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ISSN(Online): 2319-8753

ISSN (Print): 2347-6710

International Journal of Innovative Research in Science,


Engineering and Technology
(An ISO 3297: 2007 Certified Organization)

Vol. 4, Issue 12, December 2015

Influence of Fillers on Paving Grade Bitumen


Ishfaq Mohi Ud Din1, Supriya Marik 2
P.G. Student, Department of Civil Engineering, Lovely Professional University, Phagwara, Punjab, India1
Associate Professor, Department of Civil Engineering, Lovely Professional University, Phagwara, Punjab, India2

ABSTRACT. This study is about the effect of fillers on paving grade bitumen under various conditions. The basis of
the thesis is to find out change in the physical properties of the bitumen by modifying it with different fillers. The types
of fillers used in project are Cement, Fly ash and Stone dust. Fillers help in filling the voids and change the physical
and chemical properties. Fillers modify the properties, increase the performance of, and provide improved Durability to
various construction materials (Such as concrete and asphalt). The effects of fillers are therefore of vital importance.
When bitumen is combined with filler, mastic is formed. This mastic can be viewed as the component of the asphalt
mixture that binds the aggregates together and also the component of the asphalt that undergoes deformation when the
pavement is stressed under traffic loading. The characteristics of the filler can significantly influence the properties of
the mastic, and thus the filler properties can have significant effects on asphalt mixture performance. Different
percentage of fillers is used to modify the bitumen. Various physical tests were conducted on Virgin and Modified
Bitumen to evaluate its physical properties. Marshall Test was conducted on bituminous mix prepared using modified
and Virgin Bitumen and the results were analysed and compared. The study indicated that use of fillers improves the
physical properties of Bitumen. Further it also indicated that use of fillers improves Marshall Stability and Flow in the
bituminous mix

KEYWORDS: Mastic, Deformation, Marshall Test, Stability, virgin, modified.

I. INTRODUCTION
Pavement is a durable coating laid in the targeted area to support vehicles or pedestrians. In the past, widespread use of
cobblestones and granite was made, but now these surfaces are mostly replaced by asphalt or concrete. Road surfaces
are regularly marked to guide vehicular traffic. Fillers modify the properties, accelerate the performance, and offer
greater durability to composites, polymers, rubber, adhesives, coatings and building materials (such as concrete and
asphalt). Fillers are used to reduce the cost of materials, increase the stiffness and provide special features to a material
(such as colour or fireproof). The effects of fillers are therefore crucial
Typical fillers are fine powders having particle size less than 75m. Fillers can be naturally occurring like calcium
carbonate, manufactured or derived from industrial waste such as fly ash from power plant. Other conventional fillers
include silica, kaolin, mica, and silica materials. Fillers modify the system in two ways. Firstly, the manner in which
shape, particle size and the size distribution of the particles of the filler affect the system by filling the liquid with solid
particles. Secondly, the way that the interactions between the solid and liquid phase of the mixture meets the material.
Second interactions may vary by strong chemical bonds or physical interactions leading reinforced materials strength.
Asphalt is a vital building material. Most of the roads are built or paved with asphalt. In 2003, about 300 million tons of
asphalt was produced in Europe and 500 million tons in the United States (EAPA, 2004). The effect of repeated stress
manifests itself in two ways, permanent deformation, commonly known as "rutting" and "cracking", due to fatigue of
asphalt.
The asphalt is composed of three major components; aggregates, binder and fillers. The relationship between these
different components leads to a family of asphalt mixtures with different properties. HMA typically includes a
proportion of air, which is often regarded as the fourth component. Minimizing the amount of air through the proper
design and a proper compaction is essential to ensure a durable product. Furthermore, very little air, caused by
overfilling aggregate structure can lead to rutting. The most commonly used filler in asphalt is limestone (Kavussi and
Hicks (1997)), which is derived from microorganisms during the formation of the crust. Limestone is the general term
for the rocks in which the form of calcite is predominant mineral. Limestone may also contain a proportion of

Copyright to IJIRSET DOI:10.15680/IJIRSET.2015.0412167 12549


ISSN(Online): 2319-8753
ISSN (Print): 2347-6710

International Journal of Innovative Research in Science,


Engineering and Technology
(An ISO 3297: 2007 Certified Organization)

Vol. 4, Issue 12, December 2015

magnesium carbonate, silica, clays, iron oxides and organic matter. Basically, gaps/voids are measured in the air and do
not take into account the interactions between bitumen and filler. Charge interactions in the different types of bitumen
can lead to changes in different ways. The filler may cause variations in the viscosity of the liquid phase as a result of
the restructuring, changes or other physical effects.

II. RELATED WORK


M. Jovanovich, A. Mujkanovic and A. Seper (2011) in their study devolved samples of bituminous aggregate
mixtures having fly ash, cement and lime as a filler with varying percentage of bitumen. After preparing various
samples, laboratory investigation was done. The following results were observed:
Fly ash as a filler can be used in asphalt mixtures successfully.
With the addition of filler, optimum bitumen content was observed to be lower in mixtures
For flexible pavements, lower proportion of optimum moisture content is considered better. It leads to fewer voids in
sub grade. Thus with the usage of pavement, there will be less settlement.

Konstantin Sobolev, Ismael Flores and Justin David Bohler (2013) determined the feasibility of fillers in asphalt
concrete was determined. Two different binders were used. These binders were fully blended with filler materials i.e.
fly ash, lime and cement .The study result demonstrated that:
Rheological properties of the asphalt were greatly improved with the addition of these fillers.
Fly ash also appears in improving the aging resistance of mastics
With the addition of fillers, compatibility of mixtures was not affected .

III. RESEARCH METHODOLOGY


This research consists of three stages: characterizing the material, designing mixtures for the three different fillers and
suitability of fillers in the bituminous mixtures. In the first step, properties of bitumen, fillers and aggregates were
established while in second step, optimum bitumen content for each of these mixtures was determined according to
Marshall Mix design method, and in the third level, suitability of different fillers was evaluated.
Conventional bitumen grade VG 30 is used in the present laboratory work. For the preparation of bituminous mixes,
aggregate gradation is done according to the MORT&H specifications. Gradation should be within the limits as per
MORT&H. The sieves are arranged with one another according to the size. About 2.5 to 3kg of aggregates are then
sieved through various sizes. The percent passing through each sieve is observed. When tested, the combined grading
of coarse and fine aggregates and for the specific mixture shall be within the limits

Asphalt binder: Asphalt used in the study is of penetration grade 60/70, since it is used to a great extent and is good
enough to temperature condition. It was purchased from the local distributor. Several tests have been conducted in
laboratory to evaluate the physical properties of Asphalt Binder.

Fillers: Three different types of fillers were selected in this study. These are stone dust, cement and fly ash. Cement
was bought from the local distributor of the ACC plant, Phagwara. Lime and fly ash was brought from various local
sources. The filler material is screened by No. 200 sieve. Specific Gravity of the stone dust, lime and fly ash was
calculated and noted down.

Aggregates: In combination to the binder, and mineral fillers used in Marshall Technique, crushed stone will be used
in the preparation of bituminous mixture samples. Aggregate having desirable properties such as strength, hardness,
toughness, specific gravity and shape is selected. The determination of physical properties of aggregates is done by
performing various tests. The coarse aggregates and fine aggregates are isolated into different screen sizes. Aggregates
are sieved, examined and recombined in laboratory to meet the specific gradation

Marshall Mix Designs: Marshall Stability test is performed to determine the optimum bitumen content and the test
samples shall be prepared by combining varying percentages of bitumen ranging from 4.5% by the weight of
aggregates to 6.5% with an increase of 0.5 % for each type of fillers. The Specimen preparation, compaction and

Copyright to IJIRSET DOI:10.15680/IJIRSET.2015.0412167 12550


ISSN(Online): 2319-8753
ISSN (Print): 2347-6710

International Journal of Innovative Research in Science,


Engineering and Technology
(An ISO 3297: 2007 Certified Organization)

Vol. 4, Issue 12, December 2015

testing will take place according to Marshall Mix Design Method. Marshall Stability and Flow Tests are conducted on
each sample. The bulk specific gravity, density, and percent air voids will be determined for each sample

IV. EXPERIMENTAL RESULTS


Observations evaluated from Marshall Test : Fillers used were limited to 3 percent in each mix where as
Bitumen was varied from 4.5 percent to 6 percent with an increment of 0.5 percent.
Flow Value: It is observed that flow value increases with increases in binder content. For Dense Bituminous Macadam
(DBM), flow value should be within 2 to 4 mm . As we can conclude from the diagram, that with the use of fly ash ,
maximum flow value was observed.

4
virgin
3.5
Flow (mm)

cement
fly ash
3
stone dust
2.5
2
4 4.5 5 5.5 6
% Bitumen

Unit weight: It is observed that unit weight increases with increase in binder content up to certain binder content and
after that it decreases. With the addition of cement, maximum unit weight was observed.

2.6
2.55 virgin
Unit weight (g/cc)

2.5
2.45 cement

2.4
fly ash
2.35
2.3
stone
2.25 dust
2.2
4 4.5 5 5.5 6 6.5
% Bitumen

Stability: It is observed that stability value increases with increase in binder content up to certain binder content and
after that it starts decreasing. Maximum Stability was observed with the use of cement as it fills the fine gaps and helps
in making bitumen mixes as a compact mass with its strength

Copyright to IJIRSET DOI:10.15680/IJIRSET.2015.0412167 12551


ISSN(Online): 2319-8753
ISSN (Print): 2347-6710

International Journal of Innovative Research in Science,


Engineering and Technology
(An ISO 3297: 2007 Certified Organization)

Vol. 4, Issue 12, December 2015

15.5
15 virgin
14.5
14
13.5 cement
13
Stability (kN)

12.5
12
11.5 fly ash
11
10.5
10
9.5 stone dust
9
8.5
8
4 4.5 5 5.5 6 6.5
% Bitumen

Air voids: It is observed that with increase in binder content, air voids decreases. With the use of fly ash , minimum
air voids were observed. Virgin bitumen and modified bitumen with cement as filler show almost same percentage of
air voids. Thus air voids goes on decreasing with the use of fly ash as filler

6
5.5
5 virgin
Air voids (%)

4.5 cement
4 fly ash
3.5
stone dust
3
2.5
2
4 4.5 5 5.5 6
% Bitumen

V .CONCLUSION

Based on the results of the experimental investigations conducted on Virgin and modified bitumen using fillers, the
following summaries have been drawn:

Copyright to IJIRSET DOI:10.15680/IJIRSET.2015.0412167 12552


ISSN(Online): 2319-8753
ISSN (Print): 2347-6710

International Journal of Innovative Research in Science,


Engineering and Technology
(An ISO 3297: 2007 Certified Organization)

Vol. 4, Issue 12, December 2015

Modified bitumen by using different fillers show less penetration value, thus low grade bitumen can be modified to
withstand higher loads.

The ductility value decreased with the use of fillers as these fillers cause the bitumen to become stiffer.

From Marshall Stability test, the stability values were found to be increased with the use of fillers. With the use of
cement as filler, maximum stability was found followed by fillers fly ash and stone dust. These fillers tend to fill
more voids between aggregate grains. Thus mix will continue to gain strength, leading to increased stability of
bituminous mix

The Marshall Flow value also increases with the use of fillers being maximum with the use of fly ash followed by
stone dust and cement respectively. This indicates improvements in the resistance to permanent deformation of
bituminous mixes with addition of these fillers.

The density of bituminous mixes prepared with using modified binder increases up to certain limits and then
decreases.

From the above results, it is observed that fly ash being a waste product can be effectively used as a filler
to improve the properties of bituminous mix. Fly ash also being cost effective as compared to cement and lime.

VI ACKNOWLEDGMENT

I am extremely grateful to Associate Professor Supriya Marik for his exemplary guidance, monitoring and constant
encouragement throughout the course of this thesis. The guidance and help provided by him from time to time shall
carry me a long way in the journey of life on which I am about to embark.
I am highly indebted to School of Civil Engineering, Lovely Professional University for their guidance and constant
supervision as well as for providing necessary information regarding the project and also for their support in
completing the project.
Lastly I thank Almighty, my parents, friends and classmates for their constant encouragement without which this
assignment would not be possible.

REFERENCES

1. American Society for Testing and Materials (ASTM): Road and Paving Materials; Vehicle Pavement System, Annual Book of ASTM
Standards, Section 4, Volume 04, 2003
2. Anderson, D.A., H.U. Bahia, and R. Dongre. Rheological Properties of Mineral Filler - Asphalt Mastics and its Importance to Pavement
Performance. American Society for Testing and Materials, STP 1147, 1992.
3. Anderson, D.A., J.P. Tarris, and D. Brock. Dust Collector Fines and Their Influence on
4. Mixture Design. Journal of the Association of Asphalt Paving Technologists, Vol. 51, 1982
5. Breuer, J.V. Testing the Water Sensitivity of Stone Dust Fillers, Bitumen (Germany), Vol. 29, No. 3, May 1967.
6. Chapuis, R.P. and Legare, P.P., 1992. A simple method for determining the surface area of fine aggregatesand fillers in bituminous mixtures. In
Effects of Aggregate and Mineral Fillers on Asphalt Mixture Performance. STP 1147. ASTM. Philadelphia
7. Craus, J. Ishai, I., and Sides, A.: Some Physico-Chemical Aspects of the Effect and the Role of the Filler in Bituminous Paving Mixtures, J.
Assn. of Asphalt Paving Technologists, Vol. 47, 1978, 558-588,1978.
8. Determination of needle penetration of bitumen, BS EN 1426:2000, BS2000-49, BSI, London.
9. Dukatz, E.L., and D.A. Anderson. The Effect of Various Fillers on the Mechanical Behavior of Asphalt And Asphaltic Concrete. Journal of
the Association of Asphalt Paving Technologists, Vol. 49, 1980
10. Eick, J.M., and J.F. Shook. The Effects of Baghouse Fines on Asphalt Mixtures. Asphalt Institute, Research Report 78-3, November 1978
11. Geber, R. and Gomze, L.A.: Characterization of mineral materials as asphalt fillers, Material Science Forum, 659, 471-476, 2010
12. Kandhal, P.S. Evaluation of Baghouse Fines in Bituminous Paving Mixtures. Journal of the Association of Asphalt Paving Technologists,
Vol. 50, 1981.
13. Kandhal, P.S., Lynn, C.Y., and Parker, F.: Characterization tests for mineral fillers related to performance of asphalt paving mixtures. NCAT
Rep. No. 98-2, 1998
14. National Asphalt Pavement Association (NAPA) 1999. Evaluation of Baghouse Fines for Hot Mix Asphalt. Information Series 127, NAPA.
Lanham, MD

Copyright to IJIRSET DOI:10.15680/IJIRSET.2015.0412167 12553


ISSN(Online): 2319-8753
ISSN (Print): 2347-6710

International Journal of Innovative Research in Science,


Engineering and Technology
(An ISO 3297: 2007 Certified Organization)

Vol. 4, Issue 12, December 2015

15. NCHRP Report 459, (2001), Characterization of modified asphalt binders in superpave mix design, Transportation Research Board, ISBN 0-
309-06707-3.
16. Particle size analysis Part 1: General principles BS ISO13320-1:1999, BSI, London, Puzinauskas, V.P. Filler in Asphalt Mixtures.
Proceedings, Canadian Technical Asphalt, Association, Vol. 13, 1968.
17. Tests for Filler aggregate used in bituminous mixtures. Part 2: Bitumen number, BS EN 13179-2:2000, BSI, London.
18. Tests for geometrical properties of aggregates. Assessment of fines. Grading of fillers. BS EN 933-10 2002, BSI, London.
19. Zulkati, A., Diew, W. Y. and Delai, D.S.: Effects of Fillers on properties of Asphalt-Concrete Mixture, Journal of Transportation Engineering.
ASCE, Vol. 138, No. 7, 902-910, 2012.

BIOGRAPHY

Ishfaq Mohi Ud Din is a P.G. Student, Department of Civil Engineering, Lovely Professional
University, Phagwara, Punjab, India1

Copyright to IJIRSET DOI:10.15680/IJIRSET.2015.0412167 12554