Presented by:

Group 4, Sec. A – 4L
INTRODUCTION

Introduction | Principles
Introduction | Principles
 To know the
concentration of
an acid or base,
the ACID – BASE
TITRATION is
used.
Introduction | Principles
 TITRATION is the gradual addition of one
solution until the solute in the first solution
has reacted completely with the solute in
the second solution
Introduction | Principles
Introduction | Principles
OBJECTIVES

Introduction | Objectives
REAGENTS

0.5 gram Sodium Hydroxide (NaOH) Pellets

0.150 gram Potassium Acid Phthalate (HKC8H4O4)
Four 75 mL Soft drinks Sample
(Colorless or Slightly Colored)
Phenolphthalein

Materials | Reagents
APPARATUS

50 mL Buret
250 mL Beaker
10 mL Pipet
100 mL Volumetric Flask
Two 250 mL Erlenmeyer Flask
Triple Beam Balance

Materials | Apparatus
APPARATUS

Iron Stand and Ring

Bunsen Burner
Stirring Rod
Buret Clamp
Wire Gauze

Materials | Apparatus
I. Preparation of a 0.125 M Sodium
Hydroxide (NaOH) Solution

Procedure | Preparation of a 0.125 NaOH Solution

Procedure | Preparation of a 0.125 NaOH Solution
Procedure | Preparation of a 0.125 NaOH Solution
Procedure | Preparation of a 0.125 NaOH Solution
II. Standardization of the NaOH
Solution

Procedure | Standardization of the NaOH Solution

Procedure | Standardization of the NaOH Solution
III. Determination of the Acidity
of Soft drinks

Procedure | Determination of the Acidity of Softdrinks

Procedure | Determination of the Acidity of Softdrinks
Table 1. Preparation of the NaOH Solution
MASS (IN GRAMS)

Pellets + Beaker 111.90 g

(before standing)
Pellets + Beaker 111.94 g
(after standing)
Beaker 111.40 g

Pellets (Before Standing) 0.50 g

Pellets (After Standing) 0.54 g

Data and Observations

Table 2. Standardization of the NaOH Solution
TRIAL 1 TRIAL 2

Mass of Potassium Acid 0.15 g 0.15 g

Phthalate (grams)
Final Reading of Buret 7.40 mL 14.80 mL
(mL)
Initial Reading of Buret 0.00 mL 7.40 mL
(mL)
Volume of NaOH solution 7.40 mL 7.40 mL
used (mL)
Molarity of the NaOH 0.099 mol/L 0.099 mol/L
Solution (mol/L)
Average Molarity of the 0.099 mol/L
NaOH Solution (mol/L) (9.9 x 10-2 mol/L)

Data and Observations

Table 3. Titration of the Soft drink sample with
NaOH solution
SOFTDRINK SAMPLE 1 SOFTDRINK SAMPLE 2
Sprite Mountain Dew
TRIAL 1 TRIAL 2 TRIAL 1 TRIAL 2
Volume of Softdrink 20.00 mL 20.00 mL 20.00 mL 20.00 mL
sample used (mL)
Final Buret Reading 21.90 mL 32.3 mL 36.7 mL 41.3 mL
(mL)
Initial Buret Reading 18.20 mL 28.50 mL 32.3 mL 36.9 mL
(mL)
Volume of NaOH used 3.70 mL 3.80 mL 4.2 mL 4.4 mL
(mL)
Moles NaOH used 0.00037 0.00038 0.00042 0.00044
(moles) moles moles moles moles

Data and Observations

Table 4. Acidity of Softdrinks

SOFTDRINK SAMPLE 1 SOFTDRINK SAMPLE 2

Sprite Mountain Dew
TRIAL 1 TRIAL 2 TRIAL 1 TRIAL 2
Moles Acid present in a 0.00037 0.00038 0.00042 0.00044
20 mL Softdrink sample moles moles moles moles
Concentration (in 0.0185 M 0.019 M 0.021 M 0.022 M
molarity ) of Acid
Average Molarity of Acid 0.01875 M 0.0215 M

Mass of Citric Acid

present in an 8 ounce 0.088 g 1.0 g
bottle

Data and Observations

Table 1. Preparation of the NaOH Solution

Sample Calculations
 MASS (IN GRAMS)
Pellets (Before Standing) 0.50 g
Pellets (After Standing) 0.54 g

Sample Calculations
Table 2. Standardization of the NaOH Solution

Sample Calculations
Sample Calculations
Sample Calculations
Sample Calculations
Sample Calculations
Table 2. Standardization of the NaOH Solution

Sample Calculations
Sample Calculations
Sample Calculations
Sample Calculations
Sample Calculations
Table 3. Titration of the Soft drink sample with
NaOH solution

Sample Calculations
Sample Calculations
Sample Calculations
Sample Calculations
Sample Calculations
Sample Calculations
REFERENCES
General Chemistry and Chemical Education Division,
Institute of Chemistry, College of Arts and Sciences,
UPLB. 2005. Laboratory Manual for Chemistry 16. 3rd
Ed. Los Baños: University of the Philippines – Los
Baños. pp. 71 - 74

References