is large enough to be an appropriate fraction of the
variety of forms of shrinkage cavities. Production radio- material thickness. However, diffraction mottling will
graphs showing shrinkage shall be judged by the most not occur in materials within the thickness range of
representative reference radiograph. this standard.
6.7 Production radiographs showing porosity, gas, or 6.10 Hot tears and cracks exhibited on production
inclusions shall be evaluated by the overall condition radiographs may at times resemble linear type shrinkage.
with regard to size, number, and distribution. The When doubt exists whether such indications are cracks
aggregate size of the discontinuities shall not exceed or tears, or are linear shrinkage, all surfaces in the
the total accumulation in area of the discontinuities of area of interest shall be ground and magnetic particle
the reference radiograph. It is not the intent that the or liquid penetrant inspected as applicable. The extent
maximum size of the illustrated discontinuity shall be and depth of grinding may require engineering judgment.
the limiting size for a single production radiographic If the indication does not appear on the surface, it
discontinuity, or that the number of discontinuities shall be considered to be shrinkage.
shown on the reference radiograph shall be the limiting
number of production radiographs. Also, caution should 6.11 The radiographic density of discontinuities in
be exercised in judging a large discontinuity against a comparison with background density is a variable depen-
collection of small discontinuities on the basis of size dent on technical factors. It shall not be used as a
alone. Each of the factors of size, number, and distribu- criterion for acceptance or rejection in comparison with
tion must be considered in balance. reference radiographs.
307
SE-242 ARTICLE 22 RADIOGRAPHIC STANDARDS SE-242
309
SE-242 1998 SECTION V SE-242
m p linear absorption coefficient, and of X-ray or gamma ray energy and film types or both
x p section thickness. are changed.
As the above equation shows, the minimum thickness
of detectable discontinuity (dx) is: 4.3 Film Deterioration Radiographic films are
subject to wear and tear from handling and use. The
3.2.1 a function of X-ray energy; extent to which the image deteriorates over time is a
function of storage conditions, care in handling and
3.2.2 a function of section thickness, and
amount of use. Reference radiograph films are no
3.2.3 an inverse function of film gradient. exception and may exhibit a loss in image quality over
time. The radiographs should therefore be periodically
3.3 Although not clearly indicated by the above examined for signs of wear and tear, including scratches,
relation, the size of detectable discontinuity is also a abrasions, stains, and so forth. Any reference radio-
function of unsharpness, see Guide E 94. graphs which show signs of excessive wear and tear
which could influence the interpretation and use of the
radiographs should be replaced.
4. Radiographic Illustrations
4.1 A series of 36 radiographs, each on 10 by 12
in. (254 by 305 mm) film, were taken of a 12 by 12 5. Use of Reference Radiographs
in. welded steel plate which contained discontinuities
5.1 As radiation energy increases, the radiographic
in the weld. These were taken to illustrate the differences
appearance of a given discontinuity becomes less distinct
in appearance of the radiographic image when tech-
because of the greater penetration of the radiation; that
niques for taking radiographs are varied by changing
is, because of decreasing subject contrast. The reference
the factors listed in Section 3. A 2 by 2 in. (51 by
radiographs permit a comparison of the radiographic
51 mm) area, which includes the identical image of
appearance of the weld, at particular thickness over a
the discontinuities in the weld, was selected and cut
range of X-ray or gamma ray energies.
out from each 10 by 12 in. radiograph and arranged
so as to make four composite illustrations identified 5.2 Another condition that affects radiographic ap-
as Fig. 1 through Fig. 4. These composite illustrations pearance is the variation of thickness for a given X-
are an abridged version of the original 36 radiographs ray or gamma ray energy. As the thickness of inspected
and serve as the reference radiographs for this document. material is increased, a discontinuity becomes less
Following are brief descriptions of these figures. distinct in the radiographic image. This is due to two
predominant factors:
4.1.1 Figure 1 Composite Illustration A consists
of cutouts from the 10 radiographs taken of the 1 in. 5.2.1 The X-ray or gamma ray beam divergence
(25 mm) thick welded steel plate. which produces unsharpness on the film when traversing
a large thickness.
4.1.2 Figure 2 Composite Illustration B consists
of cutouts from the 10 radiographs taken of the welded 5.2.2 Scattered radiation within the material, which
steel plate, built up to 2 in. in thickness. reduces the radiographic contrast.
4.1.3 Figure 3 Composite Illustration C consists 5.2.3 The above processes are a function of material
of cutouts from the 10 radiographs taken of the welded thickness and X-ray or gamma ray energy. This effect
steel plate, built up to 4 in. in thickness. is illustrated in this document by the composite set
4.1.4 Figure 4 Composite Illustration D consists of radiographs or by direct reference to the full-size
of cutouts from the 6 radiographs taken of the welded radiographs.
steel plate, built up to 6 in. (152 mm) in thickness.
4.2 The radiographic appearance of discontinuities
6. Film and Screens
in 1, 2, 4, and 6 in. thick steel is shown in the
series of composite radiographs. (These are full-scale 6.1 The X-ray films used in obtaining the illustrative
reproductions of the same selected area from all the data were of two types: Very Fine Grain, Type I, and
reference radiographs.) All composite sets of radio- Fine Grain, Type II (Guide E 94). Comparison of these
graphs show the change in radiographic appearance in two types of film are illustrated in the composite
the specified thickness of steel plate as the parameters radiographs.
310
SE-242 ARTICLE 22 RADIOGRAPHIC STANDARDS SE-242
6.2 Several different lead foil screen combinations 7.3 All other factors remaining constant, as the film
were used. The specific combination of lead foil screens is changed from Type I to Type II, the radiographic
for each radiograph is noted in Table 1. appearance of the discontinuities becomes less distinct.
7.4 For specimens of uniform thickness, these data
reveal that the most distinct radiographic appearance
7. Conclusions and Summary of the discontinuities occurs when the finest grain film
and the lowest X-ray or gamma ray energy are used,
7.1 For a constant specimen thickness, the radio- consistent with the given specimen thickness and practi-
graphic appearance of the discontinuities changes as cal exposure time.
the X-ray or gamma ray energy is varied.
7.2 As the section thickness of specimen increases,
8. Keywords
the radiographic appearance of the discontinuities be-
comes less distinct, the radiation energy remaining 8.1 film types; discontinuities; gamma rays; reference
constant. radiographs; steel; unsharpness; welds; x-ray
EXPLANATORY NOTES
NOTE 1 Total unsharpness factors such as source size, source- may be explored to complete the work at other energy levels. The
film distance, screens, film graininess, etc., must be considered in radiographs included in this document are illustrative and not intended
establishing techniques (Guide E 94). to be either inclusive or conclusive.
TABLE 1
TECHNIQUE DATA
Note 1 in. p 25.4 mm.
Composite Illustration
A B C D
Lead Screens Steel Thickness
Source Front, in. Back, in. 1 in. 2 in. 4 in. 6 in. Film Notes
150 kVp 0.005 0.005 x ... ... ... Type II 1 in. lead mask
4
250 kVp 0.005 0.005 ... x ... ... Type II 1 in. lead mask
4
311
SE-242 1998 SECTION V SE-242
APPENDIX
(Nonmandatory Information)
X1. ADDITIONAL TECHNICAL ing the image of the two drilled holes in the plate
INFORMATION was between 1.90 and 2.10.
X1.1 Radiation source was centered over drilled hole X1.3 All films were developed using procedures
in center specimen [as seen in the 10 in. by 12 in. recommended in Guide E 94.
(254 by 305 mm) full-size reproduction]. In 1 MV
X1.4 Good contact between film and screens was
radiography, the radiation was projected towards the
maintained.
specimen through the target, using a transmitted beam.
X1.2 Radiographic exposure was such that the film
density in the radiograph at the center of a line connect-
312
SE-280 ARTICLE 22 RADIOGRAPHIC STANDARDS SE-280
1.2 Radiographs for evaluation are to be compared 1.4.3.3 Type 3 Severity levels 1 through 5.
with these reference radiographs for classification on
1.4.4 Category D Crack; one illustration D3
the basis of the category and severity level of the
in pre-1972 documents.
discontinuity. These reference radiographs are applicable
to nominal section thicknesses of 41 / 2 to 12 in. (114 1.4.5 Category E Hot tear; one illustration
to 305 mm). D3 in pre-1972 documents.
1.3 These reference radiographs consist of two 1.4.6 Category F Insert; one illustration EB3
separate sets as follows: in pre-1972 documents.
1.3.1 2-MV X-rays and Cobalt-60 (called gamma 1.5 The use of this document is not intended to
rays in previous editions). This includes cobalt-60 or be restricted to the specific energy level or to the
equivalent isotope radiation and from 2-MV up to 4- absolute thickness limits that are contained in the
MV X-rays. document title. The title is intended to be descriptive
and not restrictive. The document may be used, where
1.3.2 4-MV to 30-MV X-rays (called 10 to 24- there is no other applicable document, for other energy
MeV X-rays in previous editions). levels or thicknesses, or both, for which it is found
to be applicable and for which agreement has been
1.4 Each set is for comparison only with the
reached between purchaser and manufacturer.
radiographs produced with equivalent radiation and
consists of three categories of graded discontinuities NOTE The two sets of reference radiographs consist of 56
in increasing severity levels, and three categories of radiographic reproductions (28 for each set) in 81 / 2 by 11-in. ring
binders. In 1972, the number of categories was increased from five
ungraded discontinuities furnished as examples only, to six and the number of radiographic reproductions reduced from
as follows: 37 to 28 for each set.
1.4.1 Category A Gas porosity; severity levels 1.6 The values stated in inch-pound units are to
1 through 5. be regarded as the standard.
313
SE-280 1998 SECTION V SE-280
314
SE-280 ARTICLE 22 RADIOGRAPHIC STANDARDS SE-280
radiographs showing shrinkage shall be judged by the 6.8.2 When the source has been placed diametri-
most representative reference radiograph. cally or into the diameter of the gas hole, evaluate the
production radiograph with a gas reference radiograph.
6.7 Production radiographs showing porosity, gas, 6.9 A diffraction mottling pattern can occur on
or inclusions shall be evaluated by the overall condition radiographs of parts and sections where the grain size
with regard to size, number, and distribution. The is large enough to be an appropriate fraction of the
aggregate size of the discontinuities shall not exceed material thickness. However, diffraction mottling will
the total accumulation in area of the discontinuities of not occur in materials within the thickness range of
the reference radiograph. It is not the intent that the this standard.
maximum size of the illustrated discontinuity shall be 6.10 Hot tears and cracks exhibited on production
the limiting size for a single production radiographic radiographs may at times resemble linear type shrinkage.
discontinuity, or that the number of discontinuities When doubt exists whether such indications are cracks
shown on the reference radiograph shall be the limiting or tears, or are linear shrinkage, all surfaces in the
number of production radiographs. Also, caution should area of interest shall be ground and magnetic particle
be exercised in judging a large discontinuity against a or liquid penetrant inspected as applicable. The extent
collection of small discontinuities on the basis of size and depth of grinding may require engineering judgment.
alone. Each of the factors of size, number, and distribu- If the indication does not appear on the surface, it
tion must be considered in balance. shall be considered to be shrinkage.
6.11 The radiographic density of discontinuities
6.8 Reference radiographs in this standard do not in comparison with background density is a variable
illustrate elongated or worm hole type of gas disconti- dependent on technical factors. It shall not be used as
nuities. When this condition occurs in a production a criterion for acceptance or rejection in comparison
radiograph, it shall be evaluated by comparison with with reference radiographs.
the most representative reference radiograph.
7. Keywords
6.8.1 When the source has been placed perpendicu-
lar to the length of the gas hole, evaluate the production 7.1 castings; discontinuities, gamma rays; reference
radiograph with a shrinkage reference radiograph. radiographs; steel; x-ray
315
SE-446 ARTICLE 22 RADIOGRAPHIC STANDARDS SE-446
317
SE-446 1998 SECTION V SE-446
Volume III: 2-MV to 4-MV X Rays and Cobalt-60 Reference Radio- 3.2 Film Deterioration Radiographic films are
graphs Set of 34 illustrations (5 by 7 in.) in a 15 by 17-in.
ring binder. subject to wear and tear from handling and use. The
extent to which the image deteriorates over time is a
NOTE 3 Although Category G Mottling is listed for all the function of storage conditions, care in handling and
volumes, the appearance of mottling is dependent on the level of
radiation energy. Mottling appears reasonably prominent in Volume amount of use. Reference radiograph films are no
I: however, because of the higher radiation energy levels mottling exception and may exhibit a loss in image quality over
may not be apparent in Volume II nor Volume III. time. The radiographs should therefore be periodically
1.3 The use of this document is not intended to examined for signs of wear and tear, including scratches,
be restricted to the specific energy level or to the abrasions, stains, and so forth. Any reference radio-
absolute thickness limits that are contained in the graphs which show signs of excessive wear and tear
document title. The title is intended to be descriptive which could influence the interpretation and use of the
and not restrictive. The document may be used, where radiographs should be replaced.
there is no other applicable document, for other energy
levels or thicknesses, or both, for which it is found
to be applicable and for which agreement has been
4. Determination of Radiographic Classification
reached between purchaser and manufacturer.
4.1 For purposes of evaluation of castings, a determi-
1.4 The values stated in inch-pound units are to
nation must be made of the radiographic classification
be regarded as the standard.
to be assigned to individual castings or specific areas
of castings. The determination of the applicable radio-
graphic classification shall be based on an evaluation
2. Referenced Documents of the casting applications, design, and service require-
2.1 ASTM Standard: ments. In these evaluations, consideration shall be given
E 94 Guide for Radiographic Testing to such factors as pressure, temperature, section thick-
E 142 Method for Controlling Quality of Radiographic ness, applicable design safety factor (preferably based on
Testing stress analysis), vibration, shock, resistance to corrosion,
E 186 Reference Radiographs for Heavy-Walled [2 to involvement of penetrating radiations or radiation prod-
41 / 2 in. (51 to 114 mm)] Steel Castings ucts, and involvement of dangerous gases or liquids.
E 242 Reference Radiographs for Appearances of Radio-
4.2 For each portion of casting radiographed, the
graphic Images as Certain Parameters Are Changed
severity level for each class of discontinuity category
E 280 Reference Radiographs for Heavy-Walled [41 / 2 to
should be clearly specified. Thus, Severity Level 2
12 in. (114 to 305 mm)] Steel Castings
might be specified for Shrinkage, Category CA, and
2.2 Adjuncts: Severity Level 3 for Gas Porosity, Category A, since
Reference Radiographs for Steel Castings Up to 2 in. (51 the latter are generally much less deleterious to tensile
mm) in Thickness: properties.
Volume I, 1-MV X-Rays and Iridium-192
Volume II, 2-MV X-Rays and Cobalt-60
Volume III, 4-MV to 30-MV X-Rays
5. Classification Specifications
5.1 The applicable radiographic severity classification
3. Method of Preparation should be designated by the contracting agency in
formal specifications or drawings and in the specific
3.1 The original radiographs used to prepare these
contract or order. The specifications, drawings, contract,
three sets of reference illustrations were made from
or order should also designate the sampling plan for
selected sections of actual production castings by the
the castings to be radiographed and the extent of
respective use of 2.50 kVp X rays, iridium-192 radiation
radiographic coverage, radiographic practice to be fol-
and cobalt-60 radiation on Class I and II film with a
lowed (Guide E 94 and Method E 142), image quality
sensitivity as determined by standard 2-2T penetrameters
desired (Note 4) as well as the severity of the acceptable
(Guide E 94 and Method E 142). The illustrations have
discontinuity for the graded categories.
been prepared to an H and D density of from 2.00 to
2.25 and they have been made to retain the contrast NOTE 4 For description of sensitivity or quality levels, see Guide
of the original radiographs. E 94, Method E 142, and Reference Radiographs E 242.
318
SE-446 ARTICLE 22 RADIOGRAPHIC STANDARDS SE-446
6. Procedure for Evaluation alone. Each of the factors of size, number, and distribu-
tion must be considered in balance.
6.1 Compare the production radiographs of the
casting submitted for evaluation with the reference 6.8 Reference radiographs in this standard do not
radiographs of similar thickness that were exposed at illustrate elongated or worm hole type of gas disconti-
an equivalent energy range. nuities. When this condition occurs in a production
6.2 When the severity level of discontinuities in radiograph, it shall be evaluated by comparison with
the production radiograph being evaluated is equal to the most representative reference radiograph.
or better than the severity level in the specified reference
6.8.1 When the source has been placed perpendicu-
radiograph, that part of the casting represented by lar to the length of the gas hole, evaluate the production
the production radiograph shall be acceptable. If the radiograph with a shrinkage reference radiograph.
production radiograph shows discontinuities of greater
severity than the reference radiograph, that part of the 6.8.2 When the source has been placed diametri-
casting shall be rejected. cally or into the diameter of the gas hole, evaluate the
production radiograph with a gas reference radiograph.
6.3 An area of like size to the reference radiograph
shall be the unit area by which the production radiograph 6.9 A diffraction mottling pattern can occur on
is evaluated, and any such area or any area that shares films of parts and sections where the grain size is large
a discontinuity with an adjacent film area shall meet enough to be an appropriate fraction of the material
the requirements as defined for acceptability. When the thickness (Note 5). If diffraction mottling is suspected,
area of interest of a production radiograph is less than there are a number of ways to demonstrate its presence.
the unit area, such area of interest shall be prorated The diffraction mottling pattern shown in these cases
to the reference radiographic area. is dependent principally upon the crystal geometry and
6.4 When two or more categories of discontinuity the orientation of the crystals to the incident radiation.
are present in the same production radiograph, the Therefore, for a given specimen, any change in this
predominating discontinuities, if unacceptable, shall orientation will affect the diffraction pattern dramati-
govern without regard to the other categories of disconti- cally. This can be accomplished by a slight, 1 to 5
nuities, and the casting rejected until satisfactorily re- tilt of the part, with respect to the radiation beam or
paired. simply by shifting the center line of the radiation beam
to a slightly different location from the first exposure.
6.5 When two or more categories of discontinuity Indications from any porosity, shrinkage, or other dis-
are present to an extent equal to the maximum permissi- continuity will move only slightly, while any mottling
ble level as shown in the pertinent standards for each patterns present will change dramatically. If it is neces-
category, then that part of the casting shall be judged sary or desirable to eliminate the mottling, the kV may
by the most representative reference radiograph. be raised to reduce the amount of diffraction radiation.
6.6 Reference radiographs are provided showing However, caution should be used so that the kV is
a variety of forms of shrinkage cavities. Production not raised to the point that sensitivity is reduced exces-
radiographs showing shrinkage shall be judged by the sively. If diffraction mottling is demonstrated to be
most representative reference radiograph. present on a radiograph, this condition shall not be
considered as prejudicial in evaluating the radiograph.
6.7 Production radiographs showing porosity, gas,
or inclusions shall be evaluated by the overall condition NOTE 5 Mottling is often associated with thin sections of
austenitic steels, and copper base alloys such as copper nickel, tin
with regard to size, number, and distribution. The bronzes, and nickel copper.
aggregate size of the discontinuities shall not exceed
the total accumulation in area of the discontinuities of 6.10 Hot tears and cracks exhibited on production
the reference radiograph. It is not the intent that the radiographs may at times resemble linear type shrinkage.
maximum size of the illustrated discontinuity shall be When doubt exists whether such indications are cracks
the limiting size for a single production radiographic or tears, or are linear shrinkage, all surfaces in the
discontinuity, or that the number of discontinuities area of interest shall be ground and magnetic particle
shown on the reference radiograph shall be the limiting or liquid penetrant inspected as applicable. The extent
number of production radiographs. Also, caution should and depth of grinding may require engineering judgment.
be exercised in judging a large discontinuity against a If the indication does not appear on the surface, it
collection of small discontinuities on the basis of size shall be considered to be shrinkage.
319
SE-446 1998 SECTION V SE-446
7. Keywords
7.1 castings; discontinuities, gamma rays; reference
radiographs; steel; x-ray
320
SE-747 ARTICLE 22 RADIOGRAPHIC STANDARDS SE-747
Practice SE-747 in Section V of that Code. 5 Annual Book of ASTM Standards, Vol 03.03.
321
TABLE 1 TABLE 2
WIRE IQI SIZES AND WIRE IDENTITY NUMBERS WIRE DIAMETER TOLERANCES (mm)
0.032 (0.81) 11 0.10 (2.5) 16 Wire Diameter (d), in. Tolerance, in.
0.040 (1.02) 12 0.126 (3.2) 17
0.050 (1.27) 13 0.160 (4.06) 18 0.000 < d 0.005 0.0001
0.063 (1.6) 14 0.20 (5.1) 19 0.005 < d 0.010 0.0002
0.080 (2.03) 15 0.25 (6.4) 20 0.010 < d 0.020 0.0004
0.100 (2.5) 16 0.32 (8) 21 0.020 < d 0.063 0.0008
AThe 0.0032 wire may be used to establish a special quality level as
0.063 < d 0.160 0.0012
0.160 < d 0.320 0.0020
agreed upon between the purchaser and the supplier.
322
323
324
325
1T, 2T, and 4T holes in the IQI. This table can be constituent. The materials are listed in order of increas-
used for determining 1T, 2T, and 4T quality levels. ing radiation absorption.
Appendix X1 gives the equation for calculating other
equivalencies if needed. 7.1.3 The heavy metal groups, steel, copper-base,
nickel-base, and kindred alloys, are identified 1 through
6.2 In specifying quality levels, the contract, purchase 5. The materials increase in radiation absorption with
order, product specification, or drawing should clearly increasing numerical designation.
indicate the thickness of material to which the quality
level applies. Careful consideration of required quality 7.1.4 Common trade names or alloy designations
levels is particularly important. have been used for clarification of the pertinent mate-
rials.
7. Material Groups
7.1.5 The materials from which the IQI for the
7.1 General: group are to be made are designated in each case and
7.1.1 Materials have been designated in eight these IQIs are applicable for all materials listed in
groups based on their radiographic absorption character- that group. In addition, any group IQI may be used
istics: groups 03, 02, and 01 for light metals and groups for any material with a higher group number, provided
1 through 5 for heavy metals. the applicable quality level is maintained.
7.1.2 The light metal groups, magnesium (Mg), 7.2 Materials Groups:
aluminum (Al), and titanium (Ti), are identified 03,
02, and 01 respectively, for their predominant alloying 7.2.1 Materials Group 01:
326
7.2.1.1 Image quality indicators (IQIs) shall be 7.2.4.1 Image quality indicators (IQIs) shall be
made of titanium or titanium shall be the predominant made of carbon steel or Type 300 series stainless steel.
alloying constituent.
7.2.1.2 Use on all alloys of which titanium is 7.2.4.2 Use on all carbon steel, low-alloy steels,
the predominant alloying constituent. stainless steels, and manganese-nickel-aluminum bronze
(Superston).6
7.2.2 Materials Group 02:
7.2.2.1 Image quality indicators (IQIs) shall be 7.2.5 Materials Group 2:
made of aluminum or aluminum shall be the predomi-
nant alloying constituent. 7.2.5.1 Image quality indicators (IQIs) shall be
made of aluminum bronze (Alloy No. 623 of Specifica-
7.2.2.2 Use on all alloys of which aluminum tion B 150) or equivalent, or nickel-aluminum bronze
is the predominant alloying constituent. (Alloy No. 630 of Specification B 150) or equivalent.
7.2.3 Materials Group 03:
7.2.5.2 Use on all aluminum bronzes and all
7.2.3.1 Image quality indicators (IQIs) shall nickel-aluminum bronzes.
be made of magnesium or magnesium shall be the
predominant alloying constituent.
7.2.6 Materials Group 3:
7.2.3.2 Use on all alloys of which magnesium
is the predominant alloying constituent.
6 Superston is a registered trademark of Superston Corp., Jersey
7.2.4 Materials Group 1: City, NJ.
327
TABLE 4
WIRE SIZES EQUIVALENT TO CORRESPONDING 1T, 2T, AND 4T HOLES IN VARIOUS HOLE TYPE PLAQUES
Plaque Thickness, Plaque IQI Identification Diameter of wire with EPS of hole in plaque, in. (mm)
in. (mm) Number 1T 2T 4T
0.005 (0.13) 5 0.0038 (0.09) 0.006 (0.15)
0.006 (0.16) 6 0.004 (0.10) 0.0067 (0.18)
0.008 (0.20) 8 0.0032 (0.08) 0.005 (0.13) 0.008 (0.20)
0.009 (0.23) 9 0.0035 (0.09) 0.0056 (0.14) 0.009 (0.23)
0.010 (0.25) 10 0.004 (0.10) 0.006 (0.15) 0.010 (0.25)
0.012 (0.30) 12 0.005 (0.13) 0.008 (0.20) 0.012 (0.28)
0.015 (0.38) 15 0.0065 (0.16) 0.010 (0.25) 0.016 (0.41)
0.017 (0.43) 17 0.0076 (0.19) 0.012 (0.28) 0.020 (0.51)
0.020 (0.51) 20 0.010 (0.25) 0.015 (0.38) 0.025 (0.63)
0.025 (0.64) 25 0.013 (0.33) 0.020 (0.51) 0.032 (0.81)
0.030 (0.76) 30 0.016 (0.41) 0.025 (0.63) 0.040 (1.02)
0.035 (0.89) 35 0.020 (0.51) 0.032 (0.81) 0.050 (1.27)
0.040 (1.02) 40 0.025 (0.63) 0.040 (1.02) 0.063 (1.57)
0.050 (1.27) 50 0.032 (0.81) 0.050 (1.27) 0.080 (2.03)
0.060 (1.52) 60 0.040 (1.02) 0.063 (1.57) 0.100 (2.54)
0.070 (1.78) 70 0.050 (1.27) 0.080 (2.03) 0.126 (3.20)
0.080 (2.03) 80 0.063 (1.57) 0.100 (2.54) 0.160 (4.06)
0.100 (2.5) 100 0.080 (2.03) 0.126 (3.20) 0.200 (5.08)
0.120 (3.05) 120 0.100 (2.54) 0.160 (4.06) 0.250 (6.35)
0.140 (3.56) 140 0.126 (3.20) 0.200 (5.08) 0.320 (8.13)
0.160 (4.06) 160 0.160 (4.06) 0.250 (6.35)
0.200 (5.08) 200 0.200 (5.08) 0.320 (8.13)
0.240 (6.10) 240 0.250 (6.35)
0.280 (7.11) 280 0.320 (8.13)
7 Inconelis a registered trademark of The International Nickel Co., 9 All Haynes alloys are registered trademarks of Union Carbide Corp.,
Inc., Huntington, WV 25720. New York, NY.
8 Monel is a registered trademark of The International Nickel Co., 10 All Hastelloys and Haynes Stellite alloys are registered trademarks
328
GMR-235 Alloy, Haynes Alloy No. 93, Inconel X,7 percentage figure is based on the radiographic density
Inconel 718, and Haynes Stellite Alloy No. S-816. of the IQI material.
(3) Group 4 Hastelloy Alloy F, Hastelloy Alloy
7.3.2 It shall always be permissible to use IQIs
X, and Multimeter Alloy Rene 41.
of similar composition as the material being examined.
(4) Group 5 Alloys in order of increasing attenua-
tion: Hastelloy Alloy B, Hastelloy Alloy C, Haynes
Stellite Alloy No. 31, Thetaloy, Haynes Stellite No. 3, 8. Image Quality Indicator (IQI) Certification
Haynes Alloy No. 25. Image quality indicators (IQIs) 8.1 Documents shall be provided by the IQI manufac-
of any of these materials are considered applicable for turer attesting to the following:
the materials that follow it.
8.1.1 IQI identification alternate, if used.
NOTE 2 The committee formulating these recommendations
recommends other materials may be added to the materials groups
8.1.2 Material type.
listed as the need arises or as more information is gained, or that 8.1.3 Conformance to specified tolerances for di-
additional materials groups may be added.
mensional values.
7.3 Method for Other Materials: 8.1.4 ASTM standard designation, for example,
ASTM E 747 (year designation) used for manufac-
7.3.1 For materials not herein covered, IQIs of turing.
the same materials, or any other material, may be used
if the following requirements are met. Two blocks of
equal thickness, one of the material to be examined 9. Precision and Bias
(production material) and one of the IQI material, shall 9.1 Precision and Bias No statement is made
be radiographed on one film by one exposure at the about the precision or bias for indicating the quality
lowest energy level to be used for production. Transmis- of images since the results merely state whether there
sion densitometer measurements of the radiographic is conformance to the criteria for success specified in
image of each material shall be made. The density of this practice.
each image shall be between 2.0 and 4.0. If the image
density of the IQI material is within 1.00 to 1.15 times
10. Keywords
(0% to +15%) the image density of the production
material, IQIs made of that IQI material may be 10.1 density; image quality level; IQI; radiologic;
used in radiography of that production material. The radiology; x-ray and gamma radiation
ANNEX
(Mandatory Information)
329
330
331
332
332.1
TABLE A1.1
PENETRAMETER SIZES WIRE DIAMETER, in. (mm)
SET A SET B
332.2
APPENDIX
(Nonmandatory Information)
332.3
FIG. X1.1 CONVERSION CHART FOR 2-T QUALITY LEVEL HOLES TO PERCENTAGE WIRE SENSITIVITY
332.4
FIG. X1.2 CONVERSION CHART FOR 1-T QUALITY LEVEL HOLES TO PERCENTAGE WIRE SENSITIVITY
332.5
333
SE-999 1998 SECTION V SE-999
4. Significance and Use 5.3.3 If large tanks are used for mixing, carefully
mark the volume levels to be certain that volumes are
4.1 The provisions in this guide are intended to
correct.
control the reliability or quality of the image develop-
ment process only and are not intended for controlling 5.3.4 Use of impeller-type mixers provides rapid,
the acceptability or quality of industrial radiographic thorough mixing but take care to position the impeller
films or of the materials or products radiographed. It at such an angle and depth that the minimum amount
is further intended that this guide be used as an adjunct of air will be drawn into the solution. Over-mixing
to and not a replacement for Guide E 94. of the solutions can cause oxidation, especially with
developers, and should be avoided. Rinse the shaft,
impeller, and mounting clamp with water after use.
5. Chemical Mixing for Manual and Automatic
Processes 5.4 Maintaining Equipment:
5.1 Any equipment that comes in contact with pro- 5.4.1 Immediately clean all mixing equipment
cessing solutions should be made of glass, hard rubber, after use.
polyethylene, PVC, enameled steel, stainless steel, or 5.4.2 In addition to cleaning equipment immedi-
other chemically inert materials. This includes materials ately after use, wash any mixing apparatus that has
such as plumbing, mixing impellers, and the cores of been idle for a long period of time to eliminate dust
filter cartridges. Do not allow materials such as tin, and dirt that may have accumulated.
copper, steel, brass, aluminum, or zinc to come into
contact with processing solutions. These materials can 5.4.3 Processing hangers and tanks should be free
cause solution contamination that may result in film of corrosion and chemical deposits. Encrusted deposits
fogging or rapid oxidation. that accumulate in tanks, trays, and processing equip-
ment and that are difficult to remove by conventional
5.2 Mixing Chemicals: cleaning can be removed by using the specially formu-
lated cleaning agents recommended by the chemical or
5.2.1 Do not mix powdered chemicals in processor
equipment manufacturer.
tanks, since undissolved particles may be left in the
square corners of the tank. Mix solutions in separate
containers made from materials specified in 4.1. 6. Storage of Solutions
5.2.2 Carefully follow the manufacturers package 6.1 In Original Containers Follow the manufactur-
directions or formulas for mixing the chemicals. Start ers storage and capacity recommendations packaged
with the correct volume of water at the temperature with the chemicals. Do not use chemicals that have
specified in the instructions, and add chemicals in the been stored longer than recommended.
order listed. 6.2 In Replenisher or Process Tanks Wherever
5.2.3 Caution During the mixing and use of possible, protect solutions in tanks with floating lids
photographic processing chemicals, be sure to observe and dust covers. In addition to preventing contaminants
all precautionary information on chemical containers from entering solutions, floating lids and dust covers
and in instructions. help to minimize oxidation and evaporation from the
surface of the solutions. Evaporation can concentrate
5.3 Contamination of Solutions: solutions and reduce temperatures causing precipitation
5.3.1 Thoroughly clean all mixing equipment im- of some of the solution constituents.
mediately after use to avoid contamination when the 6.2.1 Store replenisher solutions for small volume
next solution is mixed. When mixing fixer from powder, operations in airtight containers. The caps of these
make sure to add the powder carefully to the water containers should be free of corrosion and foreign
in the mixing tank so that fixer dust does not get into particles that could prevent a tight fit.
other processing solutions. When mixing any chemical,
protect nearby tank solutions with floating lids and 6.3 Temperature Store all solutions at normal
dust covers. The use of a vent hood is recommended room temperature, between 40 to 80F (4 to 27C).
as a safety precaution. Storing solutions, particularly developer, at elevated
temperatures can produce rapid oxidation resulting in
5.3.2 The water supply should either be distilled loss of activity and a tendency to stain the film. Storage
or filtered so that it is clean and sediment-free. at too low a temperature can cause some solution to
334
SE-999 ARTICLE 22 RADIOGRAPHIC STANDARDS SE-999
crystallize, and the crystals may not redissolve even time is included. Draining time should be consistent
with heating and stirring. from solution to solution. The darkroom timers used
should be periodically checked for accuracy.
6.4 Deterioration Photographic chemicals can
deteriorate either with age or with usage. Carefully 7.1.4 Agitate at specified intervals for the times
follow the manufacturers recommendations for storage recommended by the film or solution manufacturer.
life and useful capacity. Discard processing solutions
when the recommended number of films have been 7.1.5 During film processing certain constituents
processed or the recommended storage life of the within the solutions undergo chemical transformations
prepared solution has been reached, whichever oc- that render them useless for further processing functions.
curs first. In addition, some solution adheres to the film and is
carried on into the next solution during processing. In
6.5 Contamination:
order to compensate for these reductions in solution
6.5.1 Liquid chemicals are provided in containers activity and volume, add replenishment solution. The
with tight-fitting tops. To avoid contamination, never volume of replenishment necessary is governed primar-
interchange the top of one container with another. ily by the number, size, and density of films processed.
Manufacturers recommendations for replenishment are
6.5.2 Clearly label replenisher storage tanks with based on these criteria and will generally provide
the solution that they contain and use that container suitable results for the expected life of the solution.
only with that solution. If more than one developer or In any case, maintain solution levels to ensure complete
one fixer formulation are being used, a separate replen- immersion of the film.
isher tank should be dedicated to each chemical. Differ-
ences in developer or fixer formulations from one 7.1.6 The functional constituents in a freshly mixed
manufacturer to another may contaminate similar solu- developer solution tend to overreact on the initial films
tions. processed and may develop unexposed areas on the
films. For this reason, measures should be taken to
stabilize the activity of the solution and thus season
7. Processing
the developer. This can be accomplished by the use
7.1 Manual Processing: of developer starter solution or by processing a series
of seasoning films (see Note 1) in the freshly mixed
7.1.1 Follow the temperature recommendations
solution. When using developer starter solution follow
from the film or solution manufacturer and check
the manufacturers recommendations for the product.
thermometers. Check thermometers and temperature-
When using seasoning films expose the films with
controlling devices periodically to be sure that the
visible light and then develop these films in the solution
process temperatures are correct. Process temperatures
to be seasoned. Use three 14 by 17-in. (35 by 43-cm)
should be checked at least once per shift. Keep the
films, or equivalent, per gallon (3.8 L) of developer.
temperature of the stop (if used), fixer, and wash water
within 65F (63C) of the developer temperature. NOTE 1 Seasoning films may be new films or films that may
not be generally suitable for production purposes due to excessive
7.1.2 Caution An unprotected mercury-filled gross fog (base plus fog) density, expiration of shelf life, or other
thermometer should never be used for photographic reasons.
processing applications because accidental breakage
could result in serious mercury contamination of the
7.1.7 Handle all films carefully during the pro-
process.
cessing cycle and allow adequate time for the film to
7.1.3 Control of processing solution temperature sufficiently drain before transferring it to the next
and immersion time relationships are instrumental con- solution. The use of a stop bath or clear water rinse
siderations when establishing a processing procedure between developing and fixing may also be appropriate.
that will consistently produce radiographs of desired The stop bath or clear water rinse serves to arrest
density and quality. The actual time and temperature development and also aids in minimizing the amount of
relationships established are governed largely by the developer carried over into the fixer solution. Insufficient
industrial radiographic films and chemicals used and bath-to-bath drain time may cause excessive solution
should be within the limits of the manufacturers recom- carry-over which can contaminate and shorten the life
mendations for those materials. When determining the of solutions in addition to causing undesirable effects
immersion time for each solution assure that the draining on processed radiographs.
335
SE-999 1998 SECTION V SE-999
7.1.8 When washing films, a wettening agent may 7.2.5 For seasoning freshly mixed developer solu-
be appropriate to use to prevent water spots and streak- tion, refer to the provisions in 7.1.5.
ing during drying.
7.2.6 Always fill the fixer tank first, following
7.1.9 Caution Prior to placing films in the the manufacturers instructions, then rinse and fill the
dryer, ensure that the dryer is clean and that adequate developer tank. This minimizes the possibility of fixer
heat and ventilation are provided. During drying, visu- accidentally splashing into the developer solution. When
ally examine the films to determine the length of time replacing or removing processor racks, always use
required for sufficient drying. a splash guard to further reduce the possibility of
contamination.
7.2 Automated Processing:
7.2.7 Drying:
7.2.1 Immersion time and solution temperature
7.2.7.1 Make sure the dryer is clean and that
relationships can be more closely controlled with auto-
no foreign material has settled on the rollers. Routinely
matic processing since the equipment provides external
examine the ventilation system to ensure that air paths
gages for monitoring purposes. As a general guideline,
are not blocked and that films are uniformly dried.
follow the manufacturers recommendations for indus-
The heat setting used for air temperature should be
trial processing materials. However, the actual procedure
compatible with the film manufacturers recommenda-
used should be based on the variables encountered
tions.
by the user and his particular needs. Check solution
temperatures daily with a thermometer to ensure that the 7.2.7.2 The dryer efficiency can be tested by
processors thermometers are accurate [61F (0.5C)]. processing six consecutive 14 by 17-in. (35 by 43-cm)
production films, or equivalent, and examining them
7.2.2 Check the machine speed by measuring the
immediately after the drying cycle is complete. If
time it takes for a given length of film to pass a
damp or undried areas are observed, increase the dryer
specific point. (For example, if the indicated machine
temperature. Should an increase in temperature not dry
speed is 2 ft/min, place two marks on a length of film
the film, retest the fixer activity.
1 ft apart. The second mark should pass a specific
location, such as the entrance to the processor, exactly 7.3 Dry Processing:
30 s after the first mark has passed the same point.)
An optional method for measuring processor speed is 7.3.1 Follow manufacturers recommendations for
to install a tachometer on the main drive motor and thermal processor warm-up requirements.
determine desired RPM/processing speed relationships. 7.3.2 Follow time-temperature recommendations
from the manufacturer.
7.2.3 Agitation is provided by the action of the
processor rollers, recirculation pumps, wash water flow,
and no external agitation is needed. 8. Activity Testing of Solutions for Manual and
Automatic Processing
7.2.4 For processors with replenishment systems,
use the replenishment rates recommended by the film 8.1 Developer A suggested method of testing
or solution manufacturer. developer activity is by processing a production radio-
graphy with a known aim density in the area of interest,
7.2.4.1 Accurate replenishment increases the use- and then measuring the actual density in that area. The
ful life of solutions to a great extent by replacing actual density should be within 60.15 log E units of
ingredients that are depleted and maintains the process the expected aim density.
at a constant, efficient level.
NOTE 2 The term known aim density refers to an area on a
routinely radiographed part (such as a flange or a step wedge) whose
7.2.4.2 Check replenishment systems at least thickness or composition is consistent. This area provides a benchmark
daily to ensure that correct volumes are being injected density for the process, and can serve the function normally associated
into the solutions. For installations processing very with a process control strip.
large amounts of film (in excess of two tank turnovers
8.2 Fixer:
of replenisher per week), checks on replenishment rates
should be made more frequently. Processor manufactur- 8.2.1 Fixer solution activity can be tested by
ers recommendations will generally provide an ade- determining the time required to remove the silver from
quate procedure for checking replenishment volumes. an unexposed film. The film should be periodically
336
SE-999 ARTICLE 22 RADIOGRAPHIC STANDARDS SE-999
agitated during processing. An active fixer solution is also recommended to retard the growth of organisms
should remove the silver (the cloudy appearance in the within the wash bath.
fixer bath should disappear) in approximately one-half
of the time recommended for the process. 9. Records
8.2.2 If physical examination shows unfixed spots 9.1 Accurate records should be kept of the following
or areas, the fixer should be discarded. Unfixed areas items:
may appear as dull, nonreflective areas that may be
yellowish in color depending on the actual lack of 9.1.1 Brand name and model of processor, if used.
fixer activity. 9.1.2 Brand names and batch number of chemi-
cals used.
8.3 Wash:
9.1.3 Time of development.
8.3.1 Proper washing is necessary to remove resid-
ual fixer from the film. If not removed from the film, 9.1.4 Temperature of processing chemicals.
these chemicals will cause subsequent damage (staining) 9.1.5 Date new chemicals were placed in use.
and deterioration of the radiographic image, especially
in low density areas. 9.1.6 Replenishment rates.
337
SE-1025 ARTICLE 22 RADIOGRAPHIC STANDARDS SE-1025
Practice SE-1025 in Section II of that Code. 4 Annual Book of ASTM Standards, Vol 02.04.
3 Annual Book of ASTM Standards, Vol 02.01. 5 Annual Book of ASTM Standards, Vol 03.03.
339
SE-1025 1998 SECTION V SE-1025
NOTE 1 This practice does not recommend or suggest specific NOTE 3 These groups were established experimentally at 180
IQI sets to be procured. Section 5 is an aid in selecting IQIs based kV on 34-in. (19-mm) thick specimens. They apply from 125 kV
on specific needs. to the multivolt range.
340
SE-1025 ARTICLE 22 RADIOGRAPHIC STANDARDS SE-1025
341
SE-1025 1998 SECTION V SE-1025
TABLE 1
TYPICAL IMAGE QUALITY LEVELS
342
SE-1025 ARTICLE 22 RADIOGRAPHIC STANDARDS SE-1025
7.3.3.1 Image quality indicators (IQIs) shall be 7.3.8.2 Use on tin bronzes including gun-metal
made of titanium or titanium shall be the predominant and valve bronze, leaded-tin bronze of higher lead
alloying constituent. content than valve bronze. Group 5 IQIs may be used
on bronze of higher lead content since leaded bronze
7.3.3.2 Use on all alloys of which titanium is increases in attenuation with increase in lead content.
the predominant alloying constituent. This would be equivalent to using a lower group IQI.
NOTE 4 In developing the eight listed materials groups, a number
7.3.4 Materials Group 1: of other trade names or other nominal alloy designations were
evaluated. For the purpose of making this practice as useful as
7.3.4.1 Image quality indicators (IQIs) shall be possible, these materials are listed and categorized, by group, as
made of carbon steel or Type 300 series stainless steel. follows:
(1) Group 2 Haynes Alloy IN-100.9
(2) Group 3 Haynes Alloy No. 713C, Hastelloy D,10 G.E. Alloy
7.3.4.2 Use on all carbon steel, all low-alloy SEL, Haynes Stellite Alloy No. 21,10 GMR-235 Alloy, Haynes Alloy
steels, all stainless steels, manganese-nickel-aluminum No. 93, Inconel X,7 Inconel 718, and Haynes Stellite Alloy No. S-816.
bronze (Superston).6 (3) Group 4 Hastelloy Alloy F, Hastelloy Alloy X, and Multime-
ter Alloy Rene 41.
(4) Group 5 Alloys in order of increasing attenuation: Hastelloy
7.3.5 Materials Group 2: Alloy B, Hastelloy Alloy C, Haynes Stellite Alloy No. 31, Thetaloy,
Haynes Stellite No. 3, Haynes Alloy No. 25. IQIs of any of these
7.3.5.1 Image quality indicators (IQIs) shall be materials are considered applicable for the materials that follow it.
made of aluminum bronze (Alloy No. 623, of Specifica-
tion B 150) or equivalent, or nickel-aluminum bronze NOTE 5 The committee formulating these recommendations,
recommended other materials may be added to the materials groups
(Alloy No. 630 of Specification B 150) or equivalent.
7.3.5.2 Use on all aluminum bronzes and all 7 Inconelis a registered trademark of The International Nickel Co.,
nickel-aluminum bronzes. Inc., Huntington, WV 25720.
8 Monel is a registered trademark of The International Nickel Co.,
7.3.6 Materials Group 3: Inc., Huntington, WV 25720.
9 All Haynes alloys are registered trademarks of Union Carbide Corp.,
343
SE-1025 1998 SECTION V SE-1025
listed as the need arises or as more information is gained, or that 7.4.2 It shall always be permissible to use IQIs
additional materials groups may be added.
of similar composition as the material being examined.
7.4 Radiographic Method for Other Materials:
8. IQI Certification
7.4.1 For materials not herein covered, IQIs of 8.1 Records shall be available that attest to the
the same materials, or any other material, may be used conformance of the material type, grouping (notches),
if the following requirements are met. Two blocks of and dimensional tolerances of the IQIs specified by
equal thickness, one of the material to be examined this practice.
(production material) and one of the IQI material, shall
be radiographed on one film by one exposure at the
lowest energy level to be used for production. Transmis- 9. Precision and Bias
sion densitometer readings for both materials shall be 9.1 Precision and Bias No statement is made
read from the film and shall be between 2.0 and about the precision or bias for indicating the quality
4.0 (radiographic) density for both materials. If the of radiographs since the results merely state whether
radiographic image density of the material from which there is conformance to the criteria for success specified
the IQIs are to be fabricated is within +15 to 0% in this practice.
of the radiographic image density of the production
material, the IQI material may be used to fabricate
10. Keywords
IQIs for examination of the production material. The
percentage figure is based on the radiographic density 10.1 density; image quality level; IQI; radiologic;
of the IQI material. radiology; X-ray and gamma radiation
APPENDIX
(Nonmandatory Information)
!
100 TH X 0.5
ap ,
X 2
100H 100 0.0625
Bp p p 12.5%
where: X 0.5
ap equivalent IQI sensitivity, %,
Xp section thickness to be examined, in.,
Tp IQI Thickness, in., and
Hp hole diameter, in.
X1.2 Alternate method for determining EPS using X1.3 Proceed to the nomograph (Fig. X1.1) and
Fig. X1.1 Nomograph: draw a line joining the 1.0% Value A and the 12.5%
Value B and look on the center percent scale where
Example:
the line crosses it and read the answer 2.5%. Thus
11 OConnor,
under the given conditions, equivalent IQI (penetrame-
D. T., and Criscuolo, E. L., The Quality of Radiographic
Inspection, ASTM Bulletin, ASTM, Vol 213, 1956, p. 52. ter) sensitivity (EPS) is 2.5%.
344
SE-1025 ARTICLE 22 RADIOGRAPHIC STANDARDS SE-1025
345
SE-1030 ARTICLE 22 RADIOGRAPHIC STANDARDS SE-1030
Test Method SE-1030 in Section II of that Code. 3 Annual Book of ASTM Standards, Vol 03.03
347
SE-1030 1998 SECTION V SE-1030
2.2 ASNT/ANSI Standards: 5.1.4 Procedure Requirements (see 9.1, 9.1.1, 9.3,
Recommended Practice No. SNT-TC-1A Personnel and 9.7.7) shall be specified.
Qualification and Certification in Nondestructive 5.1.5 Records Record retention (see 12.1) shall
Testing4 be specified.
CP-189 Qualification and Certification of Nondestructive
Testing Personnel4
6. Apparatus
2.3 Military Standard:
6.1 Radiation Sources:
MIL-STD-410 Nondestructive Testing Personnel Quali-
fication and Certification5 6.1.1 X Radiation Sources Selection of appro-
priate X-ray voltage and current levels is dependent
upon variables regarding the specimen being examined
(material type and thickness) and economically permissi-
3. Terminology ble exposure time. The suitability of these X-ray parame-
3.1 Definitions For definitions of terms used in ters shall be demonstrated by attainment of required
this test method, see Terminology E 1316. penetrameter (IQI) sensitivity and compliance with all
other requirements stipulated herein. Guide E 94 con-
tains provisions concerning exposure calculations and
charts for the use of X-ray sources.
4. Significance and Use
6.1.2 Gamma Radiation Sources Isotope
4.1 The requirements expressed in this test method sources, when used, shall be capable of demonstrating
are intended to control the quality of the radiographic the required radiographic sensitivity.
images, to produce satisfactory and consistent results,
6.2 Film Holders and Cassettes Film holders and
and are not intended for controlling the acceptability
cassettes shall be light-tight and shall be handled prop-
or quality of materials or products.
erly to reduce the likelihood that they may be damaged.
They may be flexible vinyl, plastic, or any durable
4 Available from the American Society for Nondestructive Testing, material; or, they may be made from metallic materials.
(ASNT), 1711 Arlingate Plaza, P.O. Box 28518, Columbus, OH In the event that light leaks into the film holder and
43228.
5 Available from Standardization Documents Order Desk, Bldg. 4
produces images on the film extending into the area
Section D, 700 Robbins Ave., Philadelphia, PA 19111-5094, Attn: of interest, the film shall be rejected. If the film holder
NPODS. exhibits light leaks, it shall be repaired before reuse
348
SE-1030 ARTICLE 22 RADIOGRAPHIC STANDARDS SE-1030
or discarded. Film holders and cassettes should be 6.6 Penetrameters (IQI) Unless otherwise specified
routinely examined to minimize the likelihood of by the applicable job order or contract, only those
light leaks. penetrameters that comply with the design and identifi-
cation requirements specified in Practice E 747 or
6.3 Intensifying Screens: Practice E 1025 shall be used.
6.3.1 Lead-Foil Screens: 6.7 Shims and Separate Blocks Shims or separate
blocks made of the same or radiographically similar
6.3.1.1 Intensifying screens of the lead-foil type materials (as defined in Method E 142) may be used
are generally used for all production radiography. Lead- to facilitate penetrameter positioning. There is no restric-
foil screens shall be of the same approximate area tion on shim or separate block thickness provided
dimensions as the film being used and they shall be the penetrameter and area-of-interest density tolerance
in direct contact with the film during exposure. requirements of 9.7.6.2 are met.
6.3.1.2 For X-ray voltages between 200 kV and 6.8 Radiographic Location and Identification Mark-
1 MeV, front and rear screen thicknesses shall be a ers Lead numbers and letters are used to designate
minimum of 0.005 in. (0.13 mm) thick. Below 200 the part number and location number. The size and
kV, front screen thicknesses up to 0.005 in. (0.13 mm) thickness of the markers shall depend on the ability
and rear screen thicknesses of at least 0.005 in. of the radiographic technique to image the markers on
(0.13 mm) should be used if they improve radiographic the radiograph. As a general rule, markers 116 in. (1.58
quality. For isotope and high-voltage X-radiography mm) thick will suffice for most low energy (less than
(greater than 1 MeV) increased thicknesses may be 1 MeV) X-ray and Iridium-192 radiography; for higher
appropriate for improvements in radiographic quality energy radiography it may be necessary to use markers
and should be used accordingly. Intermediate screens that are 18 in. (3.17 mm) or more thick.
(between multiloaded film) may be used if desired.
6.9 Radiographic Density Measurement Apparatus
6.3.1.3 Sheet lead, with or without backing, Either a transmission densitometer or a step-wedge
used for screens should be visually examined for dust, comparison film shall be used for judging film density
dirt, oxidation, cracking or creasing, foreign material requirements. Step wedge comparison films or densitom-
or other conditions that could render undesirable nonrel- eter calibration, or both, shall be verified by comparison
evant images on the film. with a calibrated step-wedge film traceable to the
National Institute of Standards and Technology.
6.3.1 Fluorescent or Fluorometallic Screens:
349
SE-1030 1998 SECTION V SE-1030
stipulated in Appendix X1. In addition, a radiographic 8.7.3 Film Viewing Facilities Viewing facilities
standard shooting sketch (RSS), Fig. X1.1, shall be shall provide subdued background lighting of an inten-
prepared similar to that shown in Appendix X1 and sity that will not cause troublesome reflections, shadows,
shall be available for review during interpretation of or glare on the radiograph. The viewing light shall be
the film. of sufficient intensity to review densities up to 4.0 and
be appropriately controlled so that the optimum intensity
8.2 Radiographic Coverage Unless otherwise spec- for single or superimposed viewing of radiographs may
ified by a purchaser and supplier agreement, the extent be selected.
of radiographic coverage shall be the maximum practical
volume of the casting. Areas that require radiography 8.7.4 Storage of Radiographs When storage is
shall be designated as illustrated in Fig. X1.2(a) and required by the applicable job order or contract, the
(b) of Appendix X1. When the shape or configuration radiographs should be stored in an area with sufficient
of the casting is such that radiography is impractical, environmental control to preclude image deterioration
these areas shall be so designated on drawings or or other damage. The radiograph storage duration and
sketches that accompany the radiographs. Examples location after casting delivery shall be as agreed upon
of casting geometries and configurations that may be between purchaser and supplier. (See Guide E 1254
considered impractical to radiograph are illustrated in for storage information.)
Appendix X2.
8.3 Radiographic Film Quality All radiographs 9. Procedure
shall be free of mechanical, chemical, handling-related,
9.1 Time of Examination Unless otherwise speci-
or other blemishes which could mask or be confused
fied by the applicable job order or contract, radiography
with the image of any discontinuity in the area of
may performed prior to heat treatment and in the as-
interest on the radiograph. If any doubt exists as to
cast, rough-machined, or finished-machined condition.
the true nature of an indication exhibited by the film,
the radiograph shall be retaken or rejected. 9.1.1 Penetrameter (IQI) Selection Unless other-
wise specified in the applicable job order or contract,
8.4 Radiographic Quality Level The applicable
penetrameter (IQI) selection shall be based on the
job order or contract shall dictate the requirements for
following: if the thickness to be radiographed exceeds
radiographic quality level. (See Practice E 1025 or
the design thickness of the finished piece, the penetrame-
Practice E 747 for guidance in selection of quality
ter (IQI) size shall be based on a thickness which does
level.)
not exceed the design thickness of the finished piece
8.5 Acceptance Level Radiographic acceptance by more than 20% or 14 in. (6.35 mm), whichever is
levels and associated severity levels shall be stipulated greater. In no case shall the penetrameter (IQI) size
by the applicable contract, job order, drawing, or other be based on a thickness greater than the thickness to
purchaser and supplier agreement. be radiographed.
8.6 Radiographic Density Limitations Radio- 9.2 Surface Preparation The casting surfaces shall
graphic density in the area of interest shall be within be prepared as necessary to remove any conditions
1.5 to 4.0 for either single or superimposed viewing. that could mask or be confused with internal casting
discontinuities.
8.7 Film Handling:
9.3 Source-to-Film Distance Unless otherwise
8.7.1 Darkroom Facilities Darkroom facilities specified in the applicable job order or contract, geomet-
should be kept clean and as dust-free as practical. ric unsharpness (Ug) shall not be greater than one
Safelights should be those recommended by film manu- percent of the maximum part thickness being interpreted
facturers for the radiographic materials used and should on the radiograph, or 0.070 in. (1.8 mm), whichever
be positioned in accordance with the manufacturers is less. Geometric unsharpness values shall be deter-
recommendations. All darkroom equipment and materi- mined as specified in Guide E 94.
als should be capable of producing radiographs that
are suitable for interpretation. 9.4 Direction of Radiation The direction of radia-
tion shall be governed by the geometry of the casting
8.7.2 Film Processing Radiographic film pro- and the radiographic coverage and quality requirements
cessing shall be controlled in accordance with Guide stipulated by the applicable job order or contract.
E 999. Whenever practicable, place the central beam of the
350
SE-1030 ARTICLE 22 RADIOGRAPHIC STANDARDS SE-1030
radiation perpendicular to the surface of the film. Appen- at least three penetrameters (IQIs) shall be used. On
dix X2 provides examples of preferred source and film partial circumference exposures, a penetrameter (IQI)
orientations and examples of casting geometries and shall be placed at each end of the length of the image
configurations on which radiography is impractical or to be evaluated on the radiograph with the intermediate
very difficult. penetrameters (IQIs) placed at equal divisions of the
length covered. For full circumferential coverage, three
9.5 Back-Scattered Radiation Protection:
penetrameters (IQIs) spaced 120 apart shall be used,
9.5.1 Back-Scattered Radiation (secondary radi- even when using a single length of roll film.
ation emanating from surfaces behind the film, that is,
walls, floors, etc.) serves to reduce radiographic contrast 9.7.4 When an array of individual castings in a
and may produce undesirable effects on radiographic circle is radiographed, the requirements of 9.7.1 or
quality. A 18-in. (3.17 mm) lead sheet placed behind 9.7.2, or both, shall prevail for each casting.
the film generally furnishes adequate protection against 9.7.5 If the required penetrameter (IQI) sensitivity
back-scattered radiation. does not show on any one film in a multiple film
9.5.2 To detect back-scattered radiation, position technique (see 9.11), but does show in composite
a lead letter B [approximately 18 in. (3.17 mm) thick (superimposed) film viewing, interpretation shall be
by 12 in. (12.7 mm) high] on the rear side of the film permitted only by composite film viewing for the
holder. If a light image (lower density) of the lead respective area.
letter B appears on the radiograph, it indicates that
9.7.6 When it is not practicable to place the
more back-scatter protection is necessary. The appear-
penetrameter(s) (IQI) on the casting, a shim or separate
ance of a dark image of the lead letter B should be
block conforming to the requirements of 6.7 may
disregarded unless the dark image could mask or be
be used.
confused with rejectable casting defects.
9.6 Penetrameter (IQI) Placement Place all pene- 9.7.6.1 The penetrameter (IQI) shall be no closer
trameters (IQI) being radiographed on the source side to the film than the source side of that part of the
of the casting. Place penetrameters (IQIs) in the radio- casting being radiographed in the current view.
graphic area of interest, unless the use of a shim or
9.7.6.2 The radiographic density measured adja-
separate block is necessary, as specified in 9.7.6.
cent to the penetrameter (IQI) through the body of the
9.7 Number of Penetrameters (IQIs): shim or separate block shall not exceed the density
measured in the area of interest by more than 15%.
9.7.1 One penetrameter (IQI) shall represent an
The density may be lighter than the area of interest
area within which radiographic densities do not vary
density, provided acceptable quality level is obtained
more than +30% to 15% from the density measured
and the density requirements of 8.6 are met.
through the body of the penetrameter (IQI).
9.7.2 When the film density varies more than 9.7.6.3 The shim or separate block shall be
15% to +30%, two penetrameters (IQIs) used as placed at the corner of the film holder or close to that
follows will be acceptable: if one penetrameter (IQI) part of the area of interest that is furthest from the
shows acceptable sensitivity representing the most dense central beam. This is the worst case position from a
portion of the exposure, and the second penetrameter beam angle standpoint that a discontinuity would be in.
(IQI) shows acceptable sensitivity representing the least
dense portion of the exposure, then these two penetrame- 9.7.6.4 The shim or separate block dimensions
ters (IQIs) shall qualify the exposure location within shall exceed the penetrameter (IQI) dimensions such
these densities, provided the density requirements stipu- that the outline of at least three sides of the penetrameter
lated in 8.6 are met. (IQI) image shall be visible on the radiograph.
9.7.3 For cylindrical or flat castings where more 9.7.7 Film Side Penetrameter (IQI) In the case
than one film holder is used for an exposure, at least where the penetrameter (IQI) cannot be physically
one penetrameter (IQI) image shall appear on each placed on the source side and the use of a separate
radiograph. For cylindrical shapes, where a panoramic block technique is not practical, penetrameters (IQIs)
type source of radiation is placed in the center of the placed on the film side may be used. The applicable
cylinder and a complete or partial circumference is job order or contract shall dictate the requirements for
radiographed using at least four overlapped film holders, film side radiographic quality level (see 8.4).
351
SE-1030 1998 SECTION V SE-1030
9.8 Location Markers The radiographic image of 10.2 Film Evaluation Determine the acceptance
the location markers for the coordination of the casting or rejection of the casting by comparing the radiographic
with the film shall appear on the film, without interfering image to the agreed upon acceptance criteria (see 8.5).
with the interpretation, in such an arrangement that it
is evident that the required coverage was obtained.
These marker positions shall be marked on the casting 11. Reference Radiographs
and the position of the markers shall be maintained
on the part during the complete radiographic cycle. 11.1 Reference Radiographs E 155, E 186, E 192,
The RSS shall show all marker locations. E 272, E 280, E 310, E 446, E 505, E 689, and E
802 are graded radiographic illustrations of various
9.9 Radiographic Identification A system of posi- casting discontinuities. These reference radiographs may
tive identification of the film shall be provided. As a be used to help establish acceptance criteria and may
minimum, the following shall appear on the radiograph: also be useful as radiographic interpretation training
the name or symbol of the inspecting laboratory, the aids.
date, the casting identification number, and whether it
is an original or subsequent exposure.
9.10 Subsequent Exposure Identification All repair 12. Report
radiographs after the original (initial) shall have an
12.1 The following radiographic records shall be
inspection status designation that indicates the reason.
maintained as agreed upon between purchaser and
Subsequent radiographs made by reason of a repaired
supplier:
area shall be identified with the letter R followed
by the respective repair cycle (that is, R-1 for the first 12.1.1 Radiographic standard shooting sketch,
repair, R-2 for the second repair, etc.). Subsequent
radiographs that are necessary as a result of additional 12.1.2 Weld repair documentation,
surface preparation should be identified by the letters
REG. 12.1.3 Film,
9.11 Multiple Film Techniques Two or more films 12.1.4 Film interpretation record containing as a
of equal or different speeds in the same cassette are minimum:
allowed, provided prescribed quality level and density
requirements are met (see 9.7.2 and 9.7.5). 12.1.4.1 Disposition of each radiograph (accept-
able or rejectable),
9.12 Radiographic Techniques:
9.12.1 Single Wall Technique Except as pro- 12.1.4.2 If rejectable, cause for rejection (shrink,
vided in 9.12.2, radiography shall be performed using gas, etc.),
a technique in which the radiation passes through only
one wall. 12.1.4.3 Surface indication verified by visual
examination (mold, marks, etc.), and
9.12.2 Double Wall Technique For castings
with an inside diameter of 4 in. or less, a technique 12.1.4.4 Signature of the film interpreter.
may be used in which the radiation passes through
both walls and both walls are viewed for acceptance
on the same film. An adequate number of exposures 13. Precision and Bias
shall be taken to ensure that required coverage has
been obtained. 13.1 No statement has been made about either the
precision or bias of this test method since the result
9.13 Safety Radiographic procedures shall comply merely states whether there is conformance to the
with applicable city, state, and federal regulations. criteria for success specified in the procedure.
352
SE-1030 ARTICLE 22 RADIOGRAPHIC STANDARDS SE-1030
APPENDICES
(Nonmandatory Information)
X1. RADIOGRAPHIC STANDARD SHOOTING niques for inspection of any particular one. The RSS
SKETCH (RSS) provides a map of location marker placement, directions
for source and film arrangement, and instructions for
X1.1 The radiographic standard shooting sketch (RSS)
all other parameters associated with radiography of a
provides the radiographic operator and the radiographic
casting. This information serves to provide the most
interpreter with pertinent information regarding the ex-
amination of a casting. The RSS is designed to standard- efficient method for controlling the quality and consist-
ize radiographic methodologies associated with casting ency of the resultant radiographic representations.
inspection; it may also provide a means of a purchaser
and supplier agreement, prior to initiation of the inspec- X1.2 The RSS usually consists of an instruction
tion on a production basis. The use of a RSS is sheet and sketch(es) of the casting: the instruction sheet
advantageous due to the many configurations associated specifies the radiographic equipment, materials, and
with castings and the corresponding variations in tech- technique-acceptance parameters for each location; the
sketch(es) illustrate(s) the location, orientation, and the X1.2.1.2 Casting identification including:
source and film arrangement for each location. Figures (a) Drawing number,
X1.1 and X1.2(a) and (b) of this appendix provide a (b) Casting identification number,
typical instruction sheet and sketch sheets. As a mini- (c) Descriptive name (for example, pump casting,
mum, the RSS should provide the following information. valve body, etc.),
All spaces shall be filled in unless not applicable; in (d) Material type and material specification,
those cases, the space shall be marked NA. (e) Heat number, and
(f) Pattern number.
X1.2.1 The instruction sheet should provide the
following:
X1.2.1.1 Company preparing RSS and activity X1.2.1.3 Surface condition at time of radiogra-
performing radiography. phy (as cast, rough machined, finished machined).
354
SE-1030 ARTICLE 22 RADIOGRAPHIC STANDARDS SE-1030
FIG. X1.2(b)
(b) VIEWS ILLUSTRATING LAYOUT AND EXTENT OF COVERAGE
X1.2.1.4 Spaces for approval (as applicable). (i) Required penetrameter (IQI) quality level,
(j) Radiographic acceptance standard, and
X1.2.1.5 Radiographic Technique Parameters (k) Applicable radiographic severity level.
for Each Location:
(a) Radiographic location designation,
X1.2.2 The sketch(es) should provide the fol-
(b) Source type and size,
lowing:
(c) Finished thickness,
(d) Thickness when radiographed,
(e) Penetrameters, X1.2.2.1 Location marker placement.
(f) Source to film distance,
(g) Film type and quantity, X1.2.2.2 Location of foundrys identification pad
(h) Film size, or symbol on the casting.
355
SE-1030 1998 SECTION V SE-1030
X1.2.2.3 Designation of areas that require radiog- pilot radiographs to the purchaser for review. Purchaser
raphy (as applicable). approval of the technique shall be addressed in the
applicable job order or contract.
X1.2.2.4 Designation of areas that are considered
impractical or very difficult to radiograph (see 1.2
and 8.2). X2. PREFERRED SOURCE AND FILM
ALIGNMENT FOR FLANGE
X1.2.2.5 Radiographic source and film arrange-
RADIOGRAPHY AND EXAMPLES OF
ment and radiation beam direction for each location.
AREAS THAT ARE CONSIDERED
NOTE X1.1 The RSS should designate the involved locations IMPRACTICAL TO RADIOGRAPH
and stipulate that the technique for those locations is typical, for
sections of the casting on which a continuing series of locations are X2.1 Preferred Source and Film Alignment for Flange
to be radiographed with the same basic source and film arrangement Radiography The effective use of radiography for
for each location.
assessing material soundness in casting areas where a
flange joins a body is somewhat limited by the source
X1.2.3 Figure X1.1 of this appendix provides a and film alignment that the geometric configuration of
sample RSS that has been developed for a typical these areas requires. The following figures describe
production application, and Fig. X1.2(a) and (b) provide source and film alignments that can be employed and
sample RSS sketches that have been developed for a discusses the limits and benefits of each.
typical production application.
X1.2.4 The RSS may not provide what is consid-
X3. EXAMPLES OF AREAS THAT ARE
ered to be the most effective means of technique control
CONSIDERED TO BE IMPRACTICAL TO
for all radiographic activities, but, in any event, some
RADIOGRAPH
means of technique standardization should be employed.
As a general rule, it is a beneficial practice for the X3.1 Certain casting geometry configuration are inac-
supplier to solicit purchaser approval of the radiographic cessible for conventional source and film arrangements
methodology prior to performing production radiogra- that will provide meaningful radiographic results. These
phy. This generally entails the demonstration of the areas generally involve the juncture of two casting
adequacy of the methodology by submitting the pro- sections. The following illustrations provide typical
posed technique parameters and a corresponding set of examples of such areas.
356
SE-1030 ARTICLE 22 RADIOGRAPHIC STANDARDS SE-1030
FIG. X2.2 PERMISSIBLE SOURCE AND FILM ALIGNMENT WHEN FIG. X2.1
CANNOT BE APPLIED DUE TO CASTING GEOMETRY
357
SE-1030 1998 SECTION V SE-1030
358
SE-1079 ARTICLE 22 RADIOGRAPHIC STANDARDS SE-1079
CALIBRATION OF TRANSMISSION
DENSITOMETERS1
SE-1079
5. Apparatus
1 This practice is under the jurisdiction of ASTM Committee E-7 5.1 Apparatus should consist of the following:
on Nondestructive Testing and is the direct responsibility of Subcom-
mittee E07.01 on Radiology (X and Gamma) Method. 5.1.1 A calibrated step tablet shall be used. The
Current edition approved Aug. 10, 1997. Published February 1998. step tablet may be a NIST X-ray Step Tablet (Standard
Originally published as E 1079-85. Last previous edition E 1079-95.
2 For ASME Boiler and Pressure Vessel Code applications, see related
Practice SE-1079 in Section V of that Code. 4 Available from American National Standards Institute, 11 West
3 Annual Book of ASTM Standards, Vol 03.03. 42nd Street, 13th Floor, New York, NY 10036.
359
Reference Material SRM 1001)5 or alternately a step densities at 0.3, 3.0, and 3.9 steps should not vary
tablet from another supplier, which is traceable to the more than 0.05 density units. If any of the recorded
NIST SRM 1001 X-ray Step Tablet. The step tablet density values vary more than 0.05 density units
shall have at least five step densities ranging from 0.3 from the density values on the calibrated step tablet,
through 3.9. The step tablet may have additional step the linearity of the densitometer is out of tolerance
densities less than 0.3 and greater than 3.9. A calibration and should be corrected.
certificate shall be provided with the step tablet indicat-
ing the tablet ID and recorded values for each step
density. For suppliers of step tablets other than NIST, 7. Records and Associated Documentation
the certificate shall indicate conformance of traceability 7.1 Note and record the calibrated readings, required
to NIST instrumentation used in the calibration process, by 6.1.2 in an appropriate calibration log. A pressure-
applicable ANSI standards used, verification of measure- sensitive label or tag that indicates the date the calibra-
ment on a NIST SRM 1001 step tablet, the ID number tion was performed, and the identification of the individ-
of the SRM 1001 step tablet, and calibration date of ual performing the calibration, may be applied to the
the step tablet. Precautions should be taken in the densitometer to verify the calibration reference check
storage, handling, and use of the step tablet. In the recorded in the calibration log.
event it becomes scratched, blemished, or exhibits other
signs of deleterious wear, it should be replaced immedi- 7.2 An alternative calibration documentation system
ately. The step tablet shall be replaced four years from may be used provided the calibration traceability re-
date of first use. quirements identified in 7.1 can be satisfied and docu-
mented properly.
5.1.2 Transmission Densitometers, with either
direct-scale readout or digital readout displays specifi-
cally manufactured for the purpose of measuring the 8. Periodic Verification
range of film densities described in 5.1.1 may be used.
8.1 Periodic calibration verification checks using the
5.1.3 Manufacturers Operating Instructions for procedure described in Section 6 should be performed
Appropriate Transmission Densitometer. at the beginning of each shift, after 8 h of continuous
operation, or change of apertures, whichever occurs first.
6.1.3 Compare the densities recorded with the 8.2 Consult the Manufacturers Technical Manual
actual density values on the calibrated step tablet or for troubleshooting information.
the density values listed on the calibration certificate.
If the densitometer has been calibrated properly, the
9. Keywords
5 Standard Reference Material 1001 is available from the National 9.1 calibration; densitometer; density; periodic verifi-
Institute of Standards and Technology, Gaithersburg, MD. cation; radiographic film
360
1. Scope 3. Terminology
1.1 This test method covers the determination of the 3.1 For definitions of terms relating to this test
focal size of an iridium-192 radiographic source. The method, refer to Terminology E 1316.
determination is based upon measurement of the image
of the iridium metal source in a projection radiograph
of the source assembly and comparison to the measure- 4. Significance and Use
ment of the image of a reference sample in the same
radiograph. 4.1 One of the factors affecting the quality of a
radiographic image is geometric unsharpness. The de-
1.2 This standard does not purport to address all of gree of geometric unsharpness is dependent upon the
the safety concerns, if any, associated with its use. It focal size of the source, the distance between the source
is the responsibility of the user of this standard to and the object to be radiographed, and the distance
establish appropriate safety and health practices and between the object to be radiographed and the film.
determine the applicability of regulatory limitations This test method allows the user to determine the focal
prior to use. size of the source and to use this result to establish
source to object and object to film distances appropriate
for maintaining the desired degree of geometric un-
sharpness.
360.1
360.2
TABLE 1
EXAMPLES OF TYPICAL X-RAY GENERATOR
OUTPUT REQUIREMENTS FOR RELATED IRIDIUM192
SOURCE ACTIVITIES
Typical X-ray
Subject Iridium192 Source Generator
Radiation Output Requirements
Activity Output
(Curie) (R/h at 1 m) Potential Current
30 14.4 160 kV 5 mA
or 200 kV 3 mA
100 48.0 160 kV 10 mA
or 250 kV 4 mA
200 96.0 160 kV 20 mA
or 250 kV 8 mA
or 300 kV 6 mA
360.3
360.4
360.5
360.6
360.7
360.8
TABLE 1
PINHOLE DIAPHRAGM DESIGN REQUIREMENTS (DIMENSION)A
NOTE The pinhole diaphragm shall be made from one of the following materials:
(1) An alloy of 90% gold and 10% platinum,
(2) Tungsten,
(3) Tungsten carbide,
(4) Tungsten alloy,
(5) Platinum and 10% Iridium alloy, or
(6) Tantalum.
0.3 to 1.2 (0.011 to 0.046) incl 0.030 (0.0011) 0.030 0.005 0.075 0.010
(0.0011 0.0002) (0.0029 0.0004)
>1.2 to 2.5 (0.046 to 0.097) incl 0.075 (0.0029) 0.075 0.005 0.350 0.010
(0.0029 0.0002) (0.014 0.0004)
>2.5 (0.097) 0.100 (0.0039) 0.100 0.005 0.500 0.010
(0.0039 0.0002) (0.02 0.0004)
A See Fig. 3.
B Nominal focal spot dimensions may be obtained from the X-ray tube manufacturer.
360.9
360.10
6.4 Expose the film such that the density of the 6.6.3.1 Direction A Parallel to the axis of
darkest portion of the focal spot image conforms to the tube.
the limits specified in Table 4. Density measurement
shall be as illustrated in Fig. 8. Density shall be 6.6.3.2 Direction B Perpendicular to the axis
controlled by exposure time only. of the tube.
6.5 Process the film in accordance with Guide E 999.
6.6 Focal Spot Measurement:
6.6.1 Back Lighting Back lighting shall be such 7. Calculation of Results
that the focal spot image can be easily and comfortably
viewed. 7.1 Multiply the measured A direction dimension
by a correction factor of 0.7 to determine the actual
6.6.2 Place the magnification graticule (handheld A dimension (see Note 4). The measured B direction
optical comparator) in intimate contact with the film for dimension is representative of actual size.
the measurement determination. Determine an imaginary
box that represents the perceptible edges of the NOTE 4 The need for the 0.7 fractional multiplier for correction
focal spot image [see Fig. 9(a)] for the extremities of the measured image length arises from the fact that the lengthwise
distribution of energy in the focal spots of line-focus tubes tends
measurement. to be peaked in the center and diminishes gradually to zero at the ends.
Hence, the effective length, (that is, resultant effect on radiographic
6.6.3 Measure the focal spot image in two direc- definition and film density distribution) cannot be stated as equal to
tions [see Fig. 9(b)]: the measured length.
360.11
TABLE 3
TEST VOLTAGE AND CURRENT
8. Report
8.1 A report documenting the focal spot size determi-
nation should include the machine model number and
FIG. 6 EXPOSURE SET-UP SCHEMATIC serial number, the X-ray tube serial number, the focal
spot(s) that was measured (some machines have dual
focal spots), the set-up and exposure parameters (for
example, kilovoltage, milliamps, enlargement factor,
and the like) date, name of organization, and estimated
beam time hours (if available).
10. Keywords
10.1 focal spots; pinhole camera; pinhole imaging;
FIG. 7 ALIGNMENT COLLIMATOR x-ray; x-ray tube
360.12
TABLE 4
DENSITY RANGE FOR DARKEST AREA OF FOCAL
SPOT IMAGE (See Fig. 7)
Transmission
Densitometer For images whose For images whose
Aperture minimum dimension minimum dimension is
Diameter, is less than 2 mm greater than 2 mm
mm (in.) (0.078 in.) (0.078 in.)
1 (0.039) 0.8 to 2.0 density 1.0 to 3.0 density
2 (0.078) 0.5 to 1.8 density 1.0 to 3.6 density
360.13
360.14
361
SE-1255 1998 SECTION V SE-1255
host computer, which incorporates the software neces- test object within the radiation beam, and a detection
sary to not only operate the system components, but system. The system may be as simple as a directly
to make accept /reject decisions as well. Systems having viewed fluorescent screen with suitable radiation
a wide range of capabilities between these extremes shielding for personnel protection that meets applicable
can be assembled using available components. Guide radiation safety codes.
E 1000 lists many different system configurations.
5.1.2 A more complex system might include the
3.2 This practice provides details for applying radio- following components:
scopic examination techniques, however, supplemental
5.1.2.1 A microfocus X-ray system to facilitate
requirements are necessary to address areas that are
high-resolution projection imaging;
application and performance specific. Annexes A1 and
A2 provide the detailed supplemental requirements for 5.1.2.2 A multiple axis test part manipulation
government contracts (Annex A1) and nongovernment system to provide dynamic, full volumetric test part
contracts (Annex A2). manipulation under operator joystick or automated pro-
gram control;
362
SE-1255 ARTICLE 22 RADIOGRAPHIC STANDARDS SE-1255
the examination outcome for the selected system con- ulation system, detection system, information processing
figuration such as: source energy, intensity, focal spot system, image display, automatic evaluation system,
size, range of source to object distances, range of object and examination record archiving system.
to image plane distances, and source to image plane
distances 6.1.1 Radiation Sources. While the radioscopic
examination systems may utilize either radioisotope or
5.2.1.4 Image Processing Parameters a listing X-ray sources, X-radiation is used for most radioscopic
of all the image processing variables necessary to examination applications. This is due to the energy
enhance fine detail detectability in the test object and spectrum of the X-radiation which contains a blend of
to achieve the required sensitivity level. These would contrast enhancing longer wavelengths, as well as the
include, but are not limited to, techniques such as noise more penetrating, shorter wavelengths. X-radiation is
reduction, contrast enhancement, and spatial filtering. adjustable in energy and intensity to meet the radio-
Great care should be exercised in the selection of scopic examination test requirements, and has the added
directional image processing parameters such as spatial safety feature of discontinued radiation production when
filtering, which may emphasize features in certain orien- switched off. A radioisotope source has the advantages
tations and suppress them in others. The listing should of small physical size, portability, simplicity, and uni-
indicate the means for qualifying image processing formity of output.
parameters.
6.1.1.1 X-ray machines produce a more intense
5.2.1.5 Image Display Parameters a listing X-ray beam emanating from a smaller focal spot than
of the techniques and the intervals at which they are do radioisotope sources. X-ray focal spot sizes range
to be applied for standardizing the video image display from a few millimetres down to a few micrometres.
as to brightness, contrast, focus, and linearity Reducing the source size reduces geometric unsharpness,
thereby enhancing detail sensitivity. X-ray sources may
5.2.1.6 Accept-Reject Criteria a listing of offer multiple or variable focal spot sizes. Smaller focal
the expected kinds of test object imperfections and the spots produce higher resolution and provide reduced
rejection level for each X-ray beam intensity, while larger focal spots provide
higher X-ray intensity and produce lower resolution.
5.2.1.7 Performance Evaluation a listing of
Microfocus X-ray tubes are available with focal spots
the qualification tests and the intervals at which they are
which may be adjusted to as small as a few micrometres
to be applied to ensure that the radioscopic examination
in diameter, while still producing an X-ray beam of
system is suitable for its intended purpose
sufficient intensity so as to be useful for the radioscopic
5.2.1.8 Image Archiving Requirements a list- examination of finely detailed test objects.
ing of the requirements, if any, for preserving a historical
record of the examination results. The listing may 6.1.1.2 Conventional focal spots of 1.0 mm and
larger are useful at low geometric magnification values
include examination images along with written or elec-
close to 1. Fractional focal spots ranging from 0.4
tronically recorded alpha-numeric or audio narrative
information, or both, sufficient to allow subsequent mm up to 1.0 mm are useful at geometric magnifications
reevaluation or repetition of the radioscopic exami- of up to approximately 2. Minifocus spots in the
nation. range of 0.1 mm up to 0.4 mm are useful at geometric
magnifications up to about 6. Greater magnifications
5.2.1.9 Operator Qualifications a listing of suggest the use of a microfocus spot size of less than
the minimum operator certification level necessary to 0.1 mm in order to minimize the effects of geometric
perform the listed radioscopic examination unsharpness. Microfocus X-ray tubes are capable of
focal spot sizes of less than 10 micrometres (108 m)
and are useful for geometric magnifications of more
6. Radioscopic Examination System than 100.
Performance Considerations and
6.1.2 Manipulation System. The test part manipula-
Measurement
tion system has the function of holding the test object
6.1 Factors Affecting System Performance. Total and providing the necessary degrees of freedom, ranges
radioscopic examination system performance is deter- of motion, and speeds of travel to position the test
mined by the combined performance of the system object areas of interest in the radiation beam in such
components which includes the radiation source, manip- a way as to maximize the radioscopic examination
363
SE-1255 1998 SECTION V SE-1255
systems response. In some applications it may be 6.1.5 Automatic Evaluation System. Some radio-
desirable to manipulate the radiation source and detec- scopic examination applications can be fully automated
tion system instead of, or in addition to, the test object. including the accept /reject decision through computer
The manipulation system must be capable of smooth techniques. The automatic evaluation systems response
well-controlled motion, especially so for high magnifi- to various test object conditions must be carefully
cation microfocus techniques, to take full advantage of determined under actual operating conditions. The po-
the dynamic aspects of the radioscopic examination. tential for rejecting good test objects and accepting
defective test objects must be considered. Automatic
6.1.3 Detection System. The detection system is evaluation system performance criteria should be mutu-
a key element. It has the function of converting the ally determined by the provider and user of radioscopic
radiation input signal containing test part information, examination services.
into a corresponding optical or electronic output signal
while preserving the maximum amount of test object 6.1.6 Image Display
information. The detector may be of one-dimensional
6.1.6.1 The function of the image display is to
design, providing test part information one line at a time,
convey radioscopic information about the test object
or may be a two-dimensional area detector providing an
to the system operator. For manual evaluation systems,
area field of view.
the displayed image is used as the basis for accepting
6.1.4 Information Processing of System or rejecting the test object, subject to the operators
interpretation of the radioscopic image. The image
6.1.4.1 The function of the information pro- display performance, size, and placement are important
cessing system is to take the output of the detection radioscopic system considerations.
system and present a useful image for display and
operator interpretation, or for automatic evaluation. The 6.1.6.2 When employing a television image pre-
information processing system may take many different sentation, vertical and horizontal resolution are often
forms, and may process analog or digital information, not the same. Therefore, the effect of raster orientation
or a combination of the two. upon the radioscopic examination systems ability to
detect fine detail, regardless of orientation, must be
taken into account.
6.1.4.2 The information processing system in-
cludes all of the optics, electronics, and interfaces after
6.1.7 Radioscopic Examination Record Archiving
the detection system to and including the image display
System. Many radioscopic examination applications re-
and automatic evaluation system. Information system
quire an archival quality examination record of the
components include such devices as lenses, fiber optic
radioscopic examination. The archiving system may
couplings, light amplifiers, video cameras, image proces-
take many forms, a few of which are listed in 6.1.7.1
sors, and in general any device that processes radio-
through 6.1.7.10. Each archiving system has its own
scopic examination information after the detection
peculiarities as to image quality, archival storage proper-
system.
ties, equipment, and media cost. The examination record
archiving system should be chosen on the basis of
6.1.4.3 The digital image processing system these and other pertinent parameters, as agreed upon
warrants special attention, since it is the means by by the provider and user of radioscopic examination
which radioscopic examination information may be services. The reproduction quality of the archival method
enhanced. Great care must be exercised in determining should be sufficient to demonstrate the same image
which image processing techniques are most beneficial quality as was used to qualify the radioscopic examina-
for the particular application. Directional spatial filtering tion system.
operations, for example, must be given special attention
as certain feature orientations are emphasized while 6.1.7.1 Film or paper radiograph of the test object
others are suppressed. While many digital image pro- made under the same conditions as the radioscopic
cessing operations occur sufficiently fast to follow time examination image;
dependent radioscopic system variables, others do not.
Some image processing operations require significant 6.1.7.2 Spot film camera used to photograph
image acquisition and processing time, so as to limit the examination image directly from the output of an
the dynamic response of the radioscopic examination X-ray image intensifier without the intervening televi-
system. sion chain limitations;
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6.1.7.3 Photograph of the actual image display; the interval set forth in 6.2.1 for system performance
monitoring.
6.1.7.4 Multiformat camera used to make a
photograph of the examination image from the video 6.2 Performance Measurement. Radioscopic examina-
signal; tion system performance parameters must be determined
initially and monitored regularly to assure consistent
6.1.7.5 Video hard copy device used to create results. The best measure of total radioscopic examina-
a paper facsimile image from the video signal; tion system performance can be made with the system
in operation, utilizing a test object similar to the test
6.1.7.6 Video tape recorder used to record the
part under actual operating conditions. This indicates
video signal on magnetic tape; characterized by long
the use of an actual or simulated test object or calibration
recording time at video frame rates; useful for capturing
block containing actual or simulated features that must
test part motion;
be reliably detected. Such a calibration block will
6.1.7.7 Digital recording on magnetic disk or provide a reliable indication of the radioscopic examina-
tape used to store the image of the test object digitally, tion systems capabilities. Conventional wire or plaque
characterized by limited storage capacity at video frame type IQIs may be used in place of, or in addition to, the
rates, therefore limiting the ability to capture test part simulated test object or calibration block. Performance
motion; measurement methods are a matter of agreement be-
tween the provider and user of radioscopic examination
6.1.7.8 Digital recording on optical disk used services.
to store the image of the test object digitally; offers
larger storage capacity than magnetic disk or tape; 6.2.1 Performance Measurement Intervals. System
performance measurement techniques should be stan-
6.1.7.9 Electronic digital memory such as ROM dardized so that performance measurement tests may
(read only memory) or EPROM (erasable programmable be readily duplicated at specified intervals. Radioscopic
read only memory), characterized by relatively limited examination system performance should be evaluated
capacity; and at sufficiently frequent intervals, as may be agreed
upon by the supplier and user of radioscopic examination
6.1.7.10 Hologram used to store high density services, to minimize the possibility of time dependent
digital image data on film at high information density. performance variations.
6.1.8 Examination Record Data. The examination 6.2.2 Measurement With IQIs. Radioscopic exami-
record should contain sufficient information to allow nation system performance measurement using IQIs
the radioscopic examination test to be re-evaluated or shall be in accordance with accepted industry standards
duplicated. Examination record data should be recorded describing the use of IQIs. IQIs should be placed on
contemporaneously with the radioscopic examination the test object as close as possible to the region of
image, and may be in writing or a voice narrative, interest. The use of wire type IQIs should also take
providing the following minimum data: into account the fact that the radioscopic examination
system may exhibit asymmetrical sensitivity, in which
6.1.8.1 Radioscopic examination system designa-
case the wire diameter axis shall be oriented along the
tion, test date, operator identification, operating turn or
systems axis of least sensitivity. Selection of IQI
shift, and other pertinent test and customer data;
thickness should be consistent with the test part radiation
6.1.8.2 Specific test part data as to part number, path length thickness.
batch, serial number, etc. (as applicable); 6.2.3 Measurement With a Calibration Block. The
6.1.8.3 Test part orientation and examination calibration block may be an actual test object with
site information by manipulation system coordinate data known features that are representative of the range of
or by reference to unique test part features within the features to be detected, or may be fabricated to simulate
field of view; and the test object with a suitable range of representative
features. Alternatively, the calibration block may be a
6.1.8.4 System performance monitoring by re- one-of-a-kind or few-of-a-kind reference test object
cording the results of the prescribed radioscopic exami- containing known imperfections that have been verified
nation system performance monitoring tests, as set forth independently. Calibration blocks containing known,
in Section 5, at the beginning and end of a series of natural defects are useful on a single-task basis, but
radioscopic examination examinations, not to exceed are not universally applicable. Where standardization
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among two or more radioscopic examination systems to the performance measurements for the IQI or the
is required, a duplicate manufactured calibration block calibration block set forth in 6.2.2 and 6.2.3. It is
should be used. The calibration blocks should approxi- permissible to adjust the X-ray energy and intensity to
mate the test object as closely as is practical, being obtain a usable line pair test pattern image brightness.
made of the same material with similar dimensions In the case of a radioisotope or X-ray generating system
and features in the radioscopic examination region of where the energy or intensity may not be adjusted,
interest. Manufactured calibration blocks should include additional filtration may be added at the radiation source
features at least as small as those that must be reliably to reduce the brightness to a useful level. Contrast
detected in the actual test objects in locations where sensitivity shall be evaluated at the same energy and
they are expected to occur in the actual test object. intensity levels as are used for the radioscopic technique.
Where features are internal to the test object, it is
permissible to produce the calibration block in sections. 6.2.4.4 A system that exhibits a spatial resolution
Calibration block details are a matter of agreement of 3 line pairs /mm, a thin section contrast sensitivity
between the user and supplier of radioscopic examina- of 3%, and a thick section contrast sensitivity of 2%
tion services. may be said to have an equivalent performance level
of 3% 2% 3 lp /mm.
6.2.3.1 Use of a Calibration Block. The calibra-
tion block should be placed into the radioscopic exami- 6.2.4.5 The line pair test pattern and the step
nation system in the same position as the actual test wedge may be used to make more frequent periodic
object and may be manipulated through the same range system performance checks than required under para-
of motions as are available for the actual test object graph 6.2.1. Resolution and contrast sensitivity checks
so as to maximize the radioscopic examination systems must be correlated with IQI or calibration block perform-
response to the simulated imperfection. ance measurements. This may be done by first evaluating
system measurement in accordance with 6.2.2 or 6.2.3
6.2.3.2 Radioscopic Examination Techniques and immediately thereafter determining the equivalent
(radiation beam energy, intensity, focal spot size, en- spatial resolution and contrast sensitivity values.
largement, digital image processing parameters, manipu-
lation scan plan, scanning speed, and other system 6.2.5 Importance of Proper Environmental Condi-
variables) utilized for the calibration block shall be tions. Environmental conditions conducive to human
identical to those used for the actual examination of comfort and concentration will promote examination
the test object. efficiency and reliability, and must be considered in
the performance of manual evaluation radioscopic exam-
6.2.4 Use of Calibrated Line Pair Test Pattern ination systems. A proper examination environment will
and Step Wedge take into account temperature, humidity, dust, lighting,
access, and noise level factors. Proper reduced lighting
6.2.4.1 A calibrated line pair test pattern and
intensity is extremely important to provide for high
step wedge may be used, if so desired, to determine
contrast glare-free viewing of radioscopic examination
and track radioscopic system performance in terms of
images.
spatial resolution and contrast sensitivity. The line pair
test pattern is used without an additional absorber to
evaluate system spatial resolution. The step wedge is
7. Radioscopic Examination Interpretation and
used to evaluate system contrast sensitivity.
Acceptance Criteria
6.2.4.2 The step wedge must be made of the 7.1 Interpretation. Interpretation may be done either
same material as the test part with steps representing by an operator in a manual evaluation radioscopic
100%, 99%, 98%, and 97% of both the thickest and environment, or by means of a computer and appropriate
the thinnest material sections to be examined. The software in the case of an automated radioscopic exami-
thinner steps shall be contiguous to their respective nation system. A hybrid environment may also be
100% section thicknesses in order to facilitate discerning utilized whereby the computer and software present to
the minimum visible thickness step. Other thickness the operator a recommended interpretation, which is
steps are permissible upon agreement between the pro- then subject to the operators final disposition.
vider and the user of radioscopic services.
7.2 Operator. The supplier and user should reach
6.2.4.3 The line pair test pattern and the step- an agreement as to operator qualifications including
wedge tests shall be conducted in a manner similar duty and rest periods. Recommended Practice SNT-
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ANNEXES
(Mandatory Information)
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A1.3.9 written procedure in radioscopy, a series examinations shall be specified in the contract docu-
of steps that are to be followed in a regular definite ments. The optional radioscopic examinations are not
order. The radioscopic system operator follows the specified in the contract documents.
written procedure to consistently obtain the desired
A1.4.4.1 Radioscopic Examination Record. The
results and image quality level when performing radio-
recorded radioscopic examination record for mandatory
scopic examination. The development of a radioscopic
examinations shall include the written results of the
technique usually precedes the preparation of a written
radioscopic examination and the radioscopic image, if
procedure.
an image is utilized in the accept /reject decision-
A1.3.10 Other definitions not given herein shall making process. The recorded radioscopic image shall
be as specified in Terminology E 1316. be provided with such additional information as may
be required to allow the subsequent off-line review of
A1.4 General Requirements
the radioscopic examination results and, if necessary,
A1.4.1 Equipment Qualification Radioscopic the repeating of the radioscopic examination.
system qualification shall be in accordance with Practice
E 1411 and can best be evaluated with IQIs similar A1.4.4.2 Image Recording Media. The radio-
to the flaw type being investigated. A common IQI is scopic image shall be recorded on a media that is
described in MIL-STD-453. appropriate to the radioscopic examination requirement.
The recorded image shall reference the examination
A1.4.2 Personnel Qualification. Radioscopic per- zones in such a way that the reviewer can confirm
sonnel shall be qualified and certified in accordance that all zones have been covered. The recorded radio-
with the general requirements of MIL-STD-410, until scopic image shall provide an image quality at least
specific requirements for radioscopy are included. Ra- equal to that for which the radioscopic system is
dioscopic system qualification, the development of ra- qualified. The recording media shall be capable of
dioscopic examination test techniques, scan plans, and maintaining the required image quality for the required
the overall implementation of radioscopic examination record storage period or not less than five years from
in accordance with this Annex, shall be under the the recording date. The radioscopic image record shall
control and supervision of a qualified MIL-STD-410 be maintained in an operable condition for the duration
Level III with additional radioscopy training and experi- of the record storage period, measured from the date
ence or in conjunction with an individual having the when the last radioscopic image was recorded.
necessary training and experience in radioscopic exami-
nation. A1.4.4.3 Recording Media Storage Conditions.
Media storage and handling shall be in accordance
A1.4.3 Safety. The performance or radioscopic
with Guide E 1453.
examination shall present no hazards to the safety of
personnel or property. Applicable Federal, state, and A1.4.5 Image Quality Indicators. Image quality
local radiation safety codes shall be adhered to. All indicators must be chosen with care to demonstrate the
radioscopic procedures shall be performed in a safe radioscopic systems ability to detect discontinuities or
manner, such that personnel in that area are not exposed other features that are of interest. MIL-STD-453, Prac-
to any radiation dosage and shall in no case exceed tice E 1025 plaque-type, and Test Method E 747 wire-
Federal, state, and local limits. type IQIs and calibration blocks with real or simulated
A1.4.4 Archival Recording of Mandatory Radio- defects, to match the application, are all acceptable
scopic Examination. When required by contractual unless a particular IQI is specified in the contract
agreement, the radioscopic examination record shall documents. The selected IQI or calibration block shall
contain the results of mandatory radioscopic examina- be detailed in the written procedure. An IQI or calibra-
tions. The radioscopic examination record shall be tion block may not be required for the following
suitably archived for a period of time not less than radioscopic examinations:
five years from the examination date or as may otherwise A1.4.5.1 When conducting radioscopy to check
be required in the contract documents. Efficient radio- for adequate defect removal or grind-out, the final
scopic examination record recall shall be available at any acceptance radioscopic examination shall include an IQI,
time over the record retention period. The radioscopic
examination record shall be traceable to the test object A1.4.5.2 Examination to show material details
(by serial number or other means) or to the batch or or contrast between two or more dissimilar materials,
lot number, if tested in groups. Mandatory radioscopic in component parts or assemblies, including honeycomb
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SE-1255 1998 SECTION V SE-1255
areas for the detection fabrication irregularities or the positions(s) of the detector, and applicable IQI for each
presence or absence of material, and all variations of the test object orientation and
beam energy. This requirement may be expressed in
A1.4.5.3 Examinations of electronic components coordinates for automated systems having calibrated
for contamination, loose or missing elements, solder manipulation systems,
balls, broken or misplaced wires or connectors, and
potted assemblies, including honeycomb areas for the A1.5.2.2 A physical description of the test object,
detection of fabrication irregularities or the presence including size, thickness, weight, and composition,
or absence of material,
A1.5.2.3 Classification of the test object into
A1.4.5.4 Optional radioscopic examinations, and zones for radioscopy,
A1.4.5.5 Where the use of an IQI is impractical A1.5.2.4 Test part masking, if used, for each
or ineffective, an alternate method may be used, subject required view,
to the approval of the contracting agency.
A1.5.2.5 Added radiation field dimensions at
1.4.6 Classification of Test Zones for Radioscopy. the test object source side, for each required view,
The classification of test objects into zones for various
accept /reject criteria shall be determined from the con- A1.5.2.6 Detector field of view for each re-
tract documents. quired view,
A1.5.1.1 New Applications. Radioscopy may be A1.5.2.8 The allowable range of radiation energy
used where appropriate for new examination require- and beam current or source intensity and the focal spot
ments, provided the required performance, including or source size for each required view,
image quality, can be met.
A1.5.2.9 Added beam filtration, if used, for each
A1.5.1.2 Replacement of Existing Radiographic required view,
Applications. When agreed to by the contracting officer,
radioscopy may be used to replace or augment existing A1.5.2.10 The inspection geometry and coverage
radioscopic results that correlate favorably with the for each required view,
results obtained with X-ray film produced in accordance
A1.5.2.11 Type of IQI or calibration block used
with MIL-STD-453. Favorable correlation means that
and the required quality level,
the radioscopic and film images show similar sensitivity
to test object features that are of interest. A1.5.2.12 All hardware and software settings
that can be changed by the operator to affect the
A1.5.2 Written Procedure. It shall be the responsi-
outcome of the radioscopic examination. Such settings
bility of the NDE facility to develop a written radio-
include, but are not limited to, video camera and display
scopic examination procedure to ensure the effective and
settings and image processor variables, and
repeatable radioscopic examination of the test object. A
test object scan plan, meeting the requirements of A.1.5.2.13 The recording media and storage
Practice E 1255 (see 5.2.1.2), shall be included in image format for mandatory radioscopic image storage.
the written procedure. Those portions of the contract
document that specify and detail radioscopic examina- A1.5.3 Test Object Examination. The number of
tion shall become an appendix to the written procedure. test objects to be examined and the coverage required
The written procedure must be approved by the Level for each test object shall be specified in the contract
III of the NDE facility. Where required, the written documents. If not specified, all test objects shall receive
procedure shall be approved by the contracting agency 100% radioscopic coverage as detailed in the written
prior to use. The written procedure shall include as a procedure.
minimum the following information:
A1.5.4 Image Quality. Unless otherwise specified
A1.5.2.1 A drawing, sketch, or photograph of in the contract documents, the required image quality
the component that shows the radiation beam axis, level is 2-2T. Image quality assessment shall be per-
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SE-1255 ARTICLE 22 RADIOGRAPHIC STANDARDS SE-1255
formed using the same system parameters as in the qualification tests exceed one year. The qualification
inspection and as documented in the written procedure. statement shall be posted on the radioscopic system.
The results of qualification tests shall be maintained
A1.5.4.1 The IQI may be placed on the test in the radioscopic system equipment file until the
object or on a mounting block, at or near the test completion of the next qualification procedure or the
object location, following the requirements of MIL- expiration of the archival image retention period, which-
STD-453. In the case of small radioscopic fields of ever is longer.
view or other situations where it is not practical to
place the IQI in the field of view with the test object A1.5.9 Image Interpretation:
and maintain it normal to the X-ray beam, the IQI
A1.5.9.1 Static Imaging. Radioscopic system
may be imaged immediately before and after the test
qualification in accordance with Practice E 1411 applies
object examination. Batch quantities of similar parts
to static imaging conditions only where the test part
need not have IQI images made between each part, at the
is stationary with respect to the X-ray beam. Therefore,
discretion of the Level III. The radioscopic examination
all performance measurements are based upon static
results shall be invalid, if the before and after IQI
image quality. All mandatory radioscopic examination
images fail to demonstrate the required sensitivity. The
accept /reject decisions shall be based upon the assess-
before and after IQI images shall be considered a part
ment of static images.
of the test object for radioscopic image interpretation
and archiving purposes. A1.5.9.2 Dynamic Imaging. Dynamic or in-mo-
tion imaging may be used to gain useful information
A1.5.4.2 With written permission from the con-
about the test object. However, unless dynamic imaging
tracting agency, other IQIs or calibration block with
is specified, the final assessment of image formation
natural or artificial flaws may be used instead of the
for mandatory radioscopic examinations shall be made in
specified IQI.
the static mode. When the contracting agency specifies
A1.5.5 Radioscopic System Qualification. The ra- dynamic inspection, all aspects of the procedure must
dioscopic system, including mandatory radioscopic im- be approved by MIL-STD-410 Level III personnel. For
age archiving devices, shall be qualified to the image dynamic inspection, the image quality shall be measured
quality level required for test object examination. Radio- under the same procedure as the inspection.
scopic system initial qualification shall be in accordance
A1.5.10 Feature Size Determination. Where feature
with Practice E 1411.
measurement from the radioscopic image is required,
A1.5.6 Radioscopic System Requalification. The the written procedure shall include methodology for
radioscopic system, including mandatory image archiv- determining and maintaining the accuracy of the selected
ing devices, shall be periodically requalified at intervals measurement method.
frequent enough to ensure the required level of radio-
A1.5.10.1 Feature Measurement by the Test
scopic system performance. Each requalification shall
Object Displacement. For those radioscopic systems
be carried out in accordance with Practice E 1411.
with calibrated manipulation systems, the more accurate,
A1.5.7 Inspection Image Control. The radioscopic and therefore preferred, method of measurement is to
system shall be checked for performance before each manipulate the extremities of the feature to be measured
days production usage using the method and devices to a common central reference point within the radio-
that were initially used to qualify the written procedure. scopic image field of view. The dimension may then
A log shall be maintained to document any changes be read from the manipulation system position display.
in system performance requiring changes in operating
parameters and listing all equipment maintenance. Sys- A1.5.10.2 Feature Measurement by Comparison.
tem requalification shall be required whenever image A second method involves comparing the test object
quality requirements can no longer be met. feature with a known, observable dimension which
must be wholly within the radioscopic field of view.
A1.5.8 Repair of Radioscopic System. Repair or Many digital image processors facilitate this type of
replacement of key radioscopic system components measurement by counting pixels over the feature length.
including, but not limited to, the radiation source, image The pixel number is often converted to engineering
forming, image transmission, image processing, and units by comparison with a known length. However,
image display subsystems shall be cause for system the orientation and position along the X-ray beam
requalification. In no case shall the interval between (magnification) of both the feature and the calibrating
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reference length affect the accuracy of such measure- standard commercially available software packages or
ments. to traceable software documentation which complies
with DOD-STD-2167 where a separate copy of the
A1.5.11 Gray Scale Range. The gray scale range software is maintained.
required to meet initial qualification contract sensitivity
requirements for image quality shall be recorded and A1.5.17 Radioscopic Reexamination of Repairs.
monitored. For systems using human image assessment, When repair has been performed as the result of
it is particularly important that the gray scale range radioscopic examination, the repaired areas shall be
and the number of gray scale steps be closely matched reexamined using the same radioscopic technique to
to the response of the human eye. The written procedure evaluate the effectiveness of the repair. Each repaired
shall include a means for monitoring the required gray area shall be identified with R1, R2, R3 and so forth,
scale range using a contract sensitivity gage, step wedge, to indicate the number of times repair was performed.
or similar device made of the test object or IQI material. A1.5.18 Retention of Radioscopic Examination
A1.5.12 Timing of Radioscopic Examination. Ra- Records. Mandatory radioscopic examination records
dioscopic examination shall be performed at the time and associated radioscopic images shall be stored in a
of manufacturing, assembly, or rework as required by proper repository at the contractors plant for five years
the contract documents. from the date from which they were made. Special
instructions, such as storage for other periods of time,
A1.5.13 Identification. A means shall be provided making backup copies, copying the records to other
for the positive identification of the test object to media, or having the records destroyed shall be specified
the archival radioscopic inspection record. Archived in the contract documents.
radioscopic images shall be annotated to agree with
A1.5.19 Rejection of Test Objects. Test objects
the test object identification.
containing defects exceeding the permissible limits spec-
A1.5.14 Locating the Radioscopic Examination ified in the contract documents shall be separated
Areas. Whenever more than one image is required for from acceptable material, appropriately identified as
a weldment or other test object, location markers shall discrepant, and submitted for material review when
be placed on the test object in order that the orientation required by the contract documents.
of the test object and the location of test features relative
A1.5.20 Reexamination. When there is a reasonable
to the radioscopic field of view may be established. This
doubt as to the ability to interpret the radioscopic
requirement shall not apply to automated systems having
results because of improper execution or equipment
programmed radioscopic examination sequences where
malfunction, the test objects shall be reviewed by the
coverage has been proven during the development of
Level III of the NDE facility and adjusted, if necessary.
the scan plan. Also, this requirement does not apply
Reference exposures may be made using radiography
to the radioscopic examination of simple or small shapes
if necessary. If the reexamination was caused by equip-
where the test part orientation is obvious and coverage
ment malfunction, the equipment may not be returned
is not in question.
to service until the malfunction is repaired and the
A1.5.15 Surface Preparation. Test objects may be equipment is requalified to the current qualification
inspected without surface preparation, except when requirements in accordance with Practice E 1411.
required to remove surface conditions that may interfere A1.5.21 Test Object Marking. The marking of test
with proper interpretation of the radioscopic image or objects shall be as specified in MIL-STD-453.
that may create a safety hazard.
A1.5.16 Detailed Data. The provider of radioscopic
A1.6 Notes
examination services shall keep the written procedure,
A1.6.1 This section contains information of a
qualification documentation, and the signed inspection
general or explanatory nature and is not mandatory.
reports or tabulated results, or both, for five years
from the radioscopic examination date, unless otherwise A1.6.1.1 Caution Active electronic compo-
specified in the contract documents. For software-based nents and some materials, such as tetrafluorethylene,
automated radioscopic systems using custom software, are subject to radiation damage if exposed to large
a copy of the source code and the related inspection doses of radiation. While normal radioscopic examina-
parameters shall also be maintained on file for a like tions should cause no problem, extended periods of
period of time. This requirement shall not apply to radiation exposure should be avoided.
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A1.6.1.2 Human Factors. The success of radio- Should this Annex conflict with any other requirements
scopic examinations which involve human image inter- of Practice E 1255, this Annex shall prevail. The
pretation are, like radiography, subject to human factors. requirements of this Annex are intended to control the
Careful attention should be given to the human environ- quality of the radioscopic examination and not to specify
ment where image interpretation takes place, to make the accept /reject criteria for the test object.
it as conducive to correct, consistent image interpretation Accept /reject criteria are provided in other contract
as possible. Measures should also be implemented to documents.
ensure that fatigue does not interfere with correct and
consistent radioscopic image interpretation.
A2.2 Terminology
A1.6.1.3 Use of IQI(s). As with radiography, A2.2.1 component the test part or parts de-
the achievement of the required IQI sensitivity does scribed, assembled, or processed to the extent specified
not guarantee the ability to find all defects down to by the drawing
minimum defect size. This is due to the fact that many A2.2.2 contract documents the procuring con-
defects, especially those of a planar nature, are very tract and all drawings, specifications, standards, and
orientation sensitive. Care must be taken to see that other information included with or referred to by the
the scan plan includes sufficient manipulations to max- procuring contract
imize the possibility that orientation-sensitive defects
will be found. It is for this reason that the use of A2.2.3 contractor a contractor having first level
calibration blocks with real or simulated defects may responsibility for the design, manufacture, and delivery
more accurately characterize the ability of the radio- of an end item. When radioscopic examination is re-
scopic system to find orientation-sensitive defects. quired, the contractor is the user of radioscopic examina-
tion services.
A1.6.1.4 Use of Image-Processing Techniques.
A2.2.4 mandatory radioscopic examination
Care should be exercised in applying digital image
those radioscopic examinations which are a part of
processing techniques to evaluate the overall effect
the required radiographic examinations specified in the
upon image quality. For example, contract enhancement
contract documents
techniques may emphasize contrast in one brightness
range, while decreasing contrast in other brightness A2.2.5 NDE facility the organization that is
ranges. Some spatial filters have directional aspects, responsible for providing nondestructive examination
whereby features in one direction are emphasized while services
those in the orthogonal direction are deemphasized. Such
A2.2.6 optional radioscopic examination those
cautions are intended to cause the careful evaluation of
radioscopic examinations that are conducted for process
digital image-processng techniques and not to discour-
verifications or information only and are not a part of
age their use.
the required radiographic examinations specified in the
A1.6.1.5 Feature Size Determination. As with contract documents
radiography, great care must be exercised in trying to A2.2.7 provider of radioscopic services a con-
assess test part feature dimensions from a two-dimen- tractor, subcontractor or other entity that provides radio-
sional projected view. scopic examination services
A2.2.8 test object the material, component, or
assembly that is the subject of the radioscopic examina-
A2. NONGOVERNMENT CONTRACT tion services
SUPPLEMENTAL REQUIREMENTS
A2.2.9 user of radioscopic services a contractor,
A2.1 Scope subcontractor, or other entity that procures radioscopic
A2.1.1 Purpose. This Annex is to be used in examination services. The provider and user of radio-
conjunction with Practice E 1255. This Annex includes scopic examination services may be a part of the same
application specific details as may be agreed upon by the organization or different organizations.
purchaser and the supplier of radioscopic examination
services. A2.2.10 written procedure in radioscopy, a
series of steps that are to be followed in a regular
A2.1.2 Application. This document satisfies the definite order. The radioscopic system operator follows
requirements of 3.2 and 5.2.1 of Practice E 1255. the written procedure to consistently obtain the desired
373
SE-1255 1998 SECTION V SE-1255
results and image quality level when performing radio- radioscopic examination and the radioscopic image, if
scopic examination. The development of a radioscopic an image is utilized in the accept /reject decision-
technique usually precedes the preparation of a written making process. The recorded radioscopic image shall
procedure. be provided with such additional information as may
be required to allow the subsequent off-line review of
A2.2.11 Other definitions not given herein shall
the radioscopic examination results and, if necessary,
be as specified in Terminology E 1316.
the repeating of the radioscopic examination.
374
SE-1255 ARTICLE 22 RADIOGRAPHIC STANDARDS SE-1255
375
SE-1255 1998 SECTION V SE-1255
A2.4.7 Inspection Image Control. The radioscopic A2.4.10.2 Feature Measurement by Comparison.
system shall be checked for performance before each A second method involves comparing the test object
days production usage using the method and devices feature with a known, observable dimension which
that were initially used to qualify the written procedure. must be wholly within the radioscopic field of view.
A log shall be maintained to document any changes Many digital image processors facilitate this type of
in system performance requiring changes in operating measurement by counting pixels over the feature length.
parameters and listing all equipment maintenance. Sys- The pixel number is often converted to engineering
tem requalification shall be required whenever image units by comparison with a known length. However,
quality requirements can no longer be met. the orientation and position along the X-ray beam
(magnification) of both the feature and the calibrating
A2.4.8 Repair of Radioscopic System. Repair or reference length affect the accuracy of such measure-
replacement of key radioscopic system components ments.
including but not limited to the radiation source, image
forming, image transmission, image processing, and A2.4.11 Gray Scale Range. The gray scale range
image display subsystems shall be cause for system required to meet initial qualification contrast sensitivity
requalification. In no case shall the interval between requirements for image quality shall be recorded and
qualification tests exceed one year. The qualification monitored. For systems using human image assessment,
statement shall be posted on the radioscopic system. it is particularly important that the gray scale range
The results of the qualification tests shall be maintained and the number of gray scale steps be closely matched
in the radioscopic system equipment file at least until to the response of the human eye. The written procedure
completion of the next qualification procedure or the shall include a means for monitoring the required gray
expiration of the archival image retention period, which- scale range using a contrast sensitivity gage, step wedge,
ever is longer. or similar device made of the test object or IQI material.
376
SE-1255 ARTICLE 22 RADIOGRAPHIC STANDARDS SE-1255
A2.4.12 Timing of Radioscopic Examination. Ra- the date from which they were made. Special instruc-
dioscopic examination shall be performed at the time tions, such as storage for other periods of time, making
of manufacturing, assembly, or rework as required by backup copies, copying the records to other media, or
the contract documents. having the records destroyed shall be specified in the
contract documents.
A2.4.13 Identification. A means shall be provided
for the positive identification of the test object to A2.4.19 Rejection of Test Objects. Test objects
the archival radioscopic inspection record. Archived containing defects exceeding the permissible limits spec-
radioscopic images shall be annotated to agree with ified in the contract documents shall be separated
the test object identification. from acceptable material, appropriately identified as
A2.4.14 Locating the Radioscopic Examination discrepant, and submitted for material review when
Areas. Whenever more than one image is required for required by the contract documents.
a weldment or other test object, location markers shall
A2.4.20 Reexamination. Where there is an inability
be placed on the test object in order that the orientation
to interpret the radioscopic results because of improper
of the test object and the location of test object features
execution or equipment malfunction, the test object
relative to the radioscopic field of view may be estab-
shall be reexamined using the correct procedure. If the
lished. This requirement shall not apply to automated
problem is not resolved by reexamination, the procedure
systems having programmed radioscopic examination
shall be reviewed by the Level III of the NDE facility
sequences where coverage has been proven during the
and adjusted, if necessary. Reference exposures may
development of the scan plan. Also, this requirement
be made using radiography if necessary. If the reexami-
does not apply to the radioscopic examination of simple
nation was caused by equipment malfunction, the equip-
or small shapes where the test part orientation is obvious
ment may not be returned to service until malfunction
and coverage is not in question.
is repaired and the equipment is requalified to the
A.2.4.15 Surface Preparation. Test objects may current qualification requirements in accordance with
be inspected without surface preparation except as may Practice E 1411.
be required to remove surface conditions which may
interfere with proper interpretation of the radioscopic A2.4.21 Test Object Disposition. Test objects that
image or create a safety hazard. have undergone radioscopic examination shall be
marked or physically separated in such a maner so as
A2.4.16 Detailed Data. The provider of radioscopic to minimize the possibility of rejected or questionable
examination services shall keep the written procedure, test objects being confused with acceptable ones.
qualification documentation, and the signed inspection
reports or tabulated results for five years from the
radioscopic examination date unless otherwise specified A2.5 Notes
in the contract documents. For software-based automated A2.5.1 This section contains information of a
radioscopic systems using custom software, a copy of general or explanatory nature and is not mandatory.
the source code and the related inspection parameters
shall also be maintained on file for a like period of A2.5.1.1 Caution Active electronic compo-
time. This requirement shall not apply to standard nents and some materials, such as tetrafluorethylene,
commercially available software packages where a sepa- are subject to radiation damage if exposed to large
rate copy of the software is maintained. doses of radiation. While normal radioscopic examina-
A2.4.17 Radioscopic Reexamination of Repairs. tions should cause no problem, extended periods of
When repair has been performed as the result of radiation exposure should be avoided.
radioscopic examination, the repaired areas shall be
A2.5.1.2 Human Factors. The success of radio-
reexamined using the same radioscopic technique to
scopic examinations which involve human image inter-
evaluate the effectiveness of the repair. Each repaired
pretation are, like radiography, subject to human factors.
area shall be identified with R1, R2, R3, and so forth,
Careful attention should be given to the human environ-
to indicate the number of times repair was performed.
ment where image interpretation takes place, to make
A2.4.18 Retention of Radioscopic Examination it as conducive to correct, consistent image interpretation
Record. Mandatory radioscopic examination records and as possible. Measures should also be implemented to
associated radioscopic images shall be stored in a proper ensure that fatigue does not interfere with correct and
repository at the contractors plant for one year from consistent radioscopic image interpretation.
377
SE-1255 1998 SECTION V SE-1255
A2.5.1.3 Use of IQI. As with radiography, the processing techniques to evaluate the overall effect
achievement of the required IQI sensitivity does not upon image quality. For example, contrast enhancement
guarantee the ability to find all defects down to the techniques may emphasize contrast in one brightness
minimum defect size. This is due to the fact that many range while decreasing contrast in other brightness
defects, especially those of a planar nature, are very ranges. Some spatial filters have directional aspects
orientation sensitive. Care must be taken to see that whereby features in one direction are emphasized while
the scan plan includes sufficient manipulation to max- those in the orthogonal direction are deemphasized. Such
imize the possibility that orientation-sensitive defects cautions are intended to cause the careful evaluation of
will be found. It is for this reason that the use of digital image-processing techniques and not to discour-
calibration blocks with real or simulated defects may age their use.
more accurately charactierize the ability of the radio-
scopic system to find orientation-sensitive defects. A2.5.1.5 Feature Size Determination. As with
radiography, great care must be exercised in trying to
A2.5.1.4 Use of Image-Processing Techniques. assess test part feature dimensions from a two-dimen-
Care should be exercised in applying digital image- sional projected view.
378
SE-1416 ARTICLE 22 RADIOGRAPHIC STANDARDS SE-1416
1.2 This test method applies only to the use of 1.6 This standard does not purport to address all of
equipment for radioscopic examination in which the the safety concerns, if any, associated with its use. It
image is finally presented on a television monitor for is the responsibility of the user of this standard to
operator evaluation. The examination may be recorded establish appropriate safety and health practices and
for later review. It does not apply to fully automated determine the applicability of regulatory limitations
systems where evaluation is automatically performed prior to use. Specific precautionary statements are given
by computer. in Section 7.
378.1
3.1.1 Definitions of terms applicable to this test 5.5 Collimation Selection of appropriate collima-
method may be found in Terminology E 1316. tion is dependent upon the geometry of the object being
examined. It is generally useful to select collimation to
limit the primary radiation beam to the weld and the
4. Materials immediately adjacent base material in order to improve
radioscopic image quality.
4.1 Recording Media Recording media for storage
of images shall be in a format agreed by the purchaser 5.6 Filters and Masking Filters and masking
and supplier. This may include either analog or digital may be used to improve image quality from contrast
media. reductions caused by low-energy scattered radiation.
Guidance on the use of filters and masking can be
found in Guide E 94.
5. Apparatus
5.7 Image Quality Indicators (IQI) Unless other-
5.1 Radiation Source (X-Ray or Gamma-Ray) wise specified by the applicable job order or contract,
Selection of the appropriate source is dependent upon image quality indicators shall comply with the design
variables regarding the weld being examined, such as and identification requirements specified in Practices E
material composition and thickness. The suitability of 747 or E 1025.
the source shall be demonstrated by attainment of the
required image quality and compliance with all other 5.8 Shims, Separate Blocks, or Like Sections
requirements stipulated herein. Guidance on the selec- Shims, separate blocks, or like sections made of the
tion of the radiation source may be found in Guide E same or radioscopically similar materials (as defined
1000 and Practice E 1255. in Practice E 1025) may be used to facilitate image
quality indicator positioning as described in 9.10.3. The
5.2 Manipulation System Selection of the appro- like section should be geometrically similar to the
priate manipulation system (where applicable) is depen- object being examined.
dent upon variables such as the size and orientation
of the object being examined and the range of motions, 5.9 Location and Identification Markers Lead
speed of manipulation, and smoothness of motion. numbers and letters should be used to designate the
The suitability of the manipulation system shall be part number and location number. The size and thickness
demonstrated by attainment of the required image qual- of the markers shall depend on the ability of the
ity and compliance with all other requirements stipulated radioscopic technique to discern the markers on the
herein. Guidance on the selection of the manipulation images. As a general rule, markers from 0.06 to 0.12
system may be found in Practice E 1255. in. (1.5 to 3 mm) thick will suffice for most low energy
(less than 1 MeV) X-ray and iridium-192 radioscopy.
3 Available
For higher energy (greater than 1 MeV and cobalt-60)
from ASNT, 1711 Arlingate Plaza, P.O. Box 28518,
Columbus, OH 43228-0518. radioscopy, it may be necessary to use markers that
4 Available from the Superintendent of Documents, U.S. Government are thicker [0.12 in. (3 mm) thick or more]. In cases
Printing Office, Washington, DC 20402. where the system being used provides a display of
378.2
object position within the image, this shall be acceptable written procedure. Specific requirements regarding the
as identification of object location. preparation and approval of the written procedures shall
be as agreed by purchaser and supplier. The production
procedure shall address all applicable portions of this
6. Basis of Application test method and shall be available for review during
interpretation of the images. The written procedure shall
6.1 Personnel Qualification NDT personnel shall include the following:
be qualified in accordance with a nationally recognized
NDT personnel qualification practice or standard such 8.1.1 Material and thickness range to be examined,
as ANSI/ASNT-CP-189, SNT-TC-1A, MIL STD 410, 8.1.2 Equipment to be used, including specifications
or a similar document. The practice or standard used of source parameters (such as tube voltage, current,
and its applicable revision shall be specified in the focal spot size) and imaging equipment parameters (such
contractual agreement between the using parties. as detector size, field of view, electronic magnification,
6.2 Qualification of Nondestructive Testing Agen- camera black level, gain),
cies If specified in the contractual agreement, NDT 8.1.3 Examination geometry, including source-to-
agencies shall be qualified and evaluated as described object distance, object-to-detector distance and orien-
in Practice E 543. The applicable edition of Practice tation,
E 543 shall be specified in the contractual agreement.
8.1.4 Image quality indicator designation and
6.3 Time of Examination The time of examination placement,
shall be in accordance with 9.1 unless otherwise spec-
ified. 8.1.5 Test-object scan plan, indicating the range
of motions and manipulation speeds through which the
6.4 Procedures and Techniques The procedures test object shall be manipulated in order to ensure
and techniques to be utilized shall be as described in satisfactory results (see description in 5.2.1.2 of Practice
this test method unless otherwise specified. Specific E 1255),
techniques may be specified in the contractual
agreement. 8.1.6 Image-processing parameters,
6.5 Extent of Examination The extent of examina- 8.1.7 Image-display parameters, and
tion shall be in accordance with 8.3 unless otherwise 8.1.8 Image storage.
specified.
8.2 Radioscopic Coverage Unless otherwise speci-
6.6 Reporting Criteria/Acceptance Criteria Re- fied by purchaser and supplier agreement, the extent
porting criteria for the examination results shall be in of radioscopic coverage shall include 100% of the
accordance with Section 10 unless otherwise specified. volume of the weld and the adjacent base metal.
Acceptance criteria shall be specified in the contractual
agreement. 8.3 Examination Speed For dynamic examination,
the speed of object motion relative to the radiation
6.7 Reexamination of Repaired/Reworked Items source and detector shall be controlled to ensure that
Reexamination of repaired/reworked items is not ad- the required radioscopic quality level is achieved.
dressed in this test method and if required shall be
specified in the contractual agreement. 8.4 Radioscopic Image Quality All images shall
be free of marks or other blemishes that could mask
or be confused with the image of any discontinuity in
7. Safety the area of interest. It may be possible to prevent
blemishes from masking discontinuities or being con-
7.1 Radioscopic procedures shall comply with appli- fused with discontinuities by moving the object being
cable city, state, and federal safety regulations. examined relative to the imaging device. If any doubt
exists as to the true nature of an indication exhibited
in the image, the image shall be rejected and a new
8. Requirements image of the area shall be made.
8.1 Procedure Requirement Unless otherwise spec- 8.5 Radioscopic Quality Level Radioscopic quality
ified by the applicable job order or contract, radioscopic level shall be determined upon agreement between the
examination shall be performed in accordance with a purchaser and supplier and shall be specified in the
378.3
applicable job order or contract. Radioscopic quality upon the achievement of the required radioscopic quality
shall be specified in terms of equivalent penetrameter level at that examination speed.
(IQI) sensitivity and shall be measured using image
9.5 Direction of the Radiation Direct the central
quality indicators conforming to Practices E 747 or
beam of radiation perpendicularly toward the center of
E 1025.
the effective area of the detector or to a plane tangent
8.6 Acceptance Level Accept and reject levels to the center of the image, to the maximum extent
shall be stipulated by the applicable contract, job order, possible, except for double-wall exposure-double-wall
drawing, or other purchaser and supplier agreement. viewing elliptical projection techniques, as described
in 9.14.2.
8.7 Image-Viewing Facilities Viewing facilities
shall provide subdued background lighting of an inten- 9.6 Scattered Radiation Scattered radiation (radia-
sity that will not cause troublesome reflection, shadows, tion scattered from the test object and from surrounding
or glare on the image. structures) reduces radioscopic contrast and may pro-
duce undesirable effects on radioscopic quality. Use
8.8 Storage of Images When storage is required precautions such as collimation of the source, collima-
by the applicable job order or contract, the images tion of the detector, and additional shielding as appro-
should be stored in a format stipulated by the applicable priate to minimize the detrimental effects of this scat-
contract, job order, drawing, or other purchaser and tered radiation.
supplier agreement. The image-storage duration and
location shall be as agreed between purchaser and 9.7 Image Quality Indicator Selection For selection
supplier. of the image quality indicator, the thickness on which
the image quality indicator is based is the single-wall
thickness plus the lesser of the actual or allowable
reinforcement. Backing strips or rings are not considered
9. Procedure
as part of the weld or reinforcement thickness for
9.1 Time of Examination Unless otherwise speci- image quality indicator selection. For any thickness,
fied by the applicable job order or contract, perform an image quality indicator acceptable for thinner materi-
radioscopy prior to heat treatment. als may be used, provided all other requirements for
radioscopy are met.
9.2 Surface Preparation Unless otherwise agreed
upon, remove the weld bead ripple or weld-surface 9.8 Number of Image Quality Indicators:
irregularities on both the inside and outside (where
accessible) by any suitable process so that the image 9.8.1 Place at least one image quality indicator
of the irregularities cannot mask, or be confused with, (Practices E 747 or E 1025) in the area of interest
the image of any discontinuity. Interpretation can be representing an area in which the brightness is relatively
optimized if surface irregularities are removed such uniform. The degree of brightness uniformity shall be
that the image of the irregularities is not discernible. agreed upon between purchaser and supplier. If the
image brightness in an area of interest differs by
9.3 Source to Detector Distance Unless otherwise more than the agreed amount, use two image quality
specified in the applicable job order or contract, geomet- indicators. Use one image quality indicator to demon-
ric unsharpness (Ug) shall not exceed the following: strate acceptable image quality in the darkest portion
of the image and use one image quality indicator to
Material Thickness Ug, max, in. (mm)
under 2 in. (50 mm) 0.020 (0.50)
demonstrate acceptable image quality in the lightest
2 through 3 in. (50 through 75 mm) 0.030 (0.75) portion of the image.
over 3 through 4 in. (75 through 0.040 (1.00)
100 mm) 9.8.2 When a series of images are made under
greater than 4 in. (100 mm) 0.070 (1.75) identical conditions, it is permissible for the image
quality indicators to be used only on the first and last
Determine geometric unsharpness values as specified in images in the series, provided this is agreed upon
Guide E 94. between the purchaser and supplier. In this case, it is
not necessary for the image quality indicators to appear
9.4 Examination Speed For dynamic examination,
in each image.
determine the speed of object motion relative to the
radiation source and detector upon agreement between 9.8.3 Always retain qualifying images, on which
the purchaser and supplier. Base this determination one or more image quality indicators were imaged
378.4
during exposure, as part of the record to validate ness of the weld reinforcement plus the wall thickness,
the required image quality indicator sensitivity and backing ring and strip.
placement.
9.11.1 Shim Dimensions and Location When
9.9 Image Quality Indicator Placement: hole-type image quality indicators are used, the shim
dimensions and location shall exceed the image quality
9.9.1 Place the image quality indicator on the indicator dimensions by at least 0.12 in. (3 mm) on
source side adjacent to the weld being examined. Where at least three sides. At least three sides of the image
the weld metal is not radioscopically similar to the quality indicator shall be discernible in accordance with
base material or where geometry precludes placement 9.10.4 except that only the two ends of the image
adjacent to the weld, place the image quality indicator quality indicator need to be discernible when located
over the weld or on a separate block, as described on piping less than 1 in. (25 mm) nominal pipe size.
in 9.10. Place the shim so as not to overlap the weld image
including the backing strip or ring.
9.9.2 Detector-Side Image Quality Indicators
In those cases where the physical placement of the 9.11.2 Shim Image Brightness The image bright-
image quality indicators on the source side is not ness of the shim image shall be similar to the image
possible, place the image quality indicators on the brightness of the area of interest.
detector side. The applicable job order or contract shall
specify the applicable detector-side quality level. The 9.12 Location Markers Place location markers
accompanying documents shall clearly indicate that the outside the weld area. The radioscopic image of the
image quality indicators were located on the detector location markers for the identification of the part location
side. with the image shall appear on the image without
interfering with the interpretation and with such an
9.10 Separate Block When configuration or size arrangement that it is evident that complete coverage
prevents placing the image quality indicators on the was obtained.
object being examined, use a shim, separate block or
like section conforming to the requirements of 5.8 9.12.1 Double-Wall Technique When using a
provided the following conditions are met: technique in which radiation passes through two walls
and the welds in both walls are simultaneously viewed
9.10.1 The image quality indicator is no closer to for acceptance, and the entire image of the object being
the detector than the source side of the object being examined is displayed, only one location marker is
examined (unless otherwise specified). required in the image.
9.10.2 The radioscopic brightness in the area of 9.12.2 Series of Images For welds that require
the image quality indicator including the shim, separate a series of images to cover the full length or circumfer-
block, or like section and IQI where applicable are ence of the weld, apply the complete set of location
similar to the brightness in the area of interest. markers at one time, wherever possible. A reference
or zero position for each series must be identified on
9.10.3 The shim, separate block, or like section the component. A known feature on the object (for
is placed as close as possible to the object being example, keyway, nozzle, and axis line) may also be
examined. used for establishment of a reference position. Indicate
this feature on the radioscopic record.
9.10.4 When hole-type image quality indicators
are used, the shim, separate block, or like section 9.12.3 Similar Welds On similar type welds
dimensions shall exceed the image quality indicator on a single component, the sequence and spacing of
dimensions such that the outline of at least three sides the location markers must conform to a uniform system
of the image quality indicator image is visible on the that shall be positively identified in the radioscopic
image. procedure or interpretation records. In addition, refer-
ence points on the component will be shown on the
9.11 Shim Utilization When a weld reinforcement
sketch to indicate the direction of the numbering system.
or backing ring and strip is not removed, place a shim
of material that is radioscopically similar to the backing 9.13 Image Identification Provide a system of
ring and strip under the image quality indicators to positive identification of the image. As a minimum,
provide approximately the same thickness of material the following shall appear on the image: the name or
under the image quality indicator as the average thick- symbol of the company performing radioscopy, the
378.5
date, and the weld identification number traceable to 10.1.1 Radioscopic standard shooting sketch, in-
part and contract. Identify subsequent images made of cluding examination geometry, source-to-object dis-
a repaired area with the letter R. tance, object-to-detector distance and orientation,
378.6
2. Referenced Documents
2.3 NIST/ANSI Standards:
2.1 ASTM Standards: NIST/ANSI Handbook 114 General Safety Standard for
B 139 Specification for Phosphor Bronze Rod, Bar, and Installations Using Non-Medical X-ray and Sealed
Shapes2 Gamma Ray Sources, Energies to 10 MeV6
B 150 Specification for Aluminum Bronze Rod, Bar, and
Shapes 2
3 Annual Book of ASTM Standards, Vol 02.04.
4 Annual Book of ASTM Standards, Vol 03.03.
1 This practice is under the jurisdiction of ASTM Committee E-7
on Nondestructive Testing and is the direct responsibility of Subcom- 5 Availablefrom the Superintendent of Documents, U.S. Government
mittee E07.01 on Radiology (X and Gamma) Method. Printing Office, Washington, DC 20402.
Current edition approved Nov. 15, 1994. Published January 1995. 6 Availablefrom American Society for Nondestructive Testing, 1711
2 Annual Book of ASTM Standards, Vol 02.01. Arlingate Plaza, P.O. Box 28518, Columbus, OH 43228-0518.
379
SE-1647 1998 SECTION V SE-1647
3. Terminology
3.1 Definitions Definitions of terms applicable to TABLE 2
this test method may be found in Terminology E 1316. CONTRAST SENSITIVITY GAGE DIMENSIONS
Gage
4. Summary of Practice Size B DIM. C DIM. D DIM. E DIM. F,G DIM.
4.1 It is often useful to evaluate the contrast sensitivity 1 0.750 in. 3.000 in. 0.250 in. 0.625 in. 0.250 in.
19.05 mm 76.20 mm 6.35 mm 15.88 mm 6.35 mm
of a penetrating radiation imaging system separate and 2 1.500 in. 6.000 in. 0.500 in. 1.250 in. 0.500 in.
apart from spatial resolution measurements. Conven- 38.10 mm 152.40 mm 12.70 mm 31.75 mm 12.7 mm
tional image quality indicators (IQIs), such as Test 3 2.250 in. 9.000 in. 0.750 in. 1.875 in. 0.750 in.
Method E 747 wire and Practice E 1025 plaque IQIs, 57.15 mm 228.60 mm 19.05 mm 47.63 mm 19.05 mm
combine the contrast sensitivity and resolution measure- 4 3.000 in. 12.000 in. 1.000 in. 2.500 in. 1.000 in.
76.20 mm 304.80 mm 25.40 mm 63.50 mm 25.4 mm
ments into an overall performance figure of merit. Such
figures of merit are often not adequate to detect subtle
changes in imaging system performance. For example,
in a high contrast image, spatial resolution can degrade TABLE 3
with almost no noticeable effect upon overall image CONTRAST SENSITIVITY GAGE APPLICATION
quality. Similarly, in an application in which the imaging
system provides a very sharp image, contrast can fade Gage Size Use on Thicknesses
with little noticeable effect upon the overall image 1 Up to 1.5 in. (38.1 mm)
quality. These situations often develop and may go 2 Over 1.5 in. (38.1 mm) to 3.0 in. (76.2 mm)
unnoticed until the system performance deteriorates 3 Over 3.0 in. (76.2 mm) to 6.0 in. (152.4 mm)
4 Over 6.0 in. (152.4 mm)
below acceptable image quality limits.
380
SE-1647 ARTICLE 22 RADIOGRAPHIC STANDARDS SE-1647
381
SE-1647 1998 SECTION V SE-1647
cation B 164) or equivalent, or 70 to 30 copper-nickel formation, processing, analysis, display, and viewing
alloy (Alloy G of Specification B 161) or equivalent. variables shall accurately simulate the actual examina-
tion environment.
6.3.7.2 Use for nickel, copper, all nickel-copper
series or copper-nickel series of alloys and all brasses
(copper-zinc alloys) and all leaded brasses.
8. Contrast Sensitivity Gage Measurement
6.3.8 Materials Group 5: Steps (see Table 1)
6.3.8.1 The gage shall be made of tin-bronze 8.1 The gage thickness T shall be within 65% of the
(Alloy D of Specification B 139). test object thickness value at which contrast sensitivity is
being determined.
6.3.8.2 Use for tin bronzes including gun-metal
and valve bronze and leaded-tin bronzes. 8.2 The gage thickness tolerance shall be within
6.4 Where the material to be examined is a composite 61% of the gage design thickness T or 0.001 in.
material or for some reason cannot be obtained to (0.02 mm), whichever is greater.
fabricate a gage, an equivalent material may be utilized,
8.3 The gage recess depth tolerance shall be within
provided it is no more radio-opaque than the test
610% of the design value for the shallowest recess
object under comparable penetrating radiation energy
or 0.001 in. (0.02 mm), whichever is greater.
conditions. To determine the suitability of a substitute
material, radiograph identical thicknesses of both materi- 8.4 The gage recess inside and outside corner radius
als on one film using the lowest penetrating radiation shall not exceed 0.062 in. (1.80 mm). To facilitate
energy to be used in the actual examination. Transmis- fabrication, the gage may be assembled from three
sion densitometer readings for both materials shall be individually machined components: (1) the machined
in the range from 2.0 to 4.0. If the radiographic density center section containing the 1% T, 2% T, 3% T, and
of the substitute material is within +15% to 0% of 4% T milled slots; (2) the front rail, and (3) the rear
the test material, the substitute material is acceptable. rail. The assemblage of the three components forms
6.4.1 All contrast sensitivity gages shall be suitably the complete gage similar to that shown in Appendix X1.
marked by vibro-engraving or etching. The gage thick-
ness and material type shall be clearly marked. 8.5 The gage dimensional tolerances shall be held
to within 60.010 in. (0.25 mm) of the dimensions
specified in Table 2.
7. Imaging System Performance Levels
7.1 Imaging system performance levels are designated
by a two-part measurement expressed as C(%) 9. Acceptable Performance Levels
U(mm). The first part of the expression C(%) refers
9.1 Nothing in this test method implies a mandatory
to the depth of the shallowest flat-bottom hole that can
or an acceptable contrast sensitivity performance level.
be reliably and repeatably imaged. The second part of
That determination is to be agreed upon between the
the expression refers to the companion spatial resolution
supplier and user of penetrating radiation examination
measurement made with a resolution gage expressed
services.
in terms of millimeters unsharpness. Where contrast
sensitivity is measured for both thin and thick section 9.2 The recess depths specified in Table 1 provide
performance, the performance level is expressed as Cmin measurement points at 1%, 2%, 3%, and 4% that
(%)Cmax(%)U(mm). will accommodate many imaging system configurations.
7.2 Each contrast sensitivity gage has four flat-bottom Other contrast sensitivity measurement points may be
recesses that represent 1%, 2%, 3%, and 4% of the obtained by placing the gage on a shim made of
gage total thickness. The shallowest recess that can be the gage material. The resulting contrast sensitivity
repeatably and reliably imaged shall determine the measurement expressed as a percentage is given by
limiting contrast sensitivity. the following formula:
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SE-1647 ARTICLE 22 RADIOGRAPHIC STANDARDS SE-1647
APPENDIX
(Nonmandatory Information)
X1. ASSEMBLING THE CONTRAST sensitivity gage from a milled center section with front
SENSITIVITY GAGE and rear rails attached to form the complete contrast
sensitivity gage. The example shown (see Fig. X1.1)
X1.1 Suggested method of assembling the contrast is for use with a 0.500 in. thick test object.
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SE-1815 ARTICLE 22 RADIOGRAPHIC STANDARDS SE-1815
385
SE-1815 1998 SECTION V SE-1815
lished by the manufacturers of the film and processing which are capable of providing known image qualities.
chemicals. See 7.2.
3.2.2 gradient G the slope of the characteristic
curve at a certain density, D, and a measure of the 5. Sampling and Storage
contrast of the film system.
5.1 For determination of the gradient and granularity
3.2.3 granularity, sD the stochastic density of a film system, it is important that the samples
fluctuations in the radiograph that are superimposed to evaluated yield the average results obtained by users.
the object image. This will require evaluating several different batches
3.2.4 ISO speed S determined by the dose Ks, periodically, under the conditions specified in this test
measured in gray at a specified optical density, D, in method. Prior to evaluation, the samples shall be stored
the radiograph. according to the manufacturers recommendations for
a length of time to simulate the average age at which
the product is normally used. Several independent evalu-
4. Significance and Use ations shall be made to ensure the proper calibration
of equipment and processes. The basic objective in
4.1 This test method provides a relative means for selecting and storing samples as described above is to
classification of film systems used for industrial radiog- ensure that the film characteristics are representative
raphy. The film system consists of the film and associ- of those obtained by a consumer at the time of use.
ated processing system (the type of processing and
processing chemistry). Section 6 describes specific pa-
rameters used for this test method. In general, the 6. Procedure
classification for hard X rays, as described in Section
6, can be transferred to other radiation energies and 6.1 Principle:
metallic screen types, as well as screens without films. 6.1.1 Film to be tested shall be exposed to X rays
The usage of film system parameters outside the energy from tungsten target tubes. Inherent filtration of the
ranges specified may result in changes to a film/system tube, plus an additional copper filter located as close
performance classification. to the target as possible, shall provide filtration equiva-
4.1.1 The film performance is described by signal lent to 8.00 6 0.2 mm of copper.
and noise parameters. The signal is represented by
6.1.2 The film system includes a front and a back
gradient and the noise by granularity.
screen of 0.02 to 0.25-mm lead. If single-coated films
4.1.2 A film is assigned a particular class if it are used, the emulsion-coated surface must face the
meets all four of the minimum performance parameters: X-ray tube. Vacuum or pressure cassettes may be used
for Gradient G at D p 2.0 and D p 4.0, granularity to ensure sufficient contact between the film and screen.
sD at D p 2.0, and gradient/noise ratio at D p 2.0.
6.2 X-ray Spectral Quality:
4.2 This test method describes how the parameters
6.2.1 Use the same X-ray spectral quality for
shall be measured and demonstrates how a classification
determining both the film gradient and its root mean
table can be constructed.
square granularity. Make the film exposures with an
4.3 Manufacturers of industrial radiographic film 8-mm (0.32-in.) copper filter at the X-ray tube and the
systems will be the users of this test method. The kilovoltage set such that the half value layer in copper
result is a classification table as shown by the example is 3.5 mm (0.14 in.). The kilovoltage setting will be
given in Table 1. This table also includes speed data approximately 220 kV.
for user information. Users of industrial radiographic
film systems may also perform the tests and measure- 6.2.2 Determine the required kilovoltage setting
ments outlined in this test method, provided that the by making an exposure (or exposure rate) measurement
required test equipment is used and the methodology with the detector placed at a distance of at least 750
is followed strictly. mm (29.5 in.) from the tube target and an 8-mm (0.32-
in.) copper filter at the tube. Then make a second
4.4 The publication of classes for industrial radiogra- measurement with a total of 11.5 mm (0.45 in.) of
phy film systems will enable specifying bodies and copper at the tube. These filters should be made of
contracting parties to agree to particular system classes, 99.9% pure copper.
386
SE-1815 ARTICLE 22 RADIOGRAPHIC STANDARDS SE-1815
TABLE 1
TYPICAL FILM SYSTEM CLASSIFICATION
6.2.3 Calculate the ratio of the first and second automatic). The film processing and record requirements
readings. If this ratio is not 2, adjust the kilovoltage shall be in accordance with Guide E 999.
up or down and repeat the measurements until a ratio
of 2 (within 5%) is obtained. Record the machine 6.5 Exposure Conditions:
setting of the kilovoltage for use with the film tests.
6.5.1 The plane of the film shall be normal to
6.3 Film Cassette and Screens: the central ray of the X-ray beam. Use a diaphragm
at the tube to limit the field of radiation to the film
6.3.1 The film cassette (holder) shall provide a
area. The X-ray tube target to film distance shall be
means of ensuring good film screen contact. A vacuum
adequate to ensure that the exposure over the useful
cassette may be used.
area of each exposure step is uniform to within 3%.
6.3.2 Lead-foil screens shall be used with the front
screen thickness being 0.130 6 0.013 mm (0.005 6 6.5.2 To minimize the effects of backscattered
0.05 in.) and the back screen thickness being 0.250 6 radiation, use a 6.3 6 0.8 mm (14 6 132 in.) thick
0.025 mm (0.010 6 0.001 in.). lead shielding behind the cassette. The shielding lead
shall extend at least 25 mm (1 in.) beyond each edge
NOTE These thicknesses reflect commercially available tolerances of the cassette. Alternatively, the shielding lead may
in lead foil for use as radiographic screens. be omitted, provided that the cassette is supported such
that the X-ray beam strikes no scattering material, other
6.3.3 It is especially important that the exposure than air, for a distance of at least 2 m (78.7 in.) behind
to the film specimen for the granularity measurements the cassette.
be spatially uniform. Any nonuniformities in X-ray
transmission of the cassette front or nonuniformities or 6.5.3 Modulation of the X-ray exposure may be
defects in the lead-foil screens could influence the accomplished by changing the exposure time or tube
granularity measurement. Therefore, exercise consider- target to film distance. Changing the tube current is
able care in selection and maintenance of the cassette not recommended but may be done, provided it is
and lead screens to minimize these effects. verified by measurement (see 6.2) that the X-ray spectral
quality does not change.
6.3.4 Expose single-coated films with the emulsion-
coated surface in contact with the front screen.
6.5.4 Measure exposures with an air-ionization
6.4 Film Processing The film image quality will chamber, or other types of X-ray detectors, having
vary with the processing variables, such as chemistry, linear response over the range of X-ray intensities and
temperature, and method of processing (manual or exposure times used for the film exposures.
387
SE-1815 1998 SECTION V SE-1815
6.5.5 During and after exposure, prior to pro- and after exposure, prior to processing, maintain the
cessing, keep the film at a temperature of 23 6 5C film specimen at the temperature and relative humidity
(5.97 6 5F) and a relative humidity of 50 6 20%. conditions specified in 6.5.5. The film processing chemi-
Start processing of the film between 30 min and 8 h cals and procedures shall be the same as those used
after exposure. Process an unexposed specimen of the for determining gradient, and they shall be described
film sample with the X-ray-exposed specimen in order completely as specified in 6.4.
to determine the base plus fog density.
6.7.4 The film specimen for granularity measure-
6.5.6 Measure the visual diffuse transmission den- ment shall have a diffuse density of 2.00 6 0.05 above
sity of the processed films with a densitometer comply- base plus fog. As an alternative, three or more samples
ing with the requirements of ANSI PH 2.19 and ISO of the film specimen at different density levels, within
5-2 and calibrated by the method of Practice E 1079. the range from 1.80 to 2.20, may be measured, and
Use a minimum aperture of 7 mm (0.275 in.). the granularity value at a diffuse density of 2.00, above
base plus fog, shall be taken from a smooth curve
6.6 Measurement of Gradient G:
drawn through a plot of the data points. The granularity
6.6.1 Gradient G relates to a D versus log K value shall be in terms of diffuse density.
curve. In the scope of this test method, G is calculated
6.7.4.1 The microdensitometer scanner output is
from the slope of a D versus K curve at density (D
measured as projection density. Thus to obtain the
Do), as follows:
desired diffuse density, convert the data using the slope
of the curve of diffuse density versus projection density
dD K dD
Gp p at the mean density value of the granularity film
d log K log e dK
specimen. Determine this curve using a film having a
stepped series of densities, which is prepared using the
where: same type film, exposure, and processing techniques
K p dose required for density D Do, and as used for the granularity film specimen. Measure the
Do p fog and base density. diffuse density of each step with a microdensitometer.
6.6.2 The D versus K curve is approximated by The specimen film shall be scanned using identical
a polynomial of the third order. To obtain a regular microdensitometer settings. A limited range of densities
and reliable shape of this curve, make a series of can typically be measured for a given microdensitometer
exposures to obtain at least 12 uniformly distributed gain setting. The stepped series of densities shall lie
measuring points between density 1.0 and 5.0 above Do. within that range. Choose the number of steps such
that the slope of the curve, at the mean density of the
6.6.3 Average the Gradient G measurements, with granularity film specimen, is determined to an accuracy
a maximum inaccuracy of 65%. of 65%.
6.7 Root Mean Square (rms) Granularity, sD: 6.7.5 Determine the granularity of the film speci-
6.7.1 Determine the rms granularity of the film men by evaluating no fewer than three samples of the
in accordance with ANSI PH 2.40, with the following specimen and determining their mean so that a maximal
exceptions: uncertainty of 10% is achieved.
6.7.2 The procedure is limited to the measurement 6.7.6 Adjust the optical system of the microdensi-
of continuous tone black-and-white industrial X-ray tometer so that both emulsions, or the one emulsion
films viewed by transmitted light. The film may have in the case of a single-coated film, are in focus at all
emulsion coated on one side or both sides of the film points in the scan.
support.
6.7.7 Scan the film specimen along three different
6.7.3 Expose the film specimen with X rays having paths within the test area. Take the median of the
the spectral quality described in 6.2. The cassette and three granularity readings as the granularity of the film
lead-foil screens shall be as specified in 6.3. Expose specimen at the mean measured density.
the film specimen in accordance with the exposure
6.7.8 Microdensitometer Requirements:
conditions of 6.5. Exercise care to ensure that the film
specimen does not contain density variations arising 6.7.8.1 The influx aperture of the microdensitom-
from the exposing equipment (such as nonuniform beam eter shall be approximately circular in shape, with a
filters or damaged or defective lead screens). During diameter (referred to the plane of the specimen) not
388
SE-1815 ARTICLE 22 RADIOGRAPHIC STANDARDS SE-1815
TABLE 2 TABLE 3
DETERMINATION OF ISO SPEED S FROM DOSE, Ks , LIMITING VALUES FOR GRADIENT, GRADIENT/
NEEDED FOR A FILM DENSITY, D p 2.0, ABOVE Do GRANULARITY RATIO, AND GRANULARITY
log10Ks Minimum
Minimum Gradient G at Gradient/
From To ISO Speed SA Granularity Maximum
3.05 2.96 1000 ASTM Ratio, G/sD Granularity,
2.95 2.86 800 System D p 2.0 D p 4.0 at D p 2.0 sD , at D p 2.0
2.85 2.76 640 Class Above DoA Above Do Above Do Above Do
2.75 2.66 500 Special 4.5 7.5 300 0.018
2.65 2.56 400 I 4.1 6.8 150 0.028
2.55 2.46 320 II 3.8 6.4 120 0.032
2.45 2.36 250 III 3.5 5.0 100 0.039
2.35 2.26 200 W-A 3.6 5.7 135 0.027
2.25 2.16 160 W-B 3.5 5.0 110 0.032
2.15 2.06 125 W-C <3.5 <5.0 80 0.039
2.05 1.96 100
ADo = density of an unexposed and processed film including base (fog
1.95 1.86 80
1.85 1.76 64 and base density).
1.75 1.66 50
1.65 1.56 40
1.55 1.46 32
1.45 1.36 25
1.35 1.26 20 6.7.8.7 The electronic band-pass filter, used to re-
1.25 1.16 16 duce the unwanted signal caused by system artifacts, shall
1.15 1.06 12
1.05 0.96 10
have its low-frequency boundary set so the system re-
0.95 0.86 8 sponse is 3 dB down at a temporal frequency corresponding
0.85 0.76 6 to a spatial frequency of 0.1 cycles/mm. Its high-frequency
0.75 0.66 5 boundary shall be set so that the system response is 3 dB
0.65 0.56 4 down at a temporal frequency corresponding to the first
A See ISO 7004. zero in the spatial frequency response of the circular aper-
ture. Mathematical procedures that can be shown to pro-
less than 1.2 or more than 2 the diameter of the duce equivalent reductions in the effects of system artifacts
efflux aperture. are acceptable alternatives to the use of this filter.
6.7.8.2 Both the influx objective and the efflux 6.8 Measurement of ISO Speed S The ISO Speed
objective shall be a high-quality microscope objective S is evaluated for an optical density, D p 2.0, above
having a numerical aperture no greater than 0.10. fog and base, Do. Use Table 2 for determination of
the ISO speed.
6.7.8.3 The reduction of the influx aperture by
the influx optics and the magnification of the specimen
7. Range of Classification and Limiting Values
onto the efflux aperture by the efflux optics shall lie
in the range from 20 to 100. The two magnifications 7.1 There are film system classes that differ by their
need not be equal. gradients and granularities. The limiting values are
assigned to the film classes whose observance must be
6.7.8.4 The efflux (or measuring aperture) shall proved by the measuring methods in 6.6 and 6.7.
be circular in shape. Its effective diameter referred to
the specimen plane shall be 100 6 2 mm. 7.1.1 In order to assign a film system to a system
class, it must meet all four limiting values of the
6.7.8.5 The scan path of the microdensitometer gradient (at D p 2.0 and D p 4.0), the granularity
may be linear or circular. If circular, the radius of the (at D p 2.0), and the gradient/granularity parameter
path shall not be less than 16 mm. In either case, the of the system class. The classification is valid only for
total scan length shall not be less than 100 mm (3.94 in.). the complete film system.
6.7.8.6 The spectral response of the microdensi- 7.2 Film system manufacturers will provide their
tometer system shall be visual, as specified by ANSI classification table, upon request, with a classification
PH 2.18 and ISO 5-3. table that contains full data on the four parameters
389
SE-1815 1998 SECTION V SE-1815
according to Table 3. In addition, the following two classification of industrial radiographic film since the
parameters (see Table 2 for data) will be listed with results state merely whether there is conformance to
the classification table: ISO speed S, and dose, Ks . the criteria for success specified in the procedure.
7.2.1 The classification table will additionally con-
tain the following information on the processing system:
manual or automatic, type of chemistry, developer
immersion time, and developer temperature.
7.3 For examples of a classification table, see Table 1.
9. Keywords
8. Precision and Bias
9.1 ASTM system class; film system; film system
8.1 No statement is made about either the precision classification; gradient; gradient/noise; granularity; in-
or bias of this test method for measuring a film system dustrial radiographic film; speed.
APPENDIX
(Nonmandatory Information)
X1. GENERAL PRINCIPLES OF E 94-83, speed, contrast, and graininess were specified
CLASSIFICATION as limiting values, but only in a subjective way. Ac-
cording to this guide, a range of films was classified
X1.1 The purpose of this test method is to classify in order of increasing speed and decreasing image
industrial radiographic film systems based on their quality (contrast and graininess). Image quality was
image quality performance over the practical working optimized for a given speed.
range of densities (for example, from 2.0 to 4.0). The
classes are differentiated in image quality performance X1.2.2 This test method has similar classes: Spe-
based on limiting values for four measurable image cial, I, II, and III (see Table 3). The film systems that
quality parameters, that is, gradient at density 2.0 and will generally fit this classification are of high-contrast
4.0 and granularity and gradient/granularity ratio at technology. Image quality is optimized for every speed.
density 2.0. See Table 3. Granularity increases with speed, and gradient is a
X1.1.1 The result of classification can be docu- maximum for the slower speed film systems.
mented in a table with the following details:
X1.2.3 The slower film systems give the highest
X1.1.1.1 Description of the film system (film image quality, through a combination of low granularity
and processing), and high gradient for both Density 2.0 and 4.0 and a
corresponding high gradient/granularity ratio.
X1.1.1.2 Values for four image quality parame-
ters and the corresponding system class, and
X1.2.4 Four classes of this test method were
X1.1.1.3 Speed of the film system. selected to correspond to the former film classification
standard table of Guide E 94-83. See Table X1.1.
X1.1.2 The optimal film system based on system
classification (imaging performance) and speed (expo- X1.2.5 Table X1.2 provides classification of wide
sure time) can be selected with this information. See latitude film systems. In comparison to traditional high-
Table 1 for an example. contrast technology, these film systems are generally
characterized by a lower gradient for a given speed,
X1.2 Significance of Classes
producing wider exposure latitude and correspondingly
X1.2.1 Various codes and specifications require lower image quality. The gradient will be lower at
film selection based on a class (Type 1, 2, or 3) from density 2.0 and significantly lower at high densities.
a version of Guide E 94 dated before 1984. In Guide Limiting values for image quality parameters are as
390
SE-1815 ARTICLE 22 RADIOGRAPHIC STANDARDS SE-1815
TABLE X1.1
CLASSIFICATION COMPARISON OF TEST METHOD E 1815 AND GUIDE E 94-83 FOR HIGH-CONTRAST FILM
SYSTEMS
Minimum
Gradient/
Test Method Minimum Gradient G at Granularity Maximum Guide Description
SE-1815 Ratio at Granularity at E 94-83
System Class D p 2.0 D p 4.0 D p 2.0 D p 2.0 Film Type Speed Contrast Graininess
391