Beruflich Dokumente
Kultur Dokumente
Arranged by:
MillatiHaqq 3314100059
WidyaPrihestiIswarani 3314100074
SarasHanifati 3314100089
KhonsaRofifah 3314100090
NadiaNafisa 3314100107
Lecturer :
Dr. Eng. Arie Dipareza Syafei, ST., MEPM
CHAPTER 1
INTRODUCTION
1.1. PURPOSE
1.2. PRINCIPLE
Equipments :
- Spektrophotometer - Erlenmeyer
- GPS - Impinger
- Pinset - Anemometer
- Psychrometer
Emission and Ambient Control | 2016
Materials :
- Reagent of NOx :
o Acetic acid
o Aquadest
- Reagent of Oxidator :
o KMnO4
o H3PO4
o H2SO4
o Aquadest
- Reagen O3 :
o KH2PO4
o NaH2PO4
o KI
o Aquadest
- Reagen NH3 :
o H2SO4
o Aquadest
- Reagen SOx :
o Reagen NH3
o Aquadest
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o H2O2
A.GasParameter
Filling up the tubes with
Assembling reagents that has been
up the made before: 1 tube of
Impinger 20ml NOx, 1 tube of 0ml
SOx, 1 tube of 20ml O3,
1 tube of 20ml NH3, and
an oksidator solution
After 30 minutes,
the push the off The
button. The Impinger Impinger
reagents from need to be hoses
each tubes need located near need to be
to be taken away the street rechecked
for further and being so that
analysis with operated for the
DHL Meter (SOx) about 30 Impinger
and minutes could
Turbidimeter(NO operate
x, NH3, O3) properly
B.ParticulateParameter
C.MeasurementofHumidity,TemperatureandWindSpeed
Operate the
Attach the tool and
connection for record the
Prepare the the
temperature
Hygro-Thermo- measurement
of humidity and
Anemometer
and humidity
temperature that are
readable
Noted the
results min. Change
and max. Operate connection with a
legible on the the tool for fan-shaped
tool during the about 5 connection at the
measurement minutes end to wind
period speed
measurement
D.NoiseMeasurement
Noted the
Operate by results min.
Prepare the pressing the and max.
instrument power button on legible on
of sound the monitoring the tool
level meter sites for 5 during the
minutes measureme
nt period
E.CoordinatesLocationDetermination
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CHAPTER 2
THEORY
The harmful effects of air pollutants on human beings have been the major
reason for efforts to understand and control their sources. During the past two
decades, research on acidic deposition on water-based ecosystems and greenhouse
gas emissions on climate has helped to reemphasize the importance of air
pollutants in other receptors, such as soil-based ecosystems.
Another example of an air pollutant that affects the total body burden is
carbon monoxide (CO). In addition to CO in ambient air, there are other sources
for inhalation. People who smoke have an elevated CO body burden compared to
nonsmokers. Individuals indoors may be exposed to elevated levels of CO from
incomplete combustion in heating or cooking stoves. CO gas enters the human
body by inhalation and is absorbed directly into the bloodstream; the total body
burden resides in the circulatory system. The human body also produces CO by
Emission and Ambient Control | 2016
(Vallero, 2008)
Ambient air is the free air in the troposphere layer of the atmosphere
which is located in the jurisdiction area of the Republic of Indonesia, which is
needed and affected the humans health, living creatures, and any other life
components. In the other hand, emission is a substance, energy, or any other
components which is produced by any kind of activities that enters the ambient
air, whether it has potency as pollutant or not. (Ministry of Living Environment,
2010)
Ozone makes up only about 0.6 parts per million of the atmosphere by
volume, but it is continuously created and destroyed in an endless photochemical
Chapman cycle, absorbing ultraviolet radiation to maintain an ozone layer
between 15 and 35 km above Earths surface. The stratosphere is heated daily
primarily by continual dissociation of molecular oxygen (O 2) and ozone (O3)
where the molecular/atomic pieces fly apart at high velocity, increasing the
average translational kinetic energy of all gas molecules, which, according to the
ideal gas law,increases the temperature of air. The optical thickness of this layer
varies regionally by the minute, time of day, season, and latitude. Ozone tends to
accumulate at the poles between mid winter and early spring when increasing sun
light forms ozone faster than it can be destroyed. More ozone during winter heats
the lower stratosphere, causing very cold temperature on Earth. (Chapman, 1930)
Nitrogen oxide is a gas that is colorless and odorless and nitrogen dioxide
(NO2) which has red-brown color are both very important as air pollutants. A
mixture of NO and NO2 known as NOx. Almost all NOx from human activity
resulting from changes in fossil fuels from sources both fixed and mobile sources.
Globally not less than 100 million metric ion NOx per year is spent on the
proficiency level of activity.
concentration of highly destructive air quality (Ahmad, 2004). Most NOx entry
into the atmosphere as NO. At a very high temperature reaction occurs:
N2 + O2 2NO
1. Continuous
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2. The semi-continuous
3. Grab sample
the air
Measuring the fow of
Flowmeter
Impinger
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a. Pump air with the pump suction tube into the impinger containing
solution catcher.
High Volume Sampling Method This method is used for the measurement
of total suspended particulate matter (TSP, SPM), which is particulate matter with
a diameter 100 m, the basic principle of the air inhaled by the flowrate of 40-
60 cfm, then suspended particulate matter (dust) with a size <100 m be sucked
and retained on the surface of the microfiber filter with a porosity of <0.3 lm.
2. Weigh the filter paper in the analytical balance using tweezers (Be
careful not to get touched hands)
3. Attach the paper to the tool TSP, with opening roof TSP appliance. Then
a paired back the roof.
5. Operate the tool by the way, turn on ("On") a suction pump and record
numbers of air flow rate).
6. Turn off the tool until the time limit has been set.
CHAPTER 3
RESULTS AND OBSERVATIONS
3.1. Reagents Preparation
A. Reagent of NOx
B. Reagent of Oxidator
C. Reagent of O3
D. Reagent of NH3
E. Reagent of SOx
impingersholesbasedon eachparameter:
- ReagentofNOx:
eachparameter.
liquid,clear,
colorless,badodor
- Reagentofoxidator:
liquidanddeep
purplecolored
- ReagentofSOx:
liquid,colorless
2 Connecteachtubestothe Thecircuithosemust
vacuumpumpthrougheach beinstalledrightso
hoses.Thenturnonthe therewontbeany
impinger. foldedhoseinorderto
lettheaircomein
fluently.
Therearesomebubble
flowswhenthe
impingerturnedon.
Turntheimpingeron
forabout30minutes.
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3 Measuretheabsorbancefor Wavelengthof
NOxinspectrophotometerand spectrophotometer:
measuretheconductivityfor NOx=450nm
SOxusingDHLmeter. Theabsorbance
valuesare:
NOx1=0,015
A
TheDHLvaluefor
SOxreagen:
Value
Parameter
DHL T
0.279
29.4o
Blanko mS/
C
cm
4.01
28.9o
SOx mS/
C
cm
B. NH3
4 Presstheoffbuttonofimpinger
after30minutesandanalyzethe
reagentsolutioninthe
laboratory
5 Preparethesolutionsamplefor Movethereagent
absorbanceanalysisusing solutionintobeaker
spectrophotometer glass
6 Pressthepowerbottonof WavelengthNH3=
spectrophotometer 410nm
7 Measuretheabsorbance Analysisresult
NH3=0,046A
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C. O3
2 Connectthetubetothesuction Thecircuithosemustbe
pumpthroughhoses(onesection correctandthehose
justforonekindofanalysis shouldntbefoldedsothat
gas). theairflowcango
smoothly.
3 Place the impinger at the Impinger placed in front
sampling location, then press the of the Department of
power button located on the side Environmental
of impinger Engineering FTSP ITS.
4 Presstheoffbuttonofimpinger
after30minutesandanalyzethe
reagentsolutioninthe
laboratory
5 Preparethesolutionsamplefor Movethereagentsolution
absorbanceanalysis intobeakerglass
6 Pressthepowerbottonof WavelengthO3=390nm
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spectrophotometer
7 Measuretheabsorbance Analysisresult
O3=0,035A
3 Attach the paper to the tool TSP, There is a noise from the
with opening roof TSP machine like buzzing
appliance. Then a paired back
the roof. After that turn on the
suction pump for 30 minutes
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4 Turn off and lay down the Weight of filter paper after
machine, and weigh the filter 30 minutes process is
paper with the analytical 0.9423 gr
balance
Equipmentconsistsoftwo
PreparetheHumidity, typesofconnection.Thefirst
TemperatureandWindSpeed tomeasurehumidityand
1
measurementtool:Hygro temperature.Thesecondone
ThermoAnemometer lookslikeafantomeasure
windspeed.
2 Installtheconnectiontomeasure MeasurementResult:
humidityandtemperature. Humidity
Begin
Operatethetoolfor5minutes
Max. 83,981
measurement,liftituptotheair
Min. 73 74,6
untilthetoolshownsomelegible
result.Writedowntheresult. Avarage 78,45
77,8
AverageHumidityResult;
=
Beginning AvFInal Av
2
0,45+ 0,5
= 2
=78,125%
Temp.
Begin
Max. 31,230,6
Min. 29,729,7
Ratarata 30,45
30,15
AverageTemperature
Result;
=
Emission and Ambient Control | 2016
30,45+30,15
= 2 =30,3
C
MeasurementResult:
Begin
WindSpeed
appliancefor5minutesand Result
recordtheresultsthatitshown. =
0,45+ 0,5
= 2
=0,475m/s
1 PreparetheGPStool GPSisadevicethatcontainsdata
ongeographicallocationbyway
ofreceivinginformationfromthe
satellites.
2 Operatebypressingthepower ThereadingresultoftheGPS
buttononsitemonitoring.Wait coordinatesforthelocation
forthetooltoreadthe nexttotheentrancewayportal
coordinates.Writedownthe ofEnvironmentalEngineering
coordinates DepartmentFTSPITSas
shownintheGPStool:
S0716'48.6"
E11247'31.4"
Emission and Ambient Control | 2016
CHAPTER 4
DISCUSSION
The reagents of the experiments must be prepared at least one day before
the experiment. We prepared the reagents in the laboratory of Air Pollution on
November 8th, 2016. At first, we planned to do the experiment on November 9 th,
2016, but due to bad weather, it cancelled until November 10th, 2016.
We created 5 kinds of reagents for analyzing the ambient air quality, which
are NOx, oxidator for NOx analysis, O 3, NH3, and SOx. The volume of all
reagents should be 50 ml, because we need 20 ml reagent which is being poured
Emission and Ambient Control | 2016
into the bottle of impenger and the other 30 ml as the blank for
spectrophotometric analysis. All of the reagents were placed in the small bottle
and given labels, so it would be easy to distinguish them.
The first reagent that we made is the reagent of NOx. Here are the steps to
create reagent of NOx:
The second reagent that we made is the oxidator for NOx analysis. Here
are the steps to create reagent of oxidator:
The third reagent that we made is the reagent of O 3. Here are the steps to
create reagent of O3:
The fourth reagent that we made is the reagent of NH 3. Here are the steps
to create reagent of NH3:
We took out 0.05 ml H2SO4 and put it in the beaker glass. After that, we
diluted the solution using aquadest until it reached the volume of 50 ml. We
poured it into the bottle of reagent and add a label.
Emission and Ambient Control | 2016
The last reagent that we made is the reagent of SOx. Here are the steps to
create reagent of SOx:
The following table shows the threshold value of ambient air based on
Permen LH No 12 Tahun 2010.
Afterthereagentsareready,poureachreagentsintotheimpingerstube
basedoneachparameter.Thenturnontheimpingerspowerforabout30minutes
at the sampling location. After 30 minutes running on impinge, analyze the
absorbancevalueforNOxreagentsusingspectrophotometer,andDHLvaluefor
SOxreagent.Thencalculatetheconcentration.
Emission and Ambient Control | 2016
NOx
Gries Saltzman method is a method which usually used in determine the
concentration of pollutant gases of Nitrogen Dioxide (NOx) in the air. NOx in the
air reacted with Gries Saltzman reagent (absorbent) and formed a purple
compound. The color intensity measured with spectrophotometer with 450nm
wave length. For NOx measurement, the sample gas should be passed in the
oxidator first (such as KMnO4, Cr2O3).
On this experiment, we only measure the concentration of NO 2 because we
didnt measure the absorbance value of sample in the second tube.
Calibration curve of NOx
X Y
Absorbansi g/ml
0.005 0.005
0.014 0.01
0.031 0.02
0.057 0.04
0.09 0.06
0.121 0.08
0.153 0.1
0.184 0.12
0.235 0.16
0.273 0.18
0.303 0.2
0.2
f(x) = 0.66x + 0
l/ml R = 1
0.1
0
0 0.05 0.1 0.15 0.2 0.25 0.3
Absorbansi
Emission and Ambient Control | 2016
L 3
( 0,007 x 0,663 ) x ( 20 x 10 ) L
L
NO2concentration= L
1 x 30 minute
minute
9,282 x 105 L L
NO2concentration= =3,094 x 106 =
30 L L
L
3,094 x 106 6
=3,094 x 106 ppm
10 L
L
Note: 10 6 L isequivalentwith1ppm.
Afterobtainingtheconcentrationifppm,wemustconvertitintog/m3
usingthefollowingformula:
P x weight of the molecule
g/m3 = ppm x 1000 x RxT , P is pressure in
mmHg,Ristheuniversalconstantofthegas,andTistemperatureinKelvin.
So, NO2 concentration (g/m3 ) =
6 760 x 46 g
3,094 x 10 x 1000 x =0,043 3
8,31 x 303,3 m
g standard T g 273 g
concentration x =0,043 3 x =0,038
m 3
standard T +t m 273+ 30,3 Nm3
SOx
Sulfur dioxide in the atmosphere is usually used with conductance method.
The principal is: sulfur dioxide reacts with water to produce sulfuric acid, the
separated part and hydrogen ion, sulfide ion, conductivity is:
SO2 + H2O H2SO3
Thats why, the absorption of sulfur
x y
dioxide will increase DHL mg/L the conductivity, so we
could measure the 6.12 5 content of sulfur
13.26 10
dioxide from the sample. There are few
34.4 25
methods, but if the 74 50 sample consists
dissolved gas in water 137.3 100 and produces
258.7 200
electricity conductivity from the other gas, will
affect the accuracy of the measurement results.
Calibration curve of SOx:
SOx
mg 3
{ ( 4,010,279 ) x 0,77 } x ( 20 x 10 ) L
L 0,0575 mg mg
= =1,92 x 103
L 30 L L
1 x 30 menit
menit
mg mg mg
1,92 x 103 =1,92 x 103 =1,92 x 103 =1,92 x 103 ppm
kg kg kg
1 L x 1000 103 m3 x 1000
m3 m3
kg
1000
Note : It is assumed that the density of the reagent solution is m3
Afterobtainingtheconcentrationifppm,wemustconvertitintog/m3
usingthefollowingformula:
P x weight of the molecule
g/m3 = ppm x 1000 x RxT , P is pressure in
mmHg,Ristheuniversalconstantofthegas,andTistemperatureinKelvin.
Emission and Ambient Control | 2016
3 760 x 64 g
1,92 x 10 x 1000 x =37 3
SOxconcentration =
8,31 x 303,3 m
g standard T g 273 g
concentration x =37 3 x =33,3
m standard T +t m 273+30,3
3
Nm3
Thus,basedontheexperimentweobtainedtheSOxconcentrationis33,3
g/Nm3.Ifwecomparethisresultwiththethresholdvalue,itcanbeconcluded
thatSOxconcentrationinthesamplingareais stillbelow thethresholdvalue
whichis900g/Nm3for1houranalysis
B. NH3
The first thing to do is make the NH3 reagents that will be placed in tubes
on the impinger. Create the reagent the day before practicum. This is done so that
the reagent is completely in a state of room temperature when measuring.
After the reagent is ready to use, reagent place in the impinger tube
according to the labels that have been written on the body of impinger. Then
impinger operated for 30 minutes. After 30 minutes, the measurement is finished
and followed by measuring the absorbance value of NH3.
Ammonia from the ambient air which has been absorbed by the absorbent
solution of sulfuric acid to form ammonium sulfate. Then reacted with phenol and
sodium hypochlorite in alkaline conditions to form complex compounds indofenol
are colored blue. The intensity of blue color formed was measured using a
spectrophotometer at a wavelength of 410 nm.
x y
Absorban
ce mg/L
0.052 0.5
0.082 0.75
0.11 1
0.15 1.25
0.18 1.5
0.2 1.75
0.24 2
NH3 concentration =
mg 3
( 0,046 x 8,53 ) x ( 20 x 10 ) L
A x slope x volume of reagent L mg m
= =2,61 x 104 =2,61 x 104
volume of theair sample L L
1 x 30 menit 1L x1
menit
4
= 2,61 x 10 ppm
kg
1000
Note : It is assumed that the density of the reagent solution is m3
Emission and Ambient Control | 2016
Afterobtainingtheconcentrationifppm,wemustconvertitintog/m3
usingthefollowingformula:
P x weight of the molecule
g/m3 = ppm x 1000 x RxT , P is pressure in
mmHg,Ristheuniversalconstantofthegas,andTistemperatureinKelvin.
760 x 17 g
2,61 x 104 x 1000 x =1,338 3
NH3concentration= 8,31 x 303,3 m
NH3 concentrationing/Nm3=
g standard T g 273 g
concentration x =1,338 3 x =1,2043
m standard T +t m 273+ 30,3
3
Nm3
C. O3
The first thing to do is make the O3 reagents that will be placed in tubes on
the impinger. Create the reagent the day before practicum. This is done so that the
reagent is completely in a state of room temperature when measuring.
After the reagent is ready to use, reagent place in the impinger tube
according to the labels that have been written on the body of impinger. Then
impinger operated for 30 minutes. After 30 minutes, the measurement is finished
and followed by measuring the absorbance value of O3.
Oxidants from the ambient air which has been absorbed by the Neutral
solution of Potassium Iodide Buffer (NBKI) and reacting with iodide ions to free
iodine (I2) are colored yellow. Oxidant concentration in the solution is determined
by spectrophotometry at a wavelength of 390 nm (SNI-19-7119.8-2005).
O3 Calibration Curve
Emission and Ambient Control | 2016
x Y
Absorbanc
e g/ml
0.0061
0.086 2
0.23 0.0184
0.38 0.0306
0.54 0.0459
Kurva Kalibrasi O3
0.06
0
0 0.1 0.2 0.3 0.4 0.5 0.6
Absorbansi
O3 concentration (ppm) =
L
( 0,035 x 0,083 ) x 20 mL
A x slope x volume of the reagent mL L
= =1,936 x 103 =1,936 x 103 ppm
volume of the air L L
1 x 30 minute
minute
Afterobtainingtheconcentrationifppm,wemustconvertitintog/m3
usingthefollowingformula:
P x weight of the molecule
g/m3 = ppm x 1000 x RxT , P is pressure in
mmHg,Ristheuniversalconstantofthegas,andTistemperatureinKelvin.
Emission and Ambient Control | 2016
3 760 x 48 g
1,936 x 10 ppm x 1000 x =28,02 3
O3concentration =
8,31 x 303,3 m
O3 concentrationing/Nm3=
g standard T g 273 g
concentration x =28,02 3 x =25,22
m
3
standard T +t m 273+30,3 Nm
3
Thus,basedontheexperimentweobtainedtheO3 concentrationis25,22
g/Nm3.Ifwecomparethisresultwiththethresholdvalue,itcanbeconcluded
thatO3 concentrationinthesamplingareaisstillbelowthethresholdvaluewhich
is235g/Nm3for1houranalysis.
Particulate matter (PM) is the term for solid or liquid particles found in the
air. Particles with a size large or dark enough can be seen as soot or smoke. While
very small particles can be seen with an electron microscope. Particles originate
from various sources, both mobile and stationary engines (diesel trucks,
woodstoves, power plants, etc.), so that the chemical and physical properties of
particles is varied. Particles can be directly formed in the atmosphere when gas
pollutants such as SO2 and NOx react to form fine particles.
PM-10 standard is a small particle that is responsible for the adverse health
effects because of its ability to reach the deeper areas of the respiratory tract. PM-
10 include particles with a diameter of 10 micrometers or less. Health standards
under PP 41 tahun 1999 for PM-10 is 150 mg / Nm3 (24 hours).
air. After 30 minutes, lay down the vacuum, it is for keeping the particulate matter
in the filter paper. Take the filter paper and then weigh the filter paper in analytical
balance. This step is for knowing the weight of filter paper after the process. The
result weight of the filter paper is 0.9423 gram.
Then get the PM weight by reducing the weight of the filter paper at the
beginning and at the end of filter paper weight. The following results were
obtained:
Heavy dust = Weight of filter paper end - the beginning of filter paper weight
= 9,09 x 10-5 g / m3
= 90,9 gram / m3
We cant compare the result of the experiment with the threshold value
because we dont know the pore size of the filter paper.
According to Kep. 1996 MENLH noise threshold for the school environment or
the like is 55 dBA. The results of measurements at monitoring sites obtained 24.9 dBA,
which means it can be concluded that the noise level in Environmental Engineering
Department is still below the noise threshold and can be said to be good for the noise
parameters.
ThetoolsusedinthismeasurementisHygroThermoAnemometer.This
toolcanbeusedtomeasurehumidity,temperature,andwindspeedallatonce.
Contains of several main components, namely a connection cable for
measurementaswellasareaderofmeasurementresults.
Measurementsweremadeinawaytooperateequipmentatthemonitoring
location. For measurement of humidity and temperature can be done at once
because it will provide the data both simultaneously. For measurement of
humidity and temperature used connections with the cable end is round.
Measurements were performed two times, namely at the beginning of the lab
beganatabout8:20andattheendofaseriesofpracticumat11:30.Thisisdone
so that the resulting data is more accurate. In each measurement time
measurementswerecarriedoutfor5minutes.Willreadoutthemeasurementtool
andnotetheresults.
We then measured the wind speed by using the tool HygroThermo
Anemometerbutthecableconnectionusedformeasurementreplacedbyacable
thatendsshapedlikeafan.Thenthetoolisoperatedfor5mnwithalsotwotimes
the measurement time, and the recorded data is read on HygroThermo
Anemometer.
All data were obtained and then sorted to get the highest and lowest
values,thenlookforthevalueofhisaverage. Obtainedanaverageyieldof
78.125%humidity,windspeedof0.475m/s,andtemperatures30,3C.
AccordingtotheQualityStandardsKepmenkesNo.261,idealhumidity
rangedbetween4065%.Whencomparedwiththeresultsofmeasurementson
monitoringlocationwith78,125%humidityresultsitcanbeconcludedthatthe
humidityishighandthepotentialtocausethegrowthofmicroorganismsbecause
theairistoohumid.Asforthetemperature,accordingtotheStandardQuality
Standards in accordance Kepmenkes 261 that are considered convenient
temperatureis18270C.Whencomparedwiththeresultsofthemeasurementthat
isequalto30.3Cairtemperaturemeanslessconvenientmonitoringlocations
andexceedingqualitystandardsinaccordanceKepmenkes.Thenforwindspeed
measurementwhencomparedtoQualityStandard261Kepmenkesidealairflow
raterangedfrom0.15to0.25m/swhiletheairflowratemeasurementresultis
0.475m/s.Thisvalueisgreaterthantheairflowrateidealanddoesnotmeetthe
standards.
Emission and Ambient Control | 2016
CHAPTER 5
CONCLUSSION
1. The ambient air quality for NOx, SOx, NH 3, and O3 parameters in the
sampling area which is located in front of Department of
Environmental Engineering is good because they are all below the
threshold value based on Permen LH No 12 Tahun 2010 and PP No 41
Tahun 1999. The results are as follow :
NOx = 0,038 g/Nm3,whilethethresholdvalueis400g/Nm 3
for1houranalysis
SOx = 33,3 g/Nm3 ,whilethethresholdvalueis900g/Nm3
for1houranalysis
NH3 = 1,2043 g/Nm3 ,whilethethresholdvalueis30000
g/Nm3for1houranalysis
O3 = 25,22 g/Nm3 whilethethresholdvalueis235g/Nm3
for1houranalysis
2. We cant compare the result of the experiment with the threshold value
because we dont know the pore size of the filter paper.
3. The noise level in the sampling area which is located in front of
Department of Environmental Engineering is good because it is below
the threshold value based on Kep. 1996 MENLH. The result is 24,9 dBA,
while the threshold value is 55 dBA.
4. The humidity in the sampling area which is located in front of
Department of Environmental Engineering is over than the ideal value
based on Kepmenkes No 261 Tahun 1998. The result is 78,125%,
whiletheidealvalueisrangebetween4065%.
5. The temperature in the sampling area which is located in front of
Department of Environmental Engineering is over than the ideal value
based on Kepmenkes No 261 Tahun 1998. The result is 30.3Cwhile
theidealvalueisrangebetween18270C
Emission and Ambient Control | 2016
BIBLIOGRAPHY